CN107603493A - A kind of fungi-proofing light maintaining agent of fur clothing and preparation method thereof - Google Patents
A kind of fungi-proofing light maintaining agent of fur clothing and preparation method thereof Download PDFInfo
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- CN107603493A CN107603493A CN201710774413.9A CN201710774413A CN107603493A CN 107603493 A CN107603493 A CN 107603493A CN 201710774413 A CN201710774413 A CN 201710774413A CN 107603493 A CN107603493 A CN 107603493A
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Abstract
The invention discloses a kind of fungi-proofing light maintaining agent of fur clothing, the maintaining agent includes following components：45 parts of Brazil wax, 68 parts of beeswax, 47 parts of turpentine oil, 0.4 0.8 parts of nano phase ag_2 o, 12 parts of sodium alginate, 56 parts of glycerine.Invention also discloses the preparation method of the maintaining agent.Have the beneficial effect that：The present invention discloses that the fungi-proofing light maintaining agent cost of raw material of fur clothing is cheap, and compatibility is good between each component, can give full play to the advantages of respective, have the function that Synergistic, improves the fungi-proofing light effect of maintaining agent, and makes fur clothing more soft, high resilience.
Description
Technical field
The present invention relates to household chemicals field, more particularly, to fungi-proofing light maintaining agent of a kind of fur clothing and preparation method thereof.
Background technology
With the continuous improvement of living standards of the people, people are to leather and fur products（Leather shoes, suitcase, leather sofa）Nursing efficacy
It is required that also improving constantly, this requires the beauty decoration comprehensive function for improving leather.Currently on the market leather care products it is more with wax,
Solvent, dyestuff are primary raw material, then add some and contribute to the auxiliary agent of cleaning, glazing etc., skin after this care agent long-term use
Easily there is the aging phenomenon such as the embrittlement that hardens, dry and cracked broken skin in leather, not ideal to the nourishes effect of leather.
Prior art such as Authorization Notice No. is the B of CN 102863904 Chinese invention patent, discloses a kind of leather cleaning
Mould proof soft bright dose and preparation method thereof, the mould proof soft bright dose of addition fluorine containing silicone oil of the leather cleaning and a variety of auxiliary agents, leather cleaning are grown
It is good to support effect, can assign smooth leather, soft, waterproof, it is wear-resisting, mould proof the features such as, but the soft bright dose of production cost height, technique are multiple
It is miscellaneous.
The content of the invention
It is an object of the invention to provide a kind of fungi-proofing light maintaining agent of fur clothing, the maintaining agent compatibility is good, has association
With the effect of synergy, the fungi-proofing light effect of maintaining agent is improved.
Another object of the present invention is to provide a kind of system for the fungi-proofing light maintaining agent of fur clothing that technique is simple, cost is cheap
Preparation Method.
The present invention is directed to the problem of being mentioned in background technology, and the technical scheme taken is：A kind of fungi-proofing light maintenance of fur clothing
Agent, the maintaining agent include following components：Brazil wax 4-5 parts, beeswax 6-8 parts, turpentine oil 4-7 parts, nano phase ag_2 o 0.4-
0.8 part, sodium alginate 1-2 parts, glycerine 5-6 parts.The cost of raw material is cheap, and compatibility is good between each component, can give full play to each
From the advantages of, there is Synergistic, improve the fungi-proofing light effect of maintaining agent, and make fur clothing more soft, it is rich
Elasticity.
Preferably, the preparation method of nano phase ag_2 o is：By sucrose ester, silver nitrate and 120-130 parts 1.4%-
The 1.6%NaOH aqueous solution mixes, and adds 0.1-0.2 part active peptides, isothermal reaction 50-60min, places 20-24h,
3800-4000r/min is centrifuged, and product is respectively washed 3 times with absolute ethyl alcohol, distilled water successively, and the product after washing is placed in 60
1d is dried in DEG C vacuum drying chamber, obtains final nano phase ag_2 o.Prepared using sucrose ester as surfactant nano oxidized
Silver, it can effectively suppress the growth of crystal grain, prevent the reunion of nano-particle, improve the fungi-proofing effect of maintaining agent, and be produced into
This is low, and stability is high, meets requirement economical and environmentally friendly.
Preferably, silver nitrate concentration is 0.03-0.04mol/L.Under the conditions of being somebody's turn to do, nano-particle starts to have more during growth
High nucleus growth rate, advantageously form the less nano oxidized silver particles of particle diameter.
Preferably, sucrose ester concentration is 0.9-1.1g/L.Sucrose ester is adsorbed onto the silver oxide nucleating surface newly formed, suppression
Silver oxide nucleus is made to continue to grow up, has made the nano phase ag_2 o particle diameter of generation smaller.
Preferably, reaction temperature is 36-39 DEG C.Should under the conditions of, reduce the degree of particle Brownian movement, reduce
Collision between grain, makes the probability of particle agglomeration diminish, the granular size formed is more uniformly distributed.
Preferably, the amino acid sequence of active peptides is：
HSHACASYSCRCRRARRCGYHRGRCYCRCLRCRVLHPGKLCVCVNCSR.The active peptides added have association with NaOH
Same-action, adsorption effect of the silver oxide nucleating surface to sucrose ester is promoted, further growing up for nucleus is avoided, makes silver oxide
Particle diameter is smaller, and more preferably, the Synergistic Mechanisms need further to be verified antibacterial effect.
A kind of preparation method of the fungi-proofing light maintaining agent of fur clothing, this method are：Take Brazil wax 4-5 parts, beeswax 6-8
Part, turpentine oil 4-7 parts, sodium alginate 1-2 parts and glycerine 5-6 parts mix, and stir 30-40min at 50-55 DEG C, add
Nano phase ag_2 o 0.4-0.8 parts, 10-15min is stirred, obtains the fungi-proofing light maintaining agent of fur clothing.Under the conditions of being somebody's turn to do, various active components can
To be sufficiently mixed, the system stability formed is good, avoids the generation of layering, precipitation and particle, improves answering for product
Use effect.
Compared with prior art, the advantage of the invention is that：The present invention disclose the fungi-proofing light maintaining agent raw material of fur clothing into
This is cheap, and compatibility is good between each component, can give full play to the advantages of respective, have the function that Synergistic, improves maintenance
The fungi-proofing light effect of agent, and make fur clothing more soft, high resilience；The active peptides added have with NaOH cooperates with work
With promoting adsorption effect of the silver oxide nucleating surface to sucrose ester, avoid further growing up for nucleus, make silver oxide particle diameter
Smaller, antibacterial effect is more preferably.
Embodiment
Below by embodiment, the present invention will be further described：
Embodiment 1：
A kind of fungi-proofing light maintaining agent of fur clothing, the maintaining agent include following components：4 parts of Brazil wax, 6 parts of beeswax, turpentine oil 4
Part, 0.4 part of nano phase ag_2 o, 1 part of sodium alginate, 5 parts of glycerine.The preparation of the maintaining agent comprises the following steps：
1) preparation of nano phase ag_2 o：Sucrose ester, silver nitrate and 120 parts of 1.4%NaOH aqueous solution are mixed, silver nitrate concentration
For 0.03mol/L, sucrose ester concentration is 0.9/L, adds 0.1 part of active peptides, 36 DEG C of isothermal reaction 50min, places 20h,
Centrifuged in 3800r/min, product is respectively washed 3 times with absolute ethyl alcohol, distilled water successively, and the product after washing is placed in 60 DEG C very
1d is dried in empty drying box, obtains final nano phase ag_2 o, the amino acid sequence of active peptides is：
HSHACASYSCRCRRARRCGYHRGRCYCRCLRCRVLHPGKLCVCVNCSR.Prepared and received using sucrose ester as surfactant
Rice silver oxide, can effectively suppress the growth of crystal grain, prevent the reunion of nano-particle, improve the fungi-proofing effect of maintaining agent, and
Production cost is low, and stability is high, meets requirement economical and environmentally friendly；
2) preparation of the fungi-proofing light maintaining agent of fur clothing：Take 4 parts of Brazil wax, 6 parts of beeswax, 4 parts of turpentine oil, 1 part of sodium alginate
And 5 parts of mixing of glycerine, 30min is stirred at 50 DEG C, adds 0.4 part of nano phase ag_2 o, 10min is stirred, it is fungi-proofing to obtain fur clothing
Light maintaining agent.Should under the conditions of, various active components can be sufficiently mixed, and the system stability formed is good, avoid layering,
The generation of precipitation and particle, improve the application effect of product.
Embodiment 2：
A kind of fungi-proofing light maintaining agent of fur clothing, the maintaining agent include following components：5 parts of Brazil wax, 8 parts of beeswax, turpentine oil 7
Part, 0.8 part of nano phase ag_2 o, 2 parts of sodium alginate, 6 parts of glycerine.The preparation of the maintaining agent comprises the following steps：It is nanometer first
The preparation of silver oxide：Sucrose ester, silver nitrate and 130 parts of 1.6%NaOH aqueous solution are mixed, silver nitrate concentration 0.04mol/
L, sucrose ester concentration are 1.1g/L, add 0.2 part of active peptides, 39 DEG C of isothermal reaction 60min, 24h are placed, in 4000r/
Min is centrifuged, and product is respectively washed 3 times with absolute ethyl alcohol, distilled water successively, and the product after washing is placed in 60 DEG C of vacuum drying chambers
Middle dry 1d, obtains final nano phase ag_2 o, and the amino acid sequence of active peptides is：
HSHACASYSCRCRRARRCGYHRGRCYCRCLRCRVLHPGKLCVCVNCSR.Prepared and received using sucrose ester as surfactant
Rice silver oxide, can effectively suppress the growth of crystal grain, prevent the reunion of nano-particle, improve the fungi-proofing effect of maintaining agent, and
Production cost is low, and stability is high, meets requirement economical and environmentally friendly；Followed by the preparation of the fungi-proofing light maintaining agent of fur clothing：Take bar
Western 5 parts of palm wax, 8 parts of beeswax, 7 parts of turpentine oil, the 6 parts of mixing of 2 parts of sodium alginate and glycerine, 40min is stirred at 55 DEG C, then
0.8 part of nano phase ag_2 o is added, 15min is stirred, obtains the fungi-proofing light maintaining agent of fur clothing.Should under the conditions of, various active components can be with
It is sufficiently mixed, the system stability formed is good, avoids the generation of layering, precipitation and particle, improves the application of product
Effect.
Routine operation in the operating procedure of the present invention is well known to those skilled in the art, herein without repeating.
Technical scheme is described in detail embodiment described above, it should be understood that it is described above only
For the specific embodiment of the present invention, it is not intended to limit the invention, all any modifications made in the spirit of the present invention,
Supplement or similar fashion replacement etc., should be included in the scope of the protection.
Sequence table
<110>Lanxi City Bai Ruike science services Co., Ltd
<120>A kind of fungi-proofing light maintaining agent of fur clothing and preparation method thereof
<160> 1
<170> SIPOSequenceListing 1.0
<210> 1
<211> 48
<212> PRT
<213>Trachyostracous mussel (Mytilus coruscus)
<400> 1
His Ser His Ala Cys Ala Ser Tyr Ser Cys Arg Cys Arg Arg Ala Arg
1 5 10 15
Arg Cys Gly Tyr His Arg Gly Arg Cys Tyr Cys Arg Cys Leu Arg Cys
20 25 30
Arg Val Leu His Pro Gly Lys Leu Cys Val Cys Val Asn Cys Ser Arg
35 40 45
Claims (7)
- A kind of 1. fungi-proofing light maintaining agent of fur clothing, it is characterised in that：The composition and its parts by weight of the maintaining agent be：Babassu Wax 4-5 parts, beeswax 6-8 parts, turpentine oil 4-7 parts, nano phase ag_2 o 0.4-0.8 parts, sodium alginate 1-2 parts, glycerine 5-6 parts.
- A kind of 2. fungi-proofing light maintaining agent of fur clothing according to claim 1, it is characterised in that：The system of the nano phase ag_2 o Preparation Method is：Sucrose ester, silver nitrate and the mixing of 120-130 part 1.4%-1.6%NaOH aqueous solution, add 0.1-0.2 parts Active peptides, isothermal reaction 50-60min, 20-24h is placed, centrifuged in 3800-4000r/min, product is successively with anhydrous Ethanol, distilled water respectively wash 3 times, and the product after washing, which is placed in 60 DEG C of vacuum drying chambers, dries 1d, obtains nano phase ag_2 o.
- A kind of 3. fungi-proofing light maintaining agent of fur clothing according to claim 2, it is characterised in that：The silver nitrate concentration is 0.03-0.04mol/L。
- A kind of 4. fungi-proofing light maintaining agent of fur clothing according to claim 2, it is characterised in that：The amino of the active peptides Acid sequence is：HSHACASYSCRCRRARRCGYHRGRCYCRCLRCRVLHPGKLCVCVNCSR.
- A kind of 5. fungi-proofing light maintaining agent of fur clothing according to claim 2, it is characterised in that：The sucrose ester concentration is 0.9-1.1g/L。
- A kind of 6. fungi-proofing light maintaining agent of fur clothing according to claim 2, it is characterised in that：The reaction temperature is 36- 39℃。
- A kind of 7. preparation method of the fungi-proofing light maintaining agent of fur clothing, it is characterised in that：Methods described is：Take Brazil wax 4-5 Part, beeswax 6-8 parts, turpentine oil 4-7 parts, sodium alginate 1-2 parts and the mixing of glycerine 5-6 parts, 30- is stirred at 50-55 DEG C 40min, nano phase ag_2 o 0.4-0.8 parts are added, stir 10-15min, obtain the fungi-proofing light maintaining agent of fur clothing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710774413.9A CN107603493A (en) | 2017-08-31 | 2017-08-31 | A kind of fungi-proofing light maintaining agent of fur clothing and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710774413.9A CN107603493A (en) | 2017-08-31 | 2017-08-31 | A kind of fungi-proofing light maintaining agent of fur clothing and preparation method thereof |
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| CN107603493A true CN107603493A (en) | 2018-01-19 |
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| CN201710774413.9A Pending CN107603493A (en) | 2017-08-31 | 2017-08-31 | A kind of fungi-proofing light maintaining agent of fur clothing and preparation method thereof |
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| CN102863904A (en) * | 2012-09-18 | 2013-01-09 | 江苏雪豹日化有限公司 | Moldproof softening and brightening agent for cleaning leather and preparation method thereof |
| US20130074981A1 (en) * | 2011-09-24 | 2013-03-28 | Joanne Price | Leather and vinyl restoration composition and method |
| CN105132601A (en) * | 2015-08-26 | 2015-12-09 | 安徽冠宜箱包有限公司 | Natural leather bag antistatic conditioner and preparing method thereof |
| CN105163768A (en) * | 2013-02-20 | 2015-12-16 | 开尔弗森2200有限公司 | Antimicrobial hydrogel polymers |
| WO2016081433A1 (en) * | 2014-11-18 | 2016-05-26 | Purdue Research Foundation | Compositions and methods for treating leather |
| CN106479380A (en) * | 2016-08-29 | 2017-03-08 | 浙江奥王服饰有限公司 | A kind of fur clothing brightener |
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- 2017-08-31 CN CN201710774413.9A patent/CN107603493A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1565976A (en) * | 2003-06-10 | 2005-01-19 | 中国乐凯胶片集团公司 | Nano-class silver oxide and preparation method thereof |
| CN1824316A (en) * | 2005-02-25 | 2006-08-30 | 孔黄宽 | Liquid used for inhibiting bacterial infection and promoting skin growth |
| CN1827173A (en) * | 2006-03-24 | 2006-09-06 | 余志强 | Chelated nano-silver sterilizing disinfectant and preparation method and application thereof |
| CN101054199A (en) * | 2007-04-04 | 2007-10-17 | 厦门大学 | Shape and size controllable preparation method of micro-nano silver oxide |
| JP2009040923A (en) * | 2007-08-10 | 2009-02-26 | Soft99 Corporation | Leather polishing and protective agent |
| CN101705055A (en) * | 2009-09-25 | 2010-05-12 | 广东三和化工科技有限公司 | Environment-friendly antibiosis glazing agent and preparation method thereof |
| US20130074981A1 (en) * | 2011-09-24 | 2013-03-28 | Joanne Price | Leather and vinyl restoration composition and method |
| CN102863904A (en) * | 2012-09-18 | 2013-01-09 | 江苏雪豹日化有限公司 | Moldproof softening and brightening agent for cleaning leather and preparation method thereof |
| CN105163768A (en) * | 2013-02-20 | 2015-12-16 | 开尔弗森2200有限公司 | Antimicrobial hydrogel polymers |
| WO2016081433A1 (en) * | 2014-11-18 | 2016-05-26 | Purdue Research Foundation | Compositions and methods for treating leather |
| CN105132601A (en) * | 2015-08-26 | 2015-12-09 | 安徽冠宜箱包有限公司 | Natural leather bag antistatic conditioner and preparing method thereof |
| CN106479380A (en) * | 2016-08-29 | 2017-03-08 | 浙江奥王服饰有限公司 | A kind of fur clothing brightener |
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Application publication date: 20180119 |
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| RJ01 | Rejection of invention patent application after publication |