CN107582468B - Anti-allergic mask and preparation method thereof - Google Patents
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Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to an anti-allergic mask and a preparation method thereof.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to an anti-allergic mask and a preparation method thereof.
Background
Skin allergy causes skin immunity reduction due to skin cell damage, and if damaged cells are not repaired in time, the damaged cells are continuously divided into hypoimmunity, namely skin lipid membranes secrete incomplete skin cells, so that various sensitive skin troubles are caused, and a plurality of sequelae such as long-term skin allergy, pigmentation, redness and swelling, pores, acne, color spots, wrinkles and the like are caused. Skin allergy is a common allergic form, and when the skin is subjected to various adverse cosmetics, chemical agents, pollen, certain foods, polluted air and the like, the skin is subjected to skin allergy symptoms such as redness, itching, peeling, allergic dermatitis and the like. Therefore, attention should be paid to skin allergy symptoms.
At present, no good treatment method is available for skin allergy, antihistamine medicines are mostly used for clinical treatment, although the release amount of histamine can be inhibited, the effect is limited, especially for facial allergy, the effect is more limited, a plurality of side effects are generated, and hormone medicines are needed for severe allergy; research shows that the facial skin allergy can be nursed and repaired by using the traditional Chinese medicine components; at present, many antiallergic facial masks are sold in the market, for example, the Chinese patent application CN201610478435.6 discloses a moisturizing antiallergic repair facial mask which is prepared from hyaluronic acid, green tea extract and the like; the Chinese patent application CN201310146816.0 discloses an anti-inflammatory and antiallergic facial mask, which is prepared from chamomile extract, rose essential oil and other raw materials; although the facial mask is claimed to have anti-inflammatory and antiallergic effects, the effects are not very obvious, so that the research and development of the facial mask with better antiallergic effect are of great significance.
Disclosure of Invention
Based on the reasons, through multiple creative researches, the applicant obtains a novel anti-allergic mask, the mask raw material contains purslane extract and betaine, preferably the mask raw material contains purslane extract, betaine and tocopherol, wherein the content of the purslane extract in the mask is more than 5%, so that a good anti-allergic effect is achieved, and the stability shows that the mask has good stability.
The invention is realized by the following technical scheme.
An antiallergic facial mask comprises herba Portulacae extract and betaine.
The anti-allergic mask comprises the mask raw materials of purslane extract, betaine and tocopherol.
The anti-allergic mask comprises 8-12 parts by weight of purslane extract, 0.8-1.2 parts by weight of betaine and 0.10-0.12 part by weight of tocopherol.
The anti-allergic mask is prepared from the following raw materials: deionized water, sodium alginate, xanthan gum, glycerol, isoprene glycol, 1, 3-butanediol, 1, 2-hexanediol, ethylhexyl glycerol, tocopherol, trehalose, EDTA-disodium, betaine, PEG-40 hydrogenated castor oil, olive oil PEG-7 esters, octyl dodecanol, orange peel essential oil, a tremella extract, sodium hyaluronate, 1, 2-pentanediol, beta-glucan, a purslane extract, dipotassium glycyrrhizinate, arginine and silver.
The anti-allergic mask is prepared from the following raw materials: 80-85 parts of deionized water, 0.15-0.25 part of sodium alginate, 0.25-0.35 part of xanthan gum, 2.5-3.5 parts of glycerol, 1.0-2.0 parts of isoprene glycol, 2.5-3.5 parts of 1, 3-butanediol, 0.4-0.6 part of 1, 2-hexanediol, 0.04-0.06 part of ethylhexyl glycerol, 0.10-0.15 part of tocopherol, 0.08-0.12 part of trehalose, 0.04-0.06 part of EDTA-disodium, 0.8-1.2 part of betaine, 0.25-0.35 part of PEG-40 hydrogenated castor oil, 0.25-0.35 part of olive oil PEG-7 esters, 0.08-0.12 part of octyldodecanol, 0.04-0.06 part of orange peel essential oil, 0.001 part of tremella extract, 0.001 part of sodium hyaluronate, 1.05-0.05 part of 2-0.10 parts of pentanediol, 0.05-0.10 part of beta-glucan, 8-12 parts of purslane extract, 0.04-0.06 part of dipotassium glycyrrhizinate, 0.02-0.04 part of arginine and 0.05-0.15 part of silver.
The anti-allergic mask is prepared from the following raw materials: 82.5 parts by weight of deionized water, 0.20 part by weight of sodium alginate, 0.30 part by weight of xanthan gum, 3.0 parts by weight of glycerol, 1.5 parts by weight of isoprene glycol, 3.0 parts by weight of 1, 3-butanediol, 0.5 part by weight of 1, 2-hexanediol, 0.05 part by weight of ethylhexylglycerin, 0.12 part by weight of tocopherol, 0.10 part by weight of trehalose, 0.05 part by weight of EDTA-disodium, 1.0 part by weight of betaine, 0.30 part by weight of PEG-40 hydrogenated castor oil, 0.30 part by weight of olive oil PEG-7 esters, 0.10 part by weight of octyldodecanol, 0.05 part by weight of orange peel essential oil, 0.001 part by weight of tremella extract, 0.001 part by weight of sodium hyaluronate, 0.07 part by weight of 1, 2-pentanediol, 0.07 part by weight of beta-glucan, 10 parts by weight of purslane extract, 0.05 part by weight of dipotassium glycyrrhizinate, 0.03 part by weight of arginine and 0.10 part by weight of silver hyaluronate.
The raw materials are used in anti-allergic cosmetics.
The preparation method of the mask comprises the following steps:
adding water, glycerol, isoprene glycol, 1, 3-butanediol, betaine, 1, 2-hexanediol, sodium alginate, xanthan gum, EDTA disodium, trehalose and ethylhexylglycerin into a water phase pot, heating to 80-85 ℃, uniformly stirring, and pumping into a stirring pot;
starting the machine, stirring and mixing uniformly for 30 minutes at 1000rpm, stopping stirring, and cooling to 40 ℃; adding PEG-40 hydrogenated castor oil, oleum Olivarum PEG-7 esters, octyldodecanol, pericarpium Citri Junoris essential oil, tocopherol, Tremella extract, sodium hyaluronate, 1, 2-pentanediol, beta-glucan, herba Portulacae extract, dipotassium glycyrrhizinate, arginine, and silver, stirring, and cooling to room temperature; and (5) filling to obtain the mask.
The raw materials of the present invention are purchased from table 1:
table 1 sources of the invention
DETAILED DESCRIPTION OF EMBODIMENT (S) OF INVENTION
The technical solutions of the present invention are described below with specific examples, but the scope of the present invention is not limited thereto.
The embodiments described in this specification are merely illustrative of implementations of the inventive concept and the scope of the present invention should not be considered limited to the specific forms set forth in the embodiments but rather by the equivalents thereof as may occur to those skilled in the art upon consideration of the present inventive concept. While the following embodiments of the invention have been described, the invention is not limited to the specific embodiments and applications described above, which are intended to be illustrative, instructive, and not limiting. Those skilled in the art, having the benefit of this disclosure, may effect numerous modifications thereto without departing from the scope of the invention as defined by the appended claims.
The following tests are conclusion tests of research personnel based on multiple creative tests and on the technical scheme to be protected by the invention.
Test 1
Antiallergic test
Test 1 group: 10mg of purslane extract and 1mg of betaine are added, 100mg of 1, 3-butanediol is added, and homogenization is carried out for 4 minutes to obtain a standby sample;
test 2 groups: 10mg of purslane extract, 1mg of betaine and 0.11mg of tocopherol, 100mg of 1, 3-butanediol is added, and homogenization is carried out for 4 minutes to obtain a standby sample;
run 3 groups: 1mg of purslane extract, 10mg of betaine and 0.11mg of tocopherol, 100mg of 1, 3-butanediol is added, and homogenization is carried out for 4 minutes to obtain a standby sample;
run 4 groups: 1mg of chamomile extract, 10mg of betaine and 0.11mg of tocopherol, adding 100mg of 1, 3-butanediol, and homogenizing for 4 minutes to obtain a standby sample;
run 5 groups: 10mg of chamomile extract, 1mg of betaine and 0.11mg of tocopherol, 100mg of 1, 3-butanediol is added, and homogenization is carried out for 4 minutes to obtain a standby sample;
the test method comprises the following steps: adopting an Elson-Morgan method for hyaluronidase in-vitro inhibition test, and taking 0.1ml of 0.25mmol/L CaCl2Incubating the solution and 0.5ml hyaluronidase solution at 37 deg.C for 20 min; adding 0.5ml of sample solution, and continuing to culture at 37 ℃ for 20 min; adding 0.5ml sodium hyaluronate solution, keeping the temperature at 37 deg.C for 30min, and standing at room temperature for 5 min; adding 0.1ml of 0.4mol/L NaOH solution and 0.5ml of acetylacetone solution, heating in a boiling water bath for 15min, and immediately cooling with ice water for 5 min; adding Ellisib testThe reagent 1.0ml is diluted with 3.0ml of absolute ethanol, left for 20min to develop color, and the absorbance (A) is measured by a spectrophotometer.
Hyaluronidase inhibition rate ═ [ A-B ] - (C-D)/(A-B) ] X100%
In the formula: a is the absorbance of the control solution (the sample solution is replaced by acetic acid buffer solution); b is the absorbance of the control blank solution (the sample solution and the enzyme solution are replaced by acetic acid buffer solution); c is the absorbance value of the sample solution; d is the absorbance of the blank solution (the enzyme solution is replaced by acetic acid buffer solution); during the test, the A group samples are scanned at the wavelength of 450-700nm to determine the maximum absorption wavelength, and then the deionized water is used as a reference to respectively measure the absorbance at the maximum absorption wavelength.
And (3) test results: see table 2.
TABLE 2 Hyaluronidase in vitro inhibition
Note: hyaluronidase is an allergic reaction participant, has strong correlation with allergy, and many antiallergic drugs have strong effect of inhibiting the activity of hyaluronidase, so that in order to ensure the antiallergic effect, samples with the inhibition rate of more than 50% are reserved.
And (4) test conclusion: when the content of the purslane extract in the composition is reduced (test 3 group), the inhibition rate is also reduced by less than 50%, so the group is abandoned; the remaining test groups continued the following tests.
Test 2
Irritation test
The test method comprises the following steps: fresh rabbit blood is taken and filled in a polyethylene plastic container, and the weight ratio of the rabbit blood to the polyethylene plastic container is 1: adding citric acid buffer solution in proportion of 9 and mixing uniformly. Immediately, the mixed blood sample is kept in an incubator at a temperature of 21-22 ℃. Transporting to the laboratory within 30 min. The collected blood sample is subpackaged by a 10mL polyethylene sterile centrifuge tube and centrifuged at 3000r/min for 15min at room temperature. The supernatant was carefully aspirated. RBC was washed 2 times with 2.5 times PBS buffer (3000 r/min. times.15 min). Dissolving with PBS buffer solution to form surfactant solution with mass fraction of 0.1%Sodium Dodecyl Sulfate (SDS). Sequentially adding SDS solution of test samples 0, 10, 20, 30, 40, 50, 60, 70, 80, 90 and 100 mu L into an EP tube, adding PBS to make up to 975 mu L, and quickly adding 25 mu L of RBC; placing each tube in a shaking table, and incubating at room temperature of 180r/min for 10 min; centrifuging at room temperature of 10000r/min for 1 min; the supernatant was aspirated at 200. mu.L, and the absorbance at 530nm was measured. The results show that freshly prepared RBC suspensions have a hemilytic volume of around 60mg/L, indicating good RBC integrity. At the same time, the counting number of RBC under a microscope is 9.4 multiplied by 109one/mL. The test sample was dissolved in PBS buffer to form a mass fraction of 1%. Adding 800 μ L of test sample into EP tube, then adding PBS to make up to 975 μ L, then adding 25 μ L RBC into each tube; placing each tube in a shaking table, and incubating at room temperature of 180r/min for 10 min; terminating the incubation, and centrifuging for 1min at room temperature of 10000 r/min; the supernatant was aspirated at 200. mu.L, and the absorbance at 530nm was measured. Negative control, the hemolysis rate of 975. mu. LPBS + 25. mu. LRBC was 0%; positive control, 975. mu.L water + 25. mu.LRBC, showed 100% hemolysis. When the hemolysis rate is higher than 20%, it means that the sample is more irritating.
And (3) test results: see table 3.
TABLE 3 comparison of irritativeness of different test groups
And (4) test conclusion: the results of the irritation test show that the inventive composition is significantly less than 20% irritating and almost non-irritating, whereas the composition with chamomile extract is more than 20% irritating and clearly not suitable for use in an anti-allergy mask.
Preparation examples
Example 1
The facial mask is prepared from the following raw materials: 80g of deionized water, 0.15g of sodium alginate, 0.25g of xanthan gum, 2.5g of glycerol, 1.0g of isoprene glycol, 2.5g of 1, 3-butanediol, 0.4g of 1, 2-hexanediol, 0.04g of ethylhexyl glycerol, 0.10g of tocopherol, 0.08g of trehalose, 0.04g of EDTA-disodium, 0.8g of betaine, 0.25g of PEG-40 hydrogenated castor oil, 0.25g of olive oil PEG-7 esters, 0.08g of octyldodecanol, 0.04g of orange peel essential oil, 0.001g of tremella extract, 0.001g of sodium hyaluronate, 0.05g of 1, 2-pentanediol, 0.05g of beta-glucan, 8g of purslane extract, 0.04g of glycyrrhizic acid, 0.02g of dipotassium arginine and 0.10g of silver.
The preparation method of the facial mask comprises the following steps:
adding water, glycerol, isoprene glycol, 1, 3-butanediol, betaine, 1, 2-hexanediol, sodium alginate, xanthan gum, EDTA disodium, trehalose and ethylhexylglycerin into a water phase pot, heating to 80-85 ℃, uniformly stirring, and pumping into a stirring pot;
starting the machine, stirring and mixing uniformly for 30 minutes at 1000rpm, stopping stirring, and cooling to 40 ℃; adding PEG-40 hydrogenated castor oil, oleum Olivarum PEG-7 esters, octyldodecanol, pericarpium Citri Junoris essential oil, tocopherol, Tremella extract, sodium hyaluronate, 1, 2-pentanediol, beta-glucan, herba Portulacae extract, dipotassium glycyrrhizinate, arginine, and silver, stirring, and cooling to room temperature; and (5) filling to obtain the mask.
Example 2
The facial mask is prepared from the following raw materials: 82.5g of deionized water, 0.20g of sodium alginate, 0.30g of xanthan gum, 3.0g of glycerol, 1.5g of isoprene glycol, 3.0g of 1, 3-butanediol, 0.5g of 1, 2-hexanediol, 0.05g of ethylhexylglycerin, 0.12g of tocopherol, 0.10g of trehalose, 0.05g of EDTA-disodium, 1.0g of betaine, 0.30g of PEG-40 hydrogenated castor oil, 0.30g of olive oil PEG-7 esters, 0.10g of octyldodecanol, 0.05g of orange peel essential oil, 0.001g of tremella extract, 0.001g of sodium hyaluronate, 0.07g of 1, 2-pentanediol, 0.07g of beta-glucan, 10g of purslane extract, 0.05g of dipotassium glycyrrhizinate, 0.03g of arginine and 0.10g of silver.
The preparation method of the facial mask comprises the following steps:
adding water, glycerol, isoprene glycol, 1, 3-butanediol, betaine, 1, 2-hexanediol, sodium alginate, xanthan gum, EDTA disodium, trehalose and ethylhexylglycerin into a water phase pot, heating to 80-85 ℃, uniformly stirring, and pumping into a stirring pot;
starting the machine, stirring and mixing uniformly for 30 minutes at 1000rpm, stopping stirring, and cooling to 40 ℃; adding PEG-40 hydrogenated castor oil, oleum Olivarum PEG-7 esters, octyldodecanol, pericarpium Citri Junoris essential oil, tocopherol, Tremella extract, sodium hyaluronate, 1, 2-pentanediol, beta-glucan, herba Portulacae extract, dipotassium glycyrrhizinate, arginine, and silver, stirring, and cooling to room temperature; and (5) filling to obtain the mask.
Example 3
The facial mask is prepared from the following raw materials: 85g of deionized water, 0.25g of sodium alginate, 0.35g of xanthan gum, 3.5g of glycerol, 2.0g of isoprene glycol, 3.5g of 1, 3-butanediol, 0.6g of 1, 2-hexanediol, 0.06g of ethylhexylglycerin, 0.15g of tocopherol, 0.12g of trehalose, 0.06g of EDTA-disodium, 1.2g of betaine, 0.35g of PEG-40 hydrogenated castor oil, 0.35g of olive oil PEG-7 esters, 0.12g of octyldodecanol, 0.06g of orange peel essential oil, 0.001g of tremella extract, 0.001g of sodium hyaluronate, 0.10g of 1, 2-pentanediol, 0.10g of beta-glucan, 12g of purslane extract, 0.06g of glycyrrhizic acid, 0.04g of arginine and 0.10g of silver.
The preparation method of the facial mask comprises the following steps:
adding water, glycerol, isoprene glycol, 1, 3-butanediol, betaine, 1, 2-hexanediol, sodium alginate, xanthan gum, EDTA disodium, trehalose and ethylhexylglycerin into a water phase pot, heating to 80-85 ℃, uniformly stirring, and pumping into a stirring pot;
starting the machine, stirring and mixing uniformly for 30 minutes at 1000rpm, stopping stirring, and cooling to 40 ℃; adding PEG-40 hydrogenated castor oil, oleum Olivarum PEG-7 esters, octyldodecanol, pericarpium Citri Junoris essential oil, tocopherol, Tremella extract, sodium hyaluronate, 1, 2-pentanediol, beta-glucan, herba Portulacae extract, dipotassium glycyrrhizinate, arginine, and silver, stirring, and cooling to room temperature; and (5) filling to obtain the mask.
Comparative example:
the facial mask is prepared from the following raw materials: 85g of deionized water, 0.25g of sodium alginate, 0.35g of xanthan gum, 3.5g of glycerol, 3.5g of 1, 3-butanediol, 2.6g of 1, 2-hexanediol, 0.06g of ethylhexylglycerin, 0.15g of tocopherol, 0.12g of trehalose, 0.06g of EDTA-disodium, 1.2g of betaine, 0.35g of PEG-40 hydrogenated castor oil, 0.35g of olive oil PEG-7 esters, 0.12g of octyldodecanol, 0.06g of orange peel essential oil, 0.001g of tremella extract, 0.001g of sodium hyaluronate, 0.10g of 1, 2-pentanediol, 0.10g of beta-glucan, 12g of purslane extract, 0.06g of potassium glycyrrhizinate, 0.04g of histidine and 0.10g of silver.
The preparation method of the facial mask comprises the following steps:
adding 85.0g of water, 3.5g of glycerol, 2.0g of isoprene glycol, 3.5g of 1, 3-butanediol, 1.2g of betaine, 2.60g of 1, 2-hexanediol, 0.25g of sodium alginate, 0.35g of xanthan gum, 0.06g of EDTA disodium, 0.12g of trehalose and 0.06g of ethylhexyl glycerol into a water phase pot, heating to 80-85 ℃, uniformly stirring, and pumping into a stirring pot; starting the machine, stirring and mixing uniformly (about 30 minutes, 1000 rpm/min), stopping stirring, and cooling to 40 ℃; adding 0.35g of PEG-40 hydrogenated castor oil, 0.35g of olive oil PEG-7 esters, 0.12g of octyl dodecanol, 0.06g of orange peel essential oil, 0.15g of tocopherol, 0.001g of tremella extract, 0.001g of sodium hyaluronate, 0.10g of 1, 2-pentanediol, 0.10g of beta-glucan, 12.00g of purslane extract, 0.06g of dipotassium glycyrrhizinate, 0.04g of histidine and 0.10g of silver, continuously stirring uniformly, cooling to room temperature, and filling to obtain the mask.
The test method comprises the following steps:
heat resistance: after the facial masks of different examples and the facial masks of the comparative examples are stored for 15 days at 40 ℃, the visual observation shows that whether the characters and the colors are obviously different from those before the test, whether the phenomena of layering and oil floating exist or not.
And (3) test results: see table 4.
Table 4 comparison of stability of different masks
And (4) test conclusion: stability tests show that the mask disclosed by the invention has better stability.
Preparation examples include, but are not limited to, those described above.
Claims (2)
1. An anti-allergic mask is characterized by being prepared from the following raw materials:
82.5 parts by weight of deionized water, 0.20 part by weight of sodium alginate, 0.30 part by weight of xanthan gum, 3.0 parts by weight of glycerol, 1.5 parts by weight of isoprene glycol, 3.0 parts by weight of 1, 3-butanediol, 0.5 part by weight of 1, 2-hexanediol, 0.05 part by weight of ethylhexylglycerin, 0.12 part by weight of tocopherol, 0.10 part by weight of trehalose, 0.05 part by weight of EDTA-disodium, 1.0 part by weight of betaine, 0.30 part by weight of PEG-40 hydrogenated castor oil, 0.30 part by weight of olive oil PEG-7 esters, 0.10 part by weight of octyldodecanol, 0.05 part by weight of orange peel essential oil, 0.001 part by weight of tremella extract, 0.001 part by weight of sodium hyaluronate, 0.07 part by weight of 1, 2-pentanediol, 0.07 part by weight of beta-glucan, 10 parts by weight of purslane extract, 0.05 part by weight of dipotassium glycyrrhizinate, 0.03 part by weight of arginine and 0.10 part by weight of silver hyaluronate.
2. The anti-allergic mask according to claim 1, which is prepared by a method comprising:
adding water, glycerol, isoprene glycol, 1, 3-butanediol, betaine, 1, 2-hexanediol, sodium alginate, xanthan gum, EDTA disodium, trehalose and ethylhexylglycerin into a water phase pot, heating to 80-85 ℃, uniformly stirring, and pumping into a stirring pot;
starting the machine, stirring and mixing uniformly for 30 minutes at 1000rpm, stopping stirring, and cooling to 40 ℃; adding PEG-40 hydrogenated castor oil, oleum Olivarum PEG-7 esters, octyldodecanol, pericarpium Citri Junoris essential oil, tocopherol, Tremella extract, sodium hyaluronate, 1, 2-pentanediol, beta-glucan, herba Portulacae extract, dipotassium glycyrrhizinate, arginine, and silver, stirring, and cooling to room temperature; and (5) filling to obtain the mask.
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| CN108578290A (en) * | 2018-06-11 | 2018-09-28 | 辽宁法奈迪生物工程有限公司 | One kind containing Jiaqing oxidation resistant facial mask of sub- natural moisture preserving and preparation method thereof |
| CN114903824B (en) * | 2021-07-21 | 2023-12-29 | 广州梵之容化妆品有限公司 | Mask for relieving and preserving moisture |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104666236A (en) * | 2015-02-13 | 2015-06-03 | 安婕妤化妆品科技股份有限公司 | Moisturizing skincare mask |
| CN105193876A (en) * | 2015-10-11 | 2015-12-30 | 广州市禾基生物科技有限公司 | Purslane extract and preparation method thereof |
| CN106038345A (en) * | 2016-06-06 | 2016-10-26 | 山东水晶生物科技股份有限公司 | Mask containing gamma-aminobutyric acid |
| CN107174547A (en) * | 2017-05-25 | 2017-09-19 | 杭州千岛湖蓝色天使实业有限公司 | A kind of anti-fog haze emulsion |
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| KR101817081B1 (en) * | 2016-03-18 | 2018-01-11 | 주식회사 썬테라 | Cosmetic composition comprising ginseng powders |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104666236A (en) * | 2015-02-13 | 2015-06-03 | 安婕妤化妆品科技股份有限公司 | Moisturizing skincare mask |
| CN105193876A (en) * | 2015-10-11 | 2015-12-30 | 广州市禾基生物科技有限公司 | Purslane extract and preparation method thereof |
| CN106038345A (en) * | 2016-06-06 | 2016-10-26 | 山东水晶生物科技股份有限公司 | Mask containing gamma-aminobutyric acid |
| CN107174547A (en) * | 2017-05-25 | 2017-09-19 | 杭州千岛湖蓝色天使实业有限公司 | A kind of anti-fog haze emulsion |
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