CN107568383A - A kind of green tea probiotics effervescent tablet and preparation method thereof - Google Patents
A kind of green tea probiotics effervescent tablet and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of green tea probiotics effervescent tablet, count by weight percentage, it is made up of compound probiotic bacterium powder 0.1~0.5%, green-tea extract 10~20%, compound acid 8~19%, composite sweetener 0.7~1%, maltodextrin 30~50%, magnesium stearate 0~1%, sodium acid carbonate 10~20%, saleratus 10~20%.Present invention also offers the preparation method of above-mentioned effervescent tablet, including：A. the preparation of compound probiotic bacterium powder, the preparation of b. green-tea extracts, c. dispensings, it is granulated, d. vacuum drying, compression molding.This green tea probiotics effervescent tablet not only saves the functional component such as anti-oxidant in green tea, and by adding compound probiotic bacterium powder, has product and promote intestines peristalsis, reduce cholesterol, the function of control body weight.Meanwhile the instant effect of this green tea probiotics effervescent tablet is good, instant, it is easier to be absorption of human body.
Description
Technical field
The invention belongs to field of food, is related to a kind of effervescent tablet, specifically a kind of green tea probiotics effervescent tablet and its
Preparation method.
Background technology
Probiotics has regulation gut flora, reduces cholesterol, suppress harmful bacteria, antiallergy, improve immunity of organisms
It is the focus of society research etc. function.The trophic function and physiological function of green tea have obtained concern both domestic and external, but the depth of green tea
Processing, the preparation method of particularly convenient instant green tea food are less.Chinese invention patent application number 201510938534.3, name
Referred to as " a kind of green tea effervescence piece and preparation method thereof ", it is main to describe one kind using green tea, ural licorice root tip, leatherleaf mahonia leaf extract
Effervescent tablet prepared by raw material.Chinese invention patent application number 201410658354.5, it is entitled " a kind of fruits and vegetables probiotic tablet and
Its preparation method ", a kind of fruits and vegetables probiotic tablet and preparation method thereof is described, based on the probiotics powder agents such as Lactobacillus plantarum
Want raw material, composite modified dietary fiber, fruit vegetable powder, oligosaccharide, plant extracts, albumen powder, tea extract, Chinese herbal medicine extraction
Thing etc..Green tea effervescence piece taste is single, and in the market is rarely found, not by big well-established.Fruits and vegetables probiotics tablets are a kind of solids
Tablet, in the market is common, there is control body weight, the effect of toxin-expelling and face nourishing.
And the method that at present prepared by green tea probiotics effervescent tablet is not yet seen in report.
The content of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of green tea probiotics effervescent tablet and its preparation
It is single that method, described this green tea probiotics effervescent tablet and preparation method thereof will solve effervescent tablet function of the prior art,
Adjust the limited technical problem of the effect of functions of intestines and stomach.
The invention provides a kind of green tea probiotics effervescent tablet and preparation method thereof, by the raw material system of following mass percent
It is standby to form：
Compound probiotic bacterium powder 0.1~0.5%,
Green-tea extract 10~20%,
Compound acid 8~19%,
Composite sweetener 0.7~1%,
Maltodextrin 30~50%,
Magnesium stearate 0~1%,
Sodium acid carbonate 10~20%,
Saleratus 10~20%.
Present invention also offers above-mentioned a kind of green tea probiotics effervescent tablet and preparation method thereof, comprise the following steps：
A. prepare compound probiotic bacterium powder the step of, by bifidobacterium lactis, not tally diplobacterium, streptococcus thermophilus, guarantor
Add Leah lactobacillus, lactobacillus thermophilus, Lactobacillus plantarum bacterium powder to mix 5~15min in powder mixer, be prepared into compound benefit
Raw bacterium bacterium powder, described bifidobacterium lactis, not tally diplobacterium, streptococcus thermophilus, lactobacillus bulgaricus, lactobacillus thermophilus, plant
The mass ratio of thing lactobacillus is 1:1:2:2:2:2~6；
B. prepare green-tea extract the step of, green tea is cleaned, is put into micro-wave vacuum case, microwave power
1000~3000W, vacuum -0.09~-0.03MPa, make moisture≤5% of tealeaves, dried green tea is crushed as 30~
The granularity of 50 mesh, is then crushed with ball mill pulverizer, and ball material mass ratio is 9~12: 1, and milling time is 15~20h, rotary table
Rotating speed is 400r/min, and 325 mesh sieves, green tea powder and ethanol solution example 1 in mass ratio are crossed after crushing:5~30 mixing, ethanol and water
Volume ratio be 4:1~6, microwave radiation exaraction, microwave power is 80~800W, 30~180s of extraction time, extraction, is collected green
Tea extract, it is put into microwave vacuum freeze drying box and is dried, 800~1200W of microwave power, vacuum 0.6MPa, temperature
- 30 DEG C of degree, moisture≤5% of green-tea extract after drying；
C. a step of dispensing, granulation, compound probiotic bacterium powder, green-tea extract is weighed according to mass percent, is answered
Acid, composite sweetener, maltodextrin, magnesium stearate, sodium acid carbonate, saleratus are closed, by green-tea extract, compound tart flavour
Agent, composite sweetener, maltodextrin, magnesium stearate, sodium acid carbonate, saleratus crushed 100 mesh sieves, by compound probiotic bacterium
Powder, powder of green tea extract, compound acid, composite sweetener, maltodextrin, magnesium stearate are put in powder mixer and mix 5
~15min, then using ethanol solution wet granulation, then sodium acid carbonate and saleratus equally mixed in powder mixer
Use ethanol solution wet granulation after 5~15min, the volume ratio of ethanol and water is 4 in above-mentioned ethanol solution:1~6；
D. the step of vacuum drying, compression molding, crosses 18 mesh sieves by the material after above-mentioned granulation and obtains wet granular, be placed on
Dried in vacuum drying chamber, make moisture≤5% of material, then by dried material in tablet press machine compression molding,
Every 1g, obtain the green tea probiotics effervescent tablet.
Further, compounding acid be made up of citric acid, malic acid and fumaric acid, described citric acid, malic acid and
The mass ratio of fumaric acid is 1:0.4:0.05.
Further, compound sweetener is made up of sucrose, oligomeric maltose and xylitol, described sucrose, oligosaccharide malt
The mass ratio of sugar and xylitol is 1.2:1:0.07.
The invention provides a kind of green tea probiotics effervescent tablet using compound probiotic bacterium powder and green-tea extract as raw material,
By using microwave vacuum freeze dry technology, while the anti-oxidation function composition such as polyphenols in remaining green tea,
By adding compound probiotic bacterium powder, there is product and promote intestines peristalsis, reduce cholesterol, the function of control body weight.
The present invention does not only have the characteristics of the characteristics of solid pharmaceutical preparation, also liquid preparation.Carry easy to use, be prepared into
Effervescent tablet can be washed into beverage, and effervescent tablet is distributed rapidly, uniformly in water, and active ingredient is easy to absorb, and bioavilability is high.
The present invention compares with prior art, and its technological progress is significant.This green tea probiotics effervescent tablet not only saves
The functional component such as anti-oxidant in green tea, and by adding compound probiotic bacterium powder, there is product and promote intestines peristalsis, drop
Low cholesterol, the function of control body weight.Meanwhile the instant effect of this green tea probiotics effervescent tablet is good, instant, it is easier to be people
Body absorbs.
Embodiment
The present invention is illustrated below by embodiment, but is not intended to limit the present invention.
In various embodiments of the present invention in green tea probiotics effervescent tablet polyphenol content measure：
1 green tea probiotics effervescent tablet is taken, is put into after crushing in conical flask, 10mL boiling water is added, is extracted in boiling water bath
20min, then decompression filter, and repeat extraction once, merging filtrate.Filtrate is extracted 3 times with chloroform.Then upper solution second is taken
Acetoacetic ester extracts 3 times again, takes upper solution to be concentrated under reduced pressure at 55 DEG C, and it is prebiotic to obtain green tea into 50mL volumetric flasks for concentrate constant volume
Bacterium effervescent tablet storing solution, carried out detecting green tea probiotics effervescent tablet storing solution and Tea Polyphenols standard liquid with liquid chromatograph, used
HPLC methods carry out quantitative analysis to Tea Polyphenols in green tea probiotics effervescent tablet.
Bibliography：Zhang J,Wang H M,Jun-Yi M A,et al.HPLC Determination of Tea
Polyphenols and Caffeine in Green Tea[J].Physical Testing&Chemical Analysis,
2012.
In various embodiments of the present invention in green tea probiotics effervescent tablet number of viable measure：
2.5 green tea probiotics are taken, 22.5mL dilutions is added, homogeneous, is serially diluted by 10 times, choose 2~3 suitably
The equal liquid of sample of dilution factor, respectively takes 1mL to be separately added into sterile petri dish, and 15~20mL plate count agar cultures are added per ware
Base, mix, culture, calculate total plate count, determined according to the GB4789.2-2010 detection methods of national regulation.
Embodiment 1
A kind of preparation method of green tea probiotics effervescent tablet, is comprised the following steps that：
A. the preparation of compound probiotic bacterium powder
Using bifidobacterium lactis, not tally diplobacterium, streptococcus thermophilus, lactobacillus bulgaricus, lactobacillus thermophilus, plant breast
Bacillus bacterium powder mixes 5min in powder mixer, is prepared into compound probiotic bacterium powder, bifidobacterium lactis, not tally diplobacterium, thermophilic
Hot streptococcus, lactobacillus bulgaricus, lactobacillus thermophilus, the ratio of Lactobacillus plantarum are 1:1:2:2:2:2；
B. the preparation of green-tea extract
Green tea is cleaned, takes 200g green teas to be put into micro-wave vacuum case, power 1000W, vacuum -0.09MPa, makes
Moisture≤5% of tealeaves, the granularity for 30 mesh is crushed by pulverizer, then crushed with ball milling micronizer, crosses 325 mesh
Sieve, milling time 15h, ball material mass ratio are 9:1, rotary table rotating speed is 400r/min, in green tea powder and ethanol solution ratio
1:The volume ratio of 5 mixing, ethanol and water is 4:1, microwave power 80W, extraction time 30s, extract 2 times, collect green tea and carry
Liquid is taken, is put into microwave vacuum freeze drying box and is dried, microwave power 800W, vacuum 0.6MPa, -30 DEG C of temperature, is done
Moisture≤5% of green-tea extract after dry；
C. dispensing, by weight percentage
By probiotics bacterium powder 0.1%, green-tea extract 10%, compound acid 19%, composite sweetener 0.9%, malt
Dextrin 50%, magnesium stearate 0%, which is placed in powder mixer, mixes 5min, using ethanol solution wet granulation；Again by bicarbonate
Sodium 10% and saleratus 10% equally mix 5min in powder mixer, using ethanol solution wet granulation, above ethanol
The volume ratio of ethanol and water is 4 in solution:1；
D. vacuum drying, compression molding
Material after above-mentioned granulation is crossed into 18 mesh sieves and obtains wet granular, is placed in vacuum drying chamber and dries, makes the moisture of material
Content≤5%, then by dried material in tablet press machine compression molding, every 1g, obtain the green tea probiotics effervesce
Piece.
Packaging：Stored after being packed using packing machine.
Polyphenol content 76.7mg/g in product, number of viable 1 × 106CFU/g
Embodiment 2
A kind of preparation method of green tea probiotics effervescent tablet, is comprised the following steps that：
A. the preparation of compound probiotic bacterium powder
Using bifidobacterium lactis, not tally diplobacterium, streptococcus thermophilus, lactobacillus bulgaricus, lactobacillus thermophilus, plant breast
Bacillus bacterium powder mixes 8min in powder mixer, is prepared into compound probiotic bacterium powder, bifidobacterium lactis, not tally diplobacterium, thermophilic
Hot streptococcus, lactobacillus bulgaricus, lactobacillus thermophilus, the ratio of Lactobacillus plantarum are 1:1:2:2:2:4；
B. the preparation of green-tea extract
Green tea is cleaned, takes 200g green teas to be put into micro-wave vacuum case, power 2000W, vacuum -0.06MPa, makes
Moisture≤5% of tealeaves, the granularity for 40 mesh is crushed by pulverizer, then crushed with ball milling micronizer, crosses 325 mesh
Sieve, milling time 18h, ball material mass ratio are 10:1, rotary table rotating speed is 400r/min, in green tea powder and ethanol solution ratio
1:The volume ratio of 15 mixing, ethanol and water is 4:3, microwave power 400W, extraction time 90s, extract 2 times, collect green tea
Extract solution, it is put into microwave vacuum freeze drying box and is dried, microwave power 1000W, vacuum 0.6MPa, -30 DEG C of temperature,
Moisture≤5% of green-tea extract after drying；
C. dispensing, by weight percentage
By probiotics bacterium powder 0.3%, green-tea extract 15%, compound acid 13%, composite sweetener 0.7%, malt
DEXTRIN %, magnesium stearate 1%, which is placed in powder mixer, mixes 10min, using ethanol solution wet granulation；Again by bicarbonate
Sodium 15% and saleratus 15% equally mix 10min in powder mixer, using ethanol solution wet granulation, above ethanol
The volume ratio of ethanol and water is 4 in solution:3；
D. vacuum drying, compression molding
Material after above-mentioned granulation is crossed into 18 mesh sieves and obtains wet granular, is placed in vacuum drying chamber and dries, makes the moisture of material
Content≤5%, then by dried material in tablet press machine compression molding, every 1g, obtain the green tea probiotics effervesce
Piece.
Packaging：Stored after being packed using packing machine.
Polyphenol content 89.3mg/g in product, number of viable 2.8 × 106CFU/g
Embodiment 3
A. the preparation of compound probiotic bacterium powder
Using bifidobacterium lactis, not tally diplobacterium, streptococcus thermophilus, lactobacillus bulgaricus, lactobacillus thermophilus, plant breast
Bacillus bacterium powder mixes 15min in powder mixer, is prepared into compound probiotic bacterium powder, bifidobacterium lactis, not tally diplobacterium, thermophilic
Hot streptococcus, lactobacillus bulgaricus, lactobacillus thermophilus, the ratio of Lactobacillus plantarum are 1:1:2:2:2:6；
B. the preparation of green-tea extract
Green tea is cleaned, takes 200g green teas to be put into micro-wave vacuum case, power 3000W, vacuum -0.03MPa, makes
Moisture≤5% of tealeaves, the granularity for 50 mesh is crushed by pulverizer, then crushed with ball milling micronizer, crosses 325 mesh
Sieve, milling time 20h, ball material mass ratio are 12: 1, and rotary table rotating speed is 400r/min, in green tea powder and ethanol solution ratio
1:The volume ratio of 30 mixing, ethanol and water is 4:6, microwave power 800W, extraction time 180s, extract 2 times, collect green tea
Extract solution, it is put into microwave vacuum freeze drying box and is dried, microwave power 1200W, vacuum 0.6MPa, -30 DEG C of temperature,
Moisture≤5% of green-tea extract after drying；
C. dispensing, by weight percentage
By probiotics bacterium powder 0.5%, green-tea extract 20%, compound acid 8%, composite sweetener 1%, maltodextrin
30%th, magnesium stearate 0.5% is placed on mix 15min in powder mixer after uses ethanol solution wet granulation, then by bicarbonate
Sodium 20% and saleratus 20% equally mix 15min in powder mixer, using ethanol solution wet granulation, above ethanol
The volume ratio of ethanol and water is 4 in solution:6；
D. vacuum drying, compression molding
Material after above-mentioned granulation is crossed into 18 mesh sieves and obtains wet granular, is placed in vacuum drying chamber and dries, makes the moisture of material
Content≤5%, then by dried material in tablet press machine compression molding, every 1g, obtain the green tea probiotics effervesce
Piece.
Packaging：Stored after being packed using packing machine.
Polyphenol content 103.4mg/g in product, number of viable 5.2 × 106CFU/g
Above said content is only the basic explanation under present inventive concept, and is appointed according to what technical scheme was made
What equivalent transformation, all should belong to protection scope of the present invention.
Claims (4)
1. a kind of green tea probiotics effervescent tablet and preparation method thereof, it is characterised in that by the raw material preparation of following mass percent
Into：
Compound probiotic bacterium powder 0.1~0.5%,
Green-tea extract 10~20%,
Compound acid 8~19%,
Composite sweetener 0.7~1%,
Maltodextrin 30~50%,
Magnesium stearate 0~1%,
Sodium acid carbonate 10~20%,
Saleratus 10~20%.
2. a kind of green tea probiotics effervescent tablet described in claim 1 and preparation method thereof, it is characterised in that comprise the following steps：
A. prepare compound probiotic bacterium powder the step of, by bifidobacterium lactis, not tally diplobacterium, streptococcus thermophilus, Bao Jiali
Sub- lactobacillus, lactobacillus thermophilus, Lactobacillus plantarum bacterium powder mix 5~15min in powder mixer, are prepared into compound probiotic
Bacterium powder, described bifidobacterium lactis, not tally diplobacterium, streptococcus thermophilus, lactobacillus bulgaricus, lactobacillus thermophilus, plant breast
The mass ratio of bacillus is 1:1:2:2:2:2~6；
B. prepare green-tea extract the step of, green tea is cleaned, is put into micro-wave vacuum case, microwave power 1000~
3000W, vacuum -0.09~-0.03MPa, make moisture≤5% of tealeaves, it is 30~50 purposes that dried green tea, which is crushed,
Granularity, then crushed with ball mill pulverizer, ball material mass ratio is 9~12: 1, and milling time is 15~20h, and rotary table rotating speed is
400r/min, 325 mesh sieves, green tea powder and ethanol solution example 1 in mass ratio are crossed after crushing:The volume of 5~30 mixing, ethanol and water
Than for 4:1~6, microwave radiation exaraction, microwave power is 80~800W, 30~180s of extraction time, extraction, collects green tea extraction
Liquid, it is put into microwave vacuum freeze drying box and is dried, 800~1200W of microwave power, vacuum 0.6MPa, temperature -30
DEG C, moisture≤5% of green-tea extract after drying；
C. a step of dispensing, granulation, compound probiotic bacterium powder, green-tea extract, Compound-acid are weighed according to mass percent
Taste agent, composite sweetener, maltodextrin, magnesium stearate, sodium acid carbonate, saleratus, by green-tea extract, compound acid,
Composite sweetener, maltodextrin, magnesium stearate, sodium acid carbonate, saleratus crushed 100 mesh sieves, by compound probiotic bacterium powder,
Powder of green tea extract, compound acid, composite sweetener, maltodextrin, magnesium stearate be put in powder mixer mixing 5~
15min, then using ethanol solution wet granulation, then sodium acid carbonate and saleratus equally mixed 5 in powder mixer
Use ethanol solution wet granulation after~15min, the volume ratio of ethanol and water is 4 in above-mentioned ethanol solution:1~6；
D. the step of vacuum drying, compression molding, crosses 18 mesh sieves by the material after above-mentioned granulation and obtains wet granular, be placed on vacuum
Dried in drying box, make moisture≤5% of material, then by dried material in tablet press machine compression molding, obtain
The green tea probiotics effervescent tablet.
A kind of 3. green tea probiotics effervescent tablet as claimed in claim 1, it is characterised in that：Acid is compounded by citric acid, apple
Acid and fumaric acid composition, the mass ratio of described citric acid, malic acid and fumaric acid is 1:0.4:0.05.
A kind of 4. green tea probiotics effervescent tablet as claimed in claim 1, it is characterised in that：Compound sweetener is by sucrose, oligomeric wheat
Bud sugar and xylitol composition, the mass ratio of described sucrose, oligomeric maltose and xylitol is 1.2:1:0.07.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109287802A (en) * | 2018-09-12 | 2019-02-01 | 贵州绿色起源科技有限公司 | A kind of instant tea tablet and preparation method thereof |
| CN114027505A (en) * | 2021-11-09 | 2022-02-11 | 仙乐健康科技股份有限公司 | Effervescent tablet for buccal administration in oral cavity |
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Application publication date: 20180112 |