CN107557190A - A kind of 3D printing handmade soap and preparation method thereof - Google Patents
A kind of 3D printing handmade soap and preparation method thereof Download PDFInfo
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- CN107557190A CN107557190A CN201710818203.5A CN201710818203A CN107557190A CN 107557190 A CN107557190 A CN 107557190A CN 201710818203 A CN201710818203 A CN 201710818203A CN 107557190 A CN107557190 A CN 107557190A
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Abstract
The invention belongs to daily chemical product technical field, and in particular to a kind of 3D printing handmade soap and preparation method thereof, the invention is mainly made up of following component and its parts by weight:10 15 parts of 5 10 parts of the compoiste fermented thing of folium artemisiae argyi, 0.5 1 parts of taurine, 57 parts of cetanol, 24 parts of chitosan quaternary ammonium salt, 8 10 parts of coconut oil, 10 15 parts of palmitic acid, 15 20 parts of camellia seed oil, 5 6.8 parts of alkali, 24 parts of emollient and water; the invention has good moisturizing effect, and has good prevention effect to the desquamation of skin.
Description
Technical field
The invention belongs to daily chemical product technical field, and in particular to a kind of 3D printing handmade soap and preparation method thereof.
Background technology
The making of handmade soap is that the process of saponification generation soap occurs with alkali lye using natural oil, prepared by existing handmade soap
During easily cause the waste of heel, and moulding is simple, and the destruction of soap moulding is easily caused in cutting process;Cause
This, is with the development of 3D printing technique, increasing producer's selection production 3D printing handmade soap.
Handmade soap is incessantly attractive in appearance in moulding, and functionally also many samples, handmade soap not only have good cleaning action, and
And can be with skin care.Notification number is that CN102776087B Chinese patent discloses a kind of Multifunctional fancy soap, by weight percentage
Calculating formula includes following components:Surfactant 40%-80%, neat soap 10%-25%, essential oil 0.001%-0.1%, moisturizing
Agent 0.5%-5%, skin conditioner 0.1%-5%, chelating agent 0.05%-0.5%, the essential oil that the Multifunctional fancy soap of the invention uses into
Partial volume is volatile, and availability is low in use.
Notification number is that CN103215152B Chinese patent discloses a kind of preventing and treating pruitus Handmade soap with effect, by Chinese medicine
Extract solution 3-6 parts, olive oil 10-13 parts, coconut oil 5-7 parts, cocoa butter 2-4 parts, beeswax 0.05-0.1 parts, sodium hydroxide 2-4
Part, pure water 4-8 parts are made, and wherein Chinese medicine extract is:Schizonepeta 15-30 parts, windproof 15-30 parts, kuh-seng 30-60 parts, summer cypress
Sub- 10-20 parts, frutus cnidii 15-30 parts, the extract solution of Radix Angelicae Sinensis 10-20 parts and golden cypress 10-20 parts.The invention be by bio-oil with
Saponification reaction is made, and it is thinning that long-term use easily causes skin lipid layer, injures skin.
The content of the invention
In order to solve problems of the prior art, the invention provides a kind of 3D printing handmade soap and its preparation side
Method, the invention pH value is close to neutrality, and excitant is small, and the water soluble starch added makes handmade soap with certain with flaxseed gum
Viscosity, be unlikely to deform during use, and the obtained handmade soap of the invention has the good function of preventing the desquamation of skin.
Technical solution of the present invention is specific as follows:
A kind of 3D printing handmade soap, is mainly made up of following component and its parts by weight:The compoiste fermented thing 5-10 parts of folium artemisiae argyi, ox
Sulfonic acid 0.5-1 parts, cetanol 5-7 parts, chitosan quaternary ammonium salt 2-4 parts, coconut oil 8-10 parts, palmitic acid 10-15 parts, camellia seed oil
15-20 parts, alkali 5-6.8 parts, emollient 2-4 parts and water 9-15 parts.
Further, described 3D printing handmade soap is made up of following component and its parts by weight:The compoiste fermented thing 8 of folium artemisiae argyi
Part, 0.8 part of taurine, 6 parts of cetanol, 3 parts of chitosan quaternary ammonium salt, 9 parts of coconut oil, 13 parts of palmitic acid, 17 parts of camellia seed oil, alkali
12 parts of 5.9 parts, 3 parts of emollient and water.
Further, the preparation method of the compoiste fermented thing of described folium artemisiae argyi is:(1) folium artemisiae argyi and crab shell are cleaned, dried, with
White granulated sugar is well mixed, and is ground to 50-70 mesh, is soaked 30-40 minutes, filtering, and filter residue lucifuge, sealing are placed into 15-20
My god, temperature is 40-45 DEG C, is then down to room temperature, freeze-drying, radiation sterilizing, obtains powders A;(2) powders A is used into high energy
Nanometer impact grinding is crushed to 30-60nm, produces.
Further, the material ratio of folium artemisiae argyi in the preparation method of the compoiste fermented thing of folium artemisiae argyi, crab shell, white granulated sugar and water is 1g:
0.2-0.3g:0.2-0.4g:8-10ml。
Further, described alkali is sodium hydroxide.
Further, described emollient is 1 by weight by saualane and 2-Acetamido-2-deoxy-D-glucose:3-5 is formed.
Preferably, described emollient is 1 by weight by saualane and 2-Acetamido-2-deoxy-D-glucose:4 compositions.
Present invention also offers the preparation method of described 3D printing handmade soap, step is:
S1, water and alkali is mixed and made into alkali lye, standing is cooled to 50-55 DEG C, add while stirring palmitic acid, coconut oil and
Camellia seed oil, 1.5-2h is stirred, chitosan quaternary ammonium salt is then added, stirs, be cooled to 40-45 DEG C, add folium artemisiae argyi fermentation
Compound, taurine, emollient and cetanol, stir, and are down to room temperature, obtain gluing liquid A;
S2, using FDM 3D printer Software for Design shapes, print die, obtained gluing liquid A is then put into mould
In, after placing 2-3 days, demoulding curing 1-3 months, produce.
The present invention using the compoiste fermented thing of folium artemisiae argyi is made using folium artemisiae argyi and crab shell fermentation, and its tunning not only has good
Good antibiotic property, and there is good replenishing water and preserving moisture effect to skin.
Taurine:The present invention uses artificial synthesized taurine, and the compound in cow-bezoar earliest by separating, ox sulphur
Sour chemical property is stable, and Taurine is applied has good anti-oxidant, delaying senility function in skin care item, and taurine
Can also there is preventive and therapeutic effect to frostbite, KCN poisonings and migraines with calm, analgesia and anti-inflammatory.
Chitosan quaternary ammonium salt (CAS:9012-76-4):With its good water-soluble hygroscopicity strong compatibility it is good, can biology
Degraded, and the foam stability of handmade soap of the present invention can be strengthened.
The present invention uses the coconut oil (CAS of different plant and animal materials:8001-31-8), palmitic acid, camellia seed oil phase interworking
5 reduce traditional soap base surfactant excitant, and the chitosan quaternary ammonium salt added is advantageous to soap lye in preparation process
Dispersiveness, strengthen soil release performance.
The present invention also added the compoiste fermented thing of folium artemisiae argyi, taurine and emollient and be used cooperatively, and have to the desquamation of skin good
Good prevention effect.
Compared with prior art, the present invention has advantages below:(1) a kind of 3D printing handmade soap provided by the invention stimulates
Property is small, soil release performance is strong, foam stabilization;(2) a kind of 3D printing handmade soap soap body hardness provided by the invention is big, is not easy softening and causes
Waste, soap availability is high;(3) a kind of 3D printing handmade soap provided by the invention has good replenishing water and preserving moisture effect, and
There is good prevention effect to the desquamation of skin.
Embodiment
Technical solution of the present invention is further described by following examples, those skilled in the art is more understood
Technical solution of the present invention, present component are conventional products, wherein 2-Acetamido-2-deoxy-D-glucose CAS:7512-17-6.
A kind of 3D printing handmade soap of embodiment 1
Described 3D printing handmade soap, is made up of following component and its parts by weight:8 parts of the compoiste fermented thing of folium artemisiae argyi, taurine
0.8 part, 6 parts of cetanol, 3 parts of chitosan quaternary ammonium salt, 9 parts of coconut oil, 13 parts of palmitic acid, 17 parts of camellia seed oil, sodium hydroxide 5.9
11.1 parts of part, 3 parts of emollient and water;
Described emollient is 1 by weight by saualane and 2-Acetamido-2-deoxy-D-glucose:4 compositions;
The preparation method of the compoiste fermented thing of described folium artemisiae argyi is:(1) folium artemisiae argyi and crab shell are cleaned, dried, mixed with white granulated sugar
Close uniformly, be ground to 60 mesh, soak 35 minutes, filter, filter residue lucifuge, sealing are placed 18 days, temperature is 43 DEG C, then
Room temperature, freeze-drying are down to, radiation sterilizing, obtains powders A;(2) powders A is crushed to 35nm using high energy nanometer impact grinding,
Produce, wherein the material ratio of folium artemisiae argyi, crab shell, white granulated sugar and water is 1g:0.25g:0.3g:9ml.
The preparation method of described 3D printing handmade soap is:
S1, water and sodium hydroxide are mixed and made into alkali lye, standing is cooled to 53 DEG C, adds palmitic acid, coconut while stirring
Oil and camellia seed oil, 1.8h is stirred, chitosan quaternary ammonium salt is then added, stirs, be cooled to 43 DEG C, it is multiple to add folium artemisiae argyi fermentation
Compound, taurine, emollient and cetanol, stir, and are down to room temperature, obtain gluing liquid A;
S2, using FDM 3D printer Software for Design it is shaped as alphabetical " A ", print die, the gluing liquid A that then will be obtained
It is put into mould, after placing 2.5 days, demoulding curing 2 months, produces.
A kind of 3D printing handmade soap of embodiment 2
Described 3D printing handmade soap, is made up of following component and its parts by weight:5 parts of the compoiste fermented thing of folium artemisiae argyi, taurine
0.5 part, 5 parts of cetanol, 2 parts of chitosan quaternary ammonium salt, 8 parts of coconut oil, 10 parts of palmitic acid, 15 parts of camellia seed oil, sodium hydroxide 5
16 parts of part, 2 parts of emollient and water;
Described emollient is 1 by weight by saualane and 2-Acetamido-2-deoxy-D-glucose:4 compositions;
The preparation method of the compoiste fermented thing of described folium artemisiae argyi is:(1) folium artemisiae argyi and crab shell are cleaned, dried, mixed with white granulated sugar
Close uniformly, be ground to 50 mesh, soak 40 minutes, filter, filter residue lucifuge, sealing are placed 15 days, temperature is 45 DEG C, then
Room temperature, freeze-drying are down to, radiation sterilizing, obtains powders A;(2) powders A is crushed to 30nm using high energy nanometer impact grinding,
Produce, wherein the material ratio of folium artemisiae argyi, crab shell, white granulated sugar and water is 1g:0.2g:0.4g:8ml.
The preparation method of described 3D printing handmade soap is:
S1, water and sodium hydroxide are mixed and made into alkali lye, standing is cooled to 50 DEG C, adds palmitic acid, coconut while stirring
Oil and camellia seed oil, 1.5h is stirred, chitosan quaternary ammonium salt is then added, stirs, be cooled to 40 DEG C, it is multiple to add folium artemisiae argyi fermentation
Compound, taurine, emollient and cetanol, stir, and are down to room temperature, obtain gluing liquid A;
S2, using FDM 3D printer Software for Design it is shaped as alphabetical " B ", print die, the gluing liquid A that then will be obtained
It is put into mould, after placing 2 days, demoulding curing 1 month, produces.
A kind of 3D printing handmade soap of embodiment 3
Described 3D printing handmade soap, is made up of following component and its parts by weight:10 parts of the compoiste fermented thing of folium artemisiae argyi, taurine
1 part, 7 parts of cetanol, 4 parts of chitosan quaternary ammonium salt, 10 parts of coconut oil, 15 parts of palmitic acid, 20 parts of camellia seed oil, sodium hydroxide 6.8
9.2 parts of part, 4 parts of emollient and water;
Described emollient is 1 by weight by saualane and 2-Acetamido-2-deoxy-D-glucose:4 compositions;
The preparation method of the compoiste fermented thing of described folium artemisiae argyi is:(1) folium artemisiae argyi and crab shell are cleaned, dried, mixed with white granulated sugar
Close uniformly, be ground to 70 mesh, soak 30 minutes, filter, filter residue lucifuge, sealing are placed 20 days, temperature is 40 DEG C, then
Room temperature, freeze-drying are down to, radiation sterilizing, obtains powders A;(2) powders A is crushed to 60nm using high energy nanometer impact grinding,
Produce, wherein the material ratio of folium artemisiae argyi, crab shell, white granulated sugar and water is 1g:0.3g:0.2g:10ml.
The preparation method of described 3D printing handmade soap is:
S1, water and sodium hydroxide are mixed and made into alkali lye, standing is cooled to 55 DEG C, adds palmitic acid, coconut while stirring
Oil and camellia seed oil, 2h is stirred, chitosan quaternary ammonium salt is then added, stirs, be cooled to 45 DEG C, it is compoiste fermented to add folium artemisiae argyi
Thing, taurine, emollient and cetanol, stir, and are down to room temperature, obtain gluing liquid A;
S2, using FDM 3D printer Software for Design it is shaped as alphabetical " C ", print die, the gluing liquid A that then will be obtained
It is put into mould, after placing 3 days, demoulding curing 3 months, produces.
A kind of 3D printing handmade soap of comparative example 1
Described 3D printing handmade soap, is made up of following component and its parts by weight:8 parts of the compoiste fermented thing of folium artemisiae argyi, taurine
0.8 part, 6 parts of honey, 3 parts of chitosan quaternary ammonium salt, 9 parts of coconut oil, 13 parts of palmitic acid, 17 parts of camellia seed oil, sodium hydroxide 5.9
11.1 parts of part, 3 parts of emollient and water;
Described emollient is 1 by weight by saualane and 2-Acetamido-2-deoxy-D-glucose:4 compositions;
The preparation method of the compoiste fermented thing of described folium artemisiae argyi is similar to Example 1.
The preparation method of described 3D printing handmade soap is similar to Example 1.
Difference with embodiment 1 is that cetanol is replaced with into honey.
A kind of 3D printing handmade soap of comparative example 2
Described 3D printing handmade soap, is made up of following component and its parts by weight:8 parts of the compoiste fermented thing of folium artemisiae argyi, taurine
0.8 part, 6 parts of cetanol, 3 parts of chitosan quaternary ammonium salt, 17 parts of coconut oil, 5 parts of palmitic acid, 17 parts of camellia seed oil, sodium hydroxide 5.9
11.1 parts of part, 3 parts of emollient and water;
Described emollient is 1 by weight by saualane and 2-Acetamido-2-deoxy-D-glucose:4 compositions;
The preparation method of the compoiste fermented thing of described folium artemisiae argyi is similar to Example 1.
The preparation method of described 3D printing handmade soap is similar to Example 1.
Difference with embodiment 1 is to reduce the content of palmitic acid, increases the content of coconut oil.
A kind of 3D printing handmade soap of comparative example 3
Described 3D printing handmade soap, is made up of following component and its parts by weight:8 parts of the compoiste fermented thing of folium artemisiae argyi, taurine
0.8 part, 6 parts of cetanol, 3 parts of chitosan quaternary ammonium salt, 9 parts of coconut oil, 13 parts of palmitic acid,
11.1 parts of 17 parts of camellia seed oil, 5.9 parts of sodium hydroxide, 3 parts of emollient and water;
Described emollient is 1 by weight by saualane and hyaluronic acid:4 compositions;
The preparation method of the compoiste fermented thing of described folium artemisiae argyi is similar to Example 1.
The preparation method of described 3D printing handmade soap is similar to Example 1.
Difference with embodiment 1 is that 2-Acetamido-2-deoxy-D-glucose is replaced with into hyaluronic acid.
A kind of 3D printing handmade soap of comparative example 4
Described 3D printing handmade soap, is made up of following component and its parts by weight:8 parts of P-Cymene, 0.8 part of taurine,
6 parts of cetanol, 3 parts of chitosan quaternary ammonium salt, 9 parts of coconut oil, 13 parts of palmitic acid, 17 parts of camellia seed oil, 5.9 parts of sodium hydroxide, profit
11.1 parts of 3 parts of skin agent and water;
Described emollient is 1 by weight by saualane and 2-Acetamido-2-deoxy-D-glucose:4 compositions;
The preparation method of described 3D printing handmade soap is similar to Example 1.
Difference with embodiment 1 is that the compoiste fermented thing of folium artemisiae argyi is replaced with into P-Cymene.
Test example 1, morphological assessment
Subjects:Embodiment 1-3 and 3D printing handmade soap made from comparative example 1;
Test method:Handmade soap metamorphosis made from observation just, it is specific as shown in table 1.
From table 1 it follows that handmade soap made from 1-3 of the embodiment of the present invention has good hardness, forming.Experiment
Example 2, foam evaluations
Subjects:Embodiment 1-3 and 3D printing handmade soap made from comparative example 2;
Test method:Various soap 1.5g are taken, is dissolved, is transferred in 1000mL volumetric flasks with 200mg hard water respectively, and it is dilute
Release to scale, shake up, then solution is placed in (40 ± 0.5) DEG C water bath with thermostatic control and is aged, the total time since being added water-soluble sample
30min, subsequent Roche foam meter measure foam height, record initial foam height, and standing measures foam after 5 minutes
Highly, 2 are specifically shown in Table.
The foam height of table 2 and stability
As shown in Table 2, the soap foaming effect that prepared by 1-3 of the embodiment of the present invention is good, and foam stability is strong, wherein with
The effect of embodiment 1 is best, and soap initial foam made from comparative example 1-2 is highly low, and stability is poor, illustrates aliphatic acid
Composition influences the bubble and foam stability of soap with flaxseed gum.
Test example 3, preventing and treating furfur effect
Subjects:(all products pass through cosmetics to 3D printing handmade soap prepared by embodiment 1-3 and comparative example 3-4
Safe patch test).
Subject:Man:15-30 year, 50 people, female:15-35 year, 100 people, points 5 groups, every group of 30 people, M-F is equal.
Wherein, subject is that face has furfur, and drying caused by causing reason to have (1) environmental change or cosmetics improper use is de-
Water;(2) desquamation of skin caused by fungi.
Test method:The 3D printing handmade soap prepared using embodiment 1-3 and comparative example 3-4 carries out face cleaning, by handmade soap
Wetting massages face 1 minute after getting foam, rinses well, is used continuously 1 month, observes changes in faces, and effect is broadly divided into 4
Individual grade, take a turn for the better completely:Skin becomes smooth, and water is tender;Effectively:Skin no longer furfur, but skin is still dried;Typically:It is de-
Phenomenon is considered to be worth doing to mitigate;It is invalid:There is no any change, it is specific as shown in table 3.
The changes in faces demographics of table 3
From table 3, it is apparent that using 3D printing handmade soap prepared by 1-3 of the embodiment of the present invention with preferably anti-
Control the function of furfur.
Experiment is also tested the moisture of subject's face forehead, left face, right face and chin skin, takes average content,
As a result it is as shown in table 4.
The skin moisture content of table 4
Product | Before use | After 6 hours |
Embodiment 1 | 16.9% | 21.4% |
Embodiment 2 | 16.6% | 20.1% |
Embodiment 3 | 17.0% | 20.3% |
Comparative example 3 | 16.6% | 18.5% |
Comparative example 4 | 16.9% | 18.7% |
As can be known from Table 4,3D printing handmade soap replenishing water and preserving moisture effect is more preferable made from 1-3 of the embodiment of the present invention, comparative example
Moistening effect is poor made from 3-4, and further illustrating inventive formulation can not arbitrarily change.
Claims (8)
1. a kind of 3D printing handmade soap, it is characterised in that be mainly made up of following component and its parts by weight:The compoiste fermented thing of folium artemisiae argyi
5-10 parts, taurine 0.5-1 parts, cetanol 5-7 parts, chitosan quaternary ammonium salt 2-4 parts, coconut oil 8-10 parts, palmitic acid 10-15
Part, camellia seed oil 15-20 parts, alkali 5-6.8 parts, emollient 2-4 parts and water 9-15 parts.
2. 3D printing handmade soap according to claim 1, it is characterised in that be made up of following component and its parts by weight:Chinese mugwort
8 parts of the compoiste fermented thing of leaf, 0.8 part of taurine, 6 parts of cetanol, 3 parts of chitosan quaternary ammonium salt, 9 parts of coconut oil, 13 parts of palmitic acid, mountain
12 parts of 17 parts of tea-seed oil, 5.9 parts of alkali, 3 parts of emollient and water.
3. 3D printing handmade soap according to claim 1 or 2, it is characterised in that the system of the compoiste fermented thing of described folium artemisiae argyi
Preparation Method is:(1) folium artemisiae argyi and crab shell are cleaned, dried, be well mixed with white granulated sugar, be ground to 50-70 mesh, soak 30-
40 minutes, filtering, filter residue lucifuge, sealing are placed 15-20 days, temperature is 40-45 DEG C, is then down to room temperature, freeze-drying, spoke
According to sterilization, powders A is obtained;(2) powders A is crushed to 30-60nm using high energy nanometer impact grinding, produced.
4. 3D printing handmade soap according to claim 3, it is characterised in that ended in the preparation method of the compoiste fermented thing of folium artemisiae argyi
Leaf, crab shell, the material ratio of white granulated sugar and water are 1g:0.2-0.3g:0.2-0.4g:8-10ml.
5. 3D printing handmade soap according to claim 1 or 2, it is characterised in that described alkali is sodium hydroxide.
6. 3D printing handmade soap according to claim 1 or 2, it is characterised in that described emollient is by saualane and N-
Acetylglucosamine is 1 by weight:3-5 is formed.
7. 3D printing handmade soap according to claim 6, it is characterised in that described emollient is by saualane and N- acetyl
Glucosamine is 1 by weight:4 compositions.
8. the preparation method of the 3D printing handmade soap according to claim any one of 1-7, it is characterised in that step is:
S1, water and alkali are mixed and made into alkali lye, standing is cooled to 50-55 DEG C, adds palmitic acid, coconut oil and camellia while stirring
Seed oil, stirs 1.5-2h, then adds chitosan quaternary ammonium salt, stir, and is cooled to 40-45 DEG C, and it is compoiste fermented to add folium artemisiae argyi
Thing, taurine, emollient and cetanol, stir, and are down to room temperature, obtain gluing liquid A;
S2, using FDM 3D printer Software for Design shapes, print die, then obtained gluing liquid A is put into mould, put
After putting 2-3 days, demoulding curing 1-3 months, produce.
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