CN107555806A - A kind of heat-insulated Low E glass of individual layer durability building heat preservation and preparation method - Google Patents
A kind of heat-insulated Low E glass of individual layer durability building heat preservation and preparation method Download PDFInfo
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Abstract
The invention belongs to the preparing technical field of New Building Materials, there is provided a kind of heat-insulated Low E glass of individual layer durability building heat preservation and preparation method.By under nitrogen protection, making glass in the presence of the auxiliary agents such as fluxing agent, fining agent, high-temperature fusion; then add silver powder and be uniformly dispersed; coating liquid is formed, and coating liquid is evenly applied to glass pane surface, forms functional membrane; again through tempering; the coating process of Low E glass is not only simplified, and silver powder is closed in glass, greatly improves its durability; mechanical damage and extraneous erosion can be effectively prevented, is increased the service life.And preparation technology is simple, cost is relatively low, can accomplish scale production.
Description
Technical field
It is heat-insulated more particularly, to a kind of individual layer durability building heat preservation the present invention relates to the preparation field of New Building Materials
Low-E glass and preparation method.
Background technology
The development of construction material be with the development of society, the continuous improvement of scientific and technological level and enrich constantly, from it most
It is basic meet that living needs arrives current high-strength light, high-durability, asepsis environment-protecting, energy-conserving and environment-protective, antidetonation, etc. it is many newly
Functional requirement, make construction material from it is passive with research application based on to exploitation New function, new application new material direction
Transformation.
" New Building Materials ", abbreviation building material, it is the Building wood for being different from the building materials such as traditional ash, sandstone, brick and tile
Expect new varieties, be caused a new generation's upgrading construction material on the basis of traditional building material, in the industry by novel building material
The scope of material has been made clearly to define, and New Building Materials mainly have novel wall material, new waterproof encapsulant, new guarantor
The warm major class of heat-barrier material and decorating and renovating material four.When the low-carbon epoch arrive, energy-saving, Transformation Development is advocated in country
Overall background under, green low-carbon, energy-conserving and environment-protective have become the unavoidable mission of building material.Therefore, with it is green,
Profit is useless, heat-insulated, is incubated, prevents fires, be light, high-strength, substituting, cost is cheap, section is native, save land therefrom obtains for the building material of target
Huge development new opportunities.The industrial output value of building material grows beyond 14% year, working enterprise exceedes more than 600,000,000,000 yuan
Family more than 5000.At present, constantly building material is developed, particularly some Composites, multifunction, energy-saving, greenization, light
The building material of matter high strengthening occupies the proportion of traditional construction material more than 50%.
The construction of China's building with use the situation that to be chronically at energy high energy consumption, utilization ratio low.Building energy conservation is
It is the hot issue that people pay close attention to jointly, and a key link of architecture field the Implement of sustainable development strategy.Build in China
Energy-conservation can be divided into two parts, first, building and heating, air-conditioning and the energy-conservation of illumination;Second, the energy-conservation of building itself.And influence to build
It is architectural exterior-protecting construction to build the most direct factor of energy consumption, and the most weak link of thermal property is window in building enclosure.Building
In terms of building energy consumption, China's building doors and windows heat dissipation capacity accounts for more than the 50% of the total heat dissipation capacity of building external, therefore improves the thermal insulation separation of door and window
Hot property is to reduce the effective way of building energy consumption.
Low-E glass is also known as low emissivity glass, be glass surface plate multiple layer metal or other compound groups into film
It is product.Its film plating layer has to the characteristic of visible ray high transmission and centering far infrared high reflection, make it with simple glass and
Traditional coated glass for building is compared, and has excellent effect of heat insulation and good translucency.As insulations such as curtain walls
Special glass.
High yet with Low-E glass visible light transmissivity, solar heat is easily accessible interior, it usually needs is prepared into hollow
To lift heat-proof quality.And plated film is easily damaged, the hollow double-deck mode of generally use protects plated film, therefore, Low-E glass
Cavitation, add the cost and weight of glass curtain wall.
The content of the invention
Easily got in for existing Low-E glass sunshines thermal capacitance, the defects of plated film is easily damaged, the present invention proposes a kind of
The heat-insulated Low-E glass of individual layer durability building heat preservation and preparation method.Its technology point be under nitrogen protection, in advance by silver powder with
Melten glass liquid is scattered to form coating liquid, is ready for glass plate, glass plate is preheated, coating liquid is evenly coated in into glass plate
On, form the heat-insulated Low-E glass of individual layer durability building heat preservation.Its significant advantage is that not only have to ultraviolet lamp heat radiation
Block, and form coating liquid by the way that silver powder and glass metal are scattered so that silver powder functional membrane effectively prevents damage and the external world
Corrode.This method method preparation technology is simple, and cost is low and is easy to mass produce.
To achieve the above object, adopt the following technical scheme that:
A kind of preparation method of the heat-insulated Low-E glass of individual layer durability building heat preservation, contains silver by prefabricated under nitrogen protection
The glass coating film liquid of powder;Then coating liquid is evenly applied to glass pane surface, forms functional membrane, then through tempering, you can it is made
The heat-insulated Low-E glass of individual layer durability building heat preservation, is comprised the following steps that:
(1)Under nitrogen atmosphere, glass and fluxing agent, fining agent are added in smelting furnace by certain mass ratio, high temperature adds
Then heat adds the silver powder of certain mass, 5-10min is then stirred in thermostatic mixer, obtains coating liquid to glass melting;
(2)Glass plate is carried out by size by cutting using Full-automatic glass cutting, edging is then carried out using edge polisher;Then
Strengthening preheating processing is carried out to glass plate using the mode of heating of advection;Again by step(1)The coating liquid of gained passes through pressure
Contracting stream of nitrogen gas is uniformly applied to glass pane surface, has formed the functional membrane of stop and protective effect;
(3)By step(2)The glass plate of film is placed in progress tempering processing in annealing furnace, you can it is for building to obtain individual layer durability
Low-E glass.
Preferably, step(1)The fluxing agent is calcium carbonate, lithium borate;
Preferably, step(1)The usage amount of the fluxing agent is the 5 ~ 10% of glass quality;
Preferably, step(1)The fining agent is sodium sulphate, antimony oxide or sodium chloride;
Preferably, step(1)The usage amount of the fining agent is the 0.3 ~ 0.5% of glass quality;
Preferably, step(1)The temperature of the heating melting is 1300 ~ 1400 DEG C;
Preferably, step(1)The addition of the silver powder is the 15 ~ 20% of glass quality;
Preferably, step(1)The temperature of the thermostatic mixer is 1400 ~ 1500 DEG C, mixing speed 50-100r/min;
Preferably, step(2)Described compressed nitrogen stream pressure is 2-3.5MPa;
Preferably, step(3)The annealing furnace is forced convection oven, and its counter-flow jet is in furnace roof, to squeeze into compressed air realization
Forced convertion;The furnace temperature of the annealing furnace is 680 ~ 720 DEG C, and the tempering heat time is 30 ~ 50s.
A kind of heat-insulated Low-E glass of individual layer durability building heat preservation, is prepared by method described above.It is therein by silver
Powder is used as coating solution with being scattered in glass metal, not only simplifies the coating process of Low-E glass, and silver powder is closed
In glass, its durability is greatly improved.
Generally, during glass melting, fluxing agent is added, the silicic acid in promoting glass in the range of lower temperature
Salt reacts, simultaneously because the formation of eutectic, surface tension reduces, and viscosity reduces, and fluxing agent can also promote each group to share in the benefit
The reinforcing of wet effect, strengthen each interface cohesion.And the effect of fining agent eliminates in the bubble in glass metal is promoted, drop can be passed through
Low viscosity of glass metal or pyrolytic produce gas to realize.The smearing of coating liquid should ensure that dynamics is uniform with thickness, its thickness
The protecting effect of protective layer is directly related to, should meet that 680 ~ 720 DEG C of tempering temperature can be born, and can ensures moulded products
Damage and outside erosion can effectively be prevented.When prepared by coating liquid, effective stirring can improve operation while quality is ensured
Stability, increase yield, meanwhile, the inhomogeneities of formed glass liquid can be effectively improved, reduce the density fluctuation of glass metal,
Promote the dispersed of silver powder, improve the surface smoothness after smearing.The temperature and time of heating tempering all should be controlled effectively
System, heating-up temperature is too high or overlong time, glass film layers will burn, and causes stripping phenomenon.Heating-up temperature is too low or time mistake
Short, tempering quality is difficult to reach requirement.
A kind of heat-insulated Low-E glass of individual layer durability building heat preservation of the present invention and preparation method, by under nitrogen protection,
Make glass in the presence of the auxiliary agents such as fluxing agent, fining agent, high-temperature fusion, then add silver powder and be uniformly dispersed, form coating liquid,
And coating liquid is evenly applied to glass pane surface, form functional membrane, then through tempering, not only simplify the plated film of Low-E glass
Technique, and silver powder is closed in glass, greatly improves its durability.Compared with prior art, its protrude the characteristics of and
Excellent effect is:
1. Low-E glass produced by the present invention forms functional membrane using silver powder coating liquid, mechanical damage and the external world can be effectively prevented
Corrode, increase the service life.The defects of overcoming traditional directly plated film easy damaged.
2. Low-E glass visible ray high transmission excellent performance produced by the present invention, mid and far infrared line reflection characteristic is obvious, its
Heat-insulating property and heat-proof quality are all preferable.
3. Low-E glass produced by the present invention is single layer structure, compared with hollow double-layer structure, hence it is evident that reduce and be prepared into
The weight of sheet and unit area.
4. preparation technology of the present invention is simple, cost is relatively low, can accomplish scale production.
Embodiment
Below by way of embodiment, the present invention is described in further detail, but this should not be interpreted as to the present invention
Scope be only limitted to following example.In the case where not departing from above method thought of the present invention, according to ordinary skill
The various replacements or change that knowledge and customary means are made, should be included in the scope of the present invention.
Embodiment 1
(1)Under nitrogen atmosphere, 100kg glass and 5kg fluxing agents calcium carbonate, 0.3kg fining agent sodium sulphate are added to smelting furnace
In, it is heated at high temperature to 1300 ~ 1400 DEG C of glass meltings, 15kg silver powder is then added, 1400 ~ 1500 in thermostatic mixer
DEG C, mixing speed 50r/min;5-10min is stirred, obtains coating liquid;
(2)Glass plate is carried out by size by cutting using Full-automatic glass cutting, edging is then carried out using edge polisher;Then
Strengthening preheating processing is carried out to glass plate using the mode of heating of advection;Again by step(1)The coating liquid of gained passes through pressure
Contracting stream of nitrogen gas is uniformly applied to glass pane surface under the conditions of pressure 2MPa, has formed the functional membrane of stop and protective effect;
(3)By step(2)The glass plate of film is placed in annealing furnace, and annealing furnace is forced convection oven, its counter-flow jet in furnace roof,
Forced convertion is realized to squeeze into compressed air;The furnace temperature of the annealing furnace is 680 ~ 720 DEG C, and the tempering heat time is 30s, is carried out
Tempering processing, you can obtain individual layer durability Low-E glass for building.
The Low-E glass obtained to embodiment 1, tests its radiance, shading coefficient and heat transfer coefficient, and with common float glass process
Glass, the performance of gas phase plated film individual layer Low-E glass compare, and obtained data are as shown in table 1.
Embodiment 2
(1)Under nitrogen atmosphere, 100kg glass and 6kg fluxing agents calcium carbonate, 0.5kg fining agent antimony oxides are added to smelting furnace
In, it is heated at high temperature to 1300 ~ 1400 DEG C of glass meltings, 15kg silver powder is then added, 1400 ~ 1500 in thermostatic mixer
DEG C, mixing speed 80r/min;10min is stirred, obtains coating liquid;
(2)Glass plate is carried out by size by cutting using Full-automatic glass cutting, edging is then carried out using edge polisher;Then
Strengthening preheating processing is carried out to glass plate using the mode of heating of advection;Again by step(1)The coating liquid of gained passes through pressure
Contracting stream of nitrogen gas is uniformly applied to glass pane surface under the conditions of pressure 2.5MPa, has formed the function of stop and protective effect
Film;
(3)By step(2)The glass plate of film is placed in annealing furnace, and annealing furnace is forced convection oven, its counter-flow jet in furnace roof,
Forced convertion is realized to squeeze into compressed air;The furnace temperature of the annealing furnace is 680 ~ 720 DEG C, and the tempering heat time is 35s, is carried out
Tempering processing, you can obtain individual layer durability Low-E glass for building.
The Low-E glass obtained to embodiment 2, tests its radiance, shading coefficient and heat transfer coefficient, and with common float glass process
Glass, the performance of gas phase plated film individual layer Low-E glass compare, and obtained data are as shown in table 1.
Embodiment 3
(1)Under nitrogen atmosphere, 100kg glass and 8kg fluxing agents lithium borate, 0.4kg fining agent sodium chloride are added to smelting furnace
In, it is heated at high temperature to 1300 ~ 1400 DEG C of glass meltings, 18kg silver powder is then added, 1400 ~ 1500 in thermostatic mixer
DEG C, mixing speed 100r/min;10min is stirred, obtains coating liquid;
(2)Glass plate is carried out by size by cutting using Full-automatic glass cutting, edging is then carried out using edge polisher;Then
Strengthening preheating processing is carried out to glass plate using the mode of heating of advection;Again by step(1)The coating liquid of gained passes through pressure
Contracting stream of nitrogen gas is uniformly applied to glass pane surface under the conditions of pressure 3.0MPa, has formed the function of stop and protective effect
Film;
(3)By step(2)The glass plate of film is placed in annealing furnace, and annealing furnace is forced convection oven, its counter-flow jet in furnace roof,
Forced convertion is realized to squeeze into compressed air;The furnace temperature of the annealing furnace is 680 ~ 720 DEG C, and the tempering heat time is 40s, is carried out
Tempering processing, you can obtain individual layer durability Low-E glass for building.
The Low-E glass obtained to embodiment 3, tests its radiance, shading coefficient and heat transfer coefficient, and with common float glass process
Glass, the performance of gas phase plated film individual layer Low-E glass compare, and obtained data are as shown in table 1.
Embodiment 4
(1)Under nitrogen atmosphere, 100kg glass and 10kg fluxing agents lithium borate, 0.5kg fining agent sodium sulphate are added to smelting furnace
In, it is heated at high temperature to 1300 ~ 1400 DEG C of glass meltings, 20kg silver powder is then added, 1400 ~ 1500 in thermostatic mixer
DEG C, mixing speed 50r/min;8min is stirred, obtains coating liquid;
(2)Glass plate is carried out by size by cutting using Full-automatic glass cutting, edging is then carried out using edge polisher;Then
Strengthening preheating processing is carried out to glass plate using the mode of heating of advection;Again by step(1)The coating liquid of gained passes through pressure
Contracting stream of nitrogen gas is uniformly applied to glass pane surface under the conditions of pressure 2MPa, has formed the functional membrane of stop and protective effect;
(3)By step(2)The glass plate of film is placed in annealing furnace, and annealing furnace is forced convection oven, its counter-flow jet in furnace roof,
Forced convertion is realized to squeeze into compressed air;The furnace temperature of the annealing furnace is 680 ~ 720 DEG C, and the tempering heat time is 50s, is carried out
Tempering processing, you can obtain individual layer durability Low-E glass for building.
The Low-E glass obtained to embodiment 4, tests its radiance, shading coefficient and heat transfer coefficient, and with common float glass process
Glass, the performance of gas phase plated film individual layer Low-E glass compare, and obtained data are as shown in table 1.
Embodiment 5
(1)Under nitrogen atmosphere, 100kg glass and 8kg fluxing agents calcium carbonate, 0.3kg fining agents are added in smelting furnace, high temperature
1300 ~ 1400 DEG C of glass meltings are heated to, then add 18kg silver powder, 1400 ~ 1500 DEG C in thermostatic mixer, stirring speed
Spend for 80r/min;10min is stirred, obtains coating liquid;
(2)Glass plate is carried out by size by cutting using Full-automatic glass cutting, edging is then carried out using edge polisher;Then
Strengthening preheating processing is carried out to glass plate using the mode of heating of advection;Again by step(1)The coating liquid of gained passes through pressure
Contracting stream of nitrogen gas is uniformly applied to glass pane surface under the conditions of pressure 3.5MPa, has formed the function of stop and protective effect
Film;
(3)By step(2)The glass plate of film is placed in annealing furnace, and annealing furnace is forced convection oven, its counter-flow jet in furnace roof,
Forced convertion is realized to squeeze into compressed air;The furnace temperature of the annealing furnace is 680 ~ 720 DEG C, and the tempering heat time is 30s, is carried out
Tempering processing, you can obtain individual layer durability Low-E glass for building.
The Low-E glass obtained to embodiment 5, tests its radiance, shading coefficient and heat transfer coefficient, and with common float glass process
Glass, the performance of gas phase plated film individual layer Low-E glass compare, and obtained data are as shown in table 1.
Table 1:
From table 1:
The heat-insulated Low-E glass of individual layer durability building heat preservation produced by the present invention, with common float glass, conventional gas-phase plated film list
Layer Low-E glass is compared, and its radiance substantially reduces, and has excellent heat insulation effect and effect of heat insulation.Its durability is preferable.
Claims (9)
1. a kind of preparation method of the heat-insulated Low-E glass of individual layer durability building heat preservation, by under nitrogen protection it is prefabricated containing
The glass coating film liquid of silver powder;Then coating liquid is evenly applied to glass pane surface, forms functional membrane, then through tempering, you can system
The heat-insulated Low-E glass of individual layer durability building heat preservation is obtained, is comprised the following steps that:
(1)Under nitrogen atmosphere, glass and fluxing agent, fining agent are added in smelting furnace by certain mass ratio, high temperature adds
Then heat adds the silver powder of certain mass, 5-10min is then stirred in thermostatic mixer, obtains coating liquid to glass melting;
(2)Glass plate is carried out by size by cutting using Full-automatic glass cutting, edging is then carried out using edge polisher;Then
Strengthening preheating processing is carried out to glass plate using the mode of heating of advection;Again by step(1)The coating liquid of gained passes through pressure
Contracting stream of nitrogen gas is uniformly applied to glass pane surface, has formed the functional membrane of stop and protective effect;
(3)By step(2)The glass plate of film is placed in progress tempering processing in annealing furnace, you can it is for building to obtain individual layer durability
Low-E glass.
2. a kind of preparation method of the heat-insulated Low-E glass of individual layer durability building heat preservation, its feature exist according to claim 1
In:Step(1)The fluxing agent is calcium carbonate, lithium borate;The usage amount of the fluxing agent is the 5 ~ 10% of glass quality.
3. a kind of preparation method of the heat-insulated Low-E glass of individual layer durability building heat preservation, its feature exist according to claim 1
In:Step(1)The fining agent is sodium sulphate, antimony oxide or sodium chloride;The usage amount of the fining agent is the 0.3 of glass quality
~0.5%。
4. a kind of preparation method of the heat-insulated Low-E glass of individual layer durability building heat preservation, its feature exist according to claim 1
In:Step(1)The temperature of the heating melting is 1300 ~ 1400 DEG C.
5. a kind of preparation method of the heat-insulated Low-E glass of individual layer durability building heat preservation, its feature exist according to claim 1
In:Step(1)The addition of the silver powder is the 15 ~ 20% of glass quality.
6. a kind of preparation method of the heat-insulated Low-E glass of individual layer durability building heat preservation, its feature exist according to claim 1
In:Step(1)The temperature of the thermostatic mixer is 1400 ~ 1500 DEG C, mixing speed 50-100r/min.
7. a kind of preparation method of the heat-insulated Low-E glass of individual layer durability building heat preservation, its feature exist according to claim 1
In:Step(2)Described compressed nitrogen stream pressure is 2-3.5MPa.
8. a kind of preparation method of the heat-insulated Low-E glass of individual layer durability building heat preservation, its feature exist according to claim 1
In:Step(3)The annealing furnace is forced convection oven, and its counter-flow jet realizes forced convertion in furnace roof to squeeze into compressed air;
The furnace temperature of the annealing furnace is 680 ~ 720 DEG C, and the tempering heat time is 30 ~ 50s.
9. a kind of heat-insulated Low-E glass of individual layer durability building heat preservation, is prepared into by any one of claim 1-8 methods described
Arrive.
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CN105705474A (en) * | 2013-11-15 | 2016-06-22 | 法国圣戈班玻璃厂 | Glazing comprising a substrate coated with a stack comprising a functional layer made from silver and a thick blocking underlayer made from tiox |
CN105923992A (en) * | 2016-04-22 | 2016-09-07 | 江苏通天光学科技有限公司 | Novel heat-insulating glass and preparation method thereof |
CN106116160A (en) * | 2016-06-20 | 2016-11-16 | 东莞市银建玻璃工程有限公司 | A kind of can the off-line gold list silver LOW E glass and preparation method thereof of tempering |
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US20020142149A1 (en) * | 1999-03-31 | 2002-10-03 | Central Glass Company, Limited | Frequency selevetive plate and method for producing same |
CN101353230A (en) * | 2007-07-24 | 2009-01-28 | 费罗公司 | Ultra low-emissivity (ultra low E) silver coating |
CN201400639Y (en) * | 2009-04-28 | 2010-02-10 | 江苏蓝星玻璃有限公司 | Low-emissivity coated glass |
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CN105705474A (en) * | 2013-11-15 | 2016-06-22 | 法国圣戈班玻璃厂 | Glazing comprising a substrate coated with a stack comprising a functional layer made from silver and a thick blocking underlayer made from tiox |
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Application publication date: 20180109 |