CN105924047B - A kind of high temperature resistant environment-protective composite architectural materials and preparation method thereof - Google Patents
A kind of high temperature resistant environment-protective composite architectural materials and preparation method thereof Download PDFInfo
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- CN105924047B CN105924047B CN201610292734.0A CN201610292734A CN105924047B CN 105924047 B CN105924047 B CN 105924047B CN 201610292734 A CN201610292734 A CN 201610292734A CN 105924047 B CN105924047 B CN 105924047B
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/20—Mortars, concrete or artificial stone characterised by specific physical values for the density
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/30—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values
- C04B2201/32—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values for the thermal conductivity, e.g. K-factors
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a kind of high temperature resistant environment-protective composite architectural materials and preparation method thereof, it is prepared by silicate fiber, cement, zirconium oxide, antimony oxide, magnesium stearate, cis- isoprene rubber, crushed crude pearlite, diatomite, dibatyl phithalate, lignosulfonates, phenolic resin, line borate, epoxy resin, polyvinyl chloride resin and kayexalate, after above-mentioned each material is mixed, heating stirring, reaction is vacuumized, is cooled to, is dried, compacting, you can.The thermal coefficient of construction material of the present invention is good, it is fixed-type good, with good fire-proof high-temperature resistant effect, and the construction material can be with accumulation of heat or cold-storage, make that the hot-fluid fluctuating range between architecture indoor and outdoor weakens, action time is delayed by, to reduce fluctuations in indoor temperature, comfort is improved, saves energy consumption；It is preparation process simple process of the present invention, easy to operate.
Description
Technical field
The present invention relates to building material field, specifically a kind of high temperature resistant environment-protective composite architectural materials and preparation method thereof.
Background technology
With the development and improvement of living standard of social economy, requirement of the people to indoor environment comfort level is also increasingly
Height, air conditioning energy consumption significantly increase therewith, cause that too fast energy consumption, environmental pollution increase, network load peak-valley difference be excessive, peak
When load the problems such as supply of electric power wretched insufficiency.Energy conservation and environmental protection work is increasingly paid attention in countries in the world, and China has made and issued one
Series energy-saving environmental protection policy promotes energy conservation and environmental protection new building material industry development, the usage amount of construction material also to reach new
Peak.And resulting building and heating and refrigeration increase considerably, and will if things go on like this lead to the serious energy and environmental crisis,
Therefore, energy-saving building technology has obtained extensive concern and attention.
Construction material have developed rapidly, and uses good heat preservation technology and material in industry and building, can often play
The effect got twice the result with half the effort.Conventional insulation only has single resistive properties, does not have energy-saving and temperature-regulating function, and flameproof effect is not
It is too ideal, non-refractory, therefore research to construction material and improve the emphasis for always also being building trade.
Invention content
It is above-mentioned to solve the purpose of the present invention is to provide a kind of high temperature resistant environment-protective composite architectural materials and preparation method thereof
The problem of being proposed in background technology.
To achieve the above object, the present invention provides the following technical solutions：
A kind of high temperature resistant environment-protective composite architectural materials, are prepared by the raw material of following parts by weight：Silicate fiber 60~80
Part, 30~40 parts of cement, 20~30 parts of zirconium oxide, 15~21 parts of antimony oxide, 12~16 parts of magnesium stearate, cis- isoamyl rubber
35~45 parts of glue, 12~18 parts of crushed crude pearlite, 30~40 parts of diatomite, 25~35 parts of dibatyl phithalate, lignin sulfonic acid
27~33 parts of salt, 21~24 parts of phenolic resin, 17~19 parts of line borate, 23~25 parts of epoxy resin, 31~35 parts of polyvinyl chloride resin,
19~21 parts of kayexalate.
A kind of preparation method of the high temperature resistant environment-protective composite architectural materials, specific preparation process are as follows:
(1) silicate fiber, cement, zirconium oxide, antimony oxide, magnesium stearate and diatomite are ground respectively, mixing is equal
It is even, obtain mixture A；
(2) crushed crude pearlite, dibatyl phithalate and lignosulfonates are added in mixture A, it is heated to 100~
120 DEG C, 3~4h is stirred, mixture B is obtained；
(3) temperature of cooling mixture is separately added into cis- isoprene rubber, phenolic resin, line borate, ring to 40~50 DEG C
Oxygen resin, polyvinyl chloride resin, kayexalate, temperature rise to 130~150 DEG C, vacuumize 30~40min of reaction；
(4) 40~50 DEG C are cooled to, is dried in an oven, is suppressed, you can.
Compared with prior art, the beneficial effects of the invention are as follows：The thermal coefficient of construction material of the present invention is good, fixed-type
It is good, there is good fire-proof high-temperature resistant effect, and the construction material can be made with accumulation of heat or cold-storage between architecture indoor and outdoor
Hot-fluid fluctuating range weaken, action time is delayed by, to reduce fluctuations in indoor temperature, improve comfort, save energy consumption；This
It is the simple process of invention preparation process, easy to operate.
Specific implementation mode
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
High temperature resistant environment-protective composite architectural materials are prepared by the raw material of following parts by weight：60 parts of silicate fiber, cement 40
Part, 20 parts of zirconium oxide, 21 parts of antimony oxide, 12 parts of magnesium stearate, 45 parts of cis- isoprene rubber, 12 parts of crushed crude pearlite, diatom
40 parts of soil, 25 parts of dibatyl phithalate, 33 parts of lignosulfonates, 21 parts of phenolic resin, 19 parts of line borate, epoxy resin 23
Part, 35 parts of polyvinyl chloride resin, 19 parts of kayexalate.
The preparation process of high temperature resistant environment-protective composite architectural materials is as follows in above-described embodiment:
(1) silicate fiber, cement, zirconium oxide, antimony oxide, magnesium stearate and diatomite are ground respectively, mixing is equal
It is even, obtain mixture A；
(2) crushed crude pearlite, dibatyl phithalate and lignosulfonates are added in mixture A, are heated to 100 DEG C,
4h is stirred, mixture B is obtained；
(3) temperature of cooling mixture is separately added into cis- isoprene rubber, phenolic resin, line borate, asphalt mixtures modified by epoxy resin to 40 DEG C
Fat, polyvinyl chloride resin, kayexalate, temperature rise to 130 DEG C, vacuumize reaction 40min；
(4) 40 DEG C are cooled to, is dried in an oven, is suppressed, you can.
After testing, the thermal coefficient of construction material of the present invention is 0.07W/ (mK), and transition temperature range is 12~35 DEG C,
Latent heat of phase change value is 40J/g, apparent density 625kg/m3, compression strength 1.28MPa, water absorption rate 9%.
Embodiment 2
High temperature resistant environment-protective composite architectural materials are prepared by the raw material of following parts by weight：70 parts of silicate fiber, cement 35
Part, 25 parts of zirconium oxide, 18 parts of antimony oxide, 14 parts of magnesium stearate, 40 parts of cis- isoprene rubber, 15 parts of crushed crude pearlite, diatom
35 parts of soil, 30 parts of dibatyl phithalate, 30 parts of lignosulfonates, 22 parts of phenolic resin, 18 parts of line borate, epoxy resin 24
Part, 33 parts of polyvinyl chloride resin, 20 parts of kayexalate.
The preparation process of high temperature resistant environment-protective composite architectural materials is as follows in above-described embodiment:
(1) silicate fiber, cement, zirconium oxide, antimony oxide, magnesium stearate and diatomite are ground respectively, mixing is equal
It is even, obtain mixture A；
(2) crushed crude pearlite, dibatyl phithalate and lignosulfonates are added in mixture A, are heated to 110 DEG C,
3.5h is stirred, mixture B is obtained；
(3) temperature of cooling mixture is separately added into cis- isoprene rubber, phenolic resin, line borate, asphalt mixtures modified by epoxy resin to 45 DEG C
Fat, polyvinyl chloride resin, kayexalate, temperature rise to 140 DEG C, vacuumize reaction 35min；
(4) 45 DEG C are cooled to, is dried in an oven, is suppressed, you can.
After testing, the thermal coefficient of construction material of the present invention is 0.08W/ (mK), and transition temperature range is 15~30 DEG C,
Latent heat of phase change value is 65J/g, apparent density 577kg/m3, compression strength 1.55MPa, water absorption rate 8%.
Embodiment 3
High temperature resistant environment-protective composite architectural materials are prepared by the raw material of following parts by weight：80 parts of silicate fiber, cement 30
Part, 30 parts of zirconium oxide, 15 parts of antimony oxide, 16 parts of magnesium stearate, 35 parts of cis- isoprene rubber, 18 parts of crushed crude pearlite, diatom
30 parts of soil, 35 parts of dibatyl phithalate, 27 parts of lignosulfonates, 24 parts of phenolic resin, 17 parts of line borate, epoxy resin 25
Part, 31 parts of polyvinyl chloride resin, 21 parts of kayexalate.
The preparation process of high temperature resistant environment-protective composite architectural materials is as follows in above-described embodiment:
(1) silicate fiber, cement, zirconium oxide, antimony oxide, magnesium stearate and diatomite are ground respectively, mixing is equal
It is even, obtain mixture A；
(2) crushed crude pearlite, dibatyl phithalate and lignosulfonates are added in mixture A, are heated to 120 DEG C,
3h is stirred, mixture B is obtained；
(3) temperature of cooling mixture is separately added into cis- isoprene rubber, phenolic resin, line borate, asphalt mixtures modified by epoxy resin to 50 DEG C
Fat, polyvinyl chloride resin, kayexalate, temperature rise to 150 DEG C, vacuumize reaction 30min；
(4) 50 DEG C are cooled to, is dried in an oven, is suppressed, you can.
After testing, the thermal coefficient of construction material of the present invention is 0.12W/ (mK), and transition temperature range is 10~30 DEG C,
Latent heat of phase change value is 60J/g, apparent density 695kg/m3, compression strength 1.35MPa, water absorption rate 10%.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
Claims (2)
1. a kind of high temperature resistant environment-protective composite architectural materials, which is characterized in that be prepared by the raw material of following parts by weight：Silicic acid is fine
60~80 parts of dimension, 30~40 parts of cement, 20~30 parts of zirconium oxide, 15~21 parts of antimony oxide, 12~16 parts of magnesium stearate are suitable
35~45 parts of formula isoprene rubber, 12~18 parts of crushed crude pearlite, 30~40 parts of diatomite, 25~35 parts of dibatyl phithalate, wood
27~33 parts of mahogany sulfonate, 21~24 parts of phenolic resin, 17~19 parts of line borate, 23~25 parts of epoxy resin, polyvinyl chloride resin 31
~35 parts, 19~21 parts of kayexalate.
2. the preparation method of high temperature resistant environment-protective composite architectural materials according to claim 1, which is characterized in that specific to prepare
Steps are as follows:
(1) silicate fiber, cement, zirconium oxide, antimony oxide, magnesium stearate and diatomite are ground respectively, is uniformly mixed, obtains
Mixture A；
(2) crushed crude pearlite, dibatyl phithalate and lignosulfonates are added in mixture A, are heated to 100~120 DEG C,
3~4h is stirred, mixture B is obtained；
(3) temperature of cooling mixture is separately added into cis- isoprene rubber, phenolic resin, line borate, asphalt mixtures modified by epoxy resin to 40~50 DEG C
Fat, polyvinyl chloride resin, kayexalate, temperature rise to 130~150 DEG C, vacuumize 30~40min of reaction；
(4) 40~50 DEG C are cooled to, is dried in an oven, is suppressed, you can.
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| CN105924047B true CN105924047B (en) | 2018-07-20 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106587849A (en) * | 2016-12-22 | 2017-04-26 | 郑州丽福爱生物技术有限公司 | Environment-friendly composite building material and preparation method thereof |
| CN108002747A (en) * | 2017-12-13 | 2018-05-08 | 付主枝 | A kind of production technology of waterproof anti-corrosion construction material |
| CN110436828B (en) * | 2019-08-09 | 2021-08-20 | 长江水利委员会长江科学院 | Hydraulic asphalt concrete containing acidic stone and preparation method thereof |
| CN114560666B (en) * | 2022-04-11 | 2023-07-04 | 广东大禹工程技术有限公司 | Environment-friendly durable building material |
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Patent Citations (5)
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| CN101941825A (en) * | 2010-09-06 | 2011-01-12 | 广东绿由环保科技股份有限公司 | Environment-friendly brick produced from combustion slag of oil-bearing sludge reclaimed coal and manufacturing method thereof |
| CN102418308A (en) * | 2011-07-29 | 2012-04-18 | 河源市固体废物集中处置中心有限公司 | Water permeable bricks produced by using building waste residue and manufacturing method thereof |
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Effective date of registration: 20180521 Address after: 414000 508, 509 room, building 2, Yungang Road business incubation base, Chenglingji new port, Yueyang, Hunan Applicant after: Hunan Xinghe Construction Engineering Co., Ltd. Address before: 311811 Mei Yuan village, Feng Qiao Town, Zhuji City, Shaoxing, Zhejiang Applicant before: Zhang Xiaoxia |
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