CN105924047A - High-temperature-resisting environment-friendly composite building material and preparing method thereof - Google Patents
High-temperature-resisting environment-friendly composite building material and preparing method thereof Download PDFInfo
- Publication number
- CN105924047A CN105924047A CN201610292734.0A CN201610292734A CN105924047A CN 105924047 A CN105924047 A CN 105924047A CN 201610292734 A CN201610292734 A CN 201610292734A CN 105924047 A CN105924047 A CN 105924047A
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- China
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- parts
- building material
- mixture
- resin
- kieselguhr
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/20—Mortars, concrete or artificial stone characterised by specific physical values for the density
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/30—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values
- C04B2201/32—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values for the thermal conductivity, e.g. K-factors
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
Abstract
The invention discloses a high-temperature-resisting environment-friendly composite building material and a preparing method thereof. The building material is prepared from silicic acid fiber, cement, zirconium oxide, antimonous oxide, magnesium stearate, cis-form isoprene rubber, crushed crude pearlite, kieselguhr, dibutyl phthalate, lignosulfonate, phenolic resin, calcium borate, epoxy resin, PVC resin and sodium polystyrenesulfonate. The raw materials are mixed, heated, stirred, subjected to vacuumized reaction, cooled, dried and pressed to obtain the building material. The building material is high in heat conductivity coefficient, good in fixing and molding effect, and good in fire resistance and high temperature resistance; furthermore, thermal storage or cold storage can be achieved so that the fluctuation range of heat flow inside and outside a building can be reduced and action time can be delayed, and then indoor temperature fluctuation is reduced, comfort level is increased and energy consumption is reduced; the preparing process is simple and easy to operate.
Description
Technical field
The present invention relates to building material field, specifically a kind of high temperature resistant environment-protective composite architectural materials and preparation method thereof.
Background technology
Along with socioeconomic development and growth in the living standard, people are more and more higher to the requirement of indoor environment comfort level,
Air conditioning energy consumption the most significantly increases, and causes that energy resource consumption is too fast, environmental pollution increase, network load peak-valley difference are excessive, peak
The problem such as supply of electric power wretched insufficiency during load.Energy-conserving and environment-protective work is increasingly paid attention in countries in the world, and China has made and issued one
Series energy-saving environmental protection policy, promotes energy-conserving and environment-protective new building material industry development, and the usage amount of construction material has also reached new
Peak.And consequent building and heating and refrigeration increase considerably, and if things go on like this will cause the serious energy and environmental crisis,
Therefore, energy-saving building technology has obtained paying close attention to widely and paying attention to.
Construction material develops quickly, uses good heat preservation technology and material in industry and building, often can play thing half
The effect of merit times.Conventional insulation only has single resistive properties, does not has energy-saving and temperature-regulating function, and flameproof effect is less
Ideal, non-refractory, therefore the research of construction material and improving also always is the emphasis of building trade.
Summary of the invention
It is an object of the invention to provide a kind of high temperature resistant environment-protective composite architectural materials and preparation method thereof, to solve above-mentioned background
The problem proposed in technology.
For achieving the above object, the present invention provides following technical scheme:
A kind of high temperature resistant environment-protective composite architectural materials, is prepared from by the raw material of following weight portion: silicate fiber 60~80 parts,
Cement 30~40 parts, zirconium oxide 20~30 parts, antimony oxide 15~21 parts, magnesium stearate 12~16 parts, cis different
Penta rubber 35~45 parts, crushed crude pearlite 12~18 parts, kieselguhr 30~40 parts, phthalic acid dibutyl ester 25~35 parts,
Lignosulfonates 27~33 parts, phenolic resin 21~24 parts, Calcium pyroborate 17~19 parts, epoxy resin 23~25 parts,
Polyvinyl chloride resin 31~35 parts, kayexalate 19~21 parts.
A kind of preparation method of described high temperature resistant environment-protective composite architectural materials, concrete preparation process is as follows:
(1) silicate fiber, cement, zirconium oxide, antimony oxide, magnesium stearate and kieselguhr being ground respectively, mixing is all
Even, obtain mixture A;
(2) crushed crude pearlite, phthalic acid dibutyl ester and lignosulfonates are added in mixture A, are heated to 100~120 DEG C,
Stirring 3~4h, obtains mixture B;
(3) temperature of cooling mixture is to 40~50 DEG C, is separately added into cis isoprene rubber, phenolic resin, Calcium pyroborate, ring
Epoxy resins, polyvinyl chloride resin, kayexalate, temperature rises to 130~150 DEG C, evacuation reaction 30~40min;
(4) it is cooled to 40~50 DEG C, dries in an oven, compacting,.
Compared with prior art, the invention has the beneficial effects as follows: the heat conductivity of construction material of the present invention is good, fixed-type good,
There is good fire-proof high-temperature resistant effect, and this construction material can make between architecture indoor and outdoor with accumulation of heat or cold-storage
Hot-fluid fluctuating margin weakens, action time is delayed by, thus reduces fluctuations in indoor temperature, improves comfortableness, energy efficient;
Preparation process simple process of the present invention, easily operate.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, aobvious
So, described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, all
Belong to the scope of protection of the invention.
Embodiment 1
High temperature resistant environment-protective composite architectural materials, is prepared from by the raw material of following weight portion: silicate fiber 60 parts, cement 40
Part, zirconium oxide 20 parts, antimony oxide 21 parts, magnesium stearate 12 parts, cis isoprene rubber 45 parts, crushed crude pearlite 12
Part, 40 parts of kieselguhr, phthalic acid dibutyl ester 25 parts, lignosulfonates 33 parts, 21 parts of phenolic resin, Calcium pyroborate
19 parts, epoxy resin 23 parts, polyvinyl chloride resin 35 parts, kayexalate 19 parts.
In above-described embodiment, the preparation process of high temperature resistant environment-protective composite architectural materials is as follows:
(1) silicate fiber, cement, zirconium oxide, antimony oxide, magnesium stearate and kieselguhr being ground respectively, mixing is all
Even, obtain mixture A;
(2) crushed crude pearlite, phthalic acid dibutyl ester and lignosulfonates are added in mixture A, be heated to 100 DEG C, stir
Mix 4h, obtain mixture B;
(3) temperature of cooling mixture is to 40 DEG C, is separately added into cis isoprene rubber, phenolic resin, Calcium pyroborate, asphalt mixtures modified by epoxy resin
Fat, polyvinyl chloride resin, kayexalate, temperature rises to 130 DEG C, evacuation reaction 40min;
(4) it is cooled to 40 DEG C, dries in an oven, compacting,.
After testing, the heat conductivity of construction material of the present invention is 0.07W/ (m K), and transition temperature range is 12~35 DEG C,
Latent heat of phase change value is 40J/g, and apparent density is 625kg/m3, comprcssive strength is 1.28MPa, and water absorption rate is 9%.
Embodiment 2
High temperature resistant environment-protective composite architectural materials, is prepared from by the raw material of following weight portion: silicate fiber 70 parts, cement 35
Part, zirconium oxide 25 parts, antimony oxide 18 parts, magnesium stearate 14 parts, cis isoprene rubber 40 parts, crushed crude pearlite 15
Part, 35 parts of kieselguhr, phthalic acid dibutyl ester 30 parts, lignosulfonates 30 parts, 22 parts of phenolic resin, Calcium pyroborate
18 parts, epoxy resin 24 parts, polyvinyl chloride resin 33 parts, kayexalate 20 parts.
In above-described embodiment, the preparation process of high temperature resistant environment-protective composite architectural materials is as follows:
(1) silicate fiber, cement, zirconium oxide, antimony oxide, magnesium stearate and kieselguhr being ground respectively, mixing is all
Even, obtain mixture A;
(2) crushed crude pearlite, phthalic acid dibutyl ester and lignosulfonates are added in mixture A, be heated to 110 DEG C, stir
Mix 3.5h, obtain mixture B;
(3) temperature of cooling mixture is to 45 DEG C, is separately added into cis isoprene rubber, phenolic resin, Calcium pyroborate, asphalt mixtures modified by epoxy resin
Fat, polyvinyl chloride resin, kayexalate, temperature rises to 140 DEG C, evacuation reaction 35min;
(4) it is cooled to 45 DEG C, dries in an oven, compacting,.
After testing, the heat conductivity of construction material of the present invention is 0.08W/ (m K), and transition temperature range is 15~30 DEG C,
Latent heat of phase change value is 65J/g, and apparent density is 577kg/m3, comprcssive strength is 1.55MPa, and water absorption rate is 8%.
Embodiment 3
High temperature resistant environment-protective composite architectural materials, is prepared from by the raw material of following weight portion: silicate fiber 80 parts, cement 30
Part, zirconium oxide 30 parts, antimony oxide 15 parts, magnesium stearate 16 parts, cis isoprene rubber 35 parts, crushed crude pearlite 18
Part, 30 parts of kieselguhr, phthalic acid dibutyl ester 35 parts, lignosulfonates 27 parts, 24 parts of phenolic resin, Calcium pyroborate
17 parts, epoxy resin 25 parts, polyvinyl chloride resin 31 parts, kayexalate 21 parts.
In above-described embodiment, the preparation process of high temperature resistant environment-protective composite architectural materials is as follows:
(1) silicate fiber, cement, zirconium oxide, antimony oxide, magnesium stearate and kieselguhr being ground respectively, mixing is all
Even, obtain mixture A;
(2) crushed crude pearlite, phthalic acid dibutyl ester and lignosulfonates are added in mixture A, be heated to 120 DEG C, stir
Mix 3h, obtain mixture B;
(3) temperature of cooling mixture is to 50 DEG C, is separately added into cis isoprene rubber, phenolic resin, Calcium pyroborate, asphalt mixtures modified by epoxy resin
Fat, polyvinyl chloride resin, kayexalate, temperature rises to 150 DEG C, evacuation reaction 30min;
(4) it is cooled to 50 DEG C, dries in an oven, compacting,.
After testing, the heat conductivity of construction material of the present invention is 0.12W/ (m K), and transition temperature range is 10~30 DEG C,
Latent heat of phase change value is 60J/g, and apparent density is 695kg/m3, comprcssive strength is 1.35MPa, and water absorption rate is 10%.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and do not carrying on the back
In the case of the spirit or essential attributes of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter from
From the point of view of which point, all should regard embodiment as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all by fall in the implication of equivalency and scope of claim
Change is included in the present invention.
Claims (2)
1. a high temperature resistant environment-protective composite architectural materials, it is characterised in that be prepared from by the raw material of following weight portion: silicic acid
Fiber 60~80 parts, cement 30~40 parts, zirconium oxide 20~30 parts, antimony oxide 15~21 parts, magnesium stearate 12~
16 parts, cis isoprene rubber 35~45 parts, crushed crude pearlite 12~18 parts, kieselguhr 30~40 parts, phthalic acid two fourth
Ester 25~35 parts, lignosulfonates 27~33 parts, phenolic resin 21~24 parts, Calcium pyroborate 17~19 parts, asphalt mixtures modified by epoxy resin
Fat 23~25 parts, polyvinyl chloride resin 31~35 parts, kayexalate 19~21 parts.
The preparation method of high temperature resistant environment-protective composite architectural materials the most according to claim 1, it is characterised in that specifically make
Standby step is as follows:
(1) silicate fiber, cement, zirconium oxide, antimony oxide, magnesium stearate and kieselguhr being ground respectively, mixing is all
Even, obtain mixture A;
(2) crushed crude pearlite, phthalic acid dibutyl ester and lignosulfonates are added in mixture A, are heated to 100~120 DEG C,
Stirring 3~4h, obtains mixture B;
(3) temperature of cooling mixture is to 40~50 DEG C, is separately added into cis isoprene rubber, phenolic resin, Calcium pyroborate, ring
Epoxy resins, polyvinyl chloride resin, kayexalate, temperature rises to 130~150 DEG C, evacuation reaction 30~40min;
(4) it is cooled to 40~50 DEG C, dries in an oven, compacting,.
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CN201610292734.0A CN105924047B (en) | 2016-05-05 | 2016-05-05 | A kind of high temperature resistant environment-protective composite architectural materials and preparation method thereof |
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CN201610292734.0A CN105924047B (en) | 2016-05-05 | 2016-05-05 | A kind of high temperature resistant environment-protective composite architectural materials and preparation method thereof |
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CN105924047B CN105924047B (en) | 2018-07-20 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106587849A (en) * | 2016-12-22 | 2017-04-26 | 郑州丽福爱生物技术有限公司 | Environment-friendly composite building material and preparation method thereof |
CN108002747A (en) * | 2017-12-13 | 2018-05-08 | 付主枝 | A kind of production technology of waterproof anti-corrosion construction material |
CN110436828A (en) * | 2019-08-09 | 2019-11-12 | 长江水利委员会长江科学院 | Hydraulic asphalt concrete and preparation method thereof containing acid stone |
CN114560666A (en) * | 2022-04-11 | 2022-05-31 | 广东大禹工程技术有限公司 | Environment-friendly durable building material |
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CN102418308A (en) * | 2011-07-29 | 2012-04-18 | 河源市固体废物集中处置中心有限公司 | Water permeable bricks produced by using building waste residue and manufacturing method thereof |
CN102584126A (en) * | 2012-02-27 | 2012-07-18 | 南昌大学 | Phase-change energy-storage thermal-insulation material and preparation method thereof |
CN104817295A (en) * | 2015-05-07 | 2015-08-05 | 苏州能华节能环保科技有限公司 | Energy-saving and heat-insulating material and preparation method thereof |
CN105503056A (en) * | 2016-01-19 | 2016-04-20 | 赵东星 | Environment-friendly insulated flame-retardant building material and preparation method thereof |
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CN101941825A (en) * | 2010-09-06 | 2011-01-12 | 广东绿由环保科技股份有限公司 | Environment-friendly brick produced from combustion slag of oil-bearing sludge reclaimed coal and manufacturing method thereof |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106587849A (en) * | 2016-12-22 | 2017-04-26 | 郑州丽福爱生物技术有限公司 | Environment-friendly composite building material and preparation method thereof |
CN108002747A (en) * | 2017-12-13 | 2018-05-08 | 付主枝 | A kind of production technology of waterproof anti-corrosion construction material |
CN110436828A (en) * | 2019-08-09 | 2019-11-12 | 长江水利委员会长江科学院 | Hydraulic asphalt concrete and preparation method thereof containing acid stone |
CN110436828B (en) * | 2019-08-09 | 2021-08-20 | 长江水利委员会长江科学院 | Hydraulic asphalt concrete containing acidic stone and preparation method thereof |
CN114560666A (en) * | 2022-04-11 | 2022-05-31 | 广东大禹工程技术有限公司 | Environment-friendly durable building material |
CN114560666B (en) * | 2022-04-11 | 2023-07-04 | 广东大禹工程技术有限公司 | Environment-friendly durable building material |
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Effective date of registration: 20180521 Address after: 414000 508, 509 room, building 2, Yungang Road business incubation base, Chenglingji new port, Yueyang, Hunan Applicant after: Hunan Xinghe Construction Engineering Co., Ltd. Address before: 311811 Mei Yuan village, Feng Qiao Town, Zhuji City, Shaoxing, Zhejiang Applicant before: Zhang Xiaoxia |
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