CN107057489A - It is a kind of for fire-proof and thermal-insulation coating of interior wall and preparation method thereof - Google Patents

It is a kind of for fire-proof and thermal-insulation coating of interior wall and preparation method thereof Download PDF

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Publication number
CN107057489A
CN107057489A CN201611165401.8A CN201611165401A CN107057489A CN 107057489 A CN107057489 A CN 107057489A CN 201611165401 A CN201611165401 A CN 201611165401A CN 107057489 A CN107057489 A CN 107057489A
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Prior art keywords
parts
fire
proof
thermal
interior wall
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CN201611165401.8A
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Chinese (zh)
Inventor
周春毅
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Wuzhong District Dome High Polymer Material Technology Research Institute
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Wuzhong District Dome High Polymer Material Technology Research Institute
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Priority to CN201611165401.8A priority Critical patent/CN107057489A/en
Publication of CN107057489A publication Critical patent/CN107057489A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18Fireproof paints including high temperature resistant paints
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/63Additives non-macromolecular organic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/014Additives containing two or more different additives of the same subgroup in C08K
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/02Flame or fire retardant/resistant
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Paints Or Removers (AREA)
  • Fireproofing Substances (AREA)

Abstract

The invention discloses a kind of fire-proof and thermal-insulation coating for interior wall, the raw material containing following parts by weight:30 40 parts of aqueous acrylic emulsion, 35 parts of hydroxypropyl methyl cellulose, 12 parts of silane coupler, 5 10 parts of glass bead, 15 20 parts of silicate mineral powder, 5 10 parts of haydite, 12 parts of MethylethoxylsiliconFluid Fluid, 58 parts of fire retardant, 15 20 parts of deionized water, 24 parts of coalescents, the invention also discloses its preparation method.Coating prepared by the present invention has insulation, heat-proof quality, and excellent fire protecting performance well.Conventional coating is compared on the market, and summer coating of the present invention can effectively reduce indoor temperature more than 3 DEG C, energy-conservation, and coating quality produced by the present invention is stable, and adhesive force is strong, with good application prospect.

Description

It is a kind of for fire-proof and thermal-insulation coating of interior wall and preparation method thereof
Technical field
The present invention relates to technical field of coatings, and in particular to a kind of fire-proof and thermal-insulation coating and its preparation side for interior wall Method.
Background technology
Energy-conserving and environment-protective have become the key subjects that the 21 century whole mankind must face, and also have become our building trades Have to the important topic for putting forth effort to solve.The thermal and insulating performance for improving house is one of building energy-saving consumption reduction and important arranged Apply, many new buildings and many old buildings in exterior wall and interior wall by sticking heat insulation layer under the advocating of country Method in the hope of reaching the heat insulation and preservation effect in room:I.e. hot summer by the heat-barrier material of inner-outer wall prevent heat radiation to Transmit within doors, reduce the energy consumption of the household electrical appliance such as air-conditioning, cold winter also by the heat-barrier material of inner-outer wall prevent it is indoor compared with High-temperature is transmitted to the outdoor of cold.In addition, heat-resisting, the heat-proof quality that improve existing coating are to solve fireproof root problem. At present, on the market the heat-insulated heat resistance of fireproof coating is general.
The content of the invention
In view of the shortcomings of the prior art, the invention provides a kind of anti-fire screen for interior wall of heat-insulated Good Heat-resistance Hot coating and preparation method thereof.
To realize object above, the present invention is achieved by the following technical programs:
A kind of fire-proof and thermal-insulation coating for interior wall, the raw material containing following parts by weight:Aqueous acrylic emulsion 30-40 Part, 3-5 parts of hydroxypropyl methyl cellulose, 1-2 parts of silane coupler, 5-10 parts of glass bead, 15-20 parts of silicate mineral powder, 5-10 parts of haydite, 1-2 parts of MethylethoxylsiliconFluid Fluid, 5-8 parts of fire retardant, 15-20 parts of deionized water, 2-4 parts of coalescents.
Preferably, the raw material containing following parts by weight:35 parts of aqueous acrylic emulsion, 4.5 parts of hydroxypropyl methyl cellulose, Silane coupler 1.5,8 parts of glass bead, 16 parts of silicate mineral powder, 6 parts of haydite, 1.2 parts of MethylethoxylsiliconFluid Fluid, fire retardant 7 parts, 18 parts of deionized water, 3 parts of coalescents.
Preferably, the solid content of the aqueous acrylic emulsion is 30-40%.
Preferably, the silicate mineral powder is in talcum powder, diatomite, kaolin, montmorillonite, vermiculite, sepiolite At least one.
Preferably, the haydite is lytag.
Preferably, the fire retardant by magnesium hydroxide, aluminium hydroxide and APP according to 2:2:3 mass ratio composition.
Preferably, the coalescents are butyl acetate and ethylene glycol according to 1:1 mass ratio composition.
For the preparation method of the fire-proof and thermal-insulation coating of interior wall, step is as follows:Aqueous acrylic emulsion and suitable quantity of water are added Enter into container, dispersed with stirring 5-10min, silicate mineral powder, glass bead and haydite are added thereto, at a high speed scattered 10- 3-4h is ground after 15min again, then adds coalescents, hydroxypropyl methyl cellulose, fire retardant, silane coupler, first thereto Base oxethyl silicone oil and balance deionized water, dispersed with stirring 20-30min, are produced.
Beneficial effect of the present invention:Silicate mineral powder and haydite in instant component, with porosity height, heat transfer coefficient Low the characteristics of so that obtained coating has other component collective effects in insulation, heat-proof quality, and formula well, tool There is excellent fire protecting performance.Conventional coating is compared on the market, summer coating of the present invention can effectively reduce by 3 DEG C of indoor temperature with On, energy-conservation, and coating quality produced by the present invention is stable, adhesive force is strong, water-tolerant, with good application prospect.
Embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention, Technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is the present invention one Divide embodiment, rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art are not making The every other embodiment obtained under the premise of creative work, belongs to the scope of protection of the invention.
Embodiment 1:
A kind of fire-proof and thermal-insulation coating for interior wall, the raw material containing following parts by weight:Aqueous acrylic emulsion (solid content For 32%) 35 parts, 4.5 parts of hydroxypropyl methyl cellulose, 1.5 parts of silane coupler, 8 parts of glass bead, 8 parts of talcum powder, vermiculite 8 Part, 6 parts of lytag, 1.2 parts of MethylethoxylsiliconFluid Fluid, 7 parts of fire retardant, 18 parts of deionized water, 1.5 parts of butyl acetate, second 1.5 parts of glycol.Wherein, fire retardant by magnesium hydroxide, aluminium hydroxide and APP according to 2:2:3 mass ratio composition.
For the preparation method of the fire-proof and thermal-insulation coating of interior wall, step is as follows:Aqueous acrylic emulsion and suitable quantity of water are added Enter into container, dispersed with stirring 8min, silicate mineral powder, glass bead and haydite are added thereto, at a high speed after scattered 15min 3.5h is ground again, then adds coalescents, hydroxypropyl methyl cellulose, fire retardant, silane coupler, methyl ethoxy thereto Silicone oil and balance deionized water, dispersed with stirring 25min, are produced.
Embodiment 2:
A kind of fire-proof and thermal-insulation coating for interior wall, the raw material containing following parts by weight:Aqueous acrylic emulsion (solid content For 35%) 32 parts, 4 parts of hydroxypropyl methyl cellulose, 1.8 parts of silane coupler, 7 parts of glass bead, 9 parts of diatomite, sepiolite 9 Part, 7 parts of lytag, 1.5 parts of MethylethoxylsiliconFluid Fluid, 8 parts of fire retardant, 20 parts of deionized water, 1.5 parts of butyl acetate, second 1.5 parts of glycol.Wherein, fire retardant by magnesium hydroxide, aluminium hydroxide and APP according to 2:2:3 mass ratio composition.
For the preparation method of the fire-proof and thermal-insulation coating of interior wall, step is as follows:Aqueous acrylic emulsion and suitable quantity of water are added Enter into container, dispersed with stirring 10min, silicate mineral powder, glass bead and haydite are added thereto, at a high speed scattered 10min Grind 4h again afterwards, then add coalescents, hydroxypropyl methyl cellulose, fire retardant, silane coupler, methyl ethoxy thereto Silicone oil and balance deionized water, dispersed with stirring 30min, are produced.
Embodiment 3:
A kind of fire-proof and thermal-insulation coating for interior wall, the raw material containing following parts by weight:Aqueous acrylic emulsion (solid content For 30%) 40 parts, 3 parts of hydroxypropyl methyl cellulose, 2 parts of silane coupler, 5 parts of glass bead, 10 parts of kaolin, vermiculite 10 Part, 5 parts of lytag, 2 parts of MethylethoxylsiliconFluid Fluid, 5 parts of fire retardant, 20 parts of deionized water, 1 part of butyl acetate, ethylene glycol 2 Part.Wherein, fire retardant by magnesium hydroxide, aluminium hydroxide and APP according to 2:2:3 mass ratio composition.
For the preparation method of the fire-proof and thermal-insulation coating of interior wall, step is as follows:Aqueous acrylic emulsion and suitable quantity of water are added Enter into container, dispersed with stirring 10min, silicate mineral powder, glass bead and haydite are added thereto, at a high speed scattered 15min Grind 3h again afterwards, then add coalescents, hydroxypropyl methyl cellulose, fire retardant, silane coupler, methyl ethoxy thereto Silicone oil and balance deionized water, dispersed with stirring 20min, are produced.
Embodiment 4:
A kind of fire-proof and thermal-insulation coating for interior wall, the raw material containing following parts by weight:Aqueous acrylic emulsion (solid content For 40%) 30 parts, 5 parts of hydroxypropyl methyl cellulose, 1 part of silane coupler, 10 parts of glass bead, 5 parts of diatomite, montmorillonite 10 Part, 10 parts of lytag, 1 part of MethylethoxylsiliconFluid Fluid, 8 parts of fire retardant, 15 parts of deionized water, 2 parts of butyl acetate, ethylene glycol 2 parts.Wherein, fire retardant by magnesium hydroxide, aluminium hydroxide and APP according to 2:2:3 mass ratio composition.
For the preparation method of the fire-proof and thermal-insulation coating of interior wall, step is as follows:Aqueous acrylic emulsion and suitable quantity of water are added Enter into container, dispersed with stirring 7min, silicate mineral powder, glass bead and haydite are added thereto, at a high speed after scattered 12min 3.5h is ground again, then adds coalescents, hydroxypropyl methyl cellulose, fire retardant, silane coupler, methyl ethoxy thereto Silicone oil and balance deionized water, dispersed with stirring 30min, are produced.
Embodiment 5:
A kind of fire-proof and thermal-insulation coating for interior wall, the raw material containing following parts by weight:Aqueous acrylic emulsion (solid content For 36%) 38 parts, 4.5 parts of hydroxypropyl methyl cellulose, 1.7 parts of silane coupler, 8 parts of glass bead, 7 parts of diatomite, Hai Pao 10 parts of stone, 10 parts of lytag, 1.5 parts of MethylethoxylsiliconFluid Fluid, 8 parts of fire retardant, 20 parts of deionized water, butyl acetate 1.5 Part, 1.5 parts of ethylene glycol.Wherein, fire retardant by magnesium hydroxide, aluminium hydroxide and APP according to 2:2:3 mass ratio composition.
For the preparation method of the fire-proof and thermal-insulation coating of interior wall, step is as follows:Aqueous acrylic emulsion and suitable quantity of water are added Enter into container, dispersed with stirring 10min, silicate mineral powder, glass bead and haydite are added thereto, at a high speed scattered 15min Grind 4h again afterwards, then add coalescents, hydroxypropyl methyl cellulose, fire retardant, silane coupler, methyl ethoxy thereto Silicone oil and balance deionized water, dispersed with stirring 20min, are produced.
Performance test, its adhesive force≤1 are carried out to the obtained fire-proof and thermal-insulation coating for interior wall of the embodiment of the present invention 1 Level, when coating layer thickness is 10mm, its resistance to combustion limit >=100min.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations;Although with reference to the foregoing embodiments The present invention is described in detail, it will be understood by those within the art that:It still can be to foregoing each implementation Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic;And these modification or Replace, the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.

Claims (8)

1. a kind of fire-proof and thermal-insulation coating for interior wall, it is characterised in that the raw material containing following parts by weight:Aqueous acrylamide yogurt 30-40 parts of liquid, 3-5 parts of hydroxypropyl methyl cellulose, 1-2 parts of silane coupler, 5-10 parts of glass bead, silicate mineral powder 15-20 parts, 5-10 parts of haydite, 1-2 parts of MethylethoxylsiliconFluid Fluid, 5-8 parts of fire retardant, 15-20 parts of deionized water, coalescents 2- 4 parts.
2. it is used for the fire-proof and thermal-insulation coating of interior wall as claimed in claim 1, it is characterised in that the original containing following parts by weight Material:35 parts of aqueous acrylic emulsion, 4.5 parts of hydroxypropyl methyl cellulose, silane coupler 1.5,8 parts of glass bead, silicate 16 parts of mineral powder, 6 parts of haydite, 1.2 parts of MethylethoxylsiliconFluid Fluid, 7 parts of fire retardant, 18 parts of deionized water, 3 parts of coalescents.
3. it is used for the fire-proof and thermal-insulation coating of interior wall as claimed in claim 2, it is characterised in that the aqueous acrylic emulsion Solid content is 30-40%.
4. it is used for the fire-proof and thermal-insulation coating of interior wall as claimed in claim 2, it is characterised in that the silicate mineral powder is selected from At least one of talcum powder, diatomite, kaolin, montmorillonite, vermiculite, sepiolite.
5. it is used for the fire-proof and thermal-insulation coating of interior wall as claimed in claim 2, it is characterised in that the haydite is flyash ceramic Grain.
6. it is used for the fire-proof and thermal-insulation coating of interior wall as claimed in claim 2, it is characterised in that the fire retardant is by hydroxide Magnesium, aluminium hydroxide and APP are according to 2:2:3 mass ratio composition.
7. it is used for the fire-proof and thermal-insulation coating of interior wall as claimed in claim 2, it is characterised in that the coalescents are acetic acid fourth Ester and ethylene glycol are according to 1:1 mass ratio composition.
8. the preparation method of the fire-proof and thermal-insulation coating for interior wall as described in claim 1-7 is any, it is characterised in that step It is as follows:Aqueous acrylic emulsion and suitable quantity of water are added in container, dispersed with stirring 5-10min adds silicate mine thereto Thing powder, glass bead and haydite, grind 3-4h, then add coalescents, hydroxypropyl thereto again after scattered 10-15min at a high speed Methylcellulose, fire retardant, silane coupler, MethylethoxylsiliconFluid Fluid and balance deionized water, dispersed with stirring 20-30min, i.e., .
CN201611165401.8A 2016-12-16 2016-12-16 It is a kind of for fire-proof and thermal-insulation coating of interior wall and preparation method thereof Withdrawn CN107057489A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107573762A (en) * 2017-09-15 2018-01-12 东华大学 A kind of water paint of the anti-sagging agent containing regenerated cellulose and its preparation method and application
CN107815168A (en) * 2017-11-14 2018-03-20 安徽省神洲建材科技有限公司 A kind of Application way of flyash on interior finish
CN108410305A (en) * 2018-04-13 2018-08-17 王俊玲 A kind of coating with fireproof heat insulating sound insulation function
CN109233522A (en) * 2018-09-28 2019-01-18 佛山齐安建筑科技有限公司 A kind of building material surface fireproof coating
CN111574111A (en) * 2020-04-04 2020-08-25 江苏禾吉新材料科技有限公司 Light high-strength straw board for interior wall and preparation method and application thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104910726A (en) * 2015-06-18 2015-09-16 黎司华 Flame-retardant reflective heat-insulating paint and preparation technique thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104910726A (en) * 2015-06-18 2015-09-16 黎司华 Flame-retardant reflective heat-insulating paint and preparation technique thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107573762A (en) * 2017-09-15 2018-01-12 东华大学 A kind of water paint of the anti-sagging agent containing regenerated cellulose and its preparation method and application
CN107815168A (en) * 2017-11-14 2018-03-20 安徽省神洲建材科技有限公司 A kind of Application way of flyash on interior finish
CN108410305A (en) * 2018-04-13 2018-08-17 王俊玲 A kind of coating with fireproof heat insulating sound insulation function
CN109233522A (en) * 2018-09-28 2019-01-18 佛山齐安建筑科技有限公司 A kind of building material surface fireproof coating
CN111574111A (en) * 2020-04-04 2020-08-25 江苏禾吉新材料科技有限公司 Light high-strength straw board for interior wall and preparation method and application thereof

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