CN107551142A - A kind of processing method of bletilla striata oral powder - Google Patents
A kind of processing method of bletilla striata oral powder Download PDFInfo
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Abstract
The invention belongs to Chinese medicine manufacture field, more particularly to a kind of processing method of bletilla striata oral powder, comprise the following steps：Stock, peeling, heat treatment, dry, crushing, encapsulation；Bletilla striata oral powder is prepared according to the method for the present invention, the bletilla striata is immersed in special solution 1, then carry out radio frequency processing, promote absorption of the bletilla striata for the composition of solution 1, and reacted with bletilla striata intracellular matter, change the leaching rate of bletilla striata beneficiating ingredient so that the active constituent content in water-leach liquor increased, so that bletilla striata treatment pertussis, gastric ulcer, promotion wound healing effect are consequently increased so that the cure rate of bletilla striata treatment pertussis is up to 76%.
Description
Technical field
The invention belongs to Chinese medicine manufacture field, more particularly to a kind of processing method of bletilla striata oral powder.
Background technology
The bletilla striata, also known as Lian Jicao, Gan Gen, give free of charge, be indocalamus orchid, Zhu Lan, purple blue, purple a species of orchid, hundred large bamboo hats with a conical crown and broad brim, Pseudobulbus Bletillae (Rhizoma Bletillae), Cold boiled chicken baby, white
Root, YANGJIAOQI, are perennial herb bulbous plants, and plant is high 18-60 centimetres.The bletilla striata has extensive medical value and gardens valency
Value, has astringing to arrest bleeding, detumescence and promoting granulation effect, thus is usually used in treating hemoptysis haematemesis, traumatism and bleeding, sore swollen toxin, skin chap
Split；Pulmonary tuberculosis hemoptysis, ulcer haemorrhage.Processing of the tradition for the bletilla striata, mostly it is decoction, with processes such as sulfur fumigation, dryings,
Process is excessively simple, and very big waste is caused not only for the medical value of the bletilla striata, due to sulfur fumigation, bringing
Medicine potential safety hazard.
The content of the invention
The present invention in order to solve the above technical problems, provide a kind of processing method of bletilla striata oral powder, particular by
Following technical scheme is realized.
A kind of processing method of bletilla striata oral powder, comprises the following steps：
1) stock up：Choose fresh bletilla striata root tuber, clean it is standby；
2) remove the peel：Bletilla striata raw material is put into 55-58 DEG C of water and soaks 1-2h, filters out raw material peeling；
3) soak：The bletilla striata raw material of peeling is put into solution 1, and 6-7h is soaked at a temperature of 25-30 DEG C；
4) it is heat-treated：The bletilla striata obtained by step 3) is subjected to high temperature high pressure process；
5) dry：Drying includes being freeze-dried and dries；
6) crush：The bletilla striata will be dried to be crushed；
7) encapsulate：Dry common bletilla encapsulation preserves.
Further, described solution 1, the raw material of following mass parts is included：It is adlay 20-40 parts, Chinese gall 20-35 parts, sweet
It is careless 15-25 parts, root of Dahurain angelica 15-20 parts, chrysanthemum 10-15 parts, malt 10-15 parts, black tea 10-13 parts, fresh lily 7-9 parts, sweet
Oily 5-7 parts.
Further, described solution 1, including following preparation process：
1) the water immersion black tea 7-8min of 6-7 times of black tea quality is added, obtains black tea draw-off juice；
2) adlay, Chinese gall, radix glycyrrhizae, root of Dahurain angelica mixing, crush, 78-80 DEG C of frying 40-50min obtains powder 1, powder 1 with
Black tea draw-off juice is mixed, and 28-34 DEG C is closed 3-4 days, is obtained fermentate, fermentate Microwave Extraction, filtering, is obtained extract solution 1；
3) chrysanthemum, malt mixing, crushing, the salt solution of 2-3 times of mixed-powder quality, 90-95 DEG C of decoction 3-4h, mistake are added
Filter, obtains extract solution 2, wherein described brine strength is 0.01-0.02mol/L；
4) fresh lily is smashed to pieces mixes with glycerine, -10~-15 DEG C of placement 3-5h, adds extract solution 1,170-180r/
Min, 65-70 DEG C of reaction 2-2.5h, filtering, obtain extract solution 3, and extract solution 2 and extract solution 3 mix, both.
Further, described Microwave Extraction, microwave frequency 750MHz, 10-12min is extracted.
Further, after soaking step, in addition to radio frequency processing, frequency 800-820KHz, processing time 5-7min.
Further, described high temperature high pressure process, it in temperature is 210-230 DEG C, pressure 5.0-7.0MPa to be, during processing
Between be 7-10min.
Further, described freeze-drying, it is in -30~-24 DEG C of precoolings 1-2h, -80~-75 DEG C of freezing 27-32h.
Further, described drying, it is that the hot blast that temperature is 55-58 DEG C is passed through in the bletilla striata, continues 4-5h.
In summary, the beneficial effects of the present invention are：Method according to the present invention carries out preparing bletilla striata oral powder, leads to
Cross and be immersed in special solution 1, then carry out radio frequency processing, promote absorption of the bletilla striata for the composition of solution 1, and and the bletilla striata
Intracellular matter reacts, and changes the leaching rate of bletilla striata beneficiating ingredient so that the active constituent content in water-leach liquor has
Increased, so that bletilla striata treatment pertussis, gastric ulcer, promotion wound healing effect are consequently increased so that the bletilla striata is treated
The cure rate of pertussis is up to 76%.
Embodiment
The embodiment of the present invention is described in further detail below, but the invention is not limited in these realities
Mode is applied, any improvement or replacement on the present embodiment essence spirit, it is claimed to still fall within the claims in the present invention
Scope.
Embodiment 1
A kind of processing method of bletilla striata oral powder, comprises the following steps：
1) stock up：Choose fresh bletilla striata root tuber, clean it is standby；
2) remove the peel：Bletilla striata raw material is put into 55 DEG C of water and soaks 1h, filters out raw material peeling；
3) soak：The bletilla striata raw material of peeling is put into solution 1, soaks 6h at a temperature of 25 DEG C；
4) it is heat-treated：The bletilla striata obtained by step 3) is subjected to high temperature high pressure process；
5) dry：Drying includes being freeze-dried and dries；
6) crush：The bletilla striata will be dried to be crushed；
7) encapsulate：Dry common bletilla encapsulation preserves.
Described solution 1, include the raw material of following mass parts：Adlay 20kg, Chinese gall 20kg, radix glycyrrhizae 15kg, the root of Dahurain angelica
15kg, chrysanthemum 10kg, malt 10kg, black tea 10kg, fresh lily 7kg, glycerine 5kg.
Described solution 1, including following preparation process：
1) the water immersion black tea 7min of 6-7 times of black tea quality is added, obtains black tea draw-off juice；
2) adlay, Chinese gall, radix glycyrrhizae, root of Dahurain angelica mixing, crushing, 78 DEG C of frying 40min, obtain powder 1, powder 1 and black tea draw-off juice
Mixing, 28 DEG C are closed 3 days, are obtained fermentate, fermentate Microwave Extraction, filtering, are obtained extract solution 1；
3) chrysanthemum, malt mixing, crushing, the salt solution of 2 times of mixed-powder quality is added, 90 DEG C of decoction 3h, filtering, must be extracted
Liquid 2, wherein described brine strength is 0.01mol/L；
4) fresh lily is smashed to pieces mixes with glycerine, -10 DEG C of placement 3h, adds extract solution 1,170r/min, 65 DEG C of reactions
2h, filtering, obtains extract solution 3, and extract solution 2 and extract solution 3 mix, both.
Described Microwave Extraction, microwave frequency 750MHz, extract 10min.
After soaking step, in addition to radio frequency processing, frequency 800KHz, processing time 5min.
Described high temperature high pressure process, be temperature be 210 DEG C, pressure 5.0MPa, processing time 7min.
Described freeze-drying, it is in -30 DEG C of precoolings 1h, -80 DEG C of freezing 27h.
Described drying, it is that the hot blast that temperature is 55 DEG C is passed through in the bletilla striata, continues 4-5h.
Embodiment 2
A kind of processing method of bletilla striata oral powder, comprises the following steps：
1) stock up：Choose fresh bletilla striata root tuber, clean it is standby；
2) remove the peel：Bletilla striata raw material is put into 55 DEG C of water and soaks 1h, filters out raw material peeling；
3) soak：The bletilla striata raw material of peeling is put into solution 1, soaks 6h at a temperature of 25 DEG C；
4) it is heat-treated：The bletilla striata obtained by step 3) is subjected to high temperature high pressure process；
5) dry：Drying includes being freeze-dried and dries；
6) crush：The bletilla striata will be dried to be crushed；
7) encapsulate：Dry common bletilla encapsulation preserves.
Described solution 1, include the raw material of following mass parts：Adlay 20kg, Chinese gall 20kg, radix glycyrrhizae 15kg, the root of Dahurain angelica
15kg, chrysanthemum 10kg, malt 10kg, black tea 10kg, fresh lily 7kg, glycerine 5kg.
Described solution 1, including following preparation process：
1) the water immersion black tea 7min of 6-7 times of black tea quality is added, obtains black tea draw-off juice；
2) adlay, Chinese gall, radix glycyrrhizae, root of Dahurain angelica mixing, crushing, 78 DEG C of frying 40min, obtain powder 1, powder 1 and black tea draw-off juice
Mixing, with Microwave Extraction, filtering, obtain extract solution 1；
3) chrysanthemum, malt mixing, crushing, the salt solution of 2 times of mixed-powder quality is added, 90 DEG C of decoction 3h, filtering, must be extracted
Liquid 2, wherein described brine strength is 0.01mol/L；
4) fresh lily is smashed to pieces mixes with glycerine, -10 DEG C of placement 3h, adds extract solution 1,170r/min, 65 DEG C of reactions
2h, filtering, obtains extract solution 3, and extract solution 2 and extract solution 3 mix, both.
Described Microwave Extraction, microwave frequency 750MHz, extract 10min.
After soaking step, in addition to radio frequency processing, frequency 800KHz, processing time 5min.
Described high temperature high pressure process, be temperature be 210 DEG C, pressure 5.0MPa, processing time 7min.
Described freeze-drying, it is in -30 DEG C of precoolings 1h, -80 DEG C of freezing 27h.
Described drying, it is that the hot blast that temperature is 55 DEG C is passed through in the bletilla striata, continues 4-5h.
Embodiment 3
A kind of processing method of bletilla striata oral powder, comprises the following steps：
1) stock up：Choose fresh bletilla striata root tuber, clean it is standby；
2) remove the peel：Bletilla striata raw material is put into 55 DEG C of water and soaks 1h, filters out raw material peeling；
3) soak：The bletilla striata raw material of peeling is put into solution 1, soaks 6h at a temperature of 25 DEG C；
4) it is heat-treated：The bletilla striata obtained by step 3) is subjected to high temperature high pressure process；
5) dry：Drying includes being freeze-dried and dries；
6) crush：The bletilla striata will be dried to be crushed；
7) encapsulate：Dry common bletilla encapsulation preserves.
Described solution 1, include the raw material of following mass parts：Adlay 20kg, Chinese gall 20kg, radix glycyrrhizae 15kg, the root of Dahurain angelica
15kg, chrysanthemum 10kg, malt 10kg, black tea 10kg, fresh lily 7kg, glycerine 5kg.
Described solution 1, including following preparation process：
1) the water immersion black tea 7min of 6-7 times of black tea quality is added, obtains black tea draw-off juice；
2) adlay, Chinese gall, radix glycyrrhizae, root of Dahurain angelica mixing, crushing, obtain powder 1, and powder 1 mixes with black tea draw-off juice, 28 DEG C of closings 3
My god, fermentate is obtained, fermentate Microwave Extraction, filtering, obtains extract solution 1；
3) chrysanthemum, malt mixing, crushing, the salt solution of 2 times of mixed-powder quality is added, 90 DEG C of decoction 3h, filtering, must be extracted
Liquid 2, wherein described brine strength is 0.01mol/L；
4) fresh lily is smashed to pieces mixes with glycerine, -10 DEG C of placement 3h, adds extract solution 1,170r/min, 65 DEG C of reactions
2h, filtering, obtains extract solution 3, and extract solution 2 and extract solution 3 mix, both.
Described Microwave Extraction, microwave frequency 750MHz, extract 10min.
Described high temperature high pressure process, be temperature be 210 DEG C, pressure 5.0MPa, processing time 7min.
Described freeze-drying, it is in -30 DEG C of precoolings 1h, -80 DEG C of freezing 27h.
Described drying, it is that the hot blast that temperature is 55 DEG C is passed through in bletilla striata piece, continues 4-5h.
Embodiment 4
A kind of processing method of bletilla striata oral powder, comprises the following steps：
1) stock up：Choose fresh bletilla striata root tuber, clean it is standby；
2) remove the peel：Bletilla striata raw material is put into 55 DEG C of water and soaks 1h, filters out raw material peeling；
3) soak：The bletilla striata raw material of peeling is put into solution 1, soaks 6h at a temperature of 25 DEG C；
4) it is heat-treated：The bletilla striata obtained by step 3) is heat-treated；
5) dry：Drying includes being freeze-dried and dries；
6) crush：The bletilla striata will be dried to be crushed；
7) encapsulate：Dry common bletilla encapsulation preserves.
Described solution 1, include the raw material of following mass parts：Adlay 20kg, Chinese gall 20kg, radix glycyrrhizae 15kg, the root of Dahurain angelica
15kg, chrysanthemum 10kg, malt 10kg, black tea 10kg, fresh lily 7kg, glycerine 5kg.
Described solution 1, including following preparation process：
1) the water immersion black tea 7min of 6-7 times of black tea quality is added, obtains black tea draw-off juice；
2) adlay, Chinese gall, radix glycyrrhizae, root of Dahurain angelica mixing, crushing, 78 DEG C of frying 40min, obtain powder 1, powder 1 and black tea draw-off juice
Mixing, 28 DEG C are closed 3 days, are obtained fermentate, fermentate Microwave Extraction, filtering, are obtained extract solution 1；
3) chrysanthemum, malt mixing, crushing, the salt solution of 2 times of mixed-powder quality is added, 90 DEG C of decoction 3h, filtering, must be extracted
Liquid 2, wherein described brine strength is 0.01mol/L；
4) fresh lily is smashed to pieces mixes with glycerine, -10 DEG C of placement 3h, adds extract solution 1,170r/min, 65 DEG C of reactions
2h, filtering, obtains extract solution 3, and extract solution 2 and extract solution 3 mix, both.
Described Microwave Extraction, microwave frequency 750MHz, extract 10min.
After soaking step, in addition to radio frequency processing, frequency 800KHz, processing time 5min.
Described heat treatment, be temperature be 85-90 DEG C, decocting to the bletilla striata does not have the white heart.
Described freeze-drying, it is in -30 DEG C of precoolings 1h, -80 DEG C of freezing 27h.
Described drying, it is that the hot blast that temperature is 55 DEG C is passed through in the bletilla striata, continues 4-5h.
Embodiment 5
A kind of processing method of bletilla striata oral powder, comprises the following steps：
1) stock up：Choose fresh bletilla striata root tuber, clean it is standby；
2) remove the peel：Bletilla striata raw material is put into 55 DEG C of water and soaks 1h, filters out raw material peeling；
3) soak：The bletilla striata raw material of peeling is put into solution 1, soaks 6h at a temperature of 25 DEG C；
4) it is heat-treated：The bletilla striata obtained by step 3) is heat-treated；
5) dry：Drying includes being freeze-dried and dries；
6) crush：The bletilla striata will be dried to be crushed；
7) encapsulate：Dry common bletilla encapsulation preserves.
Described solution 1, include the raw material of following mass parts：Adlay 20kg, Chinese gall 20kg, radix glycyrrhizae 15kg, the root of Dahurain angelica
15kg, chrysanthemum 10kg, malt 10kg, black tea 10kg, fresh lily 7kg, glycerine 5kg.
Described solution 1, including following preparation process：
1) the water immersion black tea 7min of 6-7 times of black tea quality is added, obtains black tea draw-off juice；
2) adlay, Chinese gall, radix glycyrrhizae, root of Dahurain angelica mixing, crushing, 78 DEG C of frying 40min, obtain powder 1, powder 1 and black tea draw-off juice
Mixing, Microwave Extraction, filtering, obtain extract solution 1；
3) chrysanthemum, malt mixing, crushing, the salt solution of 2 times of mixed-powder quality is added, 90 DEG C of decoction 3h, filtering, must be extracted
Liquid 2, wherein described brine strength is 0.01mol/L；
4) fresh lily is smashed to pieces mixes with glycerine, -10 DEG C of placement 3h, adds extract solution 1,170r/min, 65 DEG C of reactions
2h, filtering, obtains extract solution 3, and extract solution 2 and extract solution 3 mix, both.
Described Microwave Extraction, microwave frequency 750MHz, extract 10min.
Described heat treatment, be temperature be 85-90 DEG C, decocting to the bletilla striata does not have the white heart.
Described freeze-drying, it is in -30 DEG C of precoolings 1h, -80 DEG C of freezing 27h.
Described drying, it is that the hot blast that temperature is 55 DEG C is passed through in bletilla striata piece, continues 4-5h.
Experimental example
1st, effect assessment
It is experimental group 1-5 that method according to embodiment 1-5, which prepares bletilla striata oral powder, takes each group bletilla striata oral powder 5-7g
200-250ml boiling water immersion 10-12min is added, is drunk.Clinic randomly selects 300 pertussis patients, is divided into 6 groups,
1-5 takes the bletilla striata oral powder of embodiment 1-5 preparations respectively, and the 6th group of bletilla striata oral powder for taking conventional method preparation is made
For control group, 6 groups of conditions of patients situations are observed, statistical result is as shown in table 1.
As shown in Table 1, embodiment 1 carries out preparing bletilla striata oral powder according to the method for the present invention, special by being immersed in
Solution 1 in, by radio frequency processing, promote absorption of the bletilla striata for the composition of solution 1, and occur with bletilla striata intracellular matter anti-
Should, change the leaching rate of bletilla striata beneficiating ingredient so that the active constituent content in water-leach liquor increased, and effect is also therewith
Increase.Compared with Example 1, preparation of the embodiment 2 for solution 1 is simpler；Embodiment 3 is implemented without radio frequency processing is passed through
High temperature high pressure process has been changed to traditional decoction and handled by example 4；Embodiment 5 by the processing for solution 1 it is relatively simple, do not pass through
Radio frequency processing, while high temperature high pressure process has also been changed to traditional decoction and handled.Because preparation process is different, so that real
The therapeutic effect for applying the bletilla striata oral powder of a 1-5 is different.
The bletilla striata oral powder of table 1 treats pertussis result
2nd, other clinical practice cases
1) Lee, man, Symptoms are to be spat blood caused by gastric injury, take the present invention and prepare bletilla striata oral powder two weeks
Afterwards, symptom is obviously improved.
2) money, female, performance symptom are gastric ulcer, take the present invention and prepare bletilla striata oral powder after 1 week, symptom substantially changes
It is kind.
Claims (8)
1. a kind of processing method of bletilla striata oral powder, it is characterised in that comprise the following steps：
1) stock up：Choose fresh bletilla striata root tuber, clean it is standby；
2) remove the peel：Bletilla striata raw material is put into 55-58 DEG C of water and soaks 1-2h, filters out raw material peeling；
3) soak：The bletilla striata raw material of peeling is put into solution 1, and 6-7h is soaked at a temperature of 25-30 DEG C；
4) it is heat-treated：The bletilla striata obtained by step 3) is subjected to high temperature high pressure process；
5) dry：Drying includes being freeze-dried and dries；
6) crush：The bletilla striata will be dried to be crushed；
7) encapsulate：Dry common bletilla encapsulation preserves.
2. the processing method of bletilla striata oral powder as claimed in claim 1, it is characterised in that described solution 1, including it is following
The raw material of mass parts：Adlay 20-40 parts, Chinese gall 20-35 parts, radix glycyrrhizae 15-25 parts, root of Dahurain angelica 15-20 parts, chrysanthemum 10-15 parts, wheat
Bud 10-15 parts, black tea 10-13 parts, fresh lily 7-9 parts, glycerine 5-7 parts.
3. the processing method of bletilla striata oral powder as claimed in claim 2, it is characterised in that described solution 1, including it is following
Preparation process：
1) the water immersion black tea 7-8min of 6-7 times of black tea quality is added, obtains black tea draw-off juice；
2) adlay, Chinese gall, radix glycyrrhizae, root of Dahurain angelica mixing, crushing, 78-80 DEG C of frying 40-50min, obtain powder 1, powder 1 and black tea
Juice is mixed, and 28-34 DEG C is closed 3-4 days, is obtained fermentate, fermentate Microwave Extraction, filtering, is obtained extract solution 1；
3) chrysanthemum, malt mixing, crushing, the salt solution of 2-3 times of mixed-powder quality is added, 90-95 DEG C of decoction 3-4h, filtering, is obtained
Extract solution 2, wherein described brine strength is 0.01-0.02mol/L；
4) fresh lily is smashed to pieces mixes with glycerine, -10~-15 DEG C of placement 3-5h, addition extract solution 1,170-180r/min,
65-70 DEG C of reaction 2-2.5h, filtering, obtains extract solution 3, and extract solution 2 and extract solution 3 mix, both.
4. the processing method of bletilla striata oral powder as claimed in claim 3, it is characterised in that described Microwave Extraction, microwave
Frequency is 750MHz, extracts 10-12min.
5. the processing method of bletilla striata oral powder as claimed in claim 1, it is characterised in that after soaking step, in addition to
Radio frequency processing, frequency 800-820KHz, processing time 5-7min.
6. the processing method of bletilla striata oral powder as claimed in claim 1, it is characterised in that described high temperature high pressure process,
Be temperature be 210-230 DEG C, pressure 5.0-7.0MPa, processing time 7-10min.
7. the processing method of bletilla striata oral powder as claimed in claim 1, it is characterised in that described freeze-drying, be -
30~-24 DEG C of precoolings 1-2h, -80~-75 DEG C of freezing 27-32h.
8. the processing method of bletilla striata oral powder as claimed in claim 1, it is characterised in that described drying, be by temperature
It is passed through for 55-58 DEG C of hot blast in the bletilla striata, continues 4-5h.
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| CN201710744342.8A CN107551142A (en) | 2017-08-25 | 2017-08-25 | A kind of processing method of bletilla striata oral powder |
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| CN201710744342.8A CN107551142A (en) | 2017-08-25 | 2017-08-25 | A kind of processing method of bletilla striata oral powder |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113134059A (en) * | 2021-04-29 | 2021-07-20 | 桂林丰润莱生物科技股份有限公司 | Processing method of bletilla striata tablets |
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| CN1227728A (en) * | 1998-03-01 | 1999-09-08 | 夏佩珊 | Flavouring nutritive health food capable of refreshing oneself, relieving summer heat and curing disease |
| CN103665400A (en) * | 2013-11-12 | 2014-03-26 | 唐忠海 | Preparation method and application of hyacinth bletilla hemostatic gel |
| CN104491593A (en) * | 2014-11-26 | 2015-04-08 | 山东永泰化工有限公司 | Health-care tea used for gastric ulcer |
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|---|---|---|---|---|
| CN1227728A (en) * | 1998-03-01 | 1999-09-08 | 夏佩珊 | Flavouring nutritive health food capable of refreshing oneself, relieving summer heat and curing disease |
| CN103665400A (en) * | 2013-11-12 | 2014-03-26 | 唐忠海 | Preparation method and application of hyacinth bletilla hemostatic gel |
| CN104491593A (en) * | 2014-11-26 | 2015-04-08 | 山东永泰化工有限公司 | Health-care tea used for gastric ulcer |
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| 贾天柱等: "《中药炮制化学》", 31 October 2015, 上海科学技术出版社 * |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113134059A (en) * | 2021-04-29 | 2021-07-20 | 桂林丰润莱生物科技股份有限公司 | Processing method of bletilla striata tablets |
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Application publication date: 20180109 |