CN107550867A - A kind of safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid and preparation method thereof - Google Patents
A kind of safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid and preparation method thereof Download PDFInfo
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- CN107550867A CN107550867A CN201711008783.8A CN201711008783A CN107550867A CN 107550867 A CN107550867 A CN 107550867A CN 201711008783 A CN201711008783 A CN 201711008783A CN 107550867 A CN107550867 A CN 107550867A
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- tartaric acid
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Abstract
The present invention disclose a kind of safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid, and by weight percentage, its component is ten thousand rhzomorphs of tartaric acid Thailand 20% 30%, aromatic 0.1% 0.3%, sweetener 0.1% 0.3%, solvent（Wetting agent）4% 8%, stabilizer（Dispersant）5 12%, metal ion chelation agent 0.1% 0.3%, carrier adds to 100%.Invention additionally discloses the preparation method of pre-mixing agent.The present invention can solve the problems such as safe ten thousand rhzomorph bitters of tartaric acid, Electrostatic Absorption, airborne dust and metal ion etc. react, and improve its bioavailability, improve the productivity effect and economic benefit of plant.
Description
Technical field
The invention belongs to veterinary arts field, and in particular to a kind of antistatic tartaric acid ten thousand rhzomorph pre-mixing agents of Thailand and its preparation
Method.
Background technology
Porcine mycoplasmal pneumonia is a kind of chronic, contact, also known as respiratory infectious disease, pig as caused by mycoplasma hyopneumoniae
Enzootic pneumonia, China are commonly called as swine enzootic pneumonia, and main clinical symptom is cough and asthma.It is each that this disease is distributed widely in the world
Ground, there is generation in many areas in China, sick pig or directly generation are dead, or dead as cad pig or scabies secondary infection, or growth
Development is slow, reduces growth rate, efficiency of feed utilization, causes heavy economic losses very big, is the important epidemic disease for endangering pig industry development
One of disease.
Ten thousand rhzomorphs of tartaric acid Thailand are the abbreviation of tartaric acid acetylisovaleryl tylosin, the safe happy bacterium of tartaric acid acetyl-isovaleryl
Element, it is the macrolide antibiotics of a new generation, it is a kind of obtained from semi-synthetic through biofermentation on the basis of tylosin
The special antibiotic of macrolides poultry, there are antibacterial activity, including mycoplasma to many gram-positive bacterias and some negative bacteriums,
Vibrios, conveyor screw etc., there is the effect of uniqueness to chicken Deficiency Mycoplasma, porcine mycoplasmal pneumonia, pig dysentery characterized by blood in the stool etc..
The common rhzomorph type of Thailand ten thousand has soluble powder, conventional pre-mixing agent, injection and for being coated with technique productions on the market
There is the characteristics of bitter in grain etc., safe ten thousand rhzomorphs, soluble powder has the defects of following several respects：First, palatability is poor, influence to move
The feeding of thing；Second, soluble powder proportion is small, easy airborne dust, not only causes to waste, also influence operator's health；Third, using
During easily had an effect with trace element, electrolyte, acidulant etc. in feed, reduce drug effect；Fourth, electrostatic adsorption
By force, waste is easily caused during production, use；Fifth, safe ten thousand rhzomorphs are unstable under the conditions of hydrochloric acid in gastric juice, and it is rapid to decompose, reduce life
Thing utilization rate.Injection increases labour using process, animal easily produces stress reaction using process, influences to grow.Bag
Though solving palatability problems by the granular preparation of technique productions, the production time is long, efficiency is low, cost is high, preparation may not
Uniformly, using effect is influenceed.
Therefore research and develop that a kind of palatability is good, not airborne dust, antistatic, anti-ion, while the system that cost is low, absorption rate is good
Agent and preparation method thereof is extremely urgent to improve the productivity effect of vast plant and economic benefit.
In view of this, the present inventor has specialized in a kind of safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid and its preparation side
Thus method, this case produce.
The content of the invention
It is an object of the invention to provide safe ten thousand rhzomorph pre-mixing agents of a kind of antistatic tartaric acid and preparation method thereof, to solve
The problems such as ten thousand rhzomorph bitters of tartaric acid Thailand, Electrostatic Absorption, airborne dust and metal ion react, improves its bioavailability, carries
The productivity effect and economic benefit of high plant.
In order to reach above-mentioned purpose, solution of the invention is：
A kind of safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid, by weight percentage, its component is ten thousand rhzomorph 20%- of tartaric acid Thailand
30%th, aromatic 0.1%-0.3%, sweetener 0.1%-0.3%, metal ion chelation agent 0.1% -0.3%, solvent（Wetting agent）4%-
8%, stabilizer（Dispersant）5-12%, carrier add to 100%.
A kind of preparation method of the safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid of the present invention, comprises the following steps：
Step 1：Metal ion chelation agent is dissolved in water, sweetener, aromatic are dissolved in solvent（Wetting agent）, add stabilizer
（Dispersant）, metal ion chelation agent solution is added, stirring, obtains wetting agent A；
Step 2：Safe ten thousand rhzomorphs of tartaric acid, carrier are poured into trough type mixing machine/agitation mixer, add half wetting agent A, lid
Upper mixer lid, mix 5 minutes；
Step 3：Mixer lid is opened, adds surplus solution A, close the cover, continues stirring 10 minutes；
Step 4：Lid is opened, observes combustion, agglomerating, no airborne dust should be held, it is overall uniform, continue to close if uneven
Lid is stirred until homogeneous, and obtains material B；
Step 5：Material B is crossed into 40 mesh sieves, sieves 2 times, obtains material C；
Step 6：Material C is poured into mixer, is stirred 15 minutes, produces.
The sweetener is at least one of Steviosin, sorbierite composition.
The aromatic is at least one of orange essence, lemon extract, peppermint oil composition.
The solvent（Wetting agent）Formed at least one of ethanol, propane diols
The stabilizer（Dispersant）Formed at least one of polyethylene glycol 200, polyethylene glycol 400, Macrogol 600.
The metal ion chelation agent is at least one of sodium tripolyphosphate, citric acid, disodium ethylene diamine tetraacetate group
Into.
The carrier is defatted rice bran, and 80 mesh, moisture is below 5%.
Safe ten thousand rhzomorphs of the tartaric acid meet efficient, less toxic, the low-residual bulk drug of veterinary drug standard, and it can be with sensitive bacteria
Ribosome 50S subunits combine, and by the blocking to transpeptidation and/or mRNA displacements, suppress the synthesis and extension of peptide chain, from
And the synthesis of bacterioprotein is influenceed, play restraining and sterilizing bacteria effect.Ten thousand rhzomorphs of tartaric acid Thailand are to gram-positive bacteria such as grape ball
Bacterium, bacillus, streptococcus, clostridium have antibacterial activity, also want good inhibiting effect to mycoplasma.
The present invention has advantages below：This technique uses method of granulating, makes final products that the particle of 40 mesh or so be made, no
Electrostatic interaction can occur, without drying, avoid influence of the temperature to active ingredient, avoid airborne dust situation during use；Add
Sweetener, aromatic etc. can play a part of flavoring, flavouring, improve its palatability, and metal ion chelation agent can be kept away indirectly
Exempt from the influence of ten thousand rhzomorphs of metal ion paratartaric acid Thailand in feed.
Embodiment
The present invention is further described below by specific embodiment, but is not limited to following examples：
Embodiment 1：
A kind of safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid, by weight percentage, its component is safe ten thousand rhzomorphs 20% of tartaric acid, sweet tea
Taste agent 0.1%, aromatic 0.1%, solvent（Wetting agent）4%, metal ion chelation agent solution 1.1%, stabilizer（Dispersant）6%,
Carrier 68.7%.
The preparation method of ten thousand rhzomorph pre-mixing agents of tartaric acid Thailand, is concretely comprised the following steps：By 1kg metal ion chelation agent solution 10kg
Water, 1kg sweeteners, 1kg aromatic are dissolved in 40L solvents（Wetting agent）, add 60L stabilizers（Dispersant）, add metal from
Sub- chelating agent solution, stirring, obtains wetting agent A；By safe ten thousand rhzomorphs of 200kg tartaric acid, 687kg carriers pour into trough type mixing machine/
Agitation mixer, half wetting agent A is added, cover mixer lid, mixed 5 minutes；Mixer lid is opened, is added surplus
Remaining wetting agent A, close the cover, continue stirring 10 minutes；Lid is opened, observes combustion, holds agglomerating, no airborne dust, it is overall
Uniformly, material B is obtained；Material B is crossed into 40 mesh sieves, sieves 2 times, obtains material C；Material C is poured into mixer, is stirred 15
Minute, produce.Hearing products obtained therefrom has light fragrance, takes a small amount of product and the tip of the tongue to taste out slightly sweet taste, by products obtained therefrom, together
Ten thousand rhzomorph pre-mixing agents of class tartaric acid Thailand are attached separately to seal in two dry plastics bags, rub polybag with the hands back and forth with hand, stretch afterwards
Polybag simultaneously is allowed to stand, and the present invention will not be adsorbed on polybag, and the safe ten thousand rhzomorph pre-mixing agents of similar tartaric acid can adsorb
On polybag wall, it was demonstrated that the present invention has antistatic property.Polybag is cut off afterwards, product poured out respectively, similar winestone
Ten thousand rhzomorph pre-mixing agents of sour Thailand fly away pouring out process everywhere, and dust raising phenomenon is obvious, waste serious, and the present invention is all poured on container
On, substantially without dust raising phenomenon.
Embodiment 2：
A kind of safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid, by weight percentage, its component is safe ten thousand rhzomorphs 20% of tartaric acid, sweet tea
Taste agent 0.2%, aromatic 0.2%, solvent（Wetting agent）6%, metal ion chelation agent solution 2.2%, stabilizer（Dispersant）10%,
Carrier 61.4%.
The preparation method of ten thousand rhzomorph pre-mixing agents of tartaric acid Thailand, is concretely comprised the following steps：By 2kg metal ion chelation agent solution 20kg
Water, 2kg sweeteners, 2kg aromatic are dissolved in 60L solvents（Wetting agent）, add 100L stabilizers（Dispersant）, add metal from
Sub- chelating agent solution, stirring, obtains wetting agent A；By safe ten thousand rhzomorphs of 200kg tartaric acid, 614kg carriers pour into trough type mixing machine/
Agitation mixer, half wetting agent A is added, cover mixer lid, mixed 5 minutes；Mixer lid is opened, is added surplus
Remaining wetting agent A, close the cover, continue stirring 10 minutes；Lid is opened, observes combustion, holds agglomerating, no airborne dust, it is overall
Uniformly, material B is obtained；Material B is crossed into 40 mesh sieves, sieves 2 times, obtains material C；Material C is poured into mixer, is stirred 15
Minute, produce.Hearing products obtained therefrom has comfortable fragrance, takes a small amount of product and the tip of the tongue to taste out sweet taste, by products obtained therefrom, similar
Ten thousand rhzomorph pre-mixing agents of tartaric acid Thailand are attached separately to seal in two dry plastics bags, rub polybag with the hands back and forth with hand, stretch modeling afterwards
Pocket simultaneously is allowed to stand, and the present invention will not be adsorbed on polybag, and the safe ten thousand rhzomorph pre-mixing agents of similar tartaric acid can be adsorbed and moulded
On pocket wall, it was demonstrated that the present invention has antistatic property.Polybag is cut off afterwards, product poured out respectively, similar tartaric acid
Safe ten thousand rhzomorph pre-mixing agents are flown away pouring out process everywhere, and dust raising phenomenon is obvious, waste serious, and the present invention is all poured on container,
Substantially there is no dust raising phenomenon.A paper is spread in black desktop, by this product 100g from vertically down being fallen apart from desktop 30cm at, up to
It is finished down, eye observation, substantially without airborne dust, do not wear masks also stimulates nasal cavity phenomenon, after 5 minutes, the black table of paper edge without dust
Substantially without dust on face.By like product（Without granulation）, operated with method, it is seen that obvious airborne dust, not wearing masks has the pungent sense of dust
Feel, the black desktop of paper edge has one layer of dust after 5 minutes.Illustrate pre- in contrast to safe ten thousand rhzomorphs of other tartaric acid without granulation
Mixture, this product have a clear superiority on anti-airborne dust.Granularity of dust is smaller, and being adsorbed phenomenon in the place for having electrostatic can be brighter
Aobvious, this product granularity substantially remains in 40 mesh or so, can effectively avoid Electrostatic Absorption and the embarrassment of airborne dust.
Embodiment 3：
A kind of safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid, by weight percentage, its component is safe ten thousand rhzomorphs 20% of tartaric acid, sweet tea
Taste agent 0.3%, aromatic 0.3%, solvent（Wetting agent）8%, stabilizer（Dispersant）12%, metal ion chelation agent solution 3.3%,
Carrier 56.1%.
The preparation method of ten thousand rhzomorph pre-mixing agents of tartaric acid Thailand, is concretely comprised the following steps：By 3kg metal ion chelation agent solution 30kg
Water, 3kg sweeteners, 3kg aromatic are dissolved in 80L solvents（Wetting agent）, add 120L stabilizers（Dispersant）, add metal from
Sub- chelating agent solution, stirring, obtains wetting agent A；By safe ten thousand rhzomorphs of 200kg tartaric acid, 561kg carriers pour into trough type mixing machine/
Agitation mixer, half wetting agent A is added, cover mixer lid, mixed 5 minutes；Mixer lid is opened, is added surplus
Remaining wetting agent A, close the cover, continue stirring 10 minutes；Lid is opened, observes combustion, holds agglomerating, no airborne dust, it is overall
Uniformly, material B is obtained；Material B is crossed into 40 mesh sieves, sieves 2 times, obtains material C；Material C is poured into mixer, is stirred 15
Minute, produce.Hearing products obtained therefrom has compared with giving off a strong fragrance taste, takes a small amount of product and the tip of the tongue to taste out heavier sweet taste, by products obtained therefrom, together
Ten thousand rhzomorph pre-mixing agents of class tartaric acid Thailand are attached separately to seal in two dry plastics bags, rub polybag with the hands back and forth with hand, stretch afterwards
Polybag simultaneously is allowed to stand, and the present invention will not be adsorbed on polybag, and the safe ten thousand rhzomorph pre-mixing agents of similar tartaric acid can adsorb
On polybag wall, it was demonstrated that the present invention has antistatic property.Polybag is cut off afterwards, product poured out respectively, similar winestone
Ten thousand rhzomorph pre-mixing agents of sour Thailand fly away pouring out process everywhere, and dust raising phenomenon is obvious, waste serious, and the present invention is all poured on container
On, substantially without dust raising phenomenon.
Embodiment 4
There are clinical symptoms in swinery：Dry cough, cough is overcast, frequency is low, dehisces to breathe, breathing increase, One's spirits are drooping, does not like to walk
It is dynamic, breathed when walking about obvious, in abdominal respiration and sitting position of dog gesture, cut open inspection sick dead pig, lung's point leaf has a muscle sample lesion, hilus pulumonis and
Vertical phrenic lymph nodes enlargement, pancreas have meat sample lesion, and bronchium is plump, flows out white slimy, doubtful porcine mycoplasmal lung in tube wall
Inflammation, Virus monitory with product of the present invention carry out therapeutic test after making a definite diagnosis, to prove a kind of safe ten thousand bacterium of antistatic tartaric acid of the present invention
The clinical effectiveness of plain pre-mixing agent.25 sick pigs are randomly divided into 5 groups, every group 5, product in first group of feeding embodiment 1,
The product in product, the 3rd group of feeding embodiment 3 in two groups of feeding embodiments 2, the tartaric acid of the 4th group of feeding market purchase
Safe ten thousand rhzomorph soluble powders, the 5th group does not feed medicine, and after 3 days, 1-4 groups swinery has taken a turn for the better, and centre is without death, 1-
3 groups of symptoms are substantially better than the 4th group, and best with the 2nd group of effect, the 5th group of swinery exacerbation of symptoms, dead one, it can thus be appreciated that this
Invention tartaric acid ten thousand rhzomorph pre-mixing agents of Thailand are to treating porcine mycoplasmal pneumonia positive effect, and it is soluble to be better than safe ten thousand rhzomorphs of tartaric acid
Powder, therefore using this product plant can be made to reduce economic loss, increase the benefit.
Claims (8)
- A kind of 1. safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid, it is characterised in that：By weight percentage, its component is that tartaric acid is safe Ten thousand rhzomorph 20%-30%, aromatic 0.1%-0.3%, sweetener 0.1%-0.3%, solvent 4%-8%, stabilizer 5-12%, metal ion Chelating agent 0.1%-0.3%, carrier add to 100%.
- A kind of 2. safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid as claimed in claim 1, it is characterised in that preparation method, including Following steps：Step 1：Metal ion chelation agent is dissolved in water, sweetener, aromatic are dissolved in solvent, add stabilizer, adds metal Ion chelating agent solution, stirring, obtains wetting agent A；Step 2：Safe ten thousand rhzomorphs of tartaric acid, carrier are poured into trough type mixing machine/agitation mixer, add half profit solution A, lid Upper mixer lid, mix 5 minutes；Step 3：Mixer lid is opened, adds surplus solution A, close the cover, continues stirring 10 minutes；Step 4：Lid is opened, observes combustion, agglomerating, no airborne dust should be held, it is overall uniform, continue to close if uneven Lid is stirred until homogeneous, and obtains material B；Step 5：Material B is crossed into 40 mesh sieves, sieves 2 times, obtains material C；Step 6：Material C is poured into mixer, is stirred 15 minutes, produces.
- A kind of 3. safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid as claimed in claim 1, it is characterised in that：The sweetener is At least one of Steviosin, sorbierite form.
- A kind of 4. safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid as claimed in claim 1, it is characterised in that：The solvent is second At least one of alcohol, propane diols form.
- A kind of 5. safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid as claimed in claim 1, it is characterised in that：The stabilizer is At least one of polyethylene glycol 200, polyethylene glycol 400, Macrogol 600 form.
- A kind of 6. safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid as claimed in claim 1, it is characterised in that：The aromatic is At least one of orange essence, lemon extract, peppermint oil form.
- A kind of 7. safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid as claimed in claim 1, it is characterised in that：The metal ion Chelating agent is at least one of sodium tripolyphosphate, citric acid, disodium ethylene diamine tetraacetate composition.
- A kind of 8. safe ten thousand rhzomorph pre-mixing agents of antistatic tartaric acid as claimed in claim 1, it is characterised in that：The carrier is de- Fat rice bran, 95% above by 80 mesh, and moisture is below 5%.
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| CN201711008783.8A CN107550867B (en) | 2017-10-25 | 2017-10-25 | Antistatic tavermectin tartrate premix and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109010281A (en) * | 2018-10-10 | 2018-12-18 | 新昌县九信药业有限公司 | Ten thousand rhzomorph pre-mixing agents of a kind of tartaric acid Thailand and preparation method thereof |
| CN114469869A (en) * | 2022-01-14 | 2022-05-13 | 广州市和生堂动物药业有限公司 | Tylosin tartrate premix and preparation method thereof |
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| CN106265711A (en) * | 2016-08-25 | 2017-01-04 | 浦城正大生化有限公司 | Tylosin phosphonate pre-mixing agent formula and preparation technology |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106265711A (en) * | 2016-08-25 | 2017-01-04 | 浦城正大生化有限公司 | Tylosin phosphonate pre-mixing agent formula and preparation technology |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109010281A (en) * | 2018-10-10 | 2018-12-18 | 新昌县九信药业有限公司 | Ten thousand rhzomorph pre-mixing agents of a kind of tartaric acid Thailand and preparation method thereof |
| CN109010281B (en) * | 2018-10-10 | 2021-01-05 | 新昌县九信药业有限公司 | Tylosin tartrate premix and preparation method thereof |
| CN114469869A (en) * | 2022-01-14 | 2022-05-13 | 广州市和生堂动物药业有限公司 | Tylosin tartrate premix and preparation method thereof |
| CN114469869B (en) * | 2022-01-14 | 2022-10-25 | 广州市和生堂动物药业有限公司 | Tylosin tartrate premix and preparation method thereof |
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