CN107523438A - The manual dishwashing liquid detergent and preparation method of a kind of active component containing American cockroach - Google Patents
The manual dishwashing liquid detergent and preparation method of a kind of active component containing American cockroach Download PDFInfo
- Publication number
- CN107523438A CN107523438A CN201710603250.8A CN201710603250A CN107523438A CN 107523438 A CN107523438 A CN 107523438A CN 201710603250 A CN201710603250 A CN 201710603250A CN 107523438 A CN107523438 A CN 107523438A
- Authority
- CN
- China
- Prior art keywords
- extract
- american cockroach
- active component
- component
- liquid detergent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0047—Other compounding ingredients characterised by their effect pH regulated compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2065—Polyhydric alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/34—Organic compounds containing sulfur
- C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/384—Animal products
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/90—Betaines
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Zoology (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The present invention discloses manual dishwashing liquid detergent of a kind of active component containing American cockroach and preparation method thereof, is made up of the raw material of following mass percent：Surfactant 40~51%, sterilization component 0.1~0.8%, skin care ingredient 1~3%, the active component 0.01~1% of American cockroach, sodium citrate 0.5%, deionized water surplus, above-mentioned each component sum are 100%.Skin care ingredient of the present invention by the use of plant extraction liquid as manual dishwashing liquid detergent, prevents dry skin composition, skin moisturizing ingredients, solves the phenomenon that manual dishwashing defensive position is dried, both can be degradable to environment also no pressure with skin care.By the use of sodium citrate as washing assisant and sterilization component, it can not only sterilize, be also used as pH adjusting agent, complexing agent.The bactericidal effect and skin effect of the gained more conventional liquid detergent of manual dishwashing liquid detergent of the invention are more excellent.
Description
Technical field
The invention belongs to daily chemical product technical field, specially a kind of manual dishwashing liquid detergent and preparation method thereof.
Background technology
Nowadays increasing family uses liquid detergent wash up, but many liquid detergent chemical addition agents of in the market
It is more, but fungistatic effect is poor, difficult degradation, has certain alkalescence again, there is degreasing stimulation to human body skin, easily to use
The skin of person causes dry, coarse or even decortication allergy phenomenon, long-term use of big to skin damage.
The present invention provides a kind of manual dishwashing liquid detergent of the active component containing American cockroach, has bactericidal, skin care, easily
Degraded and other effects, its particularity is mainly the addition of American cockroach active component, Chinese herbal medicine extract.American cockroach is Insecta
Pterigota Blattaria Blattidae Periplaneta insect, is one of three advantages worm kind of blattaria, its active component has very to skin
Good repair.It is reported that American cockroach active component has promotion organization repair ability, the surface of a wound and burn granulation can be promoted
Hyperblastosis；Obvious to acute gastric ulcer and ethanol-type gastric mucosa damage protecting effect, beautiful Lian worms powder can reduce enteron aisle large intestine bar
The quantity of bacterium, the intestinal mucosa of pathological change and fine hair reparation can be made intact.
Chrysanthemum indicum be composite family herbaceos perennial mother chrysanthemum capitulum, have it is clearing heat and detoxicating, to various pathogens, virus
There is the effect of killing or inhibitory activity.Aurantiamarin, aesculin are respectively provided with anti-inflammatory, antiviral, antibacterial action.The present invention also uses
Plant extracts compounding is used as skin care ingredient, respectively with ginkgo leaf, witch hazel silver, camellia, the wooden fruit of breast, Salvia japonica, rosemary
Several extracts, this several natural plant extracts compounding have excellent moistening effect together, then active with American cockroach
Composition acts synergistically, phenomena such as improving the pachylosis after washing the dishes, dry.
The content of the invention
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of hand washing of active component containing American cockroach meal
Have liquid detergent and preparation method, there is bactericidal, skin care, degradable, easy rinsing and other effects.
To achieve these goals, technical scheme provided by the present invention is：A kind of hand of the active component containing American cockroach
Wash up liquid detergent, it is made up of the raw material of following mass percent：Surfactant 40~51%, sterilization component 0.1~
0.8%th, skin care ingredient 1~3%, the active component 0.01~1% of American cockroach, sodium citrate 0.5%, deionized water surplus,
Above-mentioned each component sum is 100%.
The surfactant is made up of the component of following masses part：Sodium sulfate of polyethenoxy ether of fatty alcohol 10-13%, alkane
Agent glucosides 10~12%, neopelex 8~10%, the alkylolamides 6~8% of cocounut oil two, Cocoamidopropyl betaine 6
~8%.
The sterilization component is three in KF88, sodium citrate, Flos Chrysanthemi Indici extract, Extract from Orange Peel, buckeye extract
The mixture of kind or three kinds of any of the above ratios.
The sterilization component is made up of the component of following masses part：0~0.2 part of KF88,0.04~0.2 part of sodium citrate,
0.04~0.2 part of Flos Chrysanthemi Indici extract, 0.04~0.2 part of Extract from Orange Peel, 0.04~0.2 part of buckeye extract.
The skin care ingredient is made up of the component of following masses part：Prevent 0.5~1.5 part of dry skin composition, skin from protecting
Wet 0.5~1.5 part of composition.
It is described to prevent dry skin composition from being carried for ginkgo biloba p.e, hamamelis extract, Rosmarinus officinalis extract, camellia
Take the mixture of two or more arbitrary proportion in thing.
It is described to prevent dry skin composition from being made up of the component of following masses part：0.25~0.375 part of ginkgo biloba p.e,
0.25~0.375 part of hamamelis extract, 0.25~0.375 part of Rosmarinus officinalis extract, camellia flower extract 0.25~0.375
Part.
The skin moisturizing ingredients are made up of the component of following masses part：Wooden 0.125~0.375 part of the berry extract of breast, mouse
0.125~0.375 part of tail grass extract, 0.125~0.375 part of narcissus bulb stem extraction, D-sorbite 0.125~0.375
Part.
The active component of the American cockroach is obtained using semi-bionic extraction, specific as follows：
A, 3 kinds of cushioning liquid that pH is 2.0,7.5,8.3 are configured to respectively with citric acid, disodium hydrogen phosphate, it is standby；
B, dry American cockroach polypide is crushed, the mass concentration for adding 6 times of amounts of American cockroach worm silty amount is
95% ethanol, then handled 4 hours at a temperature of 50 DEG C, the filter residue after filtering is put into 50 DEG C of dryings of baking oven；
C, by the amount of 20ml cushioning liquid/g filter residues, the slow of the pH=2.0 that regulates is added in step B drying filter residue
Solution is rushed, 60min is extracted at a temperature of 60 DEG C of setting, is filtered, then is existed successively with pH=7.5 and pH=8.3 cushioning liquid
Extract filter residue twice under the same conditions, filtering, be concentrated by evaporation after merging each extract solution, when being concentrated to extract solution can also flow,
Concentrate is poured into evaporating dish, dried in 80 DEG C of baking oven, produces the active component of American cockroach.
The active component of American cockroach by this method extraction, and conventional method extraction comparison, retain to greatest extent
Its active ingredient, while eliminate the American cockroach specific peculiar smell that conventional method extract is left, hence it is evident that improve its application
Subjective feeling.
Another object of the present invention is to a kind of preparation for the manual dishwashing liquid detergent for providing active component containing American cockroach
Method, by following each step：
(1) material preparation of following mass percent is pressed：Surfactant 40~51%, sterilization component 0.1~0.8%,
Skin care ingredient 1~3%, the active component 0.01~1% of American cockroach, sodium citrate 0.5%, deionized water surplus, it is above-mentioned each
Component sum is 100%；
(2) surfactant of step (1) is heated in 60 DEG C of water-bath, heat while stirring 1h, is cooled to room
Temperature, sterilization component, skin care ingredient, the active component of American cockroach are added, pH value is adjusted after stirring to 6~8, is mixed
Thing；
(3) mixture of step (2) is placed in 40 DEG C of water-bath the 1h that heats while stirring, is cooled to room temperature, sealed
24h is placed, that is, obtains the manual dishwashing liquid detergent of the active component containing American cockroach.
The pH of the step (2) is to add trisodium citrate to be adjusted.
Above-mentioned chrysanthemum indicum, orange peel, seven leaves, ginkgo leaf, witch hazel, rosemary, camellia, the wooden fruit of breast, Salvia japonica, daffodil
Extractive form corm is prepared by following method：
First, corresponding chrysanthemum indicum, orange peel, seven leaves, ginkgo leaf, witch hazel, rosemary, camellia, breast wood are weighed respectively
Fruit, Salvia japonica, daffodil bulb raw material, immersion 24h is carried out with the normal-temperature distilled water for not crossing raw material respectively, then carry out 2h water-bath
Boiling, boiling temperature are 90 DEG C；Then to filter, filtrate carries out rotary evaporation, and filtrate is condensed into 1g/mL concentrate, then
Concentrate is toasted, and powder is respectively prepared, and is produced the correspondingly chrysanthemum indicum of raw material, orange peel, seven leaves, ginkgo leaf, witch hazel, fan and is changed
Perfume, camellia, the wooden fruit of breast, Salvia japonica, narcissus bulb stem extraction.
The advantages of present invention possesses and effect：Skin care of the present invention by the use of plant extracts as manual dishwashing liquid detergent into
Point, dry skin composition, skin moisturizing ingredients are prevented, solve the phenomenon that manual dishwashing defensive position is dried, both can be with skin care, to ring
Border also no pressure, it is degradable.By the use of sodium citrate as washing assisant (sterilization component), it can not only sterilize, be also used as
PH adjusting agent, complexing agent.The bactericidal effect and skin effect of the gained more conventional liquid detergent of manual dishwashing liquid detergent of the invention are more excellent
Different, its particularity is that skin care ingredient with the addition of American cockroach active component and Chinese herbal medicine extract.
Embodiment
With reference to specific embodiment, the present invention is further described.
The active component of American cockroach as described below is obtained using semi-bionic extraction, specific as follows：
(1) 3 kinds of cushioning liquid that pH is 2.0,7.5,8.3 are configured to respectively with citric acid, disodium hydrogen phosphate, it is standby；
(2) in pear-shaped flask, 100g drying American cockroach polypide is weighed, is crushed with plant pulverizer, after crushing
Beautiful Lian worms powder, then add the ethanol that 600g mass concentrations are 95%, then handle 4 hours at a temperature of 50 DEG C, filtering
Filter residue afterwards is put into 50 DEG C of dryings of baking oven；
(3) weigh with after Ethanol Treatment and dried beautiful Lian worms powder 10g, then add the pH=that 200mL is regulated
2.0 cushioning liquid, extract 60min at a temperature of 60 DEG C of setting, then use pH=7.5 and pH=8.3 buffering successively
Solution is extracted twice under the same conditions, and filtering, extract solution is concentrated by evaporation after merging, when being concentrated to extract solution can also flow,
Concentrate is poured into evaporating dish, dried in 80 DEG C of baking oven, produces the active component of the American cockroach of semi-bionic extraction method.
Chrysanthemum indicum as described below, orange peel, seven leaves, ginkgo leaf, witch hazel, rosemary, camellia, the wooden fruit of breast, Salvia japonica, water
Celestial bouquet stem extraction is prepared by following method：
First, corresponding chrysanthemum indicum, orange peel, seven leaves, ginkgo leaf, witch hazel, rosemary, camellia, breast wood are weighed respectively
Fruit, Salvia japonica, daffodil bulb raw material, immersion 24h is carried out with the normal-temperature distilled water for not crossing raw material respectively, then carry out 2h water-bath
Boiling, boiling temperature are 90 DEG C；Then to filter, filtrate carries out rotary evaporation, and filtrate is condensed into 1g/mL concentrate, then
Concentrate is toasted, and powder is respectively prepared, and is produced the correspondingly chrysanthemum indicum of raw material, orange peel, seven leaves, ginkgo leaf, witch hazel, fan and is changed
Perfume, camellia, the wooden fruit of breast, Salvia japonica, narcissus bulb stem extraction.
Embodiment 1
(1) material preparation of following mass percent is pressed：Surfactant 40%, sterilization component 0.1%, skin care ingredient
1%th, the active component 0.01% of American cockroach, sodium citrate 0.5%, deionized water surplus, above-mentioned each component sum are
100%；
The surfactant is made up of the component of following masses part：Sodium sulfate of polyethenoxy ether of fatty alcohol 10%, alkane agent
Glucosides 10%, neopelex 8%, the alkylolamides 6% of cocounut oil two, Cocoamidopropyl betaine 6%.
The sterilization component is to be made up of the component of following masses part：KF88 0.03%, Flos Chrysanthemi Indici extract 0.04%, orange
Bark extract 0.03%.
The skin care ingredient is made up of the component of following masses part：Prevent dry skin composition 0.5%, skin moisturizing ingredients
0.5%.
It is described to prevent dry skin composition from being made up of the component of following masses part：Ginkgo biloba p.e 0.25%, rosemary
Extract 0.25%.
The skin moisturizing ingredients are made up of the component of following masses part：The wooden berry extract 0.125% of breast, Salvia japonica extraction
Thing 0.125%, the extract 0.125% of daffodil bulb, D-sorbite 0.125%.
(2) surfactant of step (1) is heated in 65 DEG C of water-bath, heat while stirring 1 half h, then cools down
To room temperature, sterilization component, skin care ingredient, the active component of American cockroach are added, pH value is adjusted after stirring to 6~9, is obtained
Mixture；
(3) mixture of step (2) is placed in 40 DEG C of water-bath 1 half h that heats while stirring, is cooled to room temperature,
24h is placed in sealing, that is, obtains the manual dishwashing liquid detergent of the active component containing American cockroach.
Embodiment 2
(1) material preparation of following mass percent is pressed：Surfactant 51%, sterilization component 0.8%, skin care ingredient
3%th, the active component 1% of American cockroach, sodium citrate 0.5%, deionized water surplus, above-mentioned each component sum are 100%；
The surfactant is made up of the component of following masses part：Sodium sulfate of polyethenoxy ether of fatty alcohol 13%, alkane agent
Glucosides 12%, neopelex 10%, the alkylolamides 8% of cocounut oil two, Cocoamidopropyl betaine 8%.
The sterilization component is made up of the component of following masses part：KF88 0.2%, Flos Chrysanthemi Indici extract 0.2%, orange peel carry
Take thing 0.2%, buckeye extract 0.2%.
The skin care ingredient is made up of the component of following masses part：Prevent dry skin composition 1.5%, skin moisturizing ingredients
1.5%.
It is described to prevent dry skin composition from being made up of the component of following masses part：Ginkgo biloba p.e 0.375%, witch hazel
Extract 0.375%, Rosmarinus officinalis extract 0.375%, camellia flower extract 0.375%.
The skin moisturizing ingredients are made up of the component of following masses part：The wooden berry extract 0.375% of breast, Salvia japonica extraction
Thing 0.375%, the extract 0.375% of daffodil bulb, D-sorbite 0.375%.
(2) surfactant of step (1) is heated in 65 DEG C of water-bath, heat while stirring 1 half h, then cools down
To room temperature, sterilization component, skin care ingredient, the active component of American cockroach are added, pH value is adjusted after stirring to 6~9, is obtained
Mixture；
(3) mixture of step (2) is placed in 40 DEG C of water-bath 1 half h that heats while stirring, is cooled to room temperature,
24h is placed in sealing, that is, obtains the manual dishwashing liquid detergent of the active component containing American cockroach.
Embodiment 3
(1) material preparation of following mass percent is pressed：Surfactant 40%, sterilization component 0.11%, skin care ingredient
2%th, the active component 0.01% of American cockroach, sodium citrate 0.5%, deionized water surplus, above-mentioned each component sum are
100%；
The surfactant is made up of the component of following masses part：10 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, alkane agent
Glucosides 10%, neopelex 8%, the alkylolamides 6% of cocounut oil two, Cocoamidopropyl betaine 6%.
The sterilization component is made up of the component of following masses part：Flos Chrysanthemi Indici extract 0.04%, Extract from Orange Peel
0.03%th, buckeye extract 0.04%, KF88 0%.
The skin care ingredient is made up of the component of following masses part：Prevent dry skin composition 1%, skin moisturizing ingredients
1%.
It is described to prevent dry skin composition from being made up of the component of following masses part：Ginkgo biloba p.e 0.25%, witch hazel
Extract 0.25%, Rosmarinus officinalis extract 0.25%, camellia flower extract 0.25%.
The skin moisturizing ingredients are made up of the component of following masses part：The wooden fruit 0.25% of breast, Sage extract
0.25%th, the extract 0.25% of daffodil bulb, D-sorbite 0.25%.
(2) surfactant of step (1) is heated in 65 DEG C of water-bath, heat while stirring 1 half h, then cools down
To room temperature, sterilization component, skin care ingredient, the active component of American cockroach are added, pH value is adjusted after stirring to 6~9, is obtained
Mixture；
(3) mixture of step (2) is placed in 40 DEG C of water-bath 1 half h that heats while stirring, is cooled to room temperature,
24h is placed in sealing, that is, obtains the manual dishwashing liquid detergent of the active component containing American cockroach.
Embodiment 4
(1) material preparation of following mass percent is pressed：Surfactant 51%, sterilization component 0.6%, skin care ingredient
2.625%th, the active component 1% of American cockroach, sodium citrate 0.5%, deionized water surplus, above-mentioned each component sum are
100%；
The surfactant is made up of the component of following masses part：Sodium sulfate of polyethenoxy ether of fatty alcohol 13%, alkane agent
Glucosides 12%, neopelex 10%, the alkylolamides 8% of cocounut oil two, Cocoamidopropyl betaine 8%.
The sterilization component is made up of the component of following masses part：Flos Chrysanthemi Indici extract 0.2%, Extract from Orange Peel 0.2%,
Buckeye extract 0.2%.
The skin care ingredient is made up of the component of following masses part：Prevent dry skin composition 1.125%., skin moisture-keeping
Composition 1.5%.
It is described to prevent dry skin composition from being made up of the component of following masses part：Ginkgo biloba p.e 0.375%, witch hazel
Extract 0.375%, Rosmarinus officinalis extract 0.375%.
The skin moisturizing ingredients are made up of the component of following masses part：The wooden fruit 0.375% of breast, Sage extract
0.375%th, the extract 0.375% of daffodil bulb, D-sorbite 0.375%.
(2) surfactant of step (1) is heated in 65 DEG C of water-bath, heat while stirring 1 half h, then cools down
To room temperature, sterilization component, skin care ingredient, the active component of American cockroach are added, pH value is adjusted after stirring to 6~9, is obtained
Mixture；
(3) mixture of step (2) is placed in 40 DEG C of water-bath 1 half h that heats while stirring, is cooled to room temperature,
24h is placed in sealing, that is, obtains the manual dishwashing liquid detergent of the active component containing American cockroach.
Embodiment 5
(1) material preparation of following mass percent is pressed：Surfactant 51%, sterilization component 0.6%, skin care ingredient
2.25%th, the active component 1% of American cockroach, sodium citrate 0.5%, deionized water surplus, above-mentioned each component sum are
100%；
The surfactant is made up of the component of following masses part：Sodium sulfate of polyethenoxy ether of fatty alcohol 13%, alkane agent
Glucosides 12%, neopelex 10%, the alkylolamides 8% of cocounut oil two, Cocoamidopropyl betaine 8%.
The sterilization component is made up of the component of following masses part：KF88 0.2%, Flos Chrysanthemi Indici extract 0.2%, orange peel carry
Take thing 0.2%.
The skin care ingredient is made up of the component of following masses part：Prevent dry skin composition 0.75%, skin moisture-keeping into
Divide 1.5%.
It is described to prevent dry skin composition from being made up of the component of following masses part：Ginkgo biloba p.e 0.25%, witch hazel
Extract 0.25%, Rosmarinus officinalis extract 0.25%.
The skin moisturizing ingredients are made up of the component of following masses part：The wooden berry extract 0.375% of breast, Salvia japonica extraction
Thing 0.375%, the extract 0.375% of daffodil bulb, D-sorbitol solution 0.375%.
(2) surfactant of step (1) is heated in 65 DEG C of water-bath, heat while stirring 1 half h, then cools down
To room temperature, sterilization component, skin care ingredient, the active component of American cockroach are added, pH value is adjusted after stirring to 6~9, is obtained
Mixture；
(3) mixture of step (2) is placed in 40 DEG C of water-bath 1 half h that heats while stirring, is cooled to room temperature,
24h is placed in sealing, that is, obtains the manual dishwashing liquid detergent of the active component containing American cockroach.
Embodiment 6
(1) material preparation of following mass percent is pressed：Surfactant 51%, sterilization component 0.14%, skin care ingredient
2.25%th, the active component 1% of American cockroach, sodium citrate 0.5%, deionized water surplus, above-mentioned each component sum are
100%；
The surfactant is made up of the component of following masses part：Sodium sulfate of polyethenoxy ether of fatty alcohol 13%, alkane agent
Glucosides 12%, neopelex 10%, the alkylolamides 8% of cocounut oil two, Cocoamidopropyl betaine 8%.
The sterilization component is made up of the component of following masses part：KF88 0.03%, Flos Chrysanthemi Indici extract 0.04%, orange peel
Extract 0.03%, buckeye extract 0.04%.
The skin care ingredient is made up of the component of following masses part：Prevent dry skin composition 0.75%, skin moisture-keeping into
Divide 1.5%.
It is described to prevent dry skin composition from being made up of the component of following masses part：Ginkgo biloba p.e 0.375%, witch hazel
Extract 0.375%.
The skin moisturizing ingredients are made up of the component of following masses part：The wooden fruit 0.375% of breast, Sage extract
0.375%th, the extract 0.375% of daffodil bulb, D-sorbite 0.375%.
(2) surfactant of step (1) is heated in 65 DEG C of water-bath, heat while stirring 1 half h, then cools down
To room temperature, sterilization component, skin care ingredient, the active component of American cockroach are added, pH value is adjusted after stirring to 6~9, is obtained
Mixture；
(3) mixture of step (2) is placed in 40 DEG C of water-bath 1 half h that heats while stirring, is cooled to room temperature,
24h is placed in sealing, that is, obtains the manual dishwashing liquid detergent of the active component containing American cockroach.
Test example
First, sterilization experiment
1st, the preparation of instrument
2nd, the preparation of culture medium, physiological saline
(1) preparation of physiological saline
With physiological saline 8.5g：Distilled water 1000ml ratio is prepared
(2) preparation of culture medium
6.6g nutrient agars, 0.2g lecithin, 200ml distilled water.
6.6g nutrient agars, 0.2g lecithin, 200ml distilled water are weighed in 500ml conical flask, is shaken up, it is then, close
Close and, i.e., culture medium completes.
3rd, sterilize
A, first, by the culture medium prepared, physiological saline, the conical flask for filling sample, it is put into 115-120 DEG C of sterilizer
Middle progress 15min autoclave sterilization, after 15min, carry out heat preservation for standby use.
4th, sample dilutes
Sample is subjected to 10 times of dilutions with the physiological saline prepared.
5th, it is inoculated with
Obtained dilution is inoculated with.
6th, Bacteria Culture
14 culture dishes are put into after cultivating 48h in 37 DEG C of biochemical cultivation case and observed.
It the results are shown in Table 2：
Table 2 sterilizes testing result
As a result show, the bactericidal effect of embodiment 1,2,3,4,5,6 is better than conventional liquid detergent.
2nd, skin irritation test
1st, experimental subjects：20 women of 18-25 year.
2nd, experimental procedure：
2g liquid detergents are weighed from the sample of embodiment 1, allow 20 experiencers to be experienced, experience mode is, by what is weighed
2g liquid detergents dilute 10 times, allow experiencer directly to put his hand into dilution and are washed, after washing 10-20s, with 100ml clear water
Rinse, rinse after 20s, interval 5min is observed the hand of experiencer.Remaining embodiment is experienced successively, experience pair
As constant.The liquid detergent of 3 kinds of different brands purchased in market is compareed.
The index of aridity=hand dries number/overall experience number
Moisten rate=hand and moisten number/overall experience number
It is as follows to experience result：
As a result show, the skin effect of embodiment 1,2,3,4,5,6 is better than conventional liquid detergent.
Claims (10)
1. the manual dishwashing liquid detergent of a kind of active component containing American cockroach, it is characterised in that by the raw material of following mass percent
Composition：Surfactant 40~51%, sterilization component 0.1~0.8%, skin care ingredient 1~3%, the active component 0.01 of American cockroach
~1%, sodium citrate 0.5%, deionized water surplus, above-mentioned each component sum are 100%.
2. the manual dishwashing liquid detergent of the active component according to claim 1 containing American cockroach, it is characterised in that：The table
Face activating agent is made up of the component of following masses part：Sodium sulfate of polyethenoxy ether of fatty alcohol 10-13%, alkane agent glucosides 10~12%,
Neopelex 8~10%, the alkylolamides 6~8% of cocounut oil two, Cocoamidopropyl betaine 6~8%.
3. the manual dishwashing liquid detergent of the active component according to claim 1 containing American cockroach, it is characterised in that：It is described to kill
Bacterium composition is that the three kinds or more in KF88, sodium citrate, Flos Chrysanthemi Indici extract, Extract from Orange Peel, buckeye extract is appointed
The mixture of meaning ratio.
4. the manual dishwashing liquid detergent of the active component according to claim 1 containing American cockroach, it is characterised in that：It is described to kill
Bacterium composition is made up of the component of following masses part：0~0.2 part of KF88,0.04~0.2 part of sodium citrate, Flos Chrysanthemi Indici extract
0.04~0.2 part, 0.04~0.2 part of Extract from Orange Peel, 0.04~0.2 part of buckeye extract.
5. the manual dishwashing liquid detergent of the active component according to claim 1 containing American cockroach, it is characterised in that：The shield
Skin composition is made up of the component of following masses part：Prevent 0.5~1.5 part of dry skin composition, skin moisturizing ingredients 0.5~1.5
Part.
6. the manual dishwashing liquid detergent of the active component according to claim 5 containing American cockroach, it is characterised in that：It is described anti-
Only dry skin composition be ginkgo biloba p.e, hamamelis extract, Rosmarinus officinalis extract, two kinds in camellia flower extract or
The mixture of two or more arbitrary proportions, or described prevent dry skin composition from being made up of the component of following masses part：Ginkgo
0.25~0.375 part of leaf extract, 0.25~0.375 part of hamamelis extract, 0.25~0.375 part of Rosmarinus officinalis extract, mountain
0.25~0.375 part of Flos Camelliae Japonicae extract.
7. the manual dishwashing liquid detergent of the active component according to claim 5 containing American cockroach, it is characterised in that：The skin
Skin moisturizing ingredient is made up of the component of following masses part：Wooden 0.125~0.375 part of the berry extract of breast, Sage extract 0.125
~0.375 part, 0.125~0.375 part of narcissus bulb stem extraction, 0.125~0.375 part of D-sorbite.
8. the manual dishwashing liquid detergent of the active component according to claim 5 containing American cockroach, it is characterised in that：Described U.S.
The big Lian in continent active component is obtained using semi-bionic extraction, specific as follows：
A, 3 kinds of cushioning liquid that pH is 2.0,7.5,8.3 are configured to respectively with citric acid, disodium hydrogen phosphate, it is standby；
B, dry American cockroach polypide is crushed, the mass concentration for adding 6 times of amounts of American cockroach worm silty amount is 95% second
Alcohol, then handled 4 hours at a temperature of 50 DEG C, the filter residue after filtering is put into 50 DEG C of dryings of baking oven；
C, by the amount of 20 ml cushioning liquid/g filter residues, the buffering that pH=2.0 regulated are added in step B drying filter residue is molten
Liquid, 60min is extracted at a temperature of 60 DEG C of setting, filtered, then successively with the cushioning liquid of pH=7.5 and pH=8.3 in identical
Under the conditions of extract filter residue twice, filtering, be concentrated by evaporation after merging each extract solution, when being concentrated to extract solution can also flow, will concentrate
Liquid pours into evaporating dish, is dried in 80 DEG C of baking oven, produces the active component of American cockroach.
9. the preparation method of the manual dishwashing liquid detergent of any active component containing American cockroach of claim 1 to 8, its feature
It is by following each step：
（1）By the material preparation of following mass percent：Surfactant 40~51%, sterilization component 0.1~0.8%, skin care into
Divide 1~3%, active component 0.01~1% of American cockroach, sodium citrate 0.5%, deionized water surplus, above-mentioned each component sum is
100%；
（2）By step（1）Surfactant heated in 60 DEG C of water-bath, heat while stirring 1h, is cooled to room temperature, adds
Enter sterilization component, skin care ingredient, the active component of American cockroach, pH value is adjusted after stirring to 6~8, obtains mixture；
（3）By step（2）Mixture be placed in 40 DEG C of water-bath the 1h that heats while stirring, be cooled to room temperature, sealing is placed
24h, that is, obtain the manual dishwashing liquid detergent of the active component containing American cockroach.
10. preparation method according to claim 9, it is characterised in that：The step（2）PH value be add sodium citrate
The regulation of progress.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710603250.8A CN107523438A (en) | 2017-07-22 | 2017-07-22 | The manual dishwashing liquid detergent and preparation method of a kind of active component containing American cockroach |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710603250.8A CN107523438A (en) | 2017-07-22 | 2017-07-22 | The manual dishwashing liquid detergent and preparation method of a kind of active component containing American cockroach |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107523438A true CN107523438A (en) | 2017-12-29 |
Family
ID=60680264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710603250.8A Pending CN107523438A (en) | 2017-07-22 | 2017-07-22 | The manual dishwashing liquid detergent and preparation method of a kind of active component containing American cockroach |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107523438A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1895217A (en) * | 2006-06-20 | 2007-01-17 | 廖言 | Use of blattaria extracts as additive in fine chemical products and its preparation |
| CN101405057A (en) * | 2006-03-22 | 2009-04-08 | 宝洁公司 | Cosmetic composition comprising seabuckthorn |
| CN102925299A (en) * | 2012-11-21 | 2013-02-13 | 广州市南大实业有限公司 | Green antimicrobial cleanser essence as well as preparation method and application thereof |
| CN103497850A (en) * | 2013-10-14 | 2014-01-08 | 陈均 | Harmless dishwashing liquid |
| CN105434310A (en) * | 2015-12-22 | 2016-03-30 | 广州市娇兰化妆品有限公司 | Application of periplaneta americana active ingredient extract in cosmetic preparation |
| CN105476947A (en) * | 2015-12-28 | 2016-04-13 | 昆明东特农业科技有限公司 | Toothpaste containing periplaneta Americana and preparation method thereof |
| CN106318690A (en) * | 2015-06-19 | 2017-01-11 | 镇江市润州金山包装厂 | Hand-caring dishwashing liquid |
-
2017
- 2017-07-22 CN CN201710603250.8A patent/CN107523438A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101405057A (en) * | 2006-03-22 | 2009-04-08 | 宝洁公司 | Cosmetic composition comprising seabuckthorn |
| CN1895217A (en) * | 2006-06-20 | 2007-01-17 | 廖言 | Use of blattaria extracts as additive in fine chemical products and its preparation |
| CN102925299A (en) * | 2012-11-21 | 2013-02-13 | 广州市南大实业有限公司 | Green antimicrobial cleanser essence as well as preparation method and application thereof |
| CN103497850A (en) * | 2013-10-14 | 2014-01-08 | 陈均 | Harmless dishwashing liquid |
| CN106318690A (en) * | 2015-06-19 | 2017-01-11 | 镇江市润州金山包装厂 | Hand-caring dishwashing liquid |
| CN105434310A (en) * | 2015-12-22 | 2016-03-30 | 广州市娇兰化妆品有限公司 | Application of periplaneta americana active ingredient extract in cosmetic preparation |
| CN105476947A (en) * | 2015-12-28 | 2016-04-13 | 昆明东特农业科技有限公司 | Toothpaste containing periplaneta Americana and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 南京中医药大学编著: "《中药大辞典》", 31 March 2006, 上海科学技术出版社 * |
| 王建新主编: "《化妆品植物原料大全》", 30 June 2012, 北京：中国纺织出版社 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR101427099B1 (en) | Shampoo soap compositions including effective microorganisms fermentation liquid and native grass powder and Manufacturing method thereof | |
| KR101407051B1 (en) | A producing method for natural antimicrobial using chives | |
| CN101735898B (en) | Indigowoad root liquid soap | |
| CN105647710A (en) | Fruit and vegetable washing salt and preparing method | |
| CN104127779B (en) | A kind of Chinese herb compound washing lotion of anti-inflammation and preparation method thereof | |
| CN110327271A (en) | A kind of anti-dandruff and itching-relieving plant composition, preparation method and application | |
| CN107802547A (en) | A kind of rosemary shampoo | |
| CN105754751A (en) | Anti-bacteria and water-saving detergent prepared from pure natural Chinese herbal medicines and plants and preparation method of detergent | |
| CN109568235A (en) | A kind of wet tissue and its manufacturing method with caring function | |
| CN105434275A (en) | Shampoo salt rich in mineral trace elements and preparation method | |
| CN109010178B (en) | Shower gel and production process thereof | |
| CN111110574A (en) | Wet tissue with three-in-one functions of cleaning, sterilizing and moisturizing and preparation method thereof | |
| KR20170130690A (en) | Natural detergent composition and preparation method thereof | |
| CN106619273A (en) | Sweet-scented osmanthus oil-removing liquid soap | |
| KR101174046B1 (en) | Oriental herbal bathing material and manufacturing method thereof | |
| CN106038378A (en) | Compressed dry towel for mothers and babies and preparation method of compressed dry towel | |
| KR101606381B1 (en) | Manufacture method of complex beauty Salt using solar salt processing environmentally friendly | |
| CN103284896B (en) | Chimonanthus salicifolius sterilization hand washing solution and its preparation method | |
| CN105726415A (en) | Bacteriostasis wet tissue containing pure natural traditional Chinese herbal medicine ingredients and preparing method thereof | |
| CN107312659A (en) | A kind of infants' wear soap by hand | |
| CN105708763A (en) | Artemisia argyi Levl extract-containing floral water and preparation method thereof | |
| CN106087385A (en) | A kind of Multifunctional woolen sweater finishing agent containing sea mud | |
| KR102397833B1 (en) | Manufacturing method of functional foaming detergent using jeju green tangerine and functional foaming detergent manufactured by the same | |
| CN110870885B (en) | A medicinal liquid with cleaning, sterilizing and moisturizing effects, and its application | |
| CN107523438A (en) | The manual dishwashing liquid detergent and preparation method of a kind of active component containing American cockroach |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20180711 Address after: 650000 Yunnan Kunming Guandu District Ding Jie Xing Du business center 1 building 27 level 2704. Applicant after: Yunnan Ningkang Biological Technology Co., Ltd. Address before: 518000 C, block 2702-17, Tianli Central Commercial Plaza, Houhai Avenue East Road, Shenzhen, Guangdong, China 2702-17 Applicant before: Shenzhen noo Biological Technology Co., Ltd. |
|
| TA01 | Transfer of patent application right | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171229 |
|
| RJ01 | Rejection of invention patent application after publication |