CN107502184A - One kind building waterproof paint specially and preparation method thereof - Google Patents
One kind building waterproof paint specially and preparation method thereof Download PDFInfo
- Publication number
- CN107502184A CN107502184A CN201710893203.1A CN201710893203A CN107502184A CN 107502184 A CN107502184 A CN 107502184A CN 201710893203 A CN201710893203 A CN 201710893203A CN 107502184 A CN107502184 A CN 107502184A
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- parts
- mixture
- preparation
- waterproof paint
- methylisothiazolinone
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D187/00—Coating compositions based on unspecified macromolecular compounds, obtained otherwise than by polymerisation reactions only involving unsaturated carbon-to-carbon bonds
- C09D187/005—Block or graft polymers not provided for in groups C09D101/00 - C09D185/04
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G81/00—Macromolecular compounds obtained by interreacting polymers in the absence of monomers, e.g. block polymers
- C08G81/02—Macromolecular compounds obtained by interreacting polymers in the absence of monomers, e.g. block polymers at least one of the polymers being obtained by reactions involving only carbon-to-carbon unsaturated bonds
- C08G81/024—Block or graft polymers containing sequences of polymers of C08C or C08F and of polymers of C08G
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Plant Pathology (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention relates to one kind building waterproof paint specially and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：30 45 parts of polyacrylic resin, 49 parts of ethyl cellulose, 36 parts of methylisothiazolinone, 36 parts of titanium dioxide, 24 parts of white carbon, 38 parts of calcium carbonate, 6 10 parts of isobutyl triethoxy silane, 3 10 parts of phenolic resin, 3 10 parts of vinyl front three oxosilane, 59 parts of acrylic coating, 25 parts of CSM, 30 50 parts of deionized water, 5 10 parts of helium.Material of the present invention is easy to get, and cost is low, and environment-friendly and green, water resistance is excellent, has good waterproof, seepage control, and antimicrobial form is strong, and antiageing effect is good, increases the service life, and dispersion effect is good, and uniformity is strong, and construction is convenient.
Description
Technical field
The present invention relates to paint field, and in particular to one kind building waterproof paint specially and preparation method thereof.
Background technology
Leakage of buildings is with waterproof always in a great problem of building, current market sales of water-repellent paint engineering cost
It is high with height, complex process, cost, and have certain harm to environment, however, existing water-repellent paint can not be long-term effectively
Rainwater-proof, antiscour, therefore, it is frequently seen decoration and brushes neat and artistic building and cannot stand wind and rain and wash away and moisture etch
And color is mottled, mainly lack stable chemical performance, inorganic substances not soluble in water in these coating.
The content of the invention
A kind of building waterproof paint specially and its preparation side are provided the invention aims to overcome the shortcomings of the above
Method.
Technical scheme includes：One kind building waterproof paint specially and preparation method thereof, raw material constituent is pressed
Parts by weight are made up of following ratio：Polyacrylic resin 30-45 parts, ethyl cellulose 4-9 parts, methylisothiazolinone 3-6
Part, titanium dioxide 3-6 parts, white carbon 2-4 parts, calcium carbonate 3-8 parts, isobutyl triethoxy silane 6-10 parts, phenolic resin 3-10
Part, vinyl front three oxosilane 3-10 parts, acrylic coating 5-9 parts, CSM 2-5 parts, deionized water 30-50
Part, helium 5-10 parts.
Further improvement of the present invention is：Its preparation method is as follows：
A, polyacrylic resin and phenolic resin are subjected to high temperature polycondensation, temperature is set to 100-140 DEG C, obtains mixture A；
B, ethyl cellulose, methylisothiazolinone and isobutyl triethoxy silane are added in deionized water and mixed,
Stir speed (S.S.) is 400-600r/min, adds mixture A after 5-10min and titanium dioxide, white carbon obtain mixture B；
C, CSM will be added in acrylic coating to be stirred, stir speed (S.S.) 800-860r/min, add
Mixture B is mixed, and obtains mixture C；
D, mixture C is cooled down, fixed line, at 120-140 DEG C by it is calcium carbonate-filled enter wherein, using helium as carrier, flow
For 5-10L/min, product is obtained after cooling down room temperature.
Beneficial effects of the present invention：
Material of the present invention is easy to get, and cost is low, and environment-friendly and green, water resistance is excellent, has good waterproof, seepage control, antimicrobial form
By force, antiageing effect is good, increases the service life, and dispersion effect is good, and uniformity is strong, and construction is convenient.
Embodiment：
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and the embodiment is only used
In explaining the present invention, it is not intended to limit the scope of the present invention..
Embodiment 1
One kind building waterproof paint specially and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：It is poly-
40 parts of acrylic resin, 5 parts of ethyl cellulose, 5 parts of methylisothiazolinone, 4 parts of titanium dioxide, 3 parts of white carbon, 6 parts of calcium carbonate,
10 parts of isobutyl triethoxy silane, 4 parts of phenolic resin, 8 parts of vinyl front three oxosilane, 7 parts of acrylic coating, chlorosulfonation are gathered
4 parts of ethylene rubber, 45 parts of deionized water, 8 parts of helium.
Its preparation method is as follows：
A, polyacrylic resin and phenolic resin are subjected to high temperature polycondensation, temperature is set to 120 DEG C, obtains mixture A；
B, ethyl cellulose, methylisothiazolinone and isobutyl triethoxy silane are added in deionized water and mixed,
Stir speed (S.S.) is 500r/min, adds mixture A after 8min and titanium dioxide, white carbon obtain mixture B；
C, CSM will be added in acrylic coating to be stirred, stir speed (S.S.) 820r/min, add mixing
Thing B is mixed, and obtains mixture C；
D, mixture C is cooled down, fixed line, at 130 DEG C by it is calcium carbonate-filled enter wherein, using helium as carrier, flow 8L/
Min, product is obtained after cooling down room temperature.
Embodiment 2
One kind building waterproof paint specially and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：It is poly-
30 parts of acrylic resin, 9 parts of ethyl cellulose, 3 parts of methylisothiazolinone, 3 parts of titanium dioxide, 4 parts of white carbon, calcium carbonate 3
Part, 10 parts of isobutyl triethoxy silane, 3 parts of phenolic resin, 10 parts of vinyl front three oxosilane, 9 parts of acrylic coating, chlorine sulphur
Change 2 parts of polyethylene rubber, 50 parts of deionized water, 5 parts of helium.
Its preparation method is as follows：
A, polyacrylic resin and phenolic resin are subjected to high temperature polycondensation, temperature is set to 140 DEG C, obtains mixture A；
B, ethyl cellulose, methylisothiazolinone and isobutyl triethoxy silane are added in deionized water and mixed,
Stir speed (S.S.) is 400r/min, adds mixture A after 5min and titanium dioxide, white carbon obtain mixture B；
C, CSM will be added in acrylic coating to be stirred, stir speed (S.S.) 820r/min, add mixing
Thing B is mixed, and obtains mixture C；
D, mixture C is cooled down, fixed line, at 130 DEG C by it is calcium carbonate-filled enter wherein, using helium as carrier, flow 9L/
Min, product is obtained after cooling down room temperature.
Embodiment 3
One kind building waterproof paint specially and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：It is poly-
45 parts of acrylic resin, 9 parts of ethyl cellulose, 6 parts of methylisothiazolinone, 3 parts of titanium dioxide, 2 parts of white carbon, 3 parts of calcium carbonate,
6 parts of isobutyl triethoxy silane, 10 parts of phenolic resin, 10 parts of vinyl front three oxosilane, 9 parts of acrylic coating, chlorosulfonation
2 parts of polyethylene rubber, 50 parts of deionized water, 10 parts of helium.
Its preparation method is as follows：
A, polyacrylic resin and phenolic resin are subjected to high temperature polycondensation, temperature is set to 100 DEG C, obtains mixture A；
B, ethyl cellulose, methylisothiazolinone and isobutyl triethoxy silane are added in deionized water and mixed,
Stir speed (S.S.) is 600r/min, adds mixture A after 10min and titanium dioxide, white carbon obtain mixture B；
C, CSM will be added in acrylic coating to be stirred, stir speed (S.S.) 860r/min, add mixing
Thing B is mixed, and obtains mixture C；
D, mixture C is cooled down, fixed line, at 120-140 DEG C by it is calcium carbonate-filled enter wherein, using helium as carrier, flow
For 5L/min, product is obtained after cooling down room temperature.
Embodiment 4
One kind building waterproof paint specially and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：It is poly-
35 parts of acrylic resin, 8 parts of ethyl cellulose, 4 parts of methylisothiazolinone, 5 parts of titanium dioxide, 3 parts of white carbon, 7 parts of calcium carbonate,
7 parts of isobutyl triethoxy silane, 8 parts of phenolic resin, 9 parts of vinyl front three oxosilane, 6 parts of acrylic coating, chlorosulfonation are gathered
3 parts of ethylene rubber, 40 parts of deionized water, 6 parts of helium.
Its preparation method is as follows：
A, polyacrylic resin and phenolic resin are subjected to high temperature polycondensation, temperature is set to 120 DEG C, obtains mixture A；
B, ethyl cellulose, methylisothiazolinone and isobutyl triethoxy silane are added in deionized water and mixed,
Stir speed (S.S.) is 450r/min, adds mixture A after 8min and titanium dioxide, white carbon obtain mixture B；
C, CSM will be added in acrylic coating to be stirred, stir speed (S.S.) 840r/min, add mixing
Thing B is mixed, and obtains mixture C；
D, mixture C is cooled down, fixed line, at 130 DEG C by it is calcium carbonate-filled enter wherein, using helium as carrier, flow 6L/
Min, product is obtained after cooling down room temperature.
In above example, embodiment 1 is most preferred embodiment, and water resistance is good, and antiageing effect is strong；In above-mentioned steps D
Fill calcium carbonate discharges CO2 at high temperature, effectively fill internal structure, improve density.
Explanation embodiments of the present invention are the foregoing is only, are not intended to limit the invention, for the technology of this area
For personnel, within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., it should be included in
Within protection scope of the present invention.
Claims (2)
1. one kind building waterproof paint specially and preparation method thereof, it is characterised in that：Raw material constituent in parts by weight by with
Lower ratio composition：Polyacrylic resin 30-45 parts, ethyl cellulose 4-9 parts, methylisothiazolinone 3-6 parts, titanium dioxide 3-6
Part, white carbon 2-4 parts, calcium carbonate 3-8 parts, isobutyl triethoxy silane 6-10 parts, phenolic resin 3-10 parts, vinyl front three
Oxosilane 3-10 parts, acrylic coating 5-9 parts, CSM 2-5 parts, deionized water 30-50 parts, helium 5-10
Part.
A kind of 2. building waterproof paint specially according to claim 1 and preparation method thereof, it is characterised in that：Its preparation side
Method is as follows：
A, polyacrylic resin and phenolic resin are subjected to high temperature polycondensation, temperature is set to 100-140 DEG C, obtains mixture A；
B, ethyl cellulose, methylisothiazolinone and isobutyl triethoxy silane are added in deionized water and mixed,
Stir speed (S.S.) is 400-600r/min, adds mixture A after 5-10min and titanium dioxide, white carbon obtain mixture B；
C, CSM will be added in acrylic coating to be stirred, stir speed (S.S.) 800-860r/min, add
Mixture B is mixed, and obtains mixture C；
D, mixture C is cooled down, fixed line, at 120-140 DEG C by it is calcium carbonate-filled enter wherein, using helium as carrier, flow
For 5-10L/min, product is obtained after cooling down room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710893203.1A CN107502184A (en) | 2017-09-28 | 2017-09-28 | One kind building waterproof paint specially and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710893203.1A CN107502184A (en) | 2017-09-28 | 2017-09-28 | One kind building waterproof paint specially and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107502184A true CN107502184A (en) | 2017-12-22 |
Family
ID=60699416
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710893203.1A Withdrawn CN107502184A (en) | 2017-09-28 | 2017-09-28 | One kind building waterproof paint specially and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN107502184A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105936782A (en) * | 2016-05-27 | 2016-09-14 | 广西梧州龙鱼漆业有限公司 | Waterproof coating |
| CN106243967A (en) * | 2016-09-07 | 2016-12-21 | 马鞍山纽泽科技服务有限公司 | A kind of Environmental-protecwaterproof waterproof paint |
| CN107033769A (en) * | 2017-06-06 | 2017-08-11 | 合肥月煌新型装饰材料有限公司 | A kind of solvent-free polyurethane waterproof coating material and preparation method thereof |
| CN107189610A (en) * | 2016-01-16 | 2017-09-22 | 天津城建大学 | The preparation method of raw-soil thermal insulation waterproof coating |
-
2017
- 2017-09-28 CN CN201710893203.1A patent/CN107502184A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107189610A (en) * | 2016-01-16 | 2017-09-22 | 天津城建大学 | The preparation method of raw-soil thermal insulation waterproof coating |
| CN105936782A (en) * | 2016-05-27 | 2016-09-14 | 广西梧州龙鱼漆业有限公司 | Waterproof coating |
| CN106243967A (en) * | 2016-09-07 | 2016-12-21 | 马鞍山纽泽科技服务有限公司 | A kind of Environmental-protecwaterproof waterproof paint |
| CN107033769A (en) * | 2017-06-06 | 2017-08-11 | 合肥月煌新型装饰材料有限公司 | A kind of solvent-free polyurethane waterproof coating material and preparation method thereof |
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Application publication date: 20171222 |