CN107496240A - One kind cleans disposable spraying - Google Patents
One kind cleans disposable spraying Download PDFInfo
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- CN107496240A CN107496240A CN201710816217.3A CN201710816217A CN107496240A CN 107496240 A CN107496240 A CN 107496240A CN 201710816217 A CN201710816217 A CN 201710816217A CN 107496240 A CN107496240 A CN 107496240A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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Abstract
The invention discloses one kind to clean disposable spraying, including the composition such as fruit of glossy privet terpene, Herba Schizonepetae volatile oil, odoriflavone, caprylic/capric triglyceride, ring five dimethyl silicone polymer, VARISOFT TA100, quaternary ammonium salt 18, glycerine, cornstarch.Outside spraying is with cleaning hair function routinely, also has the function that repairing hair is damaged, and by the removing free radical of composition, strengthens the effect of activities of antioxidant enzymes, effectively antagonize the problems such as environmental damage causes withered and yellowish hairs, bifurcated, disconnected hair；And Herba Schizonepetae volatile oil can suppress growth of microorganism, there is the broad-spectrum antibiotic effect including virus with reference to fruit of glossy privet terpene, i.e., further bactericidal bacteriostasis, can solve the greasy problem caused by microorganism crosses breeding；The present invention arranges in pairs or groups containing cornstarch and other base-materials, can adsorb the grease of hair surface, and allow between hair, so that hair is more fluffy, can facilitate moulding with crosslinking support.
Description
Technical field
The present invention relates to daily necessities field, and in particular to one kind cleans disposable spraying.
Background technology
With the development of society and the improvement of people's living standards, people's liquid increasingly pay close attention to oneself and quality of the life and
External image.Except skin, also pay attention to the hair of oneself.In fact, it is also health for an enviable healthy hair
Mark.However, for various reasons, there are problems in hair, severe patient's alopecia and bald, and withered and yellowish hairs bifurcated, water shortage is done
Dry crude, fragility is easily broken to lack flexibility, and entanglement is not easy to comb, intensely dark etc..Or scalp layer microorganism is excessive, dandruff takes off
Fall, the other pollutants being infected with dust or environment, if cleaning not in time, can not only deepen the infringement of scalp layer skin, cause
It inflammation etc., can also have a strong impact on that people's is attractive in appearance, give people not focus on the bad impression of health, so, a convenience is researched and developed, is had
The disposable spraying of cleaning of effect is significantly.
The domestic and international hair products of market or report are seen largely containing excessive organic solvent, water-insoluble oil
Fat, artificial essence etc. has a composition of certain side effect, or product is excessively greasy, very uncomfortable using skin sense；More also
Product processing is complicated, and very not environmentally, has run counter to " natural, green " this objective.
The content of the invention
Based on this, it is an object of the invention to provide one kind to clean disposable spraying, and energy long-acting bacteriostatic sterilization, nourishes hair.
In order to achieve the above object, the present invention provides following technical scheme：
A kind of disposable spray of cleaning includes the component of following mass percent：Odoriflavone 0.5-2.0%, Herba Schizonepetae volatile oil
2.0-5.0%, fruit of glossy privet terpene 0.5-3.0%.
Preferably, odoriflavone 0.8-1.5%, Herba Schizonepetae volatile oil 2.5-4.0%%, fruit of glossy privet terpene 0.8-2.5%.
Optimally, odoriflavone 1.2%, Herba Schizonepetae volatile oil 3.5%, fruit of glossy privet terpene 1.8%.
The preparation method of described odoriflavone includes：Fresh dalbergia wood is gathered, is cleaned, drying, shreds piece pulverizer powder
It is broken to obtain dalbergia wood powder；According to 1：The ratio of (12-15) adds dalbergia wood powder in 30-60 DEG C of petroleum ether, using supersound process 25-
35min, taking-up are let cool, and filtering, discard petroleum ether；After the dregs of a decoction volatilize petroleum ether, 75- in 70-70% ethanol solutions is added
Extract, filter, merging filtrate under ultrasonic wave added under 85W, 48-53kHz；The dregs of a decoction are washed 2-3 times with 70-70% ethanol, and filtrate is closed
And；With 70-70% ethanol constant volume filtrates, odoriflavone is obtained.
The preparation method of described Herba Schizonepetae volatile oil includes：Fresh schizonepeta is cleaned, dried, shreds piece pulverizer into chaste tree
Mustard powder；Above-mentioned gained schizonepeta powder is soaked 10~30 minutes with 60~80% ethanol of 1-5 times of parts by weight, extraction uses 36~43
The mode of DEG C constant temperature extracting, extracting pressure 27~30MPa, CO23.5~4kg/h of flow velocity, 4~6MPa of separating pressure, extraction time
1.5~2h；Separating-purifying, obtain Herba Schizonepetae volatile oil.
The preparation method of described fruit of glossy privet terpene includes：Fresh glossy privet is gathered, is cleaned, drying is put into ceramic pan, according to
Solid-liquid ratio 1：(10-15) adds yellow rice wine, stirs evenly, covers pot cover, vexed profit 3-3.5h；Keep ceramic pan closed, be put into stainless steel steaming
Pot, 21-24h is steamed, obtains the wine fruit of glossy privet；By the above-mentioned obtained wine thereby fruit of glossy privet, dry, crush, cross 70-80 mesh sieves, obtain wine female
Loyal sub- powder；It is 1 according to solid-liquid ratio by above-mentioned obtained wine thereby fruit of glossy privet powder:25 add 85-90% ethanol solutions, and stirring is equal
It is even；The ultrasonic extraction under 250-300W power, obtain wine fruit of glossy privet granulated slag；Above-mentioned obtained wine thereby fruit of glossy privet granulated slag is depressurized
Filtering, filtrate is freeze-dried, obtains fruit of glossy privet terpene.And the condition of ultrasonic extraction is in the preparation method of loyal sub- terpene：When ultrasound is total
Between 25-35min, each ultrasonic extraction time 3s, intermittent time 2s.
Described spray also includes the component of following mass percent：Methoxyl group PEG/PPG-25/4 dimethyl silicone polymers；
Double-PEG/PPG-20/5PEG/PPG-20/5 dimethyl silicone polymers；Caprylic/capric triglyceride 0.5-1.0%, ring five poly- two
Methylsiloxane 2.0-3.0%, VARISOFT TA100 0.5-1.0%, quaternary ammonium salt -180.5-1.0%, glycerine 3.0-
5.0%th, cornstarch 0.1-0.3%, deionized water 20-30%, denatured ethyl alcohol surplus.
The present invention also provides a kind of preparation method for cleaning disposable spraying, comprises the following steps：
(1) by VARISOFT TA100, quaternary ammonium salt -18, the poly- diformazans of double-PEG/PPG-20/5PEG/PPG-20/5
Radical siloxane；Methoxyl group PEG/PPG-25/4 dimethyl silicone polymers：Caprylic/capric triglyceride 0.5-1.0%, ring five poly- two
Methylsiloxane mixing is uniformly dispersed, and A phases are made；
(2) glycerine, cornstarch, deionized water are mixed and be uniformly dispersed, B phases are made；
(3) A is added to B phases, emulsifying 2-3min under 3000-3500r/min speed, C phases is made；
(4) odoriflavone, Herba Schizonepetae volatile oil, fruit of glossy privet terpene, denatured ethyl alcohol are mixed and be uniformly dispersed, D phases are made；
(5) D is added to C phases, stirred under 1000-1500r/min speed, discharged.
Described fruit of glossy privet terpene can promote the lipid material in blood vessel to cut down, and prevent capilary from being blocked by lipid material, make
Capillary blood circulation is happier, is advantageous to the nutrient absorption of scalp and root of hair.In addition, fruit of glossy privet terpene can remove free radical,
Strengthen the defence that cell is attacked free radical simultaneously, have epochmaking effect to anti-aging, its principle is enhancing antioxidase
Activity, and then the content of lipid peroxidation material is reduced, the effect of anti-oxidative damage is finally reached, its form of expression is anti-ageing
Always.Fruit of glossy privet terpene is broad-spectrum antibiotic, there is obvious suppression growth including virus to various microorganisms.
Described Herba Schizonepetae volatile oil contains obvious antioxidation activity, can effectively remove a variety of free radicals；Can be effective
Suppress nervous centralis, produce the effect of sedation and analgesia, there can be certain mitigation to itching of the scalp.In addition, Herba Schizonepetae volatile oil
Act on, can fully suppress growth of microorganism with very strong Antimicrobial.Most of all, containing highly concentrated in Herba Schizonepetae volatile oil
The nepetalactone of degree, there is very strong arthropod avoidance effect, all kinds of insects can be reduced and approached, reach insect-expelling function.
Described odoriflavone can reduce blood viscosity, while vasodilator, alleviate the situation of blood vessel blockage, effectively enhancing
Blood plasma transports the ability of oxygen and other kinds nutriment, strengthens scalp cells and root of hair absorbs the efficiency of nutriment.Drop
Fragrant flavones has powerful oxidation resistance, chelant various metals ion while directly removing a variety of free radicals, and suppresses
The reaction of metal ion inducing cell inner lipid peroxidating.
Compared with prior art, it is the device have the advantages that as follows：(1) spraying of the invention contain fruit of glossy privet terpene,
Herba Schizonepetae volatile oil and odoriflavone active component, capillary microcirculation is can effectively improve, promote ingredient draws, reach reinforcing hair
Root, reduce the effect of alopecia；(2) disposable spraying of the invention has outside cleaning hair function routinely, also has and repairs
The impaired effect of hair, free radical is removed by composition, strengthens the effect of activities of antioxidant enzymes, effectively antagonizing environmental damage causes
The problems such as withered and yellowish hairs, bifurcated, disconnected hair；(3) Herba Schizonepetae volatile oil can suppress growth of microorganism, and have with reference to fruit of glossy privet terpene including virus
Broad-spectrum antibiotic effect inside, i.e., further bactericidal bacteriostasis, it is excessive to solve the grease caused by microorganism crosses breeding
The problem of；(4) present invention arranges in pairs or groups containing cornstarch and other base-materials, can adsorb the grease of hair surface, and allowing between hair can
With crosslinking support, so that hair is more fluffy, facilitate moulding.
Embodiment
Below in conjunction with specific embodiment, the present invention is further elaborated.
The following component title occurred in text is INCI (International Nomenclature Cosmetic
Ingredient, i.e. international cosmetic raw material name institute to defined title, including:Methoxyl group PEG/PPG-25/4 poly- two
Methylsiloxane；Double-PEG/PPG-20/5PEG/PPG-20/5 dimethyl silicone polymers；Caprylic/capric triglyceride.The first
Epoxide PEG/PPG-25/4 dimethyl silicone polymers；Double-PEG/PPG-20/5PEG/PPG-20/5 dimethyl silicone polymers；It is pungent
Acid/Triglyceride DDD is a kind of mixture.
1-5 of the embodiment of the present invention present invention cleans disposable spray formula and is shown in Table 1
Table 1
The preparation method of above-mentioned odoriflavone is as follows：
Fresh dalbergia wood is gathered, is cleaned, drying, chopping piece crushes to obtain dalbergia wood powder with pulverizer；According to 1：15 ratio will drop
Face powder is added in 50 DEG C of petroleum ethers, and using 30min is ultrasonically treated, taking-up is let cool, and is filtered, is discarded petroleum ether；Treat that the dregs of a decoction volatilize stone
After oily ether, extract, filter, merging filtrate under ultrasonic wave added under 80W in 70% ethanol solution of addition, 50kHz；70% second of the dregs of a decoction
Alcohol washs 3 times, and filtrate merges；With 70% ethanol constant volume filtrate, odoriflavone is obtained.
The preparation method of above-mentioned Herba Schizonepetae volatile oil is as follows：
Fresh schizonepeta is cleaned, dried, shreds piece pulverizer into schizonepeta powder；By above-mentioned gained schizonepeta powder with 3 times of weight
70% ethanol of part soaks 30 minutes, extracts by the way of 40 DEG C of constant temperature extractings, extracting pressure 30MPa, CO2Flow velocity 4kg/h,
Separating pressure 5MPa, extraction time 2h；Separating-purifying, obtain Herba Schizonepetae volatile oil.
The preparation method of above-mentioned fruit of glossy privet terpene is as follows：
Fresh glossy privet is gathered, is cleaned, drying is put into ceramic pan, according to solid-liquid ratio 1：15 add yellow rice wine, stir evenly, cover pot
Lid, vexed profit 3h；Keep ceramic pan closed, be put into stainless steel steamer, steam 23h, obtain the wine fruit of glossy privet；By above-mentioned obtained wine thereby glossy privet
Son, dry, crush, cross 80 mesh sieves, obtain wine fruit of glossy privet powder；By above-mentioned obtained wine thereby fruit of glossy privet powder, it is according to solid-liquid ratio
1:25 add 90% ethanol solution, stir；The ultrasonic extraction under 300W power, obtain wine fruit of glossy privet granulated slag；To above-mentioned institute
Obtain wine fruit of glossy privet granulated slag to be filtered under diminished pressure, filtrate is freeze-dried, obtains fruit of glossy privet terpene.And surpass in the preparation method of loyal sub- terpene
Sound extraction condition be：Total sonication time 30min, each ultrasonic extraction time 3s, intermittent time 2s.
A kind of preparation methods of the disposable spraying of cleaning of embodiment 1-5 are as follows：
(6) by VARISOFT TA100, quaternary ammonium salt -18, the poly- diformazans of double-PEG/PPG-20/5PEG/PPG-20/5
Radical siloxane；Methoxyl group PEG/PPG-25/4 dimethyl silicone polymers；Caprylic/capric triglyceride, the polydimethylsiloxanes of ring five
Alkane mixing is uniformly dispersed, and A phases are made；
(7) glycerine, cornstarch, deionized water are mixed and be uniformly dispersed, B phases are made；
(8) A is added to B phases, emulsifying 3min under 3000r/min speed, C phases is made；
(9) odoriflavone, Herba Schizonepetae volatile oil, fruit of glossy privet terpene, denatured ethyl alcohol are mixed and be uniformly dispersed, D phases are made；
(10) D is added to C phases, stirred under 1500r/min speed, discharged.
Comparative example 1
Difference with embodiment 1 is not add odoriflavone, and other preparation conditions and method are same as Example 1.
Comparative example 2
Difference with embodiment 1 is not add Herba Schizonepetae volatile oil, and other preparation conditions and method are same as Example 1.
Comparative example 3
Difference with embodiment 1 is not add fruit of glossy privet terpene, and other preparation conditions and method are same as Example 1.
Comparative example 4
Difference with embodiment 1 is not add odoriflavone, Herba Schizonepetae volatile oil, fruit of glossy privet terpene, other preparation conditions and side
Method is same as Example 1.
Bacteriostatic test
Using Candida albicans, staphylococcus aureus as test strain, 0.03mol/L phosphate buffers are as cloudy
Property control group, for embodiment 1-5 as test group, comparative example 1-3 carries out antibacterial effect as a control group, according to QB/T 2738-2012
Fruit is tested, as a result as shown in table 2：
Table 2
It can be seen that from the data of table 2, product bacteriostasis rate made from embodiment 1-5 shows dalbergia wood Huang apparently higher than comparative example 1-3
Three kinds of ketone, Herba Schizonepetae volatile oil, fruit of glossy privet terpene composition Synergistic fungistatic effects, Herba Schizonepetae volatile oil can suppress growth of microorganism, knot
Conjunction fruit of glossy privet terpene has the broad-spectrum antibiotic effect including virus, further bactericidal, can solve because microorganism is excessively numerous
Greasy problem caused by growing, reduces the damage to hair.
Anticreep hair care efficacy validation
Product prepared by embodiment 1-5 and comparative example 1-4 carries out Detection results on probation, while commercially available declares to have with a
It is control group to have the take care of hair spraying of effect of anticreep.
Test object：Each experimental group is volunteer's (25-50 year) of 30 easy alopecias of withered and yellowish hairs.All volunteers make
With the product of place group, try out one month by a definite date, result on trial of the 30th day statistics.
Embodiment 1-5, comparative example 1-4 are being used, trier does not occur adverse reaction, corresponding embodiment 1-5 examination
User, reaction effect is fine, and product is gently non-stimulated to scalp, and all triers complete experiment.
Experimental result is shown in Table 3
Table 3
Comparative example 1-4 and control group are far above by the obvious number of the visible embodiment 1-5 anticreep hair care effects of table 3, it is seen that this
Invention spray effect is notable；Comparative example 1-3 and the difference of embodiment 1 are to be not added with odoriflavone, Herba Schizonepetae volatile oil and female respectively
Loyal sub- terpene, contrasts the obvious number of its comparative example 1-4 anticreep hair care effects by comparative example 1-4 and embodiment and is less than embodiment 1, it is seen that
In present invention spraying, odoriflavone, Herba Schizonepetae volatile oil and fruit of glossy privet terpene Synergistic, withered and yellowish hairs bifurcated, alopecia are effectively antagonized
The problems such as.
Anti-oxidant measure
Compound concentration is 1 × 10-4Mol/L DPPH ethanol solutions.It will be made in embodiment 1-5 and comparative example 1-4
Product, with 80% ethanol be configured to concentration be respectively 0.01,0.04,0.08,0.10,0.12,0.16,0.20,0.24,
0.26 testing sample solution.5mL sample solutions and DPPH solution are taken respectively, and are well mixed, avoid light place 30min, with
80% ethanol is returned to zero, and absorbance A i is determined at 517BITI；Same method, 5mL80% alcohol solvents and sample solution are taken respectively
It is mutually mixed uniformly, absorbance A j is determined after avoid light place 30min；5mL80% alcohol solvents add 5mLDPPH solution to mix,
Avoid light place 30min, measure absorbance A c.Finally free radical scavenging activity is calculated according to below equation：IP%=[1 one (Ai-
Aj)/Ac] × 100, Ai is sample and the absorption values after DPPH effects in formula；Aj is tribute of the sample itself to absorbance
Offer；Ac is DPPH itself absorption.
The ability measurement result that DPPH is removed in spraying to embodiment 1-5 and comparative example 1-4 see the table below 4：
As shown in Table 4, it is removed DPPH ability and increased with the increase of each extraction moiety concentrations.Data above shows
The obtained spraying antioxidation activities of embodiment 1-5 are apparently higher than comparative example 1-4, it is seen that in present invention spraying, odoriflavone, schizonepeta
Volatile oil and fruit of glossy privet terpene Synergistic, effectively remove free radical, strengthen the effect of activities of antioxidant enzymes.
Above example only illustrates embodiment of the present invention, does not have any formal limitation to the present invention；Appoint
What is engaged in professional and technical personnel, all has the ability to make some changes or modification using the technology contents disclosed, turns into equivalent
The equivalent embodiment of change, according to the technology of the present invention essence, simple modification, equivalent change and modification is carried out to the present invention, belonged to
In the range of technical solution of the present invention.
Claims (9)
1. one kind cleans disposable spraying, it is characterised in that includes the component of following mass percent：Odoriflavone 0.5-2.0%,
Herba Schizonepetae volatile oil 2.0-5.0%, fruit of glossy privet terpene 0.5-3.0%.
2. a kind of disposable spraying of cleaning according to claim 1, it is characterised in that including following components：Odoriflavone
0.8-1.5%, Herba Schizonepetae volatile oil 2.5-4.0%%, fruit of glossy privet terpene 0.8-2.5%.
3. a kind of disposable spraying of cleaning according to claim 2, it is characterised in that including following components：Odoriflavone
1.2%th, Herba Schizonepetae volatile oil 3.5%, fruit of glossy privet terpene 1.8%.
4. one kind according to claim any one of 1-3 cleans disposable spraying, it is characterised in that described odoriflavone
Preparation method includes：Fresh dalbergia wood is gathered, is cleaned, drying, chopping piece crushes to obtain dalbergia wood powder with pulverizer；According to 1：(12-15)
Ratio dalbergia wood powder is added in 30-60 DEG C of petroleum ether, using 25-35min is ultrasonically treated, taking-up lets cool, and filters, discards oil
Ether；After the dregs of a decoction volatilize petroleum ether, extracted under 75-85W in addition 70-70% ethanol solutions, 48-53kHz under ultrasonic wave added, mistake
Filter, merging filtrate；The dregs of a decoction are washed 2-3 times with 70-70% ethanol, and filtrate merges；With 70-70% ethanol constant volume filtrates, dalbergia wood is obtained
Flavones.
5. one kind according to claim any one of 1-3 cleans disposable spraying, it is characterised in that described Herba Schizonepetae volatile oil
Preparation method include：Fresh schizonepeta is cleaned, dried, shreds piece pulverizer into schizonepeta powder；Above-mentioned gained schizonepeta powder is used
60~80% ethanol of 1-5 times of parts by weight soak 10~30 minutes, extract by the way of 36~43 DEG C of constant temperature extractings, extraction pressure
Power 27~30MPa, CO23.5~4kg/h of flow velocity, 4~6MPa of separating pressure, 1.5~2h of extraction time；Separating-purifying, obtain schizonepeta
Volatile oil.
6. one kind according to claim any one of 1-3 cleans disposable spraying, it is characterised in that described fruit of glossy privet terpene
Preparation method includes：Fresh glossy privet is gathered, is cleaned, drying is put into ceramic pan, according to solid-liquid ratio 1：(10-15) adds yellow rice wine,
Stir evenly, cover pot cover, vexed profit 3-3.5h；Keep ceramic pan closed, be put into stainless steel steamer, steam 21-24h, obtain the wine fruit of glossy privet；
By the above-mentioned obtained wine thereby fruit of glossy privet, dry, crush, cross 70-80 mesh sieves, obtain wine fruit of glossy privet powder；By above-mentioned obtained wine thereby female
Loyal sub- powder, it is 1 according to solid-liquid ratio:25 add 85-90% ethanol solutions, stir；Ultrasound carries under 250-300W power
Take, obtain wine fruit of glossy privet granulated slag；Above-mentioned obtained wine thereby fruit of glossy privet granulated slag is filtered under diminished pressure, filtrate is freeze-dried, obtains female
Loyal sub- terpene.
7. one kind according to right 6 cleans disposable spraying, it is characterised in that ultrasonic in the preparation method of the fruit of glossy privet terpene
The condition of extraction is：Total sonication time 25-35min, each ultrasonic extraction time 3s, intermittent time 2s.
8. one kind according to claim any one of 1-7 cleans disposable spraying, it is characterised in that the spraying also include with
The component of lower mass percent：Double-PEG/PPG-20/5PEG/PPG-20/5 dimethyl silicone polymers；Methoxyl group PEG/PPG-
25/4 dimethyl silicone polymer；Caprylic/capric triglyceride 0.5-1.0%, ring five dimethyl silicone polymer 2.0-3.0%, two
Stearyldimethylammonium chloride 0.5-1.0%, quaternary ammonium salt -180.5-1.0%, glycerine 3.0-5.0%, cornstarch 0.1-
0.3%th, deionized water 20-30%, denatured ethyl alcohol surplus.
9. a kind of preparation method of the disposable spraying of cleaning as described in any one of claim 1~8, it is characterised in that including following
Step：
(1) by VARISOFT TA100, quaternary ammonium salt -18, double-PEG/PPG-20/5PEG/PPG-20/5 poly dimethyls silicon
Oxygen alkane；Methoxyl group PEG/PPG-25/4 dimethyl silicone polymers：Caprylic/capric triglyceride 0.5-1.0%, the poly dimethyl of ring five
Siloxanes mixing is uniformly dispersed, and A phases are made；
(2) glycerine, cornstarch, deionized water are mixed and be uniformly dispersed, B phases are made；
(3) A is added to B phases, emulsifying 2-3min under 3000-3500r/min speed, C phases is made；
(4) odoriflavone, Herba Schizonepetae volatile oil, fruit of glossy privet terpene, denatured ethyl alcohol are mixed and be uniformly dispersed, D phases are made；
(5) D is added to C phases, stirred under 1000-1500r/min speed, discharged.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710816217.3A CN107496240A (en) | 2017-09-11 | 2017-09-11 | One kind cleans disposable spraying |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710816217.3A CN107496240A (en) | 2017-09-11 | 2017-09-11 | One kind cleans disposable spraying |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107496240A true CN107496240A (en) | 2017-12-22 |
Family
ID=60695335
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710816217.3A Withdrawn CN107496240A (en) | 2017-09-11 | 2017-09-11 | One kind cleans disposable spraying |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107496240A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109875918A (en) * | 2019-04-23 | 2019-06-14 | 清远市立道精细化工有限公司 | A kind of Non-water washing hair spray composite and preparation method thereof |
| WO2021007741A1 (en) * | 2019-07-15 | 2021-01-21 | Henkel Ag & Co. Kgaa | Aqueous-based non-aerosol dry shampoo composition |
-
2017
- 2017-09-11 CN CN201710816217.3A patent/CN107496240A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109875918A (en) * | 2019-04-23 | 2019-06-14 | 清远市立道精细化工有限公司 | A kind of Non-water washing hair spray composite and preparation method thereof |
| WO2021007741A1 (en) * | 2019-07-15 | 2021-01-21 | Henkel Ag & Co. Kgaa | Aqueous-based non-aerosol dry shampoo composition |
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Application publication date: 20171222 |