CN107495331A - A kind of pleurotus eryngii fructification buccal tablet and preparation method thereof - Google Patents
A kind of pleurotus eryngii fructification buccal tablet and preparation method thereof Download PDFInfo
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- CN107495331A CN107495331A CN201710952740.9A CN201710952740A CN107495331A CN 107495331 A CN107495331 A CN 107495331A CN 201710952740 A CN201710952740 A CN 201710952740A CN 107495331 A CN107495331 A CN 107495331A
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- pleurotus eryngii
- fructification
- solid
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- buccal tablet
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- 235000020637 scallop Nutrition 0.000 description 1
- PCMORTLOPMLEFB-UHFFFAOYSA-N sinapinic acid Natural products COC1=CC(C=CC(O)=O)=CC(OC)=C1O PCMORTLOPMLEFB-UHFFFAOYSA-N 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid group Chemical class S(O)(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- YIBXWXOYFGZLRU-UHFFFAOYSA-N syringic aldehyde Natural products CC12CCC(C3(CCC(=O)C(C)(C)C3CC=3)C)C=3C1(C)CCC2C1COC(C)(C)C(O)C(O)C1 YIBXWXOYFGZLRU-UHFFFAOYSA-N 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- YNJBWRMUSHSURL-UHFFFAOYSA-N trichloroacetic acid Chemical compound OC(=O)C(Cl)(Cl)Cl YNJBWRMUSHSURL-UHFFFAOYSA-N 0.000 description 1
- 210000003462 vein Anatomy 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000012224 working solution Substances 0.000 description 1
- ORZHVTYKPFFVMG-UHFFFAOYSA-N xylenol orange Chemical compound OC(=O)CN(CC(O)=O)CC1=C(O)C(C)=CC(C2(C3=CC=CC=C3S(=O)(=O)O2)C=2C=C(CN(CC(O)=O)CC(O)=O)C(O)=C(C)C=2)=C1 ORZHVTYKPFFVMG-UHFFFAOYSA-N 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L31/00—Edible extracts or preparations of fungi; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/03—Organic compounds
- A23L29/035—Organic compounds containing oxygen as heteroatom
- A23L29/04—Fatty acids or derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/206—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin
- A23L29/25—Exudates, e.g. gum arabic, gum acacia, gum karaya or tragacanth
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/20—Reducing nutritive value; Dietetic products with reduced nutritive value
- A23L33/21—Addition of substantially indigestible substances, e.g. dietary fibres
- A23L33/22—Comminuted fibrous parts of plants, e.g. bagasse or pulp
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
- A23P10/28—Tabletting; Making food bars by compression of a dry powdered mixture
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Preparation Of Fruits And Vegetables (AREA)
Abstract
The present invention relates to a kind of pleurotus eryngii fructification buccal tablet, including following raw material to be prepared：26 parts of 50 60 parts of pleurotus eryngii fructification polyphenol, 15 25 parts of pleurotus eryngii sporocarp dietary fiber, 46 parts of xylitol, 0.3 0.7 parts of flavor enhancement, 38 parts of sodium carboxymethyl starch, 5 10 parts of Arabic gum and lubricant.The invention further relates to a kind of preparation method of pleurotus eryngii fructification buccal tablet.The pleurotus eryngii fructification buccal tablet of the present invention contains pleurotus eryngii fructification polyphenol and pleurotus eryngii sporocarp dietary fiber simultaneously, has a variety of physiological functions.
Description
Technical field
The present invention relates to foods processing technique, more particularly to a kind of pleurotus eryngii fructification buccal tablet and preparation method thereof.
Background technology
Pleurotus eryngii is under the jurisdiction of Eumycota, Basidiomycetes, Agaricales, Pleurotaceae, Pleurotus.Quality is tender and crisp, particularly stem
It is dense structure, solid, milky white, can all it eat, and it is stem cunning more crisp than cap, tasty and refreshing, it is referred to as " flat mushroom king ", " dried scallop
Mushroom ", there is happy almond flavor and the mouthfeel such as abalone, pleurotus eryngii is nutritious, rich in protein, carbohydrate, dimension
The mineral matters such as raw element and calcium, magnesium, copper, zinc, can improve immune function of human body, have to human body anticancer, reducing blood lipid, ease constipation stomach with
And the effect such as beauty, firmly get liking for people.
The polyphenol substance that plant polyphenol refers in plant typically exhibits out the Set Status of a variety of cyclic compounds, i.e., many phenol
Class material occurs together, therefore is referred to as " polyphenol ", including phenolic acid, flavonoids, isoflavones, anthocyanidin, tannin, catechin, anthocyanin
Deng.Pleurotus eryngii fructification contains a variety of free phenol and with reference to phenol, is rich in removing harmful free radicals, prevents cytolipin peroxidating
Effect and ability, can effectively reduce the generation of endogenous purine, so as to significantly reduce the uric acid level in blood.
Pleurotus eryngii fructification polyphenol is added in buccal tablet can effectively reduce blood uric acid, be advantageous to control gout recurrence；It is and same
Shi Tianjia pleurotus eryngii sporocarp dietary fiber can promote gastrointestinal peristalsis, reduce blood glucose and other effects.However, in the prior art not
In the presence of addition pleurotus eryngii fructification polyphenol and the buccal tablet of abalone mushroom sporocarp dietary fiber.
The content of the invention
The technical problems to be solved by the invention are：A kind of addition pleurotus eryngii fructification polyphenol and abalone mushroom fructification meals are provided
Eat the pleurotus eryngii fructification buccal tablet of fiber；And provide a kind of preparation method of above-mentioned pleurotus eryngii fructification buccal tablet.
In order to solve the above-mentioned technical problem, the technical solution adopted by the present invention is：
A kind of pleurotus eryngii fructification buccal tablet, including following raw material are prepared：Pleurotus eryngii fructification polyphenol 50-
60 parts, pleurotus eryngii sporocarp dietary fiber 15-25 parts, xylitol 4-6 parts, flavor enhancement 0.3-0.7 parts, sodium carboxymethyl starch 3-8
Part, Arabic gum 5-10 parts and lubricant 2-6 parts.
A kind of pleurotus eryngii fructification buccal tablet, it is prepared by following percentage by weight raw material：Pleurotus eryngii fructification polyphenol
50-60%, pleurotus eryngii sporocarp dietary fiber 15-25%, xylitol 4-6%, flavor enhancement 0.3-0.7%, sodium carboxymethyl starch
3-8%, Arabic gum 5-10% and lubricant 2-6%.
A kind of preparation method of pleurotus eryngii fructification buccal tablet, comprises the following steps：
(1) pleurotus eryngii fructification is taken to be freezed, until moisture is less than 4%, the pleurotus eryngii after then freezing
Fructification is crushed, and obtains pleurotus eryngii fructification dry powder；
(2) by the pleurotus eryngii fructification dry powder and distilled water using solid-liquid ratio as 1：18-22 (g/mL) ratio mixing, so
First time extraction is carried out under conditions of 20-30 DEG C；
(3) mixed solution obtained after first time is extracted carries out first time separation of solid and liquid, after first time separation of solid and liquid
The solid residue of acquisition is with distilled water using solid-liquid ratio as 1：18-22 (g/mL) ratio mixing, then carry out soaking for second successively
Carry with second of separation of solid and liquid, by the supernatant obtained after second of separation of solid and liquid and the supernatant obtained after first time separation of solid and liquid
Liquid merges, and is then concentrated the supernatant after merging, obtains pleurotus eryngii fructification concentrate；And collect described second admittedly
The solid residue obtained after liquid separation；
(4) solid residue obtained after the pleurotus eryngii fructification concentrate and second of separation of solid and liquid is entered respectively
Row freezing processing, pleurotus eryngii fructification polyphenol and pleurotus eryngii sporocarp dietary fiber are obtained successively；
(5) each preparing raw material of the pleurotus eryngii fructification buccal tablet described in claim 1 or 2 is weighed respectively；By what is weighed
Pleurotus eryngii fructification polyphenol, pleurotus eryngii sporocarp dietary fiber, xylitol, sodium carboxymethyl starch and Arabic gum are mixed,
Ethanol is added, softwood is made, mixed mixture is granulated and drying process successively, by the particle after drying process
The flavor enhancement and lubricant weighed is separately added into, compression molding is carried out after mixing, obtains the pleurotus eryngii fructification buccal tablet.
The beneficial effects of the present invention are：
(1) extracted using distilled water, obtain the extract (supernatant) containing pleurotus eryngii fructification polyphenol and contain
The solid residue of pleurotus eryngii sporocarp dietary fiber, insoluble diedairy fiber content very abundant in solid residue, these are beneficial
Loss of the composition in the whole process segment is almost " zero ", and green safe pollution-free.
(2) it is of the invention by pleurotus eryngii fructification polyphenol and pleurotus eryngii sporocarp dietary fiber, xylitol, malic acid, carboxylic first
Base sodium starch, Arabic gum and magnesium stearate etc., the above-mentioned technique such as mixed, dried successively, finally obtained pleurotus eryngii is real
Body buccal tablet, gives off a strong fragrance, mellow in taste, rich in antioxidant polyphenol, dietary fiber and mineral matter, has health care's work(
Can, it is adapted to consuming public to carry edible, therefore, there are preferable market prospects.
Brief description of the drawings
Fig. 1 is the outside drawing of pleurotus eryngii fructification；
Fig. 2A is that pleurotus eryngii fructification polyphenol component standard items mix FT-ICR MS collection of illustrative plates in target sample liquid in embodiment 4；
Fig. 2 B are the FT-ICR MS collection of illustrative plates of pleurotus eryngii fructification polyphenol in embodiment 4；
Curve maps of the Fig. 3 for pleurotus eryngii fructification polyphenol in embodiment 4 to the clearance rate of DPPH free radicals.
Curve maps of the Fig. 4 for pleurotus eryngii fructification polyphenol in embodiment 4 to the clearance rate of Superoxide anion free radical.
Curve maps of the Fig. 5 for pleurotus eryngii fructification polyphenol in embodiment 4 to the clearance rate of hydroxyl radical free radical.
Curve maps of the Fig. 6 for pleurotus eryngii fructification polyphenol in embodiment 4 to the clearance rate of Both peroxyl radical.
Embodiment
To describe the technology contents of the present invention, the objects and the effects in detail, below in conjunction with embodiment and coordinate attached
Figure is explained.
The design of most critical of the present invention is：By the functional components in the methods of extraction of apricot abalone mushroom fructification of water extraction,
Dietary fiber, and pleurotus eryngii fructification water extract and dietary fiber dry powder are used for the preparation of buccal tablet, so as to improve buccal tablet
Beneficial function.
The present invention provides a kind of pleurotus eryngii fructification buccal tablet, including following raw material is prepared：Pleurotus eryngii
Entity polyphenol 50-60 parts, pleurotus eryngii sporocarp dietary fiber 15-25 parts, xylitol 4-6 parts, flavor enhancement 0.3-0.7 parts, carboxylic first
Base sodium starch 3-8 parts, Arabic gum 5-10 parts and lubricant 2-6 parts.
The present invention also provides a kind of pleurotus eryngii fructification buccal tablet, is prepared by following percentage by weight raw material：Apricot Bao
Massee fruiting bodies polyphenol 50-60%, pleurotus eryngii sporocarp dietary fiber 15-25%, xylitol 4-6%, flavor enhancement 0.3-0.7%,
Sodium carboxymethyl starch 3-8%, Arabic gum 5-10% and lubricant 2-6%.
The present invention also provides a kind of preparation method of pleurotus eryngii fructification buccal tablet, comprises the following steps：
(1) pleurotus eryngii fructification is taken to be freezed, until moisture is less than 4%, the pleurotus eryngii after then freezing
Fructification is crushed, and obtains pleurotus eryngii fructification dry powder；
(2) by the pleurotus eryngii fructification dry powder and distilled water using solid-liquid ratio as 1：18-22 (g/mL) ratio mixing, so
First time extraction is carried out under conditions of 20-30 DEG C；
(3) mixed solution obtained after first time is extracted carries out first time separation of solid and liquid, after first time separation of solid and liquid
The solid residue of acquisition is with distilled water using solid-liquid ratio as 1：18-22 (g/mL) ratio mixing, then carry out soaking for second successively
Carry with second of separation of solid and liquid, by the supernatant obtained after second of separation of solid and liquid and the supernatant obtained after first time separation of solid and liquid
Liquid merges, and is then concentrated the supernatant after merging, obtains pleurotus eryngii fructification concentrate；And collect described second admittedly
The solid residue obtained after liquid separation；
(4) solid residue obtained after the pleurotus eryngii fructification concentrate and second of separation of solid and liquid is entered respectively
Row freezing processing, pleurotus eryngii fructification polyphenol and pleurotus eryngii sporocarp dietary fiber are obtained successively；
(5) each preparing raw material of above-mentioned pleurotus eryngii fructification buccal tablet is weighed respectively；The pleurotus eryngii fructification that will be weighed
Polyphenol, pleurotus eryngii sporocarp dietary fiber, xylitol, sodium carboxymethyl starch and Arabic gum are mixed, and are added ethanol, are made
Softwood, mixed mixture is granulated and drying process successively, weighed being separately added into the particle after drying process
Flavor enhancement and lubricant, carry out compression molding after mixing, obtain the pleurotus eryngii fructification buccal tablet.
It was found from foregoing description, the beneficial effects of the present invention are：
(1) extracted using distilled water, obtain the extract (supernatant) containing pleurotus eryngii fructification polyphenol and contain
The solid residue of pleurotus eryngii sporocarp dietary fiber, insoluble diedairy fiber content very abundant in solid residue, these are beneficial
Loss of the composition in the whole process segment is almost " zero ", and green safe pollution-free.
(2) it is of the invention by pleurotus eryngii fructification polyphenol and pleurotus eryngii sporocarp dietary fiber, xylitol, malic acid, carboxylic first
Base sodium starch, Arabic gum and magnesium stearate etc., the above-mentioned technique such as mixed, dried successively, finally obtained pleurotus eryngii is real
Body buccal tablet, gives off a strong fragrance, mellow in taste, rich in antioxidant polyphenol, dietary fiber and mineral matter, has health care's work(
Can, it is adapted to consuming public to carry edible, therefore, there are preferable market prospects.
Further, in step (2), the first time extraction is carried out repeatedly under continuous agitation, it is described every time
The time of extraction is 1-2h for the first time.
Further, in step (3), after carrying out second of extraction and second of separation of solid and liquid successively, repeatedly enter
Second of extraction and the operation of second of separation of solid and liquid are carried out described in row successively, it is upper by being obtained after multiple second of separation of solid and liquid
The supernatant obtained after clear liquid and the first time separation of solid and liquid merges in the lump.
Further, in step (3), the temperature of the concentration is 40-50 DEG C, and in vacuum be 0.5-0.9MPa conditions
It is lower to carry out the concentration, until density is 1.20 ± 0.02g/cm3。
Further, in step (4), the freezing processing includes precooling and vacuum refrigeration successively, the precooling
Temperature is subzero 30 DEG C to subzero 50 DEG C, time 12-16h；The temperature of the vacuum refrigeration is less than 60 DEG C, time 18-
24h, vacuum 5-10Pa, until moisture completes the vacuum refrigeration when being less than 5%.
Further, in step (5), 40-60% ethanol will be first added in mixed mixture, softwood is made, then
The softwood is granulated and drying process successively.
Further, in step (5), the drying process is：Particle after granulation is subjected to microwave decompression drying, until
Water content is 2-4%, and then screening obtains particle of the same size.
Further, the temperature that above-mentioned microwave decompression is dried is 50-60 DEG C, and drying time 60-90min, vacuum is not
Less than -0.085mpa；
Further, in step (5), the sheeting thickness of the compression molding is 4-6mm, a diameter of 8-15mm, and piece weight is
200-400mg。
Further, in step (1), the tea plant mushroom fruit body of crushing is screened with aperture 0.5mm sieve.
Further, in step (3), separation of solid and liquid is carried out with Horizontal helical type centrifuge, the rotating speed of centrifuge is 4000r/
Min, 23 DEG C of centrifuging temperature, centrifugation time 10min.
Further, in step (5), pleurotus eryngii fructification polyphenol, pleurotus eryngii sporocarp dietary fiber, the xylose that will weigh
Alcohol, sodium carboxymethyl starch and Arabic gum are stirred in mixer to mix, mixer mixing time 20-40min.
Further, after step (5) compression molding, the pleurotus eryngii fructification buccal tablet of acquisition is subjected to high-tension electricity
Field pulse is sterilized, and is then weighed, packed by Different Package specification.
Further, the electric-field intensity of above-mentioned high-pressure pulse electric sterilization is 15-40kv/cm, and umber of pulse is more than 10, arteries and veins
It is 10 μ -1000 μ, processing time 20-40s to rush width.
Further, in step (1), choose the fresh pleurotus eryngii fructification that moisture is 80.93% and freezed,
Described crush is carried out using micronizer, grinding time 30s.
It was found from foregoing description, the beneficial effects of the present invention are：Employ " distilled water extraction+cryogenic vacuum concentration+true
The mode of vacuum freecing-dry+mechanical mixing+microwave drying+high-pressure pulse electric sterilization ", avoids the use of organic solvent, and
Low temperature concentration, freeze-drying can effectively reduce polyphenol, dietary fiber and be destroyed in the state of high temperature, in addition, microwave is done
Dry removing moisture and volatile materials ethanol, compared with traditional drying mode, there is big rate of drying, energy-conservation, production efficiency
Height, uniform drying, clean manufacturing, easy the advantages that realizing Automated condtrol and improving product quality, do not influence dried material
Color and institutional framework, active ingredient, the effective integration distinctive flavor of pleurotus eryngii and functional components, product safety without
Poison.High-pressure pulse electric be a kind of nom-thermal sterilization that gets up of newly-developed it can overcome traditional thermal sterilization in sterilization process
Heat-sensitive nutrition (vitamin, the protein, pigment etc. with bioactivity) destruction, volatile materials is caused to lose, day
The shortcomings of right color and luster matter, structure change.Extracted amount obtained by water extraction polyphenol of the present invention is considerable, is 20.68%, external antioxygen
Change result of the test and also confirm that pleurotus eryngii fructification polyphenol can remove free radical to a certain extent, in addition, pleurotus eryngii residue contains
There are a large amount of dietary fibers, while also containing aldehydes matter (dry weight 19.29%) is combined, itself can be used as buccal tablet adhesive
And filler, raw material is both saved, there are a variety of physiological functions again, achieve many things at one stroke.So pleurotus eryngii polyphenol meals under this invention
Fiber buccal tablet is eaten by with bigger market value.
Fig. 1-6 are refer to, embodiments of the invention 1 are：
The preparation method of the pleurotus eryngii fructification buccal tablet of the present embodiment, comprises the following steps：
Step 1：Fresh pleurotus eryngii fructification is screened, moisture 80.93%, is freezed to moisture below 4%, is surpassed
Atomizer crushes 30s or so, and sealing is put into standby in drier；
Step 2：A certain amount of pleurotus eryngii fructification dry powder in precise step 1, with solid-liquid ratio (g/mL) 1:20 ratio
Example adds distilled water, extracted many times at 25 DEG C, each 1 hour time, and accompanies by lasting stirring；
Step 3：Rotating speed is 4000r/min, 23 DEG C of temperature, centrifuges 10min, carries out separation of solid and liquid, sediment is again with 1：20
Ratio be added to distilled water, be repeated 2 times, merge supernatant, under the conditions of 40 DEG C of temperature, vacuum 0.5-0.9MPa will extraction
It is 1.20 ± 0.02g/cm that liquid, which is concentrated into density,3, in addition, residue is rich in dietary fiber, collected in addition；
Step 4：Concentrate, solid residue are respectively put into and freeze disk, refrigerating chamber is sent into after sealing and carries out precooling, control
- 30 DEG C or so of temperature is down to design temperature as terminal using indoor material temperature, 16 hours time；
Step 5：After precooling terminates, will be chilled after pleurotus eryngii polyphenol concentrate, solid residue is respectively from refrigerating chamber
It is rapid to be transferred to vacuum freeze drier working bin, vacuum refrigeration is carried out, material temperature controls less than -60 DEG C, freeze-drying time 18h, vacuum
Degree reaches 5-10Pa, is discharged when moisture is less than 5% to dry terminal；Vacuum freeze drier open a position discharging before, introduce through sterile mistake
Dry air of the filter, humidity not higher than 10% enters dryness storehouse vacuum breaker, and discharge easily moisture regain condensation, so finished product will be used in time
Bottle, bag encapsulation process, it is standby；
Step 6：In mass ratio, pleurotus eryngii fructification polyphenol 60%, pleurotus eryngii sporocarp dietary fiber 15%, wood are taken respectively
Sugar alcohol 4%, sodium carboxymethyl starch 5% and Arabic gum 10%, mixer mix 20 minutes, it is to be mixed uniformly after, add
Enter 40% ethanol moistening softwood is made, after be granulated with oscillating granulator；
Step 7：To be dried using microwave decompression, temperature 50 C, drying time 90min, vacuum is not less than -0.085Mpa,
It is 2-4% to be allowed to water content, crosses 40 mesh sieves, obtains uniform particle；
Step 8：Dried particle is added into flavor enhancement malic acid 0.3%, magnesium stearate lubricant 3.7%, Ran Houquan
Automatic tableting press compression molding, sheeting thickness are 4-6 millimeters；Diameter 8-15 millimeters, piece weight 200-400 milligrams；
Step 9：The electric-field intensity 20kv/cm of high-pressure pulse electric sterilization, umber of pulse be more than 10, the μ of pulse width 10-
1000 μ, processing time 40s, weighed after sterilization processing, packed by Different Package specification.
Embodiment 2
Step 1：Fresh pleurotus eryngii fructification is screened, moisture 80.93%, is freezed to moisture below 4%, is surpassed
Atomizer crushing 30s right-left seals are put into standby in drier；
Step 2：A certain amount of pleurotus eryngii fructification dry powder in precise step 1, with solid-liquid ratio (g/mL) 1:20 ratio
Example adds distilled water, extracted many times at 25 DEG C, each 1.5 hours time, and accompanies by lasting stirring；
Step 3：Rotating speed is 4000r/min, 23 DEG C of temperature, centrifuges 10min, carries out separation of solid and liquid, is precipitated again with 1：20
Ratio is added to distilled water, is repeated 2 times, and merges supernatant, by extract under the conditions of temperature 45 C, vacuum 0.5-0.9MPa
It is 1.20 ± 0.02g/cm to be concentrated into density3, in addition, residue is rich in dietary fiber, collected in addition；
Step 4：Concentrate, solid residue are respectively put into and freeze disk, refrigerating chamber is sent into after sealing and carries out precooling, control
- 50 DEG C or so of temperature, design temperature is down to as terminal using indoor material temperature, 12 hours time；
Step 5：After precooling terminates, will be chilled after pleurotus eryngii polyphenol concentrate, solid residue is respectively from refrigerating chamber
It is rapid to be transferred to vacuum freeze drier working bin, vacuum freeze drying is carried out, material temperature controls less than -60 DEG C, freeze-drying time 21h,
Vacuum reaches 5-10Pa, is discharged when moisture is less than 5% to dry terminal；Vacuum freeze drier open a position discharging before, introduce through nothing
Bacterium is filtered, dry air of the humidity not higher than 10% enters dryness storehouse vacuum breaker, and discharge easily moisture regain condensation, so finished product is timely
It is standby with bottle, bag encapsulation process；
Step 6：In mass ratio, pleurotus eryngii fructification polyphenol 55%, pleurotus eryngii sporocarp dietary fiber 20%, wood are taken respectively
Sugar alcohol 5%, sodium carboxymethyl starch 8% and Arabic gum 8%, mixer mix 20-40 minutes, it is to be mixed uniformly after,
Add 50% ethanol moistening softwood is made, after be granulated with oscillating granulator；
Step 7：To be dried using microwave decompression, 55 DEG C of temperature, drying time 80min, vacuum is not less than -0.085Mpa,
It is 2-4% to be allowed to water content, crosses 40 mesh sieves, obtains uniform particle；
Step 8：Dried particle is added into flavor enhancement malic acid 0.5%, magnesium stearate lubricant 4.5%, Ran Houquan
Automatic tableting press compression molding, sheeting thickness are 4-6 millimeters；Diameter 8-15 millimeters, piece weight 200-400 milligrams；
Step 9：The electric-field intensity 30kv/cm of high-pressure pulse electric sterilization, umber of pulse be more than 10, the μ of pulse width 10-
1000 μ, processing time 30s, weighed after sterilization processing, packed by Different Package specification.
Embodiment 3
Step 1：Fresh pleurotus eryngii fructification is screened, moisture 80.93%u, is freezed to moisture below 4%,
Micronizer crushes 30s or so, and sealing is put into standby in drier；
Step 2：A certain amount of pleurotus eryngii fructification dry powder in precise step 1, with solid-liquid ratio (g/mL) 1:20 ratio
Example adds distilled water, is extracted at 25 DEG C, each time 2 h, and accompany by lasting stirring；
Step 3：Rotating speed is 4000r/min, 23 DEG C of temperature, centrifuges 10min, carries out separation of solid and liquid, sediment is again with 1：20
Ratio be added to distilled water, be repeated 2 times, merge supernatant, under the conditions of temperature 50 C, vacuum 0.5-0.9MPa will extraction
It is 1.20 ± 0.02g/cm that liquid, which is concentrated into density,3, in addition, residue is rich in dietary fiber, collected in addition；
Step 4：Concentrate, solid residue are respectively put into and freeze disk, refrigerating chamber is sent into after sealing and carries out precooling, control
- 40 DEG C or so of temperature is down to design temperature as terminal using indoor material temperature, 14 hours time；
Step 5：After precooling terminates, will be chilled after pleurotus eryngii polyphenol concentrate, solid residue is respectively from refrigerating chamber
It is rapid to be transferred to vacuum freeze drier working bin, vacuum freeze drying is carried out, material temperature controls less than -60 DEG C, freeze-drying time 24h,
Vacuum reaches 5Pa-10Pa, opens a position before discharging, introduces through nothing to dry the terminal vacuum freeze drier that discharges when moisture is less than 5%
Bacterium is filtered, dry air of the humidity not higher than 10% enters dryness storehouse vacuum breaker, and discharge easily moisture regain condensation, so finished product is timely
It is standby with bottle, bag encapsulation process；
Step 6：In mass ratio, pleurotus eryngii fructification powder 50%, pleurotus eryngii sporocarp dietary fiber 25%, wood are taken respectively
Sugar alcohol 6%, sodium carboxymethyl starch 10% and Arabic gum 5%, mixer mix 20-40 minutes, it is to be mixed uniformly after,
Add 60% ethanol moistening softwood is made, after be granulated with oscillating granulator；
Step 7：To be dried using microwave decompression, 55 DEG C of temperature, drying time 70min, vacuum is not less than -0.085Mpa,
It is 2-4% to be allowed to water content, crosses 40 mesh sieves, obtains uniform particle；
Step 8：Dried particle is added into flavor enhancement malic acid 0.4%, magnesium stearate lubricant 3.6%, Ran Houquan
Automatic tableting press compression molding, sheeting thickness are 4-6 millimeters；Diameter 8-15 millimeters, piece weight 200-400 milligrams；
Step 9：The electric-field intensity 40kv/cm of high-pressure pulse electric sterilization, umber of pulse be more than 10, the μ of pulse width 10-
1000 μ, processing time 20s, weighed after sterilization processing, packed by Different Package specification.
Embodiment 4
Contain various active composition, such as a variety of organic acids, alcohol, ketone, phenol, aldehyde, ester, these compositions in pleurotus eryngii fructification
Pleurotus eryngii fructification unique fragrance smell is constituted, strong fragrance, wherein pleurotus eryngii fructification polyphenol is made it have, is considered as
It is the active ingredient that value is most extracted in pleurotus eryngii fructification.Therefore, it is more to the pleurotus eryngii fructification of extraction in an experiment
Phenol has carried out constituent analysis and antioxidation in vitro experiment, will remove DPPH, superoxide anion, hydroxyl radical free radical, hydrogen peroxide
Evaluation index of the ability as oxidation resistance.
Pleurotus eryngii fructification polyphenol component is analyzed：
Pleurotus eryngii fructification polyphenol is dissolved in the water, and after fully dissolving after 0.45 μm of membrane filtration, injects FT-ICR
MS liquid matter instrument, sampling volume are 3 μ L, while using 0.1% formic acid as mobile phase A, 100% acetonitrile is Mobile phase B, set flow velocity
0.3mL/min, 30 DEG C of column temperature, and use gradient elution mode.Elution time setting is as shown in table 1, and table 1 is FT-ICR MS ladders
Spend elution time setting table.
Table 1
Polyphenol hybrid standard liquid (gallic acid, protocatechuic acid, chlorogenic acid, caffeic acid, syringic acid, the Chinese cassia tree that will have been configured
Acid, forulic acid, folic acid, sinapic acid, tert-butyl hydroxy quinine and salicylic acid) and sample liquid by FT-ICR MS washing in setting
Liquid matter analysis is carried out under de- parameter, is obtained shown in peak figure such as A (the mixed mark of standard items), B (sample liquid), when its abscissa represents
Between；Ordinate represents relative indexing；
By reference standards (Fig. 2A) and the crest figure (Fig. 2 B) of sample, pleurotus eryngii fructification polyphenol extract is most
Few phenolic acid containing 2 kinds of different structures, is protocatechuic acid, folic acid respectively, and its mass spectrum relevant parameter is as shown in table 2, and table 2 is identification
The FT-ICR MS parameter lists of the 2 kinds of phenolic acid gone out.
Table 2
| Phenolic acid species | Retention time | Ionization form | Theoretical Mass number | Survey mass number |
| Protocatechuic acid | 5.9 | [M+CH3CN+H]+ | 196.06040 | 196.06460 |
| Folic acid | 8.8 | [M+H]+ | 442.14696 | 442.14378 |
(1) to the removing of DPPH free radicals
More phenol solutions (0.25~4mg/mL) of 0.5mL various concentrations are added in sample cell, using 1.5g/mLTBHQ as the positive
Control, is added separately to 1mL, 0.1mmol/L DPPH solution, is sufficiently mixed.After 30min being stood under two groups of lucifuges of the above, in
Light absorption value is determined at 517nm.Hydroxy radical (DPPH) clearance rate (%)=[1- (Abs517sample/ are calculated as follows
Abs517control)] x100%.As a result it is as shown in Figure 3.Fig. 3 abscissas be pleurotus eryngii fructification polyphenol concentration, ordinate
For hydroxy radical (DPPH) clearance rate (%).
From the figure 3, it may be seen that increasing with the concentration of pleurotus eryngii fructification polyphenol, the Scavenging activity of DPPH free radicals is increased rapidly
By force.The experiment shows the ability that polyphenol has good removing DPPH free radicals.
(2) ultra-oxygen anion free radical is removed
The 1mL pleurotus eryngii fructification polyphenol sample of various concentrations (0.3125-10mg/mL) and 2mL Tris-HCl
The 1mL of (16mM, pH 8.0) dissolving, 200 μm of ol/L NBT and 1mL, 312 μm of ol/L NADH, add 1mL 50 μm of ol/L
PMS, shaken well, 5min is reacted at room temperature, replace example reaction to be inhaled as negative control, 560nm wavelength measure by the use of Tris-HCl
Luminosity.Superoxide anion clearance rate (%)=[1- (Abs560sample/Abs560control)] x 100% is calculated as follows,
As a result it is as shown in Figure 4.Fig. 4 abscissas are the concentration of pleurotus eryngii fructification polyphenol, and ordinate is superoxide anion clearance rate (%).
Pleurotus eryngii fructification polyphenol is between 0.3125-0.625mg/mL as shown in Figure 4, for free to superoxide anion
Base Scavenging activity effect is not notable, and when concentration is more than 0.625mg/mL, ultra-oxygen anion free radical Scavenging activity is carried rapidly
Rise.
(3) hydroxyl radical free radical is removed
The pleurotus eryngii fructification polyphenol sample (0.625~20mg/mL) of 0.1mL various concentrations is sequentially added in test tube,
0.1mL EDTA-Fe (0.15mM), 0.69mL2- deoxy-D-riboses (2.5mM), 0.01mLH2O2 (0.1mM), 37 DEG C of temperature
Lower reaction 10min, afterwards plus 1mL 2.8% (w/v) trichloroacetic acid (t=4 DEG C), 0.5mL 1% thiobarbituricacidα-, afterwards
By 100 DEG C of water-bath 8min of sample liquid in test tube, rinsing test tube with running water makes it be rapidly cooled to room temperature, is surveyed at λ=532nm
The light absorption value Abs532sample under various concentrations is obtained, it is negative right to substitute pleurotus eryngii fructification polyphenol extract with distilled water
According to, its light absorption value Abs532control, hydroxy radical (OH) clearance rate (%)=[1- is calculated as follows
(Abs532sample/Abs532control)] x100%.As a result it is as shown in Figure 5.Fig. 5 abscissas are pleurotus eryngii fructification polyphenol
Concentration, ordinate be hydroxy radical clearance rate (%).
Increase with concentration is shown by Fig. 5 results, pleurotus eryngii fructification polyphenol is corresponding to hydroxyl radical free radical Scavenging activity
Enhancing, when pleurotus eryngii fructification polyphenol extract concentration is in 2.5-10mg/mL, to the Scavenging activity growth trend of hydroxyl radical free radical
It is the most obvious.
(4) hydrogen peroxide is removed
The pleurotus eryngii fructification polyphenol sample (0.02-2mg/mL) of various concentrations is taken, the H2O2 for adding 0.1mmol/L is mixed
15min, titer use 30% H2O2, are diluted with water to 0-1mM various concentrations；20 μ L sample liquid are taken, and are mixed into 200 μ L
Working solution (125M iron ammonium sulfates (II), the 2.5M concentrated sulfuric acids, 100mM sorbierites, 125M xylenol orange), is inoculated into 96 orifice plates
On, at room temperature, 20min is stood, its absorbance is determined under 595nm wavelength.Its clearance rate={ 1- ([H2O2] is calculated as follows
in sample/[H2O2]incontrol)}x100.As a result it is as shown in Figure 6.Fig. 5 abscissas are dense for pleurotus eryngii fructification polyphenol
Degree, ordinate is Both peroxyl radical clearance rate (%).
By Fig. 6 results show pleurotus eryngii fructification polyphenol illustrate superpower Both peroxyl radical Scavenging activity (>
50%), IC50<0.05, for concentration in 0.5-1.5mg/mL, growth trend is obvious, when reaching 1.5mg/mL, and acting on 15min,
100% is nearly reached to hydrogen peroxide Scavenging activity.
In summary, using " distilled water extraction+cryogenic vacuum concentration vacuum freeze-drying+machinery is mixed in the inventive method
Even+microwave drying+high-pressure pulse electric sterilization " mode, avoids the use of organic solvent, and low temperature concentration, freeze-drying are effective
Ground reduces polyphenol, dietary fiber and is destroyed in the state of high temperature, in addition, microwave drying removes moisture and volatile materials
Ethanol, compared with traditional drying mode, there is big rate of drying, energy-conservation, production efficiency height, uniform drying, clean manufacturing, Yi Shi
Existing Automated condtrol and the advantages that improve product quality, does not influence the color and institutional framework of dried material, effectively into
Point, the effective integration distinctive flavor of pleurotus eryngii and functional components, product safety nonhazardous.High-pressure pulse electric is a kind of new
The nom-thermal sterilization closely to grow up it can overcome traditional thermal sterilization caused in sterilization process heat-sensitive nutrition (dimension life
Element, have bioactivity protein, pigment etc.) destructions, volatile materials forfeitures, natural colored matter, structure change the shortcomings of, send out
A person of good sense confirms effectively to sterilize to food under the conditions of impulse electric field strength 12-40kv/cm, burst length 18-20 μ s；
Inventor is using high-pressure pulse electric processing cider, the results showed that 80kv/cm electric field, pulse 20 times, can effectively reduce micro-
Biological 106cfu/mL, vitamin C almost not damaged, it is 97.5%, so the product that PEF is processed is significantly better than tradition warm
Sterilization.In addition, the Determination of Polyphenols of pleurotus eryngii fructification extraction is 20.68%, illustrating the extraction process extracted amount of this invention is
Considerable, and also further confirmed by antioxidation in vitro result of the test, pleurotus eryngii fructification polyphenol to a certain extent can
Enough remove free radical.Residue is rich in dietary fiber, while also contains and largely combine aldehydes matter (dry weight 19.29%), itself
Adhesive and filler can be used as, both saves raw material, there are a variety of physiological functions again, so pleurotus eryngii under this invention
Entity buccal tablet is by with bigger market value.
Embodiments of the invention are the foregoing is only, are not intended to limit the scope of the invention, it is every to utilize this hair
The equivalents that bright specification and accompanying drawing content are made, or the technical field of correlation is directly or indirectly used in, similarly include
In the scope of patent protection of the present invention.
Claims (10)
1. a kind of pleurotus eryngii fructification buccal tablet, it is characterised in that be prepared including following raw material：Pleurotus eryngii is real
Body polyphenol 50-60 parts, pleurotus eryngii sporocarp dietary fiber 15-25 parts, xylitol 4-6 parts, flavor enhancement 0.3-0.7 parts, carboxymethyl
Sodium starch 3-8 parts, Arabic gum 5-10 parts and lubricant 2-6 parts.
2. a kind of pleurotus eryngii fructification buccal tablet, it is characterised in that be prepared by following percentage by weight raw material：Pleurotus eryngii
Entity polyphenol 50-60%, pleurotus eryngii sporocarp dietary fiber 15-25%, xylitol 4-6%, flavor enhancement 0.3-0.7%, carboxylic first
Base sodium starch 3-8%, Arabic gum 5-10% and lubricant 2-6%.
3. a kind of preparation method of pleurotus eryngii fructification buccal tablet, it is characterised in that comprise the following steps：
(1) pleurotus eryngii fructification is taken to be freezed, until moisture is less than 4%, pleurotus eryngii after then freezing is real
Body is crushed, and obtains pleurotus eryngii fructification dry powder；
(2) by the pleurotus eryngii fructification dry powder and distilled water using solid-liquid ratio as 1：18-22 (g/mL) ratio mixing, Ran Houyu
First time extraction is carried out under conditions of 20-30 DEG C；
(3) mixed solution obtained after first time is extracted carries out first time separation of solid and liquid, will be obtained after first time separation of solid and liquid
Solid residue and distilled water using solid-liquid ratio as 1：18-22 (g/mL) ratio mixing, then carry out successively second extraction and
Second of separation of solid and liquid, the supernatant obtained after second of separation of solid and liquid and the supernatant obtained after first time separation of solid and liquid are closed
And then concentrated the supernatant after merging, obtain pleurotus eryngii fructification concentrate；And collect second of solid-liquid point
From the solid residue of rear acquisition；
(4) solid residue obtained after the pleurotus eryngii fructification concentrate and second of separation of solid and liquid is carried out respectively cold
Jelly processing, obtains pleurotus eryngii fructification polyphenol and pleurotus eryngii sporocarp dietary fiber successively；
(5) each preparing raw material of the pleurotus eryngii fructification buccal tablet described in claim 1 or 2 is weighed respectively；The apricot Bao that will be weighed
Massee fruiting bodies polyphenol, pleurotus eryngii sporocarp dietary fiber, xylitol, sodium carboxymethyl starch and Arabic gum are mixed, and are added
Ethanol, softwood is made, mixed mixture is granulated and drying process successively, will be in the particle after drying process respectively
The flavor enhancement and lubricant weighed is added, compression molding is carried out after mixing, obtains the pleurotus eryngii fructification buccal tablet.
4. the preparation method of pleurotus eryngii fructification buccal tablet according to claim 3, it is characterised in that in step (2),
The first time extraction is carried out repeatedly under conditions of lasting stirring, the time of the first time extraction is 1-2h every time.
5. the preparation method of pleurotus eryngii fructification buccal tablet according to claim 3, it is characterised in that in step (3), according to
After secondary second of extraction of progress and second of separation of solid and liquid, second of extraction and second are repeatedly carried out described in progress successively
The operation of secondary separation of solid and liquid, obtain the supernatant obtained after multiple second of separation of solid and liquid and after the first time separation of solid and liquid
Supernatant merge in the lump.
6. the preparation method of pleurotus eryngii fructification buccal tablet according to claim 3, it is characterised in that in step (3), institute
The temperature for stating concentration is 40-50 DEG C, and carries out the concentration under the conditions of vacuum is 0.5-0.9MPa, until density is 1.20
±0.02g/cm3。
7. the preparation method of pleurotus eryngii fructification buccal tablet according to claim 3, it is characterised in that in step (4), institute
State freezing processing includes precooling and vacuum refrigeration successively, and the temperature of the precooling is subzero 30 DEG C to subzero 50 DEG C, the time
For 12-16h；The temperature of the vacuum refrigeration is less than 60 DEG C, time 18-24h, vacuum 5-10Pa, until moisture is low
The vacuum refrigeration is completed when 5%.
8. the preparation method of pleurotus eryngii fructification buccal tablet according to claim 3, it is characterised in that, will in step (5)
40-60% ethanol is first added in mixed mixture, softwood is made, then the softwood is granulated and dried successively place
Reason.
9. the preparation method of pleurotus eryngii fructification buccal tablet according to claim 3, it is characterised in that in step (5), institute
Stating drying process is：Particle after granulation is subjected to microwave decompression drying, until water content is 2-4%, then screening obtains big
Small consistent particle.
10. the preparation method of pleurotus eryngii fructification buccal tablet according to claim 3, it is characterised in that in step (5),
The sheeting thickness of the compression molding is 4-6mm, and a diameter of 8-15mm, piece weight is 200-400mg.
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