CN107476057A - A kind of preparation method of the real silk fabric with antibacterial hemostasis stasis function - Google Patents
A kind of preparation method of the real silk fabric with antibacterial hemostasis stasis function Download PDFInfo
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- CN107476057A CN107476057A CN201710673224.2A CN201710673224A CN107476057A CN 107476057 A CN107476057 A CN 107476057A CN 201710673224 A CN201710673224 A CN 201710673224A CN 107476057 A CN107476057 A CN 107476057A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2246—Esters of unsaturated carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/40—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing ingredients of undetermined constitution or reaction products thereof, e.g. plant or animal extracts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/46—Deodorants or malodour counteractants, e.g. to inhibit the formation of ammonia or bacteria
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/20—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing organic materials
- A61L2300/30—Compounds of undetermined constitution extracted from natural sources, e.g. Aloe Vera
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/40—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
- A61L2300/404—Biocides, antimicrobial agents, antiseptic agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/40—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
- A61L2300/418—Agents promoting blood coagulation, blood-clotting agents, embolising agents
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
- D06M2101/12—Keratin fibres or silk
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- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Hematology (AREA)
- Materials Engineering (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- Textile Engineering (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Zoology (AREA)
- Botany (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of preparation method of the real silk fabric with antibacterial hemostasis stasis function.The present invention using with the medicinal and ramie leaf of health value as raw material, using ethanol water as Extraction medium, by in extract solution processing to real silk fabric, assign the antibacterial hemostasis stasis function of real silk fabric, wherein, the reason for active ingredient is mainly chlorogenic acid, Polyphenols in extract solution, and selection and withdrawal medium is ethanol water is：Alkaline medium with water or water alcohol is also more, but silk is acidproof not alkaline-resisting, and water alcohol acid medium is just have selected for the ease of directly using.Preparation method of the present invention is simple, environmentally friendly, and product is easy to use.
Description
Technical field
The invention belongs to function textile technical field, and in particular to a kind of silk with antibacterial hemostasis stasis function is knitted
The preparation method of thing.
Background technology
As ramie is important textile fabric crop, it is referred to as " China's grass " in the world, there is long ramie kind in China
Plant history and ramie textile history, ramie yield account for the 90% of Gross World Product.For a long time, people only pay attention to whole using only accounting for
The fiber of individual ramie plant 5% or so, and the Boehmeria nivea leaves to accounting for Plant weight 40% or so do not utilize well.According to money
Material is recorded, and China's history among the people using ramie treatment disease is very long, and Ming Dynasty's Li Shizhen (1518-1593 A.D.) is in famous medical literature《Book on Chinese herbal medicine
Detailed outline》In, detailed record and elaboration have been made to the part medicinal function of ramie.With the development of science and technology, nearest tens
Nian Lai, domestic and foreign scholars apply various isolation technics, from the root, stem, leaf of ramie platymiscium separation identify it is many chemistry into
Point, and many medicinal ingredients are determined.Contain the Multiple components such as chlorogenic acid, superoxide dismutase, polyphenol in ramie leaf.Wherein
Chlorogenic acid, there is similar atriphos (ADP), or platelet is made by inducing action, release physiology is lived
Property material, so as to reach anastalsis, or played a role by influenceing the sulfydryl on platelet membrane.Superoxide dismutase,
It is a kind of free radical scavenger, has the function that to protect immunity of organism to be damaged, people and animals are had no toxic side effect, has anti-aging, resists
Radiation, anti-inflammatory etc. act on.Plant polyphenol, there are antiviral, Anti-bacterium, antitumor canceration, cardiovascular disease resistant, anti-inflammatory and born of the same parents
Rash, the anti-ageing effect of waiting for a long time.
At present, for the research of ramie leaf, the research in terms of chemical composition and medical value is limited only to, on ramie leaf
Studied in functional textile development and application, have no and have been reported that.
The content of the invention
Goal of the invention：The purpose of the present invention is by ramie leaf extract processing to real silk fabric, passes through following technical side
Case is realized：A kind of preparation method of the real silk fabric with antibacterial hemostasis stasis function.
Technical scheme：A kind of preparation method of the real silk fabric with antibacterial hemostasis stasis function, comprises the following steps：
Step 1: the preparation of ramie leaf extract：Fresh ramie leaf is gathered, dries after washing, is crushed with pulverizer；With
Volume ratio 1：0.8-1.2 alcohol-water is Extraction medium, and the solid-to-liquid ratio of ramie leaf powder and medium is 1：8-12, adjust pH value
For 4-5,2-4h is extracted at 75-85 DEG C, filters, obtains extract solution；
Step 2: real silk fabric is arrived into the processing of ramie leaf extract：After real silk fabric is soaked with warm water, ramie is added to
Handled in leaf extract, treatment temperature is 75-85 DEG C, time 50-70min, bath raio 1：8-12；After the completion of processing, washing
Drying.
As optimization：The real silk fabric includes woven fabric and knitted fabric.
As optimization：In the step 1, with volume ratio 1：1 alcohol-water is Extraction medium, ramie leaf powder and medium
Solid-to-liquid ratio be 1：10,3h is extracted at 80 DEG C, filters, obtains extract solution.
As optimization：In the step 2, treatment temperature is 80 DEG C, time 60min, bath raio 1：10.
Beneficial effect：The present invention with the medicinal and ramie leaf of health value by extraction of alcohol-water, as raw material, to be situated between
Matter, by extract solution processing on real silk fabric, assign the antibacterial hemostasis stasis function of real silk fabric, wherein, in extract solution effectively into
The reason for it is mainly chlorogenic acid, Polyphenols to divide, and selection and withdrawal medium is alcohol-water is：With water or the alkaline medium of water-alcohol
It is more than comparison, but silk is acidproof not alkaline-resisting, for the ease of directly using just have selected water-alcohol acid medium.The present invention
Preparation method is simple, environmentally friendly, and product is easy to use.
Using real silk fabric made from the above method, golden yellow relatively conventional in nature and human body skin mucous membrane is crawled
Grape coccus and Escherichia coli bacteriostasis rate are up to more than 90%.Through living animal hemostasis trial, discovery has preferable haemostatic effect.
Embodiment
The technical scheme in the embodiment of the present invention will be clearly and completely described below, so that the technology of this area
Personnel can be better understood from advantages and features of the invention, so as to make apparent boundary to protection scope of the present invention
It is fixed.Embodiment described in the invention is only part of the embodiment of the present invention, rather than whole embodiments, based on the present invention
In embodiment, the every other implementation that those of ordinary skill in the art are obtained on the premise of creative work is not made
Example, belongs to the scope of protection of the invention.
Embodiment
Embodiment 1：
A kind of preparation method of the real silk fabric with antibacterial hemostasis stasis function, comprises the following steps：
Step 1: the preparation of ramie leaf extract：Fresh ramie leaf is gathered, dries after washing, is crushed with pulverizer；With
Volume ratio 1：0.8 alcohol-water is Extraction medium, and the solid-to-liquid ratio of ramie leaf powder and medium is 1：8, regulation pH value is 4-5,
2h is extracted at 75 DEG C, filters, obtains extract solution；
Step 2: real silk fabric is arrived into the processing of ramie leaf extract：After real silk fabric is soaked with warm water, ramie is added to
Handled in leaf extract, treatment temperature is 75 DEG C, time 50min, bath raio 1：8；After the completion of processing, washing drying.
Embodiment 2：
A kind of preparation method of the real silk fabric with antibacterial hemostasis stasis function, comprises the following steps：
Step 1: the preparation of ramie leaf extract：Fresh ramie leaf is gathered, dries after washing, is crushed with pulverizer；With
Volume ratio 1：1.2 alcohol-water is Extraction medium, and the solid-to-liquid ratio of ramie leaf powder and medium is 1：12, regulation pH value is 5,
4h is extracted at 85 DEG C, filters, obtains extract solution；
Step 2: real silk fabric is arrived into the processing of ramie leaf extract：After real silk fabric is soaked with warm water, ramie is added to
Handled in leaf extract, treatment temperature is 85 DEG C, time 70min, bath raio 1：12；After the completion of processing, washing drying.
Embodiment 3：
A kind of preparation method of the real silk fabric with antibacterial hemostasis stasis function, comprises the following steps：
Step 1: the preparation of ramie leaf extract：Fresh ramie leaf is gathered, dries after washing, is crushed with pulverizer；With
Volume ratio 1：1 alcohol-water is Extraction medium, and the solid-to-liquid ratio of ramie leaf powder and medium is 1：10, regulation pH value is 4.5,
3h is extracted at 80 DEG C, filters, obtains extract solution；
Step 2: real silk fabric is arrived into the processing of ramie leaf extract：After real silk fabric is soaked with warm water, ramie is added to
Handled in leaf extract, treatment temperature is 80 DEG C, time 60min, bath raio 1：10；After the completion of processing, washing drying.
Embodiment 4：
A kind of real silk fabric with antibacterial hemostasis stasis function and preparation method thereof, comprises the following steps：
(1) preparation of ramie leaf extract：Fresh ramie leaf is gathered, dries after washing, is crushed with pulverizer, weigh powder
Last 20g, the alcohol-water with the ︰ 1 of 200mL volume ratios 1 is Extraction medium, and regulation pH value is 4.5 or so, and 3h, mistake are extracted at 80 DEG C
Filter, obtains extract solution.
(2) real silk fabric is arrived into the processing of ramie leaf extract：After real silk fabric 10g is soaked with warm water, ramie is added to
Handled in leaf extract 100mL, 80 DEG C for the treatment of temperature, time 60min.After the completion of processing, drying.
The anti-microbial property test experimental data of the present invention is as shown in table 1 below：
According to GB/T20944.3-2008《Antibacterial textile performance evaluation third portion：Succusion》Test ramie leaf processing
The antibiotic property of real silk fabric, test strain choose staphylococcus aureus relatively conventional in nature and human body skin mucous membrane and
To represent strain.
The anti-microbial property test of table 1
| Strain | Staphylococcus aureus | Escherichia coli |
| Bacteriostasis rate/% | 95 | 93 |
The experimental data compared living animal haemostatic effect of the present invention is as shown in table 2 below：
Living animal hemostasis experiment weighs the untreated silk of identical weight and carried through ramie leaf using rabbit as experimental subjects
Take the silk and each 5 parts of hospital gauze after liquid processing.Rabbit is fixed in experimental rabbit frame, does not use anesthesia.Use scalpel
Longitudinally scratched in rabbit ear, material be covered in wound rapidly, treat that blood voluntarily overflows, start timing, record the bleeding time,
Until wound not bleeding, as stop blooding, record bleeding stopping period, the material after hemostasis is weighed determines Engorged quantity immediately after.
Table 2 compares living animal haemostatic effect
| Material | Amount of bleeding/g | Bleeding stopping period/s |
| Hospital gauze | 0.792 | 235 |
| Untreated silk | 0.686 | 186 |
| Ramie leaf handles silk | 0.173 | 68 |
The present invention using with the medicinal and ramie leaf of health value as raw material, using alcohol-water as Extraction medium, by extract solution
Handling on real silk fabric, assign the antibacterial hemostasis stasis function of real silk fabric, preparation method of the present invention is simple, environmentally friendly,
Product is easy to use.
Using real silk fabric made from the above method, golden yellow relatively conventional in nature and human body skin mucous membrane is crawled
Grape coccus and Escherichia coli bacteriostasis rate are up to more than 90%.Through living animal hemostasis trial, discovery has preferable haemostatic effect.
Claims (4)
1. a kind of preparation method of the real silk fabric with antibacterial hemostasis stasis function, it is characterised in that comprise the following steps：
Step 1: the preparation of ramie leaf extract：Fresh ramie leaf is gathered, dries after washing, is crushed with pulverizer；With volume
Than 1：0.8-1.2 alcohol-water is Extraction medium, and the solid-to-liquid ratio of ramie leaf powder and medium is 1：8-12, regulation pH value are 4-
5,2-4h is extracted at 75-85 DEG C, filters, obtains extract solution；
Step 2: real silk fabric is arrived into the processing of ramie leaf extract：After real silk fabric is soaked with warm water, it is added to ramie leaf and carries
Take in liquid and handle, treatment temperature is 75-85 DEG C, time 50-70min, bath raio 1：8-12；After the completion of processing, washing drying.
2. the preparation method of the real silk fabric according to claim 1 with antibacterial hemostasis stasis function, it is characterised in that：
The real silk fabric includes woven fabric and knitted fabric.
3. the preparation method of the real silk fabric according to claim 1 with antibacterial hemostasis stasis function, it is characterised in that：
In the step 1, with volume ratio 1：1 alcohol-water is Extraction medium, and the solid-to-liquid ratio of ramie leaf powder and medium is 1：10,
3h is extracted at 80 DEG C, filters, obtains extract solution.
4. the preparation method of the real silk fabric according to claim 1 with antibacterial hemostasis stasis function, it is characterised in that：
In the step 2, treatment temperature is 80 DEG C, time 60min, bath raio 1：10.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710673224.2A CN107476057A (en) | 2017-08-09 | 2017-08-09 | A kind of preparation method of the real silk fabric with antibacterial hemostasis stasis function |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710673224.2A CN107476057A (en) | 2017-08-09 | 2017-08-09 | A kind of preparation method of the real silk fabric with antibacterial hemostasis stasis function |
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| CN107476057A true CN107476057A (en) | 2017-12-15 |
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| CN201710673224.2A Pending CN107476057A (en) | 2017-08-09 | 2017-08-09 | A kind of preparation method of the real silk fabric with antibacterial hemostasis stasis function |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101978976A (en) * | 2010-10-19 | 2011-02-23 | 南京泽朗医药科技有限公司 | Method for extracting and purifying total phenolic acid from fresh ramie leaves |
| CN102493219A (en) * | 2011-12-01 | 2012-06-13 | 江南大学 | Ecological preparation method of anti-ultraviolet wool and silk textiles based on orange peel |
| CN102634994A (en) * | 2012-03-29 | 2012-08-15 | 江南大学 | Ecological preparation method for anti-ultraviolet wool and silk textile based on granatum |
| CN102936835A (en) * | 2012-12-05 | 2013-02-20 | 苏州大学 | Preparation method of nano-silver antibacterial real silk |
| CN105316769A (en) * | 2014-06-16 | 2016-02-10 | 李林 | Meyer sedge warm keeping and bacterium resisting fiber and production method of non-woven cloth containing fiber |
-
2017
- 2017-08-09 CN CN201710673224.2A patent/CN107476057A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101978976A (en) * | 2010-10-19 | 2011-02-23 | 南京泽朗医药科技有限公司 | Method for extracting and purifying total phenolic acid from fresh ramie leaves |
| CN102493219A (en) * | 2011-12-01 | 2012-06-13 | 江南大学 | Ecological preparation method of anti-ultraviolet wool and silk textiles based on orange peel |
| CN102634994A (en) * | 2012-03-29 | 2012-08-15 | 江南大学 | Ecological preparation method for anti-ultraviolet wool and silk textile based on granatum |
| CN102936835A (en) * | 2012-12-05 | 2013-02-20 | 苏州大学 | Preparation method of nano-silver antibacterial real silk |
| CN105316769A (en) * | 2014-06-16 | 2016-02-10 | 李林 | Meyer sedge warm keeping and bacterium resisting fiber and production method of non-woven cloth containing fiber |
Non-Patent Citations (2)
| Title |
|---|
| 安健等: "黄柏抗菌成分的提取及对真丝的抗菌性研究", 《印染助剂》 * |
| 施树云等: "苎麻叶中绿原酸的提取", 《中南大学学报（自然科学版）》 * |
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Application publication date: 20171215 |