CN107473711A - A kind of Environment-friendlyceramic ceramic material and preparation method thereof - Google Patents

A kind of Environment-friendlyceramic ceramic material and preparation method thereof Download PDF

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Publication number
CN107473711A
CN107473711A CN201710826358.3A CN201710826358A CN107473711A CN 107473711 A CN107473711 A CN 107473711A CN 201710826358 A CN201710826358 A CN 201710826358A CN 107473711 A CN107473711 A CN 107473711A
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Prior art keywords
parts
environment
water
ceramic material
useless porcelain
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Inventor
黄礼辉
苏秋桂
苏冬武
章惠萍
阮旭山
陈勇浩
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GUANGDONG UNCOMMON INDUSTRIAL Co Ltd
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GUANGDONG UNCOMMON INDUSTRIAL Co Ltd
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Priority to CN201710826358.3A priority Critical patent/CN107473711A/en
Publication of CN107473711A publication Critical patent/CN107473711A/en
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    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/13—Compounding ingredients
    • C04B33/132—Waste materials; Refuse; Residues
    • C04B33/1324—Recycled material, e.g. tile dust, stone waste, spent refractory material
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3244—Zirconium oxides, zirconates, hafnium oxides, hafnates, or oxide-forming salts thereof
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427—Silicates other than clay, e.g. water glass
    • C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427—Silicates other than clay, e.g. water glass
    • C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
    • C04B2235/3472—Alkali metal alumino-silicates other than clay, e.g. spodumene, alkali feldspars such as albite or orthoclase, micas such as muscovite, zeolites such as natrolite
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    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/42—Non metallic elements added as constituents or additives, e.g. sulfur, phosphor, selenium or tellurium
    • C04B2235/422—Carbon
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    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54—Particle size related information
    • C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5436—Particle size related information expressed by the size of the particles or aggregates thereof micrometer sized, i.e. from 1 to 100 micron
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/602—Making the green bodies or pre-forms by moulding
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/612—Machining
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6567—Treatment time
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00—Technologies relating to the processing of minerals
    • Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes

Abstract

The present invention discloses a kind of Environment-friendlyceramic ceramic material and preparation method thereof.This method comprises the following steps：After useless porcelain is cleaned, it is ground, it is 250 500 mesh that grinding, which causes fineness, is obtained by pretreated useless porcelain；Water is added to mix, wherein the mass ratio of useless porcelain and water is 1：1~2；After zircon sand, spodumene, activated carbon and flyash are mixed, grinding causes 90 ~ 200 mesh, 250 500 mesh of grinding cause after clay, potassium feldspar, quartz, pyrophillite are mixed, is mixed with by pretreated useless porcelain, water is added to mix, wherein the mass ratio of mixture and water is 1：1~2；By slip casting, repair embryo and fired after at 1200 ~ 1300 DEG C, obtain Environment-friendlyceramic ceramic material.Discarded ceramic product is being reused in the present invention, applied in new ceramic product production so that defective work recycles.

Description

A kind of Environment-friendlyceramic ceramic material and preparation method thereof
Technical field
The invention belongs to ceramic field, and in particular to a kind of Environment-friendlyceramic ceramic material and preparation method thereof.
Background technology
Ceramics are the products that a kind of ceramic mud is formed after oversintering, however, during firing, are existed a certain amount of Waste product porcelain, these waste product porcelain are due to that can not degrade so that existing ceramic waste disposal has the problem of larger.Common ceramics Waste product is all directly to abandon, and does not meet the requirement of sustainable development.
The content of the invention
The present invention overcomes prior art defect, there is provided a kind of Environment-friendlyceramic ceramic material and preparation method thereof.
Technical solution of the present invention is as follows.
A kind of Environment-friendlyceramic ceramic material, as mass fraction, including following material：
Clay 40-50 parts
Potassium feldspar 20-25 parts
Quartzy 20-25 parts
Activated carbon 5-10 parts
Useless porcelain 20-30 parts
Pyrophillite 10-15 parts
Zircon sand 5-7 parts
Spodumene 10-15 parts
Flyash 5-7 parts.
Including following material preferably, as mass fraction,：
45 parts of clay
22 parts of potassium feldspar
23 parts of quartz
7 parts of activated carbon
Useless 26 parts of porcelain
12 parts of pyrophillite
6 parts of zircon sand
12 parts of spodumene
6 parts of flyash.
A kind of preparation method of Environment-friendlyceramic ceramic material, comprises the following steps：
（1）The pre-treatment of useless porcelain：After useless porcelain is cleaned, it is ground, it is 250-500 mesh that grinding, which causes fineness, is obtained by pre- place Useless porcelain after reason；Water is added to mix, wherein the mass ratio of useless porcelain and water is 1：1~2；
（2）After zircon sand, spodumene, activated carbon and flyash are mixed, grinding causes 90 ~ 200 mesh, by clay, potassium feldspar, stone Grinding causes 250-500 mesh after English, pyrophillite mixing, with step（1）In obtain mixing by pretreated useless porcelain, add water to mix Close, wherein the mass ratio of mixture and water is 1：1~2；
（3）Slip casting, repair embryo and fired after at 1200 ~ 1300 DEG C, obtain Environment-friendlyceramic ceramic material.
Fired in the above method, at described 1200 ~ 1300 DEG C and be specially：At 500 ~ 600 DEG C, 0.5 ~ 1h is fired, then Heating is caused to fire 1 ~ 2h at 900 ~ 1000 DEG C, and 1 ~ 2h is then fired at 1200 ~ 1300 DEG C.
Compared with prior art, advantage of the invention is that：Discarded ceramic product is being reused in the present invention, should For in new ceramic product production so that defective work recycles.
Embodiment
The present invention will be further described with reference to embodiments.
Embodiment 1
Take 45 parts of clay, 22 parts of potassium feldspar, 23 parts of quartz, 7 parts of activated carbon, useless 26 parts of porcelain, 12 parts of pyrophillite, 6 parts of zircon sand, lithium 12 parts of pyroxene, 6 parts of flyash；Total 10kg.
（1）After useless porcelain is cleaned, it is ground, it is 250 mesh that grinding, which causes fineness, is obtained by pretreated useless porcelain；Add Water mixes, wherein the mass ratio of useless porcelain and water is 1：1；
（2）After zircon sand, spodumene, activated carbon and flyash are mixed, grinding causes 200 mesh, by clay, potassium feldspar, quartz, leaf Grinding causes 250 mesh after cured stone mixing, with step（1）In obtain mixing by pretreated useless porcelain, add water to mix, wherein mixing The mass ratio of thing and water is 1：1；
（3）Slip casting, after repairing embryo, at 500 DEG C, 1h is fired, then heating causes to fire 2h at 1000 DEG C, is then burnt at 1200 DEG C 1h processed, is produced.
Embodiment 2
Take 40 parts of clay, 25 parts of potassium feldspar, 25 parts of quartz, 10 parts of activated carbon, useless 20 parts of porcelain, 10 parts of pyrophillite, 5 parts of zircon sand, 10 parts of spodumene, 7 parts of flyash；Total 10kg.
（1）After useless porcelain is cleaned, it is ground, it is 250 mesh that grinding, which causes fineness, is obtained by pretreated useless porcelain；Add Water mixes, wherein the mass ratio of useless porcelain and water is 1：2；
（2）After zircon sand, spodumene, activated carbon and flyash are mixed, grinding causes 200 mesh, by clay, potassium feldspar, quartz, leaf Grinding causes 500 mesh after cured stone mixing, with step（1）In obtain mixing by pretreated useless porcelain, add water to mix, wherein mixing The mass ratio of thing and water is 1：2；
（3）Slip casting, after repairing embryo, at 500 DEG C, 2h is fired, then heating causes to fire 1h at 900 DEG C, is then burnt at 1300 DEG C 1h processed, is produced.
Embodiment 3
Take 40 parts of clay, 20 parts of potassium feldspar, 20 parts of quartz, 5 parts of activated carbon, useless 30 parts of porcelain, 10 parts of pyrophillite, 7 parts of zircon sand, lithium 15 parts of pyroxene, 7 parts of flyash；Total 10kg.
（1）After useless porcelain is cleaned, it is ground, it is 250 mesh that grinding, which causes fineness, is obtained by pretreated useless porcelain；Add Water mixes, wherein the mass ratio of useless porcelain and water is 1：1；
（2）After zircon sand, spodumene, activated carbon and flyash are mixed, grinding causes 200 mesh, by clay, potassium feldspar, quartz, leaf Grinding causes 250 mesh after cured stone mixing, with step（1）In obtain mixing by pretreated useless porcelain, add water to mix, wherein mixing The mass ratio of thing and water is 1：1；
（3）Slip casting, after repairing embryo, at 500 DEG C, 1h is fired, then heating causes to fire 2h at 1000 DEG C, is then burnt at 1200 DEG C 1h processed, is produced.
It should be appreciated that the detailed description carried out above by optimal enforcement example to technical scheme is schematical It is and nonrestrictive, it is impossible to assert that the embodiment of the present invention is only limitted to this, for the general of the technical field of the invention For logical technical staff, without departing from the inventive concept of the premise, the technical scheme described in each embodiment is modified, Or equivalent substitution is carried out to which part technical characteristic, it should all be considered as belonging to what claims that the present invention submits determined Scope of patent protection.

Claims (4)

  1. A kind of 1. Environment-friendlyceramic ceramic material, it is characterised in that as mass fraction, including following material：
    Clay 40-50 parts
    Potassium feldspar 20-25 parts
    Quartzy 20-25 parts
    Activated carbon 5-10 parts
    Useless porcelain 20-30 parts
    Pyrophillite 10-15 parts
    Zircon sand 5-7 parts
    Spodumene 10-15 parts
    Flyash 5-7 parts.
  2. 2. Environment-friendlyceramic ceramic material according to claim 1, it is characterised in that as mass fraction, including following material：
    45 parts of clay
    22 parts of potassium feldspar
    23 parts of quartz
    7 parts of activated carbon
    Useless 26 parts of porcelain
    12 parts of pyrophillite
    6 parts of zircon sand
    12 parts of spodumene
    6 parts of flyash.
  3. 3. the preparation method of Environment-friendlyceramic ceramic material described in claim 1, it is characterised in that comprise the following steps：
    （1）The pre-treatment of useless porcelain：After useless porcelain is cleaned, it is ground, it is 250-500 mesh that grinding, which causes fineness, is obtained by pre- place Useless porcelain after reason；Water is added to mix, wherein the mass ratio of useless porcelain and water is 1：1~2；
    （2）After zircon sand, spodumene, activated carbon and flyash are mixed, grinding causes 90 ~ 200 mesh, by clay, potassium feldspar, stone Grinding causes 250-500 mesh after English, pyrophillite mixing, with step（1）In obtain mixing by pretreated useless porcelain, add water to mix Close, wherein the mass ratio of mixture and water is 1：1~2；
    （3）Slip casting, repair embryo and fired after at 1200 ~ 1300 DEG C, obtain Environment-friendlyceramic ceramic material.
  4. 4. the preparation method of Environment-friendlyceramic ceramic material according to claim 3, it is characterised in that burnt at described 1200 ~ 1300 DEG C System is specially：At 500 ~ 600 DEG C, fire 0.5 ~ 1h, then heating causes to fire 1 ~ 2h at 900 ~ 1000 DEG C, then 1200 ~ 1 ~ 2h is fired at 1300 DEG C.
CN201710826358.3A 2017-09-14 2017-09-14 A kind of Environment-friendlyceramic ceramic material and preparation method thereof Pending CN107473711A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108191401A (en) * 2018-04-04 2018-06-22 佛山市润辉合化工有限公司 A kind of method that ceramics are made using coal ash

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104591695A (en) * 2015-02-03 2015-05-06 朱立民 Manufacturing method of large-sized regenerated ceramic
CN105801084A (en) * 2016-01-21 2016-07-27 广东皓明陶瓷科技有限公司 Preparation method of ceramic clay body and method for preparing ceramic product from ceramic clay body

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104591695A (en) * 2015-02-03 2015-05-06 朱立民 Manufacturing method of large-sized regenerated ceramic
CN105801084A (en) * 2016-01-21 2016-07-27 广东皓明陶瓷科技有限公司 Preparation method of ceramic clay body and method for preparing ceramic product from ceramic clay body

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108191401A (en) * 2018-04-04 2018-06-22 佛山市润辉合化工有限公司 A kind of method that ceramics are made using coal ash

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Application publication date: 20171215