CN107459931A - A kind of water paint of water resistant abrasive proof - Google Patents
A kind of water paint of water resistant abrasive proof Download PDFInfo
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- CN107459931A CN107459931A CN201710522894.4A CN201710522894A CN107459931A CN 107459931 A CN107459931 A CN 107459931A CN 201710522894 A CN201710522894 A CN 201710522894A CN 107459931 A CN107459931 A CN 107459931A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D193/00—Coating compositions based on natural resins; Coating compositions based on derivatives thereof
- C09D193/04—Rosin
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
- C09D167/06—Unsaturated polyesters having carbon-to-carbon unsaturation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
- C08L2205/16—Fibres; Fibrils
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
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- Wood Science & Technology (AREA)
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Abstract
The invention discloses a kind of water paint of water resistant abrasive proof, its raw material includes by weight：70 80 parts of aliphatic urethane acrylate, 100 120 parts of abietyl hyperbranched polyester acrylic ester resin, 8 12 parts of bamboo charcoal powder, 26 parts of medical stone, 10 15 parts of polypropylene fibre, 5 10 parts of quartz sand, 5 10 parts of glass microballoon, 15 20 parts of CNT, 16 20 parts of galapectite compound, 68 parts of nano-attapulgite, 30 40 parts of lithopone, 48 parts of casein fibre, poly- 8 12 parts of boric acid ester fiber, 6 12 parts of xanthans, 8 10 parts of gelatin, 10 12 parts of pigment, 24 parts of wetting agent, 24 parts of dispersant, 24 parts of defoamer, 150 200 parts of deionized water.The present invention has super-weathering resistance and brushing resistance energy, also with anti-precipitation feature, while has high adhesion force, color development effect is good, and fade-proof decolorizing effect is excellent.
Description
Technical field
The present invention relates to technical field of aqueous paint, more particularly to a kind of water paint of water resistant abrasive proof.
Background technology
Coating, refer to that film can be formed and play protection under certain conditions by being coated on body surface, decoration or other spies
A kind of liquid or solid material that distinguished service (can insulate, antirust is mould proof, heat-resisting etc.).Our usually described paint are wherein
One kind.Because the coating of early stage is mostly using vegetable oil as primary raw material, therefore also referred to as paint.Coating belongs to organic chemical industry's macromolecule
Material, the film formed belong to high-molecular compound type.The classification for the chemical products passed through according to the modern times, coating belong to essence
Refine chemical product.
Modern coating progressively turns into a kind of multi-functional engineering material, is an important row in chemical industry
Industry.Therefore the research and development of the research and development especially batch formula of all kinds of coating, it is that development paint industry is essential.But apply at present
Expect that cost is higher, water proofing property is poor, not scrubbing resistance, it would be highly desirable to solves.
The content of the invention
Based on technical problem existing for background technology, the present invention proposes a kind of water paint of water resistant abrasive proof, had
Super-weathering resistance and brushing resistance energy, also with anti-precipitation feature, while there is high adhesion force, color development effect is good, fade-proof decolouring
Excellent effect.
A kind of water paint of water resistant abrasive proof proposed by the present invention, its raw material include by weight：Aliphatic polyurethane
Acrylate 70-80 parts, abietyl hyperbranched polyester acrylic ester resin 100-120 parts, bamboo charcoal powder 8-12 parts, medical stone 2-6
Part, polypropylene fibre 10-15 parts, quartz sand 5-10 parts, glass microballoon 5-10 parts, CNT 15-20 parts, galapectite compound
16-20 parts, nano-attapulgite 6-8 parts, lithopone 30-40 parts, casein fibre 4-8 parts, poly- boric acid ester fiber 8-12 parts, xanthan
Glue 6-12 parts, gelatin 8-10 parts, pigment 10-12 parts, wetting agent 2-4 parts, dispersant 2-4 parts, defoamer 2-4 parts, deionized water
150-200 parts.
Preferably, pigment is included more than one or both of rutile titanium dioxide, zinc oxide or lithopone.
Preferably, defoamer includes by weight：Epoxidized soybean oil 10-20 parts, vinyl-terminated silicone fluid 6-10 parts, octyl phenol
APEO 2-4 parts, zinc soap salt 12-14 parts, polyvinylether 4-8 parts.
Preferably, galapectite compound is prepared using following technique：Peanut powder, water are stirred, maleic anhydride is added and continues
Stirring, add silane coupler stirring, be subsequently added into potassium peroxydisulfate and continue to stir, filter, dry, then add galapectite,
Water is well mixed, and is added hydrogen peroxide, heating stirring, is filtered by vacuum, dries, add toluene ultrasonic disperse, washed using acetone, very
Sky filters, and dries, and adds maleic anhydride, toluene ultrasonic disperse, the lower heating stirring of nitrogen protection, vacuum filtration, using third
Ketone washs, and vacuum drying obtains galapectite compound.
Preferably, galapectite compound is prepared using following technique：By weight by 10-20 parts peanut powder, 60-70 part water
Stirring, add 1-2 part maleic anhydrides and continue to stir, add the stirring of 0.5-1 parts silane coupler, be subsequently added into 1-2 part over cures
Sour potassium continues to stir, and filters, and dries, and then adds 30-50 parts galapectite, 120-160 part water is well mixed, addition 20-30 parts
Hydrogen peroxide, heating stirring, is filtered by vacuum, and dries, and adds 120-160 part toluene ultrasonic disperses, is washed using acetone, vacuum is taken out
Filter, dry, add 1.5-2.5 parts maleic anhydride, 120-160 part toluene ultrasonic disperses, heating stirring under nitrogen protection, very
Sky filters, and is washed using acetone, and vacuum drying obtains galapectite compound.
Preferably, galapectite compound is prepared using following technique：By weight by 10-20 parts peanut powder, 60-70 part water
20-40min is stirred, whipping temp is 70-80 DEG C, adds 1-2 part maleic anhydrides and continues to stir 10-20min, adds 0.5-1
Part silane coupler stirring 10-20min, is subsequently added into 1-2 part potassium peroxydisulfates and continues to stir 30-50min, filter, dry, then
Addition 30-50 parts galapectite, 120-160 part water are well mixed, and add 20-30 part hydrogen peroxide, are warming up to 80-90 DEG C of stirring 6-
10h, it is filtered by vacuum, dries, add 120-160 part toluene ultrasonic disperse 40-60min, washed using acetone, be filtered by vacuum, does
It is dry, 1.5-2.5 parts maleic anhydride, 120-160 part toluene ultrasonic disperse 40-60min are added, is warming up under nitrogen protection
170-180 DEG C of stirring 30-40min, vacuum filtration, is washed, vacuum drying obtains galapectite compound using acetone.
Gained water paint of the invention is Environmentally friendly coatings, and containing minimal amount of volatile materials, the feature of environmental protection is good, no gas
Taste, brush on human body and environment substantially without influence.
In galapectite compound, peanut powder is under potassium peroxydisulfate cooperation by maleic anhydride, silane coupler processing, table
Face activity is high, and adhesive property is good, and with galapectite good dispersion, maleic anhydride is grafted into halloysite nanotubes surface,
While compatibility is improved, it can be blended with various kinds of resin matrix, and can be very good, which improves original halloysite nanotubes, is setting
In aliphatic radical body the problem of dispersiveness, poor compatibility, while improve base resin material water resistance, natural environmental-protective, raw material sources
Extensively, cost is low；Galapectite compound dissolves with abietyl hyperbranched polyester acrylic ester resin, aliphatic urethane acrylate
Property it is good, emulsion mechanical property can be effectively improved, while the abundant active group in nano-attapulgite surface improves the base material of emulsion
Surface adhesion force, coating waterproofing, scrub performance further enhance after solidification；And defoamer and filler, pigment and thickener
Compounding, it can be ensured that water paint it is reliable and stable, and effectively improve the viscosity of coating, it is seamless after coating dye, have preferable
Water-fast, alkaline-resisting, washability the features such as, the effect totally used is preferable, extends service life, suitable for promoting.
The present invention has a super-weathering resistance, under identical construction technology and identical environment, water paint ratio obtained by the present invention
The weatherability of like product improves 4-6 times；And under identical construction technology and identical environment, present invention gained water paint
Resistance to scrub is more than 40,000 times, and surface is without obvious brush mark, compared to similar thousands of secondary scrub numbers, water-based painting obtained by the present invention
The brushing resistance of material can be eager to excel more；There is anti-precipitation feature in addition, under identical construction technology and identical environment, the present invention
After the water paint is placed in baking oven 40 days, takes out and have no obvious layering, and layering just occurs for 6-7 days in like product, and
And the present invention has high adhesion force, compared with similar coloured aqueous coating, color development effect is good, and fade-proof decolorizing effect is excellent.
Embodiment
Below, technical scheme is described in detail by specific embodiment.
Embodiment 1
A kind of water paint of water resistant abrasive proof proposed by the present invention, its raw material include by weight：Aliphatic polyurethane
80 parts of acrylate, 100 parts of abietyl hyperbranched polyester acrylic ester resin, 12 parts of bamboo charcoal powder, 2 parts of medical stone, polypropylene are fine
15 parts of dimension, 5 parts of quartz sand, 10 parts of glass microballoon, 15 parts of CNT, 20 parts of galapectite compound, 6 parts of nano-attapulgite,
40 parts of lithopone, 4 parts of casein fibre, poly- 12 parts of boric acid ester fiber, 6 parts of xanthans, 10 parts of gelatin, 10 parts of pigment, wetting agent 4
Part, 2 parts of dispersant, 4 parts of defoamer, 150 parts of deionized water.
Embodiment 2
A kind of water paint of water resistant abrasive proof proposed by the present invention, its raw material include by weight：Aliphatic polyurethane
70 parts of acrylate, 120 parts of abietyl hyperbranched polyester acrylic ester resin, 8 parts of bamboo charcoal powder, 6 parts of medical stone, polypropylene fibre
10 parts, 10 parts of quartz sand, 5 parts of glass microballoon, 20 parts of CNT, 16 parts of galapectite compound, 8 parts of nano-attapulgite, stand
30 parts of moral powder, 8 parts of casein fibre, poly- 8 parts of boric acid ester fiber, 12 parts of xanthans, 8 parts of gelatin, 12 parts of pigment, 2 parts of wetting agent, point
4 parts of powder, 2 parts of defoamer, 200 parts of deionized water.
Galapectite compound is prepared using following technique：Peanut powder, water are stirred, maleic anhydride is added and continues to stir, then
Silane coupler stirring is added, potassium peroxydisulfate is subsequently added into and continues to stir, is filtered, is dried, then addition galapectite, water mixing are equal
It is even, hydrogen peroxide is added, heating stirring, is filtered by vacuum, dries, add toluene ultrasonic disperse, washed using acetone, be filtered by vacuum,
Dry, add maleic anhydride, toluene ultrasonic disperse, the lower heating stirring of nitrogen protection, vacuum filtration, washed using acetone,
Vacuum drying obtains galapectite compound.
Embodiment 3
A kind of water paint of water resistant abrasive proof proposed by the present invention, its raw material include by weight：Aliphatic polyurethane
78 parts of acrylate, 105 parts of abietyl hyperbranched polyester acrylic ester resin, 11 parts of bamboo charcoal powder, 3 parts of medical stone, polypropylene are fine
14 parts of dimension, 6 parts of quartz sand, 8 parts of glass microballoon, 17 parts of CNT, 19 parts of galapectite compound, 6.5 parts of nano-attapulgite,
38 parts of lithopone, 5 parts of casein fibre, poly- 11 parts of boric acid ester fiber, 8 parts of xanthans, 9.5 parts of gelatin, rutile titanium dioxide
10.5 parts, 3.5 parts of wetting agent, 2.5 parts of dispersant, 3.5 parts of defoamer, 160 parts of deionized water.
Galapectite compound is prepared using following technique：By weight by 15 parts of peanut powders, 65 parts of water stirrings, 1.5 are added
Part maleic anhydride continues to stir, and adds 0.8 part of silane coupler stirring, is subsequently added into 1.5 parts of potassium peroxydisulfates and continues to stir, mistake
Filter, dry, then 40 parts of galapectites of addition, 140 parts of water are well mixed, and add 25 parts of hydrogen peroxide, and heat up stirring, vacuum filtration,
Dry, add 140 parts of toluene ultrasonic disperses, washed using acetone, be filtered by vacuum, dry, add 2 parts of maleic anhydrides, 140
Part toluene ultrasonic disperse, the lower heating stirring of nitrogen protection, is filtered by vacuum, is washed using acetone, vacuum drying obtains galapectite and answered
Compound.
Defoamer includes by weight：15 parts of epoxidized soybean oil, 8 parts of vinyl-terminated silicone fluid, OPEO 3
Part, 13 parts of zinc soap salt, 6 parts of polyvinylether.
Embodiment 4
A kind of water paint of water resistant abrasive proof proposed by the present invention, its raw material include by weight：Aliphatic polyurethane
72 parts of acrylate, 115 parts of abietyl hyperbranched polyester acrylic ester resin, 9 parts of bamboo charcoal powder, 5 parts of medical stone, polypropylene fibre
12 parts, 8 parts of quartz sand, 6 parts of glass microballoon, 19 parts of CNT, 17 parts of galapectite compound, 7.5 parts of nano-attapulgite, stand
32 parts of moral powder, 7 parts of casein fibre, poly- 9 parts of boric acid ester fiber, 10 parts of xanthans, 8.5 parts of gelatin, 11.2 parts of pigment, wetting agent
2.5 parts, -3.4 parts of dispersant, 2.5 parts of defoamer, 180 parts of deionized water.
Galapectite compound is prepared using following technique：By weight by 10 parts of peanut powders, 70 parts of water stirring 20min, stir
Temperature is mixed as 80 DEG C, 1 part of maleic anhydride is added and continues to stir 20min, adds 0.5 part of silane coupler stirring 20min, then
Add 1 part of potassium peroxydisulfate to continue to stir 50min, filter, dry, then 30 parts of galapectites of addition, 160 parts of water are well mixed, and are added
Enter 20 parts of hydrogen peroxide, be warming up to 90 DEG C of stirring 6h, be filtered by vacuum, dry, 160 parts of toluene ultrasonic disperse 40min are added, using third
Ketone washs, and is filtered by vacuum, and dries, and 2.5 parts of maleic anhydrides, 120 parts of toluene ultrasonic disperse 60min is added, under nitrogen protection
170 DEG C of stirring 40min are warming up to, vacuum filtration, are washed using acetone, vacuum drying obtains galapectite compound.
Defoamer includes by weight：10 parts of epoxidized soybean oil, 10 parts of vinyl-terminated silicone fluid, OPEO 2
Part, 14 parts of zinc soap salt, 4 parts of polyvinylether.Pigment is rutile titanium dioxide, zinc oxide.
Embodiment 5
A kind of water paint of water resistant abrasive proof proposed by the present invention, its raw material include by weight：Aliphatic polyurethane
76 parts of acrylate, 112 parts of abietyl hyperbranched polyester acrylic ester resin, 10 parts of bamboo charcoal powder, 4 parts of medical stone, polypropylene are fine
13 parts of dimension, 7 parts of quartz sand, 7 parts of glass microballoon, 18 parts of CNT, 18 parts of galapectite compound, 6.8 parts of nano-attapulgite,
34 parts of lithopone, 6 parts of casein fibre, poly- 10 parts of boric acid ester fiber, 9 parts of xanthans, 8.9 parts of gelatin, 10.8 parts of pigment, wetting agent
2.9 parts, 2.7 parts of dispersant, 2.8 parts of defoamer, 167 parts of deionized water.
Galapectite compound is prepared using following technique：By weight by 20 parts of peanut powders, 60 parts of water stirring 40min, stir
Temperature is mixed as 70 DEG C, 2 parts of maleic anhydrides is added and continues to stir 10min, 1 part of silane coupler stirring 10min is added, then adds
Enter 2 parts of potassium peroxydisulfates to continue to stir 30min, filter, dry, then add 50 parts of galapectites, 120 parts of water are well mixed, addition
30 parts of hydrogen peroxide, 80 DEG C of stirring 10h are warming up to, is filtered by vacuum, dries, 120 parts of toluene ultrasonic disperse 60min are added, using third
Ketone washs, and is filtered by vacuum, and dries, and 1.5 parts of maleic anhydrides, 160 parts of toluene ultrasonic disperse 40min is added, under nitrogen protection
180 DEG C of stirring 30min are warming up to, vacuum filtration, are washed using acetone, vacuum drying obtains galapectite compound.
Defoamer includes by weight：20 parts of epoxidized soybean oil, 6 parts of vinyl-terminated silicone fluid, OPEO 4
Part, 12 parts of zinc soap salt, 8 parts of polyvinylether.Pigment includes rutile titanium dioxide, zinc oxide or lithopone.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (6)
1. a kind of water paint of water resistant abrasive proof, it is characterised in that its raw material includes by weight：Aliphatic polyurethane propylene
Acid esters 70-80 parts, abietyl hyperbranched polyester acrylic ester resin 100-120 parts, bamboo charcoal powder 8-12 parts, medical stone 2-6 parts, gather
Tacryl 10-15 parts, quartz sand 5-10 parts, glass microballoon 5-10 parts, CNT 15-20 parts, galapectite compound 16-20
Part, nano-attapulgite 6-8 parts, lithopone 30-40 parts, casein fibre 4-8 parts, poly- boric acid ester fiber 8-12 parts, xanthans 6-
12 parts, gelatin 8-10 parts, pigment 10-12 parts, wetting agent 2-4 parts, dispersant 2-4 parts, defoamer 2-4 parts, deionized water 150-
200 parts.
2. the water paint of water resistant abrasive proof according to claim 1, it is characterised in that pigment includes rutile-type titanium dioxide
It is more than one or both of titanium, zinc oxide or lithopone.
3. the water paint of water resistant abrasive proof according to claim 1 or claim 2, it is characterised in that defoamer includes by weight：
Epoxidized soybean oil 10-20 parts, vinyl-terminated silicone fluid 6-10 parts, OPEO 2-4 parts, zinc soap salt 12-14 parts, poly- second
Alkene ether 4-8 parts.
4. according to the water paint of any one of the claim 1-3 water resistant abrasive proofs, it is characterised in that galapectite compound is adopted
Prepared with following technique：Peanut powder, water are stirred, maleic anhydride is added and continues to stir, adds silane coupler stirring, then
Add potassium peroxydisulfate to continue to stir, filter, dry, then addition galapectite, water are well mixed, addition hydrogen peroxide, heating stirring,
Vacuum filtration, dry, add toluene ultrasonic disperse, washed using acetone, be filtered by vacuum, dry, add maleic anhydride, first
Benzene ultrasonic disperse, the lower heating stirring of nitrogen protection, vacuum filtration, is washed, vacuum drying obtains galapectite compound using acetone.
5. according to the water paint of any one of the claim 1-4 water resistant abrasive proofs, it is characterised in that galapectite compound is adopted
Prepared with following technique：10-20 parts peanut powder, 60-70 parts water are stirred by weight, 1-2 part maleic anhydrides is added and continues to stir
Mix, add the stirring of 0.5-1 parts silane coupler, be subsequently added into 1-2 part potassium peroxydisulfates and continue to stir, filter, dry, Ran Houjia
Enter 30-50 parts galapectite, 120-160 part water is well mixed, add 20-30 part hydrogen peroxide, heating stirring, be filtered by vacuum, dry,
120-160 part toluene ultrasonic disperses are added, are washed using acetone, are filtered by vacuum, are dried, add 1.5-2.5 part maleic acids
Acid anhydride, 120-160 part toluene ultrasonic disperses, the lower heating stirring of nitrogen protection, vacuum filtration, are washed using acetone, are dried in vacuo
To galapectite compound.
6. according to the water paint of any one of the claim 1-5 water resistant abrasive proofs, it is characterised in that galapectite compound is adopted
Prepared with following technique：10-20 parts peanut powder, 60-70 parts water are stirred into 20-40min, whipping temp 70-80 by weight
DEG C, add 1-2 part maleic anhydrides and continue to stir 10-20min, add 0.5-1 parts silane coupler stirring 10-20min, then
Add 1-2 part potassium peroxydisulfates to continue to stir 30-50min, filter, dry, then add 30-50 parts galapectite, 120-160 part water
It is well mixed, 20-30 part hydrogen peroxide is added, 80-90 DEG C of stirring 6-10h is warming up to, is filtered by vacuum, dries, add 120-160 parts
Toluene ultrasonic disperse 40-60min, is washed using acetone, is filtered by vacuum, and is dried, addition 1.5-2.5 parts maleic anhydride,
120-160 part toluene ultrasonic disperse 40-60min, 170-180 DEG C of stirring 30-40min is warming up under nitrogen protection, is filtered by vacuum,
Washed using acetone, vacuum drying obtains galapectite compound.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710522894.4A CN107459931A (en) | 2017-06-30 | 2017-06-30 | A kind of water paint of water resistant abrasive proof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710522894.4A CN107459931A (en) | 2017-06-30 | 2017-06-30 | A kind of water paint of water resistant abrasive proof |
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| CN108609991A (en) * | 2018-04-26 | 2018-10-02 | 蚌埠市宝运商品混凝土有限公司 | A kind of preparation method of high thermal insulation concrete brick |
| CN112720829A (en) * | 2020-12-08 | 2021-04-30 | 苏州良浦住宅工业有限公司 | Reverse beating process for air conditioner plate component production |
| CN116041997A (en) * | 2022-12-24 | 2023-05-02 | 上海墙特节能材料有限公司 | Inorganic dry powder coating and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108609991A (en) * | 2018-04-26 | 2018-10-02 | 蚌埠市宝运商品混凝土有限公司 | A kind of preparation method of high thermal insulation concrete brick |
| CN112720829A (en) * | 2020-12-08 | 2021-04-30 | 苏州良浦住宅工业有限公司 | Reverse beating process for air conditioner plate component production |
| CN116041997A (en) * | 2022-12-24 | 2023-05-02 | 上海墙特节能材料有限公司 | Inorganic dry powder coating and preparation method thereof |
| CN116041997B (en) * | 2022-12-24 | 2024-01-09 | 上海墙特节能材料有限公司 | Inorganic dry powder coating and preparation method thereof |
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Application publication date: 20171212 |
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| WW01 | Invention patent application withdrawn after publication |