CN107447493A - A kind of cleaned method of short silk flosssilk wadding silk - Google Patents
A kind of cleaned method of short silk flosssilk wadding silk Download PDFInfo
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- CN107447493A CN107447493A CN201710573479.1A CN201710573479A CN107447493A CN 107447493 A CN107447493 A CN 107447493A CN 201710573479 A CN201710573479 A CN 201710573479A CN 107447493 A CN107447493 A CN 107447493A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L1/00—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
- D06L1/12—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using aqueous solvents
- D06L1/18—Working under pressure in closed vessels
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/50—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs by irradiation or ozonisation
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/005—Compositions containing perfumes; Compositions containing deodorants
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2246—Esters of unsaturated carboxylic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
- D06M2101/12—Keratin fibres or silk
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Abstract
The invention discloses a kind of method that short silk flosssilk wadding silk is cleaned, it is characterised in that including following aspect：（1）Humidification, silk quilt moisture is promoted to 40% 50% using humidifier；（2）Sterilization cleaning, humidification silk is placed in the distillation layer of autoclave, carries out HIGH TEMPERATURE PURGE and Low-temperature cleaning respectively；（3）Soften stacte, cleaning silk is placed into steamer distillation layer, silk quilt fumigated using light-coloured vinegar, softening agent and concentrated extracting solution respectively；（4）Drying：Softening silk is dried to moisture 13% 17%；（5）Ozone decolorization, the ozone of its volume 9% 12% is passed through in insulating box, decolorization is carried out to silk quilt.Short silk flosssilk wadding silk quilt is cleaned by using the inventive method, sterilizing rate, flexibility and the fragrance of silk can be improved, shorten the surface cleaning cycle, and reduces cleaning cost 12.6%.
Description
Technical field
The invention belongs to silk quilt processing technique field, and in particular to a kind of cleaned method of short silk flosssilk wadding silk.
Background technology
Silk main component is pure natural animal protein fibre, and it constructs the degree of approximation for having 87% with the skin of the mankind, includes
A variety of necessary amino acid of human body, have it is windproof, dehumidify, calm the nerves, nourishing and the effect of balanced human's skin.Silk is smooth, it is ventilative,
Softly, moisture absorption, not perverse the features such as itching and be antistatic are the superior selection of personal clothing, and the silk quilt for making material with silk has more
There are the advantageous qualities and advantage such as personal warming, fluffy soft, Breathable healthcare, deep sleep, it is deep to be liked by people.But
It is that silk quilt can largely be grown using bacterium for a long time, the decline of yellowish, pliability becomes hardened, causes under usage comfort
Drop；Long silk flosssilk wadding silk quilt influences the use of silk quilt because its silk quality length gets wet easy adhesion after cleaning, and short silk flosssilk wadding silk quilt
Its silk quality is short, and the cleaning posterior synechia degree that gets wet is low, can carry out appropriate washing but need to clean after dismounting again, tedious process, clear
Wash cost height, it is difficult to carry out batch cleaning.Patent application：CN201611218519, the preparation method of silk cotton quilt, there is provided one
The method that the old silk quilt of kind recycles again, it is technically characterized in that：（1）8-10min is cooked through boiling water, stripping is placed in after cleaning
Silk is peeled off into from pond；Old silk quilt need to be disassembled again, process is numerous and diverse, utilizes cost height；（2）Planted to peeling off to add in pond
Thing additive, containing plant components such as a variety of saponin(es, polyphenol, there is sterilization, decontamination and antioxidant effect；In its composition predominantly
Sterilization component, old silk quilt is not softened and decolorization, and more pliability is low after re-working, and hair still occurs in silk quilt
It is yellow；（3）Every layer overlays cotton-wool during laying, and the silk quilt quality re-worked after addition cotton-wool is harder, silk quilt comfortableness and product
Matter declines.
The content of the invention
The present invention is directed to the problem of existing：Silk is cleaned, and a large amount of bacteria breeds, face occur after silk quilt long-term use
Color jaundice, pliability, which decline, becomes hardened, and usage comfort declines；If silk quality adhesion occurs after being cleaned using water, product are used
It matter degradation, can be discarded after most silk quilt long-time use, cause the wasting of resources, short silk flosssilk wadding silk quilt can carry out appropriate water
Wash, but need to disassemble again, process is numerous and diverse, cost is high.And patent application：The preparation method of silk cotton quilt, the old silkworm provided
Silk is utilized method：Old silk quilt is disassembled again, process is numerous and diverse, utilizes cost height；Old silk quilt is not softened and decolouring at
Reason, more pliability is low after re-working, and jaundice still occurs in silk quilt；After addition cotton-wool the silk quilt quality that re-works compared with
Firmly, silk quilt comfortableness and quality decline.To be cleaned to solve the above problems, the invention provides a kind of short silk flosssilk wadding silk
Method.
The present invention is achieved by the following technical solutions：
A kind of cleaned method of short silk flosssilk wadding silk, comprises the following steps：
（1）Humidification：The silk for removing quilt cover is placed into humidifying chamber, is promoted to silk quilt moisture using humidifier
40%-50%, improves when water content prevents high temperature sterilization that temperature is too high, causes silk quality to be denatured, humidification silk quilt is made；
（2）Sterilization cleaning：The distillation layer that autoclave is positioned over after silk is folded will be humidified, alcohol quality is added in pressure cooker
Concentration is 35%-40% water, and alcohol can play sterilization and the cleaning dirty effect of organic, cover pot cover, carry out high-pressure wash；First
HIGH TEMPERATURE PURGE is carried out, pressure 1.7-2.2Pa, 97-104 DEG C of temperature, breed bacteria in silk quilt, scavenging period 41- can be killed
45min, adds its quality 14%-17% concentrated cleaning solutions into pressure cooker water, and the plant extract component in concentrated cleaning solutions can
It is dirty in removing silk quilt, and bactericidal action is played, then Low-temperature cleaning is carried out, pressure 1.7-2.2Pa, 78-83 DEG C of temperature, low temperature
Plant component activity in lower holding concentrated cleaning solutions, improves cleaning and bactericidal effect, scavenging period 50-55min, obtains cleaning silk
Quilt；
（3）Soften stacte：Cleaning silk is placed into steamer distillation layer, its water quality 7%-9% light-coloured vinegar is added into steamer water,
Light-coloured vinegar acidity can separate the silk quality of adhesion, play emollescence, the boiling 24-28min at a temperature of 62-65 DEG C, then to steaming
Its water quality 6%-7% softening agent is added in pot water, contains citric acid, malic acid and other plant acid compositions in softening agent, can
Carry out a step to decompose silk adhesion part, play softening function, improve comfort level, the boiling 30- at a temperature of 85-89 DEG C
35min；Water in steamer is replaced by clear water, the boiling 10-15min at a temperature of 53-56 DEG C, then adds it into steamer water
Quality 3%-4% concentrated extracting solution, the delicate fragrance composition of a variety of flowers is extracted, nature can be kept to clean after being fumigated to silk, improved
Sleep quality, the constant boiling 26-30min of keeping temperature, obtains softening silk quilt；
（4）Drying：Softening silk is dried to moisture 13%-17%, obtains drying silk quilt；
（5）Ozone decolorization：Drying silk is placed into insulating box, its volume 9%-12% ozone is passed through into insulating box, it is smelly
Oxygen has Strong oxdiative ability and bactericidal action, will not cause to remain after carrying out decolorization, safe, in 44-47 DEG C of temperature
Lower decolouring 28-32min, silk quilt after must cleaning.
Step（2）Described concentrated cleaning solutions, its compound method are：
Azedarach 17-21 parts, camphortree leaf 9-11 parts, clove leaf 5-7 parts, tuber of pinellia 3-5 parts, Siberian cocklebur 1-3 are weighed according to quality meter part
Part, lavender 2-4 parts, are put into pot and boil 1-2h, obtain cleaning extract solution；Its quality is added in the backward cleaning extract solution of cooling
10% absolute ethyl alcohol, original volume 1/5 is then concentrated under 43-47 DEG C of low temperature, concentrated cleaning solutions are made.
Step（3）Described softening agent, it is respectively configured to sub-prime gauge part and is：Water 45-50 parts, citric acid 17-21 parts, apple
Tartaric acid 10-13 parts, orange leaf extract 4-6 parts, sulfonated castor oil 1-2 parts.
Step（3）Described concentrated extracting solution, its compound method are：
Weigh Jasmine 12-15 parts, gardenia 9-11 parts, orchid 4-6 parts, cordate telosma 1-3 parts according to quality meter part, after mixing
10-13min is soaked in water, is subsequently placed in grinding mill and smashes, flower liquid must be mixed；2-3 times of its quality is added into mixing flower liquid
Absolute ethyl alcohol, the supersonic oscillations 24-28min under 33-37 DEG C of constant temperature, extract solution is made through centrifugal filtration；Extract solution is existed
The 1/4 of its original volume is concentrated at a temperature of 33-37 DEG C, concentrated extracting solution is made.
The present invention has advantages below compared with prior art：Sterilization cleaning, the short silk flosssilk wadding silk for removing quilt cover is humidified
To moisture 40%-50%, high-moisture is kept, prevents that silk quilt silk quality is met high-temperature denatured in high temperature sterilization environment；Use
Alcohol content 35%-40% water has sterilization and high volatile, can reduce sterilization temperature in 97-104 DEG C of high temperature sterilization, alcohol,
Accelerate sterilization speed, and silk quilt is cleaned, remove pollution；Using concentrated cleaning solutions in 78-83 DEG C of cleaning treatment, concentration
For cleaning fluid by plant component extractions such as azedarach, camphortree leafs, it contains plant-derived sterilization component, silk quilt can be carried out effective
Sterilization, and infiltrate into inside silk quilt and be detained, long-term antibacterial and bactericidal action is played, sterilizing rate is high, green, security
Height, and it contains alkaloid component, can carry out high-efficiency washing to silk.Softening stacte, silk has stronger acidproof property,
Using low in acidity light-coloured vinegar, silk quilt silk adhesion part can be carried out acidifying separation by its acid ingredient, and softening effect is played to silk quilt
Fruit, improve silk quilt comfort level after processing；Reuse softening agent and carry out secondary softening, contain citric acid, malic acid in softening agent
And other plant acid compositions, a step can be carried out silk adhesion part is decomposed, play softening function, improve comfort level, tool
The advantage such as have softening degree height, safety non-pollution, processing cost low；Using colored extract component, silk quilt is fumigated, carried
The fragrance component for containing a variety of flowers in liquid is taken, stifling rear silk quilt has delicate fragrance, and its composition is naturally safe.Ozone decolorization, for a long time
Silk quilt yellowish after use, makes inorganic strong oxidizer be decolourized, and oxidizer composition can be caused to remain, and with peace
Full blast danger, ozone heating state are easily decomposed to oxygen and oxonium ion, have strong oxidizing property and bactericidal action, and silk quilt is carried out
Ozone processing, effective and rapid can decolourize, and play bactericidal action, will not cause hazard residue, have the spies such as efficient, safety
Point.
Embodiment
Embodiment 1：
A kind of cleaned method of short silk flosssilk wadding silk, comprises the following steps：
（1）Humidification：The silk for removing quilt cover is placed into humidifying chamber, is promoted to silk quilt moisture using humidifier
40%-50%, improves when water content prevents high temperature sterilization that temperature is too high, causes silk quality to be denatured, humidification silk quilt is made；
（2）Sterilization cleaning：The distillation layer that autoclave is positioned over after silk is folded will be humidified, alcohol quality is added in pressure cooker
Concentration is 36% water, and alcohol can play sterilization and the cleaning dirty effect of organic, cover pot cover, carry out high-pressure wash；First carry out
HIGH TEMPERATURE PURGE, pressure 1.9Pa, 98 DEG C of temperature, breed bacteria in silk quilt, scavenging period 42min, into pressure cooker water can be killed
Add the concentrated cleaning solutions of its quality 15%, the plant extract component in concentrated cleaning solutions can be removed dirty in silk quilt, and play
Bactericidal action, then Low-temperature cleaning is carried out, pressure 1.9Pa, 80 DEG C of temperature, keep plant component in concentrated cleaning solutions to live under low temperature
Property, cleaning and bactericidal effect, scavenging period 52min are improved, obtains cleaning silk quilt；
（3）Soften stacte：Cleaning silk is placed into steamer distillation layer, the light-coloured vinegar of its water quality 7.5% is added into steamer water,
Light-coloured vinegar acidity can separate the silk quality of adhesion, play emollescence, the boiling 25min at a temperature of 63 DEG C, then into steamer water
The softening agent of its water quality 6.2% is added, contains citric acid, malic acid and other plant acid compositions in softening agent, a step can be carried out
Silk adhesion part is decomposed, plays softening function, improves comfort level, the boiling 32min at a temperature of 86 DEG C；By in steamer
Water be replaced by clear water, the boiling 12min at a temperature of 54 DEG C, the concentration extraction of its quality 3.5% is then added into steamer water
Liquid, a variety of colored delicate fragrance compositions are extracted, nature can be kept to clean after being fumigated to silk, improve sleep quality, keeping temperature is constant
Boiling 27min, obtain softening silk quilt；
（4）Drying：Softening silk is dried to moisture 14%, obtains drying silk quilt；
（5）Ozone decolorization：Drying silk is placed into insulating box, the ozone of its volume 10%, ozone tool are passed through into insulating box
There are Strong oxdiative ability and bactericidal action, will not cause to remain in silk quilt after carrying out decolorization, it is safe, in 45 DEG C of temperature
Lower decolouring 29min, silk quilt after must cleaning.
Step（2）Described concentrated cleaning solutions, its compound method are：
18 parts of azedarach, 9.5 parts of camphortree leaf are weighed according to quality meter part, 5.5 parts of clove leaf, 3.2 parts of the tuber of pinellia, 1.5 parts of Siberian cocklebur, are smoked
2.2 parts of clothing grass, is put into pot and boils 1.5h, obtain cleaning extract solution；The nothing of its quality 10% is added in the backward cleaning extract solution of cooling
Water-ethanol, original volume 1/5 is then concentrated under 44 DEG C of low temperature, concentrated cleaning solutions are made.
Step（3）Described softening agent, it is respectively configured to sub-prime gauge part and is：46 parts of water, 18 parts of citric acid, malic acid 11
Part, 4.5 parts of orange leaf extract, 1.4 parts of sulfonated castor oil.
Step（3）Described concentrated extracting solution, its compound method are：
13 parts of Jasmine, 9.5 parts of gardenia, 4.3 parts of orchid, 1.5 parts of cordate telosma are weighed according to quality meter part, after mixing in water
11min is soaked, is subsequently placed in grinding mill and smashes, flower liquid must be mixed；The anhydrous second of 2 times of its quality is added into mixing flower liquid
Alcohol, the supersonic oscillations 25min under 35 DEG C of constant temperature, extract solution is made through centrifugal filtration；Extract solution is concentrated at a temperature of 34 DEG C
To the 1/4 of its original volume, concentrated extracting solution is made.
Embodiment 2：
A kind of cleaned method of short silk flosssilk wadding silk, comprises the following steps：
（1）Humidification：The silk for removing quilt cover is placed into humidifying chamber, is promoted to silk quilt moisture using humidifier
40%-50%, improves when water content prevents high temperature sterilization that temperature is too high, causes silk quality to be denatured, humidification silk quilt is made；
（2）Sterilization cleaning：The distillation layer that autoclave is positioned over after silk is folded will be humidified, alcohol quality is added in pressure cooker
Concentration is 39% water, and alcohol can play sterilization and the cleaning dirty effect of organic, cover pot cover, carry out high-pressure wash；First carry out
HIGH TEMPERATURE PURGE, pressure 2.0Pa, 101 DEG C of temperature, breed bacteria in silk quilt, scavenging period 44min, to pressure cooker water can be killed
The middle concentrated cleaning solutions for adding its quality 16%, the plant extract component in concentrated cleaning solutions can be removed dirty in silk quilt, and rise
To bactericidal action, then Low-temperature cleaning is carried out, pressure 2.0Pa, 81 DEG C of temperature, keep plant component in concentrated cleaning solutions to live under low temperature
Property, cleaning and bactericidal effect, scavenging period 54min are improved, obtains cleaning silk quilt；
（3）Soften stacte：Cleaning silk is placed into steamer distillation layer, the light-coloured vinegar of its water quality 8.5% is added into steamer water,
Light-coloured vinegar acidity can separate the silk quality of adhesion, play emollescence, the boiling 27min at a temperature of 64 DEG C, then into steamer water
The softening agent of its water quality 6.8% is added, contains citric acid, malic acid and other plant acid compositions in softening agent, a step can be carried out
Silk adhesion part is decomposed, plays softening function, improves comfort level, the boiling 34min at a temperature of 88 DEG C；By in steamer
Water be replaced by clear water, the boiling 14min at a temperature of 55 DEG C, the concentration extraction of its quality 3.8% is then added into steamer water
Liquid, a variety of colored delicate fragrance compositions are extracted, nature can be kept to clean after being fumigated to silk, improve sleep quality, keeping temperature is constant
Boiling 29min, obtain softening silk quilt；
（4）Drying：Softening silk is dried to moisture 16%, obtains drying silk quilt；
（5）Ozone decolorization：Drying silk is placed into insulating box, the ozone of its volume 11%, ozone tool are passed through into insulating box
There are Strong oxdiative ability and bactericidal action, will not cause to remain in silk quilt after carrying out decolorization, it is safe, in 46 DEG C of temperature
Lower decolouring 31min, silk quilt after must cleaning.
Step（2）Described concentrated cleaning solutions, its compound method are：
According to quality meter part weigh 20 parts of azedarach, 10.5 parts of camphortree leaf, 6.8 parts of clove leaf, 4.6 parts of the tuber of pinellia, 2.6 parts of Siberian cocklebur,
3.2 parts of lavender, is put into pot and boils 2h, obtains cleaning extract solution；The nothing of its quality 10% is added in the backward cleaning extract solution of cooling
Water-ethanol, original volume 1/5 is then concentrated under 46 DEG C of low temperature, concentrated cleaning solutions are made.
Step（3）Described softening agent, it is respectively configured to sub-prime gauge part and is：48 parts of water, 20 parts of citric acid, malic acid 14
Part, 5.8 parts of orange leaf extract, 1.7 parts of sulfonated castor oil.
Step（3）Described concentrated extracting solution, its compound method are：
14 parts of Jasmine, 10.5 parts of gardenia, 5.4 parts of orchid, 2.8 parts of cordate telosma are weighed according to quality meter part, in water after mixing
Middle immersion 12min, is subsequently placed in grinding mill and smashes, and must mix flower liquid；The anhydrous second of 3 times of its quality is added into mixing flower liquid
Alcohol, the supersonic oscillations 27min under 36 DEG C of constant temperature, extract solution is made through centrifugal filtration；Extract solution is concentrated at a temperature of 36 DEG C
To the 1/4 of its original volume, concentrated extracting solution is made.
Contrast 1：
This contrast 1 is compared with embodiment 1, step（2）In alcohol is not used, other steps are same as Example 1.
Contrast 2：
This contrast 2 does not carry out step compared with embodiment 1（2）The use of middle concentrated cleaning solutions, other steps and the phase of embodiment 1
Together.
Contrast 3：
This contrast 3 does not carry out step compared with embodiment 2（3）The use of middle light-coloured vinegar, other steps are same as Example 2.
Contrast 4：
This contrast 4 does not carry out step compared with embodiment 2（3）The use of middle softening agent, other steps are same as Example 2.
Contrast 5：
This contrast 5 does not carry out step compared with embodiment 2（3）The use of middle concentrated extracting solution, other steps and the phase of embodiment 2
Together.
Contrast 6：
This contrast 6 does not carry out step compared with embodiment 1（5）Ozone decolorization, other steps are same as Example 1.
Control group：
Control group silk quilt uses dismantling cleaning method, and sterilization cleaning and softening stacte, ozone decolorization is not used.
To embodiment 1, embodiment 2, contrast 1, contrast 2, contrast 3, contrast 4, contrast 5, contrast 6 and control group experiment side
Case, statistics silk quilt dirty clearance, compression rebound rate, total plate count and color and fragrance evaluation.
Color and fragrance evaluation：Wherein ﹢ ﹢ ﹢ ﹢ ﹢ are fine that preferably, ﹢ ﹢ ﹢ are general to ﹢ ﹢ ﹢ ﹢, and ﹢ ﹢ are poor, and ﹢ is very poor；Respectively
It is 70 to evaluate sample size, and evaluation result is defined by the super evaluation result of sample 2/3.
Experimental data：
| Project | Dirty clearance % | Compression rebound rate % | Total plate count cfu/g | Color and fragrance evaluation |
| Embodiment 1 | 98.7% | 85.30% | 1150 | ﹢ ﹢ ﹢ ﹢ |
| Embodiment 2 | 99.1% | 84.90% | 1210 | ﹢ ﹢ ﹢ ﹢ |
| Contrast 1 | 93.3% | 83.80% | 803 | ﹢ ﹢ ﹢ |
| Contrast 2 | 94.7% | 84.10% | 587 | ﹢ ﹢ ﹢ |
| Contrast 3 | 98.9% | 84.50% | 1120 | ﹢ ﹢ ﹢ ﹢ |
| Contrast 4 | 97.8% | 76.70% | 1180 | ﹢ ﹢ ﹢ ﹢ |
| Contrast 5 | 97.1% | 75.50% | 1145 | ﹢ ﹢ |
| Contrast 6 | 98.7% | 85.10% | 870 | ﹢ ﹢ |
| Control group | 95.3% | 67.50% | 2430 | ﹢ |
Synthesis result：Short silk flosssilk wadding silk quilt is cleaned by using the inventive method, sterilizing rate, the softness of silk can be improved
Property and fragrance, shorten the surface cleaning cycle, and reduce cleaning cost 12.6%.Wherein alcohol and dense is used in sterilization cleaning
Contracting cleaning fluid, its dirty clearance are respectively increased 6.4%, 4.0%, and total plate count reduces 347cfu/g, 563cfu/g；And use white
Vinegar and softening agent, silk quilt compression rebound rate is respectively increased as 8.2%, 9.4%；Stacte is carried out using concentrated extracting solution, can be improved
The fragrance of silk quilt, and ozone decolorization method, can effectively improve silk quilt color shade.
Claims (4)
1. a kind of cleaned method of short silk flosssilk wadding silk, it is characterised in that comprise the following steps：
（1）Humidification：The silk for removing quilt cover is placed into humidifying chamber, is promoted to silk quilt moisture using humidifier
40%-50%, humidification silk quilt is made；
（2）Sterilization cleaning：The distillation layer that autoclave is positioned over after silk is folded will be humidified, alcohol quality is added in pressure cooker
Concentration is 35%-40% water, covers pot cover, carries out high-pressure wash；First carry out HIGH TEMPERATURE PURGE, pressure 1.7-2.2Pa, temperature 97-
104 DEG C, scavenging period 41-45min, its quality 14%-17% concentrated cleaning solutions are added into pressure cooker water, then to carry out low temperature clear
Wash, pressure 1.7-2.2Pa, 78-83 DEG C of temperature, scavenging period 50-55min, obtain cleaning silk quilt；
（3）Soften stacte：Cleaning silk is placed into steamer distillation layer, its water quality 7%-9% light-coloured vinegar is added into steamer water,
The boiling 24-28min at a temperature of 62-65 DEG C, its water quality 6%-7% softening agent is then added into steamer water, at 85-89 DEG C
At a temperature of boiling 30-35min；Water in steamer is replaced by clear water, boiling 10-15min, Ran Houxiang at a temperature of 53-56 DEG C
Its quality 3%-4% concentrated extracting solution is added in steamer water, the constant boiling 26-30min of keeping temperature, obtains softening silk quilt；
（4）Drying：Softening silk is dried to moisture 13%-17%, obtains drying silk quilt；
（5）Ozone decolorization：Drying silk is placed into insulating box, its volume 9%-12% ozone is passed through into insulating box,
Decolourize 28-32min at a temperature of 44-47 DEG C, silk quilt after must cleaning.
2. the cleaned method of short silk flosssilk wadding silk as claimed in claim 1, it is characterised in that step（2）Described concentration cleaning
Liquid, its compound method are：
Azedarach 17-21 parts, camphortree leaf 9-11 parts, clove leaf 5-7 parts, tuber of pinellia 3-5 parts, Siberian cocklebur 1-3 are weighed according to quality meter part
Part, lavender 2-4 parts, are put into pot and boil 1-2h, obtain cleaning extract solution；Its quality is added in the backward cleaning extract solution of cooling
10% absolute ethyl alcohol, original volume 1/5 is then concentrated under 43-47 DEG C of low temperature, concentrated cleaning solutions are made.
3. the cleaned method of short silk flosssilk wadding silk as claimed in claim 1, it is characterised in that step（3）Described softening agent, its
Respectively being configured to sub-prime gauge part is：Water 45-50 parts, citric acid 17-21 parts, malic acid 10-13 parts, orange leaf extract 4-6 parts,
Sulfonated castor oil 1-2 parts.
4. the cleaned method of short silk flosssilk wadding silk as claimed in claim 1, it is characterised in that step（3）Described concentration extraction
Liquid, its compound method are：
Weigh Jasmine 12-15 parts, gardenia 9-11 parts, orchid 4-6 parts, cordate telosma 1-3 parts according to quality meter part, after mixing
10-13min is soaked in water, is subsequently placed in grinding mill and smashes, flower liquid must be mixed；2-3 times of its quality is added into mixing flower liquid
Absolute ethyl alcohol, the supersonic oscillations 24-28min under 33-37 DEG C of constant temperature, extract solution is made through centrifugal filtration；Extract solution is existed
The 1/4 of its original volume is concentrated at a temperature of 33-37 DEG C, concentrated extracting solution is made.
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| CN112401598A (en) * | 2020-10-27 | 2021-02-26 | 广西时宜农业科技有限公司 | Preparation method of silk quilt |
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