CN107442289A - A kind of collecting agent for alleviating high concentration low temperature gel and preparation method thereof - Google Patents
A kind of collecting agent for alleviating high concentration low temperature gel and preparation method thereof Download PDFInfo
- Publication number
- CN107442289A CN107442289A CN201710463810.4A CN201710463810A CN107442289A CN 107442289 A CN107442289 A CN 107442289A CN 201710463810 A CN201710463810 A CN 201710463810A CN 107442289 A CN107442289 A CN 107442289A
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- CN
- China
- Prior art keywords
- parts
- grease
- collecting agent
- low temperature
- high concentration
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D1/00—Flotation
- B03D1/001—Flotation agents
- B03D1/004—Organic compounds
- B03D1/012—Organic compounds containing sulfur
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D2201/00—Specified effects produced by the flotation agents
- B03D2201/02—Collectors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D2203/00—Specified materials treated by the flotation agents; specified applications
- B03D2203/02—Ores
- B03D2203/04—Non-sulfide ores
- B03D2203/06—Phosphate ores
Abstract
The present invention relates to a kind of collecting agent for alleviating high concentration low temperature gel and preparation method thereof, collecting agent is made up of following substances, each material is by weight, 60 70 parts of palm oil grease, 40 30 parts of hair oil extracted from rice husks grease, counted using the mixture after palm oil grease, hair oil extracted from rice husks fat saponification as 100 parts, then add 8 10 parts of dispersion-ness surface activity agent, preparation method：60 70 parts of palm oil greases, 40 30 parts of hair oil extracted from rice husks greases are mixed, heating the mixture to 100~120 DEG C makes it fully dissolve mixing, add 150 170 parts of sodium hydroxides, the saponification 50-70 minutes under the conditions of 70 90 DEG C, counted again using the mixture after saponification as 100 parts, it is well mixed to add 8 10 parts of dispersion-ness surface activity agent, the collecting agent for alleviating high concentration low temperature gel is made.Collecting agent of the present invention can not only ensure qualified floatation indicators, moreover it is possible to effectively alleviate make up a prescription no heat-retaining condition and with concentration it is higher select factory's medicament gel problem.
Description
Technical field
The present invention relates to mineral froth flotation collector, more particularly to a kind of collecting agent for alleviating high concentration low temperature gel and
Its preparation method
Background technology
Phosphate rock floating is progressively expanding as the ore dressing mode that a kind of skill is ripe, cost is low using area.China makees
Big country is laid in for ore, ore distribution and its extensively, therefore select that factory is also nationwide and condition differs.Select factory's condition straight
Connect determine medicament configuration and storage condition, some very colds and make up a prescription head tank without stirring attemperator or for save people
Work labour cost, the problem of all suffering from medicament gel more than 4% ore dressing plant with concentration.Medicament gel does not only result in medicament work
Property decline and influence pharmacy effect, while easily block medicament conveyance conduit and cause stop production to overhaul, it is therefore very harmful.
The content of the invention
The defects of purpose of the present invention is in order to overcome above-mentioned prior art there are problems that and, and provide and a kind of alleviate high concentration
The collecting agent of low temperature gel, a kind of collecting agent for alleviating high concentration low temperature gel provided by the invention can meet to select factory's internal control
Ensure that gel does not possess good mobility still to medicament high concentration low temperature while index.Used in the collecting agent of the present invention
Grease be different from traditional aliphatic acid, the synergy of caused glycerine and dispersion-ness surface activity agent can be effective after its saponification
Strengthen medicament dispersive property, alleviate medicament gel while medicament collecting ability is ensured.The product is meeting production target need
Solve medicament high concentration low temperature gel problem under the precondition asked, ensure production normal table operation, save manually into
It is significant in sheet.
The present invention is realized by following technology：
A kind of collecting agent for alleviating high concentration low temperature gel, it is characterised in that：It is made up of following substances, each material is by weight
Part meter, palm oil grease 60-70 parts, hair oil extracted from rice husks grease 30-40 parts, with the mixing after palm oil grease, hair oil extracted from rice husks fat saponification
Thing is 100 parts of meters, then adds dispersion-ness surface activity agent's 8-10 parts, preparation method：By 60-70 parts palm oil grease, 30-40 parts
The grease mixing of hair oil extracted from rice husks, heating the mixture to 100~120 DEG C makes it fully dissolve mixing, adds 150-170 part hydroxides
Sodium, the saponification 50-70 minutes under the conditions of 70-90 DEG C, then counted using the mixture after saponification as 100 parts, add dispersible surface and live
Property agent 8-10 parts be well mixed, be made alleviate high concentration low temperature gel collecting agent.
The palm oil grease is the palm oil grease that palmitic acid and stearic acid total content reach 80-90%.
The hair oil extracted from rice husks grease is the hair oil extracted from rice husks grease that oleic acid and linoleic acid total content reach 30-60%.
The dispersion-ness surface activity agent is neopelex.
A kind of preparation method for the collecting agent for alleviating high concentration low temperature gel, each material is by weight, it is characterised in that
Carry out according to the following steps：60-70 parts palm oil grease, 30-40 part hair oils extracted from rice husks grease are mixed, heat the mixture to 100~
120 DEG C make it fully dissolve mixing, add 150-170 part sodium hydroxides, the saponification 50-70 minutes under the conditions of 70-90 DEG C, then
Counted using the mixture after saponification as 100 parts, add dispersion-ness surface activity agent's 8-10 parts and be well mixed, it is low that alleviation high concentration is made
The collecting agent of warm gel.
Described palm oil grease, hair oil extracted from rice husks grease are all purchased from market.
Described neopelex is purchased for market.
Collecting agent provided by the invention has stable pharmaceutical collecting ability, alleviates high concentration low temperature medicament gel and good saponification
The advantages of, be applicable make up a prescription head tank without stirring attemperator or with concentration it is higher select factory, not only reduce concentrator equipment expansion
The cost of exhibition, it is significant to guarantee continuous production steady running.
The collecting agent of the present invention can be used in all phosphate rock floating workshop sections, and especially for making up a prescription, head tank is incubated without stirring
Device or with concentration it is higher select factory.Compared with other flotation collectors, the collecting agent can not only ensure that qualified flotation refers to
Mark, more can have more preferable adaptability to low temperature and high concentration.
Embodiment
With reference to embodiment, the invention will be further described, but does not limit the present invention, and each material of following examples is pressed
Parts by weight meter.Described palm oil grease, hair oil extracted from rice husks grease are all purchased from market.The neopelex is purchased for market
Put.
Embodiment 1：60 parts of palm oil grease, 40 parts of hair oil extracted from rice husks glyceride stocks are mixed, the palm oil grease is soft
Resin acid and the palm oil grease that stearic acid total content is 90%；The hair oil extracted from rice husks grease is oleic acid and linoleic acid total content is 30%
Hair oil extracted from rice husks grease；Heating the mixture to 100 DEG C makes raw material fully dissolve and mix, and 150 parts of sodium hydroxides is added, by raw material
Saponification 50 minutes under the conditions of 70 DEG C, using the mixture after saponification by 100 parts of additions, 8 parts of neopelex surfaces purchased
Activating agent is well mixed, the collecting agent finished product for the phosphate rock floating filter effect that gets a promotion.
The obtained collecting agent for alleviating high concentration low temperature gel of the present embodiment 1 is configured to the solution of 4% mass concentration, put
Constant temperature 12 hours in the water-bath that temperature is 30 DEG C are put, it is found that it fails gel and has certain fluidity, production can be met
Normal operation.
Embodiment 2：65 parts of palm oil grease, 35 parts of hair oil extracted from rice husks glyceride stocks are mixed, the palm oil grease is soft
Resin acid and the palm oil grease that stearic acid total content is 86%；The hair oil extracted from rice husks grease is oleic acid and linoleic acid total content is 35%
Hair oil extracted from rice husks grease；Heating the mixture to 110 DEG C makes raw material fully dissolve and mix, and 155 parts of sodium hydroxides is added, by raw material
Saponification 55 minutes under the conditions of 75 DEG C, using the mixture after saponification by 100 parts of additions, 8.5 parts of neopelex tables purchased
Face activating agent is well mixed, the collecting agent finished product for the phosphate rock floating filter effect that gets a promotion.
The obtained collecting agent for alleviating high concentration low temperature gel of the present embodiment 2 is configured to the solution of 4.5% mass concentration,
Constant temperature 12 hours in the water-bath that temperature is 35 DEG C are placed on, it is found that its non-gel has certain fluidity, production can met just
Often operation.
Embodiment 3：68 parts of palm oil grease, 32 parts of hair oil extracted from rice husks glyceride stocks are mixed, the palm oil grease is soft
Resin acid, the palm oil grease that stearic acid total content is 83%；The hair oil extracted from rice husks grease is oleic acid, linoleic acid total content is 33%
Hair oil extracted from rice husks grease；Heating the mixture to 115 DEG C makes raw material fully dissolve and mix, and 160 parts of sodium hydroxides is added, by raw material 78
Saponification 60 minutes under the conditions of DEG C, 9 parts of neopelex surfaces purchased are added by 100 parts using the mixture after saponification and lived
Property agent is well mixed, the collecting agent finished product for the phosphate rock floating filter effect that gets a promotion.
The obtained collecting agent for alleviating high concentration low temperature gel of the present embodiment 3 is configured to the solution of 4.8% mass concentration,
Constant temperature 12 hours in the water-bath that temperature is 38 DEG C are placed on, its non-gel is found and there is certain fluidity, production can be met
Normal operation.
Embodiment 4：70 parts of palm oil grease, 30 parts of hair oil extracted from rice husks glyceride stocks are mixed, the palm oil grease is soft
Resin acid and the palm oil grease that stearic acid total content is 88%；The hair oil extracted from rice husks grease is oleic acid and linoleic acid total content is 56%
Hair oil extracted from rice husks grease；Heating the mixture to 118 DEG C makes raw material fully dissolve and mix, and 165 parts of sodium hydroxides is added, by raw material
Saponification 65 minutes under the conditions of 80 DEG C, using the mixture after saponification by 100 parts of additions, 9.5 parts of neopelex tables purchased
Face activating agent is well mixed, the collecting agent finished product for the phosphate rock floating filter effect that gets a promotion.
The obtained collecting agent for alleviating high concentration low temperature gel of the present embodiment 4 is configured to the solution of 5% mass concentration, put
Constant temperature 12 hours in the water-bath that temperature is 40 DEG C are put, its non-gel is found and there is certain fluidity, production can met just
Often operation.
Embodiment 5：63 parts of palm oil grease, 37 parts of hair oil extracted from rice husks glyceride stocks are mixed, the palm oil grease is soft
Resin acid and the palm oil grease that stearic acid total content is 80%；The hair oil extracted from rice husks grease is oleic acid and linoleic acid total content is 60%
Hair oil extracted from rice husks grease；Heating the mixture to 120 DEG C makes raw material fully dissolve and mix, and 170 parts of sodium hydroxides is added, by raw material
Saponification 70 minutes under the conditions of 90 DEG C, using the mixture after saponification by 100 parts of additions, 10 parts of neopelex tables purchased
Face activating agent is well mixed, the collecting agent finished product for the phosphate rock floating filter effect that gets a promotion.
The obtained collecting agent for alleviating high concentration low temperature gel of the present embodiment 5 is configured to the solution of 4.2% mass concentration,
Constant temperature 12 hours in the water-bath that temperature is 32 DEG C are placed on, its non-gel is found and there is certain fluidity, production can be met
Normal operation.
Claims (5)
- A kind of 1. collecting agent for alleviating high concentration low temperature gel, it is characterised in that：It is made up of following substances, each material is by weight Meter, palm oil grease 60-70 parts, hair oil extracted from rice husks grease 30-40 parts, with the mixture after palm oil grease, hair oil extracted from rice husks fat saponification Counted for 100 parts, then add dispersion-ness surface activity agent's 8-10 parts, preparation method：By 60-70 parts palm oil grease, 30-40 part hairs Oil extracted from rice husks grease mixes, and heating the mixture to 100~120 DEG C makes it fully dissolve mixing, adds 150-170 part sodium hydroxides, The saponification 50-70 minutes under the conditions of 70-90 DEG C, then counted using the mixture after saponification as 100 parts, add dispersible surface's activity Agent 8-10 parts are well mixed, and the collecting agent for alleviating high concentration low temperature gel is made.
- A kind of 2. collecting agent for alleviating high concentration low temperature gel according to claim 1, it is characterised in that：The palm oil Grease is the palm oil grease that palmitic acid and stearic acid total content reach 80-90%.
- A kind of 3. collecting agent for alleviating high concentration low temperature gel according to claim 1, it is characterised in that：The hair oil extracted from rice husks Grease is the hair oil extracted from rice husks grease that oleic acid and linoleic acid total content reach 30-60%.
- A kind of 4. collecting agent for alleviating high concentration low temperature gel according to claim 1, it is characterised in that：The dispersiveness Surfactant is neopelex.
- 5. described in claim 1 it is a kind of alleviate high concentration low temperature gel collecting agent preparation method, each material by weight, It is characterized in that carry out according to the following steps：60-70 parts palm oil grease, 30-40 part hair oils extracted from rice husks grease are mixed, by mixture plus Hot to 100~120 DEG C make it fully dissolve mixing, add 150-170 part sodium hydroxides, the saponification 50- under the conditions of 70-90 DEG C 70 minutes, then counted using the mixture after saponification as 100 parts, add dispersion-ness surface activity agent's 8-10 parts and be well mixed, be made slow Solve the collecting agent of high concentration low temperature gel.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710463810.4A CN107442289A (en) | 2017-06-19 | 2017-06-19 | A kind of collecting agent for alleviating high concentration low temperature gel and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710463810.4A CN107442289A (en) | 2017-06-19 | 2017-06-19 | A kind of collecting agent for alleviating high concentration low temperature gel and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107442289A true CN107442289A (en) | 2017-12-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710463810.4A Pending CN107442289A (en) | 2017-06-19 | 2017-06-19 | A kind of collecting agent for alleviating high concentration low temperature gel and preparation method thereof |
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Citations (9)
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|---|---|---|---|---|
| US7624878B2 (en) * | 2006-02-16 | 2009-12-01 | Nalco Company | Fatty acid by-products and methods of using same |
| CN101791591A (en) * | 2010-01-05 | 2010-08-04 | 湖北富邦化工科技有限公司 | Phosphorite low-temperature foam flotation collector and preparation method thereof |
| CN102407188A (en) * | 2010-09-21 | 2012-04-11 | 孝感市天翔矿业科技有限公司 | Method for preparing collector for floatation of coarse grains of oxidized ore at normal temperature |
| CN103041928A (en) * | 2012-12-21 | 2013-04-17 | 张飞 | Carbonate type phosphorite foam flotation reagent and preparation method thereof |
| CN104437884A (en) * | 2014-11-05 | 2015-03-25 | 中国地质科学院矿产综合利用研究所 | Normal-temperature efficient collector for sedimentary silicon-calcium collophanite and preparation method thereof |
| CN104607321A (en) * | 2014-12-11 | 2015-05-13 | 云南铜业胜威化工有限公司 | Collophanite froth flotation collecting agent and preparation method thereof |
| CN105435969A (en) * | 2015-12-09 | 2016-03-30 | 湖北富邦科技股份有限公司 | Collecting agent improving filtering effect for phosphorite floatation and preparing method of collecting agent |
| CN106111347A (en) * | 2016-08-08 | 2016-11-16 | 湖北富邦科技股份有限公司 | A kind of except the rock phosphate in powder collecting agent in reverse floatation of calcite |
| CN106111346A (en) * | 2016-07-27 | 2016-11-16 | 湖北富邦科技股份有限公司 | A kind of phosphorite flotation collector efficiently removing sesquichloride and preparation method thereof |
-
2017
- 2017-06-19 CN CN201710463810.4A patent/CN107442289A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7624878B2 (en) * | 2006-02-16 | 2009-12-01 | Nalco Company | Fatty acid by-products and methods of using same |
| CN101791591A (en) * | 2010-01-05 | 2010-08-04 | 湖北富邦化工科技有限公司 | Phosphorite low-temperature foam flotation collector and preparation method thereof |
| CN102407188A (en) * | 2010-09-21 | 2012-04-11 | 孝感市天翔矿业科技有限公司 | Method for preparing collector for floatation of coarse grains of oxidized ore at normal temperature |
| CN103041928A (en) * | 2012-12-21 | 2013-04-17 | 张飞 | Carbonate type phosphorite foam flotation reagent and preparation method thereof |
| CN104437884A (en) * | 2014-11-05 | 2015-03-25 | 中国地质科学院矿产综合利用研究所 | Normal-temperature efficient collector for sedimentary silicon-calcium collophanite and preparation method thereof |
| CN104607321A (en) * | 2014-12-11 | 2015-05-13 | 云南铜业胜威化工有限公司 | Collophanite froth flotation collecting agent and preparation method thereof |
| CN105435969A (en) * | 2015-12-09 | 2016-03-30 | 湖北富邦科技股份有限公司 | Collecting agent improving filtering effect for phosphorite floatation and preparing method of collecting agent |
| CN106111346A (en) * | 2016-07-27 | 2016-11-16 | 湖北富邦科技股份有限公司 | A kind of phosphorite flotation collector efficiently removing sesquichloride and preparation method thereof |
| CN106111347A (en) * | 2016-08-08 | 2016-11-16 | 湖北富邦科技股份有限公司 | A kind of except the rock phosphate in powder collecting agent in reverse floatation of calcite |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171208 |