CN107421819A - Degraded except ammonia nitrogen refuse soil and compress visualizer - Google Patents
Degraded except ammonia nitrogen refuse soil and compress visualizer Download PDFInfo
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- CN107421819A CN107421819A CN201710445963.6A CN201710445963A CN107421819A CN 107421819 A CN107421819 A CN 107421819A CN 201710445963 A CN201710445963 A CN 201710445963A CN 107421819 A CN107421819 A CN 107421819A
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- gas
- visualizer
- ammonia nitrogen
- test cavity
- test
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- 239000002689 soil Substances 0.000 title claims abstract description 49
- XKMRRTOUMJRJIA-UHFFFAOYSA-N ammonia nh3 Chemical compound N.N XKMRRTOUMJRJIA-UHFFFAOYSA-N 0.000 title claims abstract description 26
- 238000012360 testing method Methods 0.000 claims abstract description 82
- 239000007789 gas Substances 0.000 claims abstract description 70
- 238000009280 upflow anaerobic sludge blanket technology Methods 0.000 claims abstract description 22
- 238000001514 detection method Methods 0.000 claims abstract description 11
- 238000006396 nitration reaction Methods 0.000 claims description 37
- 230000006835 compression Effects 0.000 claims description 16
- 238000007906 compression Methods 0.000 claims description 16
- 238000011068 loading method Methods 0.000 claims description 11
- 238000011084 recovery Methods 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 6
- 238000010992 reflux Methods 0.000 claims description 6
- 241000108664 Nitrobacteria Species 0.000 claims description 5
- 239000010802 sludge Substances 0.000 claims description 5
- 241000894006 Bacteria Species 0.000 claims description 3
- 230000003139 buffering effect Effects 0.000 claims description 2
- 239000000969 carrier Substances 0.000 claims description 2
- 238000001914 filtration Methods 0.000 claims description 2
- 238000002474 experimental method Methods 0.000 abstract description 7
- 238000000034 method Methods 0.000 abstract description 7
- 238000006065 biodegradation reaction Methods 0.000 abstract description 5
- 230000008569 process Effects 0.000 abstract description 5
- 238000012163 sequencing technique Methods 0.000 abstract description 3
- 230000008859 change Effects 0.000 description 13
- 102000001999 Transcription Factor Pit-1 Human genes 0.000 description 12
- 108010040742 Transcription Factor Pit-1 Proteins 0.000 description 12
- 239000007788 liquid Substances 0.000 description 12
- 238000006073 displacement reaction Methods 0.000 description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 6
- 239000012530 fluid Substances 0.000 description 6
- 238000012544 monitoring process Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 238000002386 leaching Methods 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 238000011049 filling Methods 0.000 description 4
- 239000010813 municipal solid waste Substances 0.000 description 4
- CVTZKFWZDBJAHE-UHFFFAOYSA-N [N].N Chemical group [N].N CVTZKFWZDBJAHE-UHFFFAOYSA-N 0.000 description 3
- 229910021529 ammonia Inorganic materials 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 3
- 238000012669 compression test Methods 0.000 description 3
- 238000007596 consolidation process Methods 0.000 description 3
- 238000006731 degradation reaction Methods 0.000 description 3
- 239000000706 filtrate Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 3
- 238000004088 simulation Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 229920005479 Lucite® Polymers 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 230000008878 coupling Effects 0.000 description 2
- 238000010168 coupling process Methods 0.000 description 2
- 238000005859 coupling reaction Methods 0.000 description 2
- 238000011026 diafiltration Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 230000005764 inhibitory process Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000004926 polymethyl methacrylate Substances 0.000 description 2
- 238000004062 sedimentation Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000002910 solid waste Substances 0.000 description 2
- 238000004454 trace mineral analysis Methods 0.000 description 2
- 239000002028 Biomass Substances 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 241001453382 Nitrosomonadales Species 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000005842 biochemical reaction Methods 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000013480 data collection Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000005284 excitation Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000004745 nonwoven fabric Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000004071 soot Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/08—Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces
- G01N3/18—Performing tests at high or low temperatures
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/02—Details
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/02—Details
- G01N3/06—Special adaptations of indicating or recording means
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/02—Details
- G01N3/06—Special adaptations of indicating or recording means
- G01N3/068—Special adaptations of indicating or recording means with optical indicating or recording means
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/0014—Type of force applied
- G01N2203/0016—Tensile or compressive
- G01N2203/0019—Compressive
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/003—Generation of the force
- G01N2203/0042—Pneumatic or hydraulic means
- G01N2203/0048—Hydraulic means
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/0058—Kind of property studied
- G01N2203/0069—Fatigue, creep, strain-stress relations or elastic constants
- G01N2203/0075—Strain-stress relations or elastic constants
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/0202—Control of the test
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/022—Environment of the test
- G01N2203/0222—Temperature
- G01N2203/0226—High temperature; Heating means
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/022—Environment of the test
- G01N2203/023—Pressure
- G01N2203/0232—High pressure
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/022—Environment of the test
- G01N2203/0236—Other environments
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/06—Indicating or recording means; Sensing means
- G01N2203/0641—Indicating or recording means; Sensing means using optical, X-ray, ultraviolet, infrared or similar detectors
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- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Processing Of Solid Wastes (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
One kind compresses visualizer except the degraded of ammonia nitrogen refuse soil, including：Experimental rig, it has test cavity, and in being provided with balancing gate pit in test cavity, load frame, temperature controlled compartment are provided with the outside of test cavity, in setting having heaters, first pressure sensor and temperature sensor in temperature controlled compartment；Leachate recirculation device, leachate recirculation device include mozzle, and it is connected with UASB reactors；Hydraulic axial pressue device, it is connected with balancing gate pit；Gas reclaims detection means, and it includes gas export line, and gas export line is provided with gas analyzer；Control system.The visualizer is intended realizing automation axial pressure using hydraulic axial pressue device, confined pressure is provided in the case where simulating varying environment temperature conditionss simultaneously, solves the limitation that degraded instrument can not simulate true confined pressure, and realize and biodegradation is accelerated by leachate recirculation, test process realizes digitlization and sequencing, human error is removed, ensure that the precision and reliability of experiment.
Description
Technical field
It is more specifically, more particularly to a kind of except ammonia nitrogen refuse soil drops the present invention relates to garbage degradation equipment technical field
Decompress visualizer.
Background technology
With the fast development of China's Urbanization Construction and sharply increasing for urban population, the phenomenon of " garbage-surrounded city " is general
All over appearance.In view of the existing trash processing way in China based on sanitary landfills, therefore conventional garbage processing method is ground
Study carefully and show, the solid waste after closing, because of the differential settlement that internal degraded induces, internal air-liquid collection system rupture is special
It is not being continuously increased with landfill body volume, it is possible to serious environmental geological Hazard can be induced, occupying safety to people causes directly
Connect threat.
With the increase of rubbish from cooking proportion in solid waste, degraded produces percolate, landfill gas etc. all can two
Secondary utilization, therefore the refuse soil after closing just becomes an available biomass energy body.Refuse soil after closing
It is substantially carried out following biology, chemistry and mechanical behavior：Biochemical degradation, sedimentation and deformation, the deformation of creep, skeleton structure and solid-liquid-gas
Dynamic evolution.The percolate that resourcebility caused by degraded utilizes contains plurality of heavy metal, if being not added with management and control to percolate,
It is likely to result in the deep layer pollution of soil.
At present, traditional soil mechanics compression test consolidation apparatus can only study conventional native characteristic, and it does not account for landfill waste
Other various factors couplings act in native degradation process, and the biodegradation in soot, settling behavior typically continue decades very
Supreme a century.In consideration of it, in order to preferably study compression and Biodegradation Mechanism of the refuse soil in outside load action, state
The scientific worker for being inside engaged in environmental geotechnical have developed based on different test objectives and be only capable of testing a certain special test mesh
Degraded sedimentation experiment instrument.In the prior art, using relatively broad refuse soil degraded settlement observation instrument compression system
More using manual systems such as lever, counterweight work pulleys, requirement of both automation and precision is unable to reach on measuring accuracy,
Visualizer can only simulate one-dimensional axial compressive force simultaneously, not be inconsistent with the stressing conditions of the refuse soil of reality, and can not monitor degraded
With Coupling with Mechanics process behavior, and test post processing part it is relatively not perfect enough, larger difference, Zhi Nengyong be present in test data
Qualitatively research and analyse.Meanwhile soil mechanics compression test consolidation apparatus matching used recharge system directly oozing discharge
Filtrate sends soil sample back to, and influence of the ammonia nitrogen of percolate middle and high concentration to the activity of biotic population in degraded body etc., directly to drop
Solution speed has an impact, such as when temperature reaches more than 70 DEG C, the bioactivity of methanogen is down to zero.
The content of the invention
(1) technical problem
In summary, how to solve traditional soil mechanics compression test to flow back existing for the supporting recharge system of consolidation apparatus percolate
There is the problem of having a strong impact on to biotic population activity, become those skilled in the art's urgent problem to be solved.
(2) technical scheme
The invention provides one kind except ammonia nitrogen refuse soil degraded compression visualizer, including：
Experimental rig, the experimental rig have the test cavity for loading test material, set in the test cavity
There is balancing gate pit, the balancing gate pit is arranged in the test cavity and can form a sealed chamber with the test cavity, in
Shower nozzle is provided with the downside of the balancing gate pit, load frame, the experiment are provided with the outside of the test cavity
Chamber is arranged in the load frame, and the madial wall of the test cavity and the load frame is arranged at intervals and forms temperature controlled compartment, in institute
State and having heaters, first pressure sensor and temperature sensor are set in temperature controlled compartment；
Leachate recirculation device, the leachate recirculation device include mozzle, one end of the mozzle with it is described
The bottom wall connection of test cavity, the other end of the mozzle is provided with the leachate collection cup for collecting percolate, and described
Leachate collection cup is connected with UASB reactors by feed pump, and the UASB reactors are connected with external gas collector,
The outlet of the UASB reactors is connected with nitration reaction device, and it is anti-that the outlet of the nitration reaction device is connected with ANAMMOX
Device is answered, the outlet of the ANAMMOX reactors is connected by reflux pump with the shower nozzle, the UASB reactors, described
Nitration reaction device, the ANAMMOX reactors and the shower nozzle are in turn connected to form leachate recirculation system；
Hydraulic axial pressue device, the hydraulic axial pressue device include pressure volume controller and with the pressure
The hydraulic control hammer of power fixing fabric structure device control connection, the hydraulic control hammer are connected with the balancing gate pit；
Gas reclaims detection means, and the gas recovery detection means includes gas export line, defeated in the gas
Go out and valve is provided with pipeline, the end of the gas export line is provided with test gas collection cups, in the experiment gas
The gas analyzer for being analyzed test gas is provided with body collection cups；
Control system, the control system include control main frame and adopted with the data that the control main frame signal is connected
Collect server, the data acquisition server is connected with the first pressure sensor and the temperature sensor signal.
Preferably, present invention additionally comprises there is percolate analytical equipment, the percolate analytical equipment includes percolate point
Analyzer, element determination instrument and PH meters, the percolate analyzer, the element determination instrument and inspection possessed by PH meters
End is surveyed to may be contained within the leachate collection cup.
Preferably, present invention additionally comprises there is secondary buffer pond, the secondary buffer pond is arranged at the nitration reaction device
Between the ANAMMOX reactors, the buffering for percolate；The bottom in the secondary buffer pond by mud return line,
The mud return line connects with the nitration reaction device, in being provided with sludge reflux pump on the mud return line.
Preferably, it is provided with tail gas collecting device on the UASB reactors and the ANAMMOX reactors.
Preferably, it is provided with first flowmeter between the ANAMMOX reactors and the shower nozzle；In the gas
Second flowmeter and air gauge are provided with body output pipe.
Preferably, the bottom of the test cavity is provided with the filter element with filtering function.
Preferably, the nitration reaction device includes nitration reaction device framework, in the nitration reaction device framework
Inside it is provided with the first agitating device and film carries nitrobacteria, is provided with the bottom of the nitration reaction device framework for filling
The air pump of gas.
Preferably, the ANAMMOX reactors include ANAMMOX reactor frameworks, in the ANAMMOX reactors structure
ANAMMOX bacteria carriers and the second agitating device are provided with frame.
Preferably, in being provided with load sensor on the bottom surface of the balancing gate pit, the load sensor and the number
Connected according to acquisition server signal.
Preferably, it is provided with the outside of the load frame for being detected to test material decrement in test cavity
Laser range sensor, the laser range sensor are connected with the data acquisition server signal.
(3) beneficial effect
Present invention aims at a kind of refuse soil degraded compression visualizer having except ammonia nitrogen function is provided, the visualizer is intended
Automation axial pressure is realized using hydraulic axial pressue device, while confined pressure is provided in the case where simulating varying environment temperature conditionss,
The limitation of confined pressure can not be provided by solving degraded instrument, and is realized and accelerated biodegradable, the amount of realizing by leachate recirculation
Change the function of monitoring solid, liquid, gas dynamic change, test process realizes digitlization and sequencing, removes human error, ensure that examination
The precision and reliability tested.
This patent has the beneficial effect that：1st, provide axle pressure using intelligent hydraulic device and confined pressure, pressure volume controller carry
The controllable setting of soil sample stress is supplied；2nd, it is incubated using the liquid for providing confined pressure, reduces experimentation cost；3rd, solves recharge
The problem of percolate middle and high concentration ammonia inhibition biodegradation, recharge liquid is improved to the biodegradable efficiency of refuse soil, is collected
PH value, COD and the BOD in percolate have been monitored while percolate, can automated setting, flow, the flow velocity of monitoring percolate；
4th, using noncontacting proximity sensor and software cooperating, the damaged mechanical property of the soil sample caused by disposing tester has been broken
Limitation, while the change of monitoring soil sample decrement in real time improves the accuracy and reliability of test data.
Brief description of the drawings
Fig. 1 is except scopic structural representation is compressed in the degraded of ammonia nitrogen refuse soil in the embodiment of the present invention；
In Fig. 1, the corresponding relation of component names and accompanying drawing number is：
Test cavity 1, balancing gate pit 2, shower nozzle 3, load frame 4, mozzle 5,
Leachate collection cup 6, UASB reactors 7, nitration reaction device 8,
ANAMMOX reactors 9, hydraulic control hammer 10, gas export line 11,
Test gas collection cups 12, gas analyzer 13, control main frame 14,
Data acquisition server 15, percolate analytical equipment 16, secondary buffer pond 17.
Embodiment
Embodiments of the present invention are described in further detail with reference to the accompanying drawings and examples.Following examples are used for
Illustrate the present invention, but can not be used for limiting the scope of the present invention.
In the description of the invention, unless otherwise indicated, " multiple " are meant that two or more；Term " on ",
" under ", "left", "right", " interior ", " outer ", " front end ", " rear end ", " head ", the orientation of the instruction such as " afterbody " or position relationship be
Based on orientation shown in the drawings or position relationship, it is for only for ease of the description present invention and simplifies description, rather than instruction or dark
Show that the device of meaning or element there must be specific orientation, with specific azimuth configuration and operation, thus it is it is not intended that right
The limitation of the present invention.In addition, term " first ", " second ", " the 3rd " etc. be only used for describe purpose, and it is not intended that instruction or
Imply relative importance.
In the description of the invention, it is necessary to which explanation, unless otherwise clearly defined and limited, term " connected ", " connects
Connect " it should be interpreted broadly, for example, it may be being fixedly connected or being detachably connected, or it is integrally connected；It can be machine
Tool connects or electrical connection；Can be joined directly together, can also be indirectly connected by intermediary.For this area
For those of ordinary skill, the concrete meaning of above-mentioned term in the present invention can be understood with concrete condition.
Fig. 1 is refer to, Fig. 1 is except scopic structural representation is compressed in the degraded of ammonia nitrogen refuse soil in the embodiment of the present invention.
The invention provides one kind except ammonia nitrogen refuse soil degraded compression visualizer, including：Experimental rig, experimental rig have
For the test cavity 1 of loading test material, in being provided with balancing gate pit 2 in test cavity 1, balancing gate pit 2 is arranged at test cavity 1
It is interior and can with test cavity 1 formed a sealed chamber, in being provided with shower nozzle 3 on the downside of balancing gate pit 2, in experiment
The outside of chamber 1 is provided with load frame 4, and test cavity 1 is arranged in load frame 4, and the madial wall interval of test cavity 1 and load frame 4 is set
Put and form temperature controlled compartment, in setting having heaters, first pressure sensor and temperature sensor in temperature controlled compartment；Percolate returns
Filling device, leachate recirculation device include mozzle 5, and one end of mozzle 5 connects with the bottom wall of test cavity 1, mozzle 5
The other end is provided with the leachate collection cup 6 for collecting percolate, and UASB is connected with by feed pump with leachate collection cup 6
Reactor 7, UASB reactors 7 are connected with external gas collector, and the outlet of UASB reactors 7 is connected with nitration reaction device
8, the outlet of nitration reaction device 8 is connected with ANAMMOX reactors 9, and the outlet of ANAMMOX reactors 9 passes through reflux pump and leaching
Bath shower nozzle 3 is connected, and UASB reactors 7, nitration reaction device 8, ANAMMOX reactors 9 and shower nozzle 3 are in turn connected to form
Leachate recirculation system；Hydraulic axial pressue device, hydraulic axial pressue device include pressure volume controller and with pressure
The hydraulic control hammer 10 of power fixing fabric structure device control connection, hydraulic control hammer 10 are connected with balancing gate pit 2；Gas recovery detection dress
Put, gas recovery detection means includes gas export line 11, defeated in gas in being provided with valve on gas export line 11
The end for going out pipeline 11 is provided with test gas collection cups 12, is used in being provided with test gas collection cups 12 to test gas
The gas analyzer 13 analyzed；Control system, control system include control main frame 14 and with the signal of control main frame 14
The data acquisition server 15 of connection, data acquisition server 15 connect with first pressure sensor and temperature sensor signal
Connect.
Experimental rig is provided with test cavity 1, the loading test soil sample in test cavity 1, and pressure is provided with the top of test cavity 1
There is a hydraulic control to hammer 10 into shape for piston 2, hydraulic axial pressue device, and hydraulic control hammer 10 is connected with balancing gate pit 2, passes through liquid
10 directly excitations of voltage-controlled system hammer produce axle power, and simulation pressurization is carried out to the experiment soil sample loaded in test cavity 1.
Pressure at right angle has load sensor by balancing gate pit 2 and loading platform transmission, and in balancing gate pit 2, can and
When feed back soil pressure force value.
A load frame 4 is provided with the outside of test cavity 1, test cavity 1 is arranged in load frame 4, test cavity 1 and load
The madial wall of frame 4 is arranged at intervals and forms temperature controlled compartment.The confined pressure fluid of simulation soil confined pressure is mounted with temperature controlled compartment.Confined pressure
Fluid has pressure and heating dual-use function simultaneously.
In the present invention, test parameters is set first with the function that presets of pressure volume controller；It
Confined pressure fluid is pressed into the temperature controlled compartment of closing further according to the parameter (confined pressure value and temperature value) of setting afterwards, while utilizes heating
Device is heated to the confined pressure fluid loaded in the temperature controlled compartment of closing, and internal confined pressure and temperature environment are filled so that simulation is actual.
Mozzle 5 is set in the bottom of test cavity 1, percolate retracting device is connected, using under the top loading platform of test cavity 1
The shower nozzle 3 of the pin umbrella shape of the controllable flow rate of installation realizes the real-time recharge of percolate.
It is in turn connected to form and is oozed by UASB reactors 7, nitration reaction device 8, ANAMMOX reactors 9 and shower nozzle 3
Filtrate recharge system, wherein, nitration reaction device 8 is that short distance nitration-Anammox removes ammonia nitrogen device, pacifies process sequence, nitre
Change reaction unit 8 to be arranged on before leachate recirculation operation.Nitration reaction device 8 includes the framework of nitration reaction device 8, in nitre
Change and the first agitating device and film load nitrobacteria are provided with the framework of reaction unit 8, in the bottom of the framework of nitration reaction device 8
It is provided with the air pump for inflation.Using nitrobacteria by the part mineralized nitrogen in percolate stoste into cultured water, then profit
With ANAMMOX bacterium under anaerobic environment, using cultured water as electron acceptor, carry out microbial reaction and directly generate N2, so as to reach
To the purpose of ammonia nitrogen removal.
Gas recovery detection means is to set gas export line 11 at the top of test cavity 1, passes through gas export line 11
Test gas collection cups 12 are introduced, further test point is carried out to the gas overflowed in test cavity 1 using gas analyzer 13
Analysis.
Control system is passed by control main frame 14 (computer), data acquisition server 15, radio temperature sensor, loading
Sensor, pressure sensor etc. carry out automatic data collection and control.
In the present invention, control system includes 14, one, a dynamic control main frame data acquisition server 15, one
Pressure volume controller and multiple sensors.Hydraulic control hammer 10 is arranged on load frame 4, in the lower end of hydraulic control hammer 10
Load bar is set, and the lower end of load bar is connected with balancing gate pit 2 and sets load sensor, and load sensor takes with data acquisition
The signal connection of business device 15.Water source is provided with pressure volume controller, pressure setting is carried out by dynamic control main frame 14, by water
Liquid in source is pressed into hydraulic control hammer 10 by mozzle 5, so as to provide axle pressure.
Test cavity 1 is set in load frame 4, the temperature controlled compartment of closing is formed between test cavity 1 and load frame 4.Diafiltration is set
Liquid collection cups 6, leachate collection cup 6 are connected by mozzle 5 with temperature controlled compartment bottom.Heater is arranged in temperature controlled compartment, it is right
Confined pressure fluid is heated, and confined pressure fluid can be used as heat insulation liquid, and to provide constant temperature, radio temperature sensor is arranged on temperature
Control is indoor, to monitor the temperature in temperature controlled compartment.
Outside in load frame 4 sets a hot recycle pump, and hot recycle pump is connected to outside temperature controlled compartment by pipeline, ensures to protect
Geothermal liquid circulation, to solve the drawbacks of heater point type heating tape is come.
Temperature controlled compartment is made up of lucite, and its bottom is provided with dismountable seal base, and bottom plate both sides are screwed.
Percolate analytical equipment 16 is made up of BOD analyzers, COD analyzers and PH meter.
Leachate recirculation device be by except the percolate after ammonia nitrogen by pin umbrella shape shower nozzle 3 into test cavity 1
Soil sample recharge, the lower end of pin umbrella shape shower nozzle 3 penetrate test cavity 1 load flat board, be arranged in test cavity 1, its end
Portion sets umbrella shape leaching shower nozzle, and the middle part of mozzle 5 sets controllable type flowmeter, control diafiltration flow quantity, its leaching intensity controlled
System is in 0.1~10mL/s.
Leachate recirculation system uses CANON techniques, and leachate recirculation system includes the (upflow type anaerobic of UASB reactors 7
Sludge bed reactor), nitration reaction device 8 (short distance nitration biological denitrificaion nitration reaction device 8) and ANAMMOX reactors 9
(anaerobic ammonia oxidation reactor) three parts.
UASB reactors 7 are provided with feed pump, are connected by feed pump with leachate collection cup 6, UASB reactors 7 and nitre
Change reaction unit 8 to be connected.The water outlet of UASB reactors 7 enters in nitration reaction device 8, and nitration reaction device 8 is connected with secondary slow
Rush pond 17.A part of sludge of secondary buffer pond 17 in secondary buffer pond 17 flows back into nitration reaction dress by sludge reflux pump
8 are put, the water outlet of another part secondary buffer pond 17 in secondary buffer pond 17 enters ANAMMOX reactors 9.
Limit herein：The dischargeable capacity of UASB reactors 7 is 8.25L；The dischargeable capacity of nitration reaction device 8 is 15L；
ANAMMOXR reactors available capacity is 8.25L.
The material of nitration reaction device 8 is lucite.Nitration reaction device 8 is divided into ten cell compartments, wherein first
Cell compartment is anoxic zone, and remaining is aerobic zone, and nitration reaction device 8 is built with the nitrobacteria with filter membrane.
It is carrier that anaerobic ammonia oxidizing bacteria is inoculated with ANAMMOXR reactors with non-woven fabrics and porous polyester polymer, and with
Stainless steel is fixed.
Gas recovery detection means includes gas collection cup, GEM2000plus refuse landfills gas analyzer 13, red-
Y smart gas mass flow controllers and valve, gas collection cup pass through conduit and the loading platform phase at the top of test cavity 1
Even, red-y smart gas mass flow controllers and valve are arranged in the middle part of conduit, for measuring and controlling the stream of aerogenesis
Amount, GEM2000plus refuse landfills gas analyzer 13 is arranged on the end of gas collection cup, to the gaseous product of collection into
Part enters Mobile state tracking and testing.
In the present invention, the physical dimension of the body of test cavity 1 is：Diameter 400mm, high 800mm copper cylindrical drum, experiment
The top of chamber 1 is provided with loading platform, and loading platform bottom is provided with balancing gate pit 2, soil body sample is placed in test cavity 1, and bottom is set
Filter layer.
The outside of test cavity 1 sets laser displacement sensor, and laser displacement sensor is erected on load frame 4, laser displacement
Sensor uses contactless structure, is connected by data acquisition unit with terminal, supporting by laser displacement sensor
GDSLAB softwares can draw the axial deformation of soil sample.
Present invention aims at a kind of refuse soil degraded compression visualizer having except ammonia nitrogen function is provided, the visualizer is intended
Automation axial pressure is realized using hydraulic axial pressue device, while confined pressure is provided in the case where simulating varying environment temperature conditionss,
The limitation of confined pressure can not be provided by solving degraded instrument, and is realized and accelerated biodegradable, the amount of realizing by leachate recirculation
Change the function of monitoring solid, liquid, gas dynamic change, test process realizes digitlization and sequencing, removes human error, ensure that examination
The precision and reliability tested.
This patent has the beneficial effect that：1st, provide axle pressure using intelligent hydraulic device and confined pressure, pressure volume controller carry
The controllable setting of soil sample stress is supplied；2nd, it is incubated using the liquid for providing confined pressure, reduces experimentation cost；3rd, solves recharge
The problem of percolate middle and high concentration ammonia inhibition biodegradation, recharge liquid is improved to the biodegradable efficiency of refuse soil, is collected
PH value, COD and the BOD in percolate have been monitored while percolate, can automated setting, flow, the flow velocity of monitoring percolate；
4th, using noncontacting proximity sensor and software cooperating, the damaged mechanical property of the soil sample caused by disposing tester has been broken
Limitation, while the change of monitoring soil sample decrement in real time improves the accuracy and reliability of test data.
Based on the above-mentioned refuse soil degraded compression visualizer having except ammonia nitrogen function, its specifically used method is：
(1) first, check between balancing gate pit 2 and temperature controlled compartment, between base and temperature controlled compartment and each external mouth of pipe it is close
Feng Xing；
(2) after determining that air-tightness is good, the soil sample made is put into test cavity 1, opens laser sensor；
(3) after the completion of filling sample, load sensor, radio temperature sensor, pressure sensor and heater are checked whether
Normal operation.Pressure volume controller, data acquisition server 15 and dynamic control main frame 14 are opened, in pressure volume controller
Middle preset pressure, carry out axially loaded according to test requirements document and confined pressure is provided, while recorded in real time using laser displacement sensor
The change of decrement；
(4) each device in leachate recirculation device and leachate recirculation system is opened, is surveyed by BOD analyzers, COD
Determine instrument and PH meters carry out the parameter such as BOD, COD and pH value to obtained percolate stoste and are measured.Meanwhile using except ammonia nitrogen
Device removes the ammonia nitrogen in percolate stoste, strong using the simulated rainfall of pin umbrella shape shower nozzle 3 and leachate recirculation, leaching
Degree is controlled with controllable type flowmeter.
(5) gas recovery detection means is opened, gas is collected using saturation Nacl solution, utilizes air gauge and red-y
Smart gas mass flow controllers monitor sample under outside stress field, temperature field and simulated rainfall environment because biochemical anti-
The change of landfill atmospheric pressure and flow caused by answering, using GEM2000plus refuse landfills gas analyzer 13 to gas
Composition enters Mobile state trace analysis.
The specific embodiment of the present invention is as follows：
First, check between balancing gate pit 2 and temperature controlled compartment, between base and temperature controlled compartment and each external mouth of pipe sealing
Property；After determining that air-tightness is good, the soil sample made is put into test cavity 1, density of soil sample 1.22g/cm3；Open and swash
Optical displacement sensor；After the completion of filling sample, pressure sensor, radio temperature sensor, load sensor, heater are checked, is opened
Pressure volume controller, data acquisition server 15 and dynamic control main frame 14, preset pressure is in pressure volume controller
100MPa, carry out axially loaded according to test requirements document and confined pressure is provided, while utilize the real-time recording compressed of laser displacement sensor
The change of amount；After axial loading system starts, each device in leachate recirculation device and leachate recirculation system is opened, is led to
The measure that BOD analyzers, COD analyzers and PH meters carry out the parameter such as BOD, COD and pH value to obtained percolate stoste is crossed,
Meanwhile using the ammonia nitrogen removed except ammonia nitrogen device in percolate stoste, using the simulated rainfall of pin umbrella shape shower nozzle 3 with oozing
Filtrate recharge, leaching intensity are controlled in 0.1~10mL/s with controllable type flowmeter 3-6.Gas recovery detection means is opened, is utilized
Saturation Nacl solution collects gas, and sample is monitored in outside using air gauge and red-y smart gas mass flow controllers
Because of the change of landfill atmospheric pressure and flow caused by biochemical reaction under stress field, temperature field and simulated rainfall environment, utilize
GEM2000plus refuse landfills gas analyzer 13 enters Mobile state trace analysis to the composition of gas.
Embodiments of the invention provide for the sake of example and description, and are not exhaustively or by this to send out
It is bright to be limited to disclosed form.Many modifications and variations are obvious for the ordinary skill in the art.Choosing
Select and describe embodiment and be to more preferably illustrate the principle and practical application of the present invention, and make one of ordinary skill in the art
It will be appreciated that the present invention is so as to designing the various embodiments with various modifications suitable for special-purpose.
Claims (10)
1. one kind is except ammonia nitrogen refuse soil degraded compression visualizer, it is characterised in that including：
Experimental rig, the experimental rig have the test cavity (1) for loading test material, are provided with the test cavity
Balancing gate pit (2), the balancing gate pit are arranged in the test cavity and can form a sealed chamber with the test cavity,
In being provided with shower nozzle (3) on the downside of the balancing gate pit, load frame (4) is provided with the outside of the test cavity,
The test cavity is arranged in the load frame, and the madial wall of the test cavity and the load frame is arranged at intervals and forms temperature
Room is controlled, in setting having heaters, first pressure sensor and temperature sensor in the temperature controlled compartment；
Leachate recirculation device, the leachate recirculation device include mozzle (5), one end of the mozzle and the examination
The bottom wall connection of chamber is tested, the other end of the mozzle is provided with the leachate collection cup (6) for collecting percolate, and described
Leachate collection cup is connected with UASB reactors (7) by feed pump, and the UASB reactors are connected with external gas collection dress
Put, the outlet of the UASB reactors is connected with nitration reaction device (8), and the outlet of the nitration reaction device is connected with
ANAMMOX reactors (9), the outlet of the ANAMMOX reactors are connected by reflux pump with the shower nozzle, the UASB
Reactor, the nitration reaction device, the ANAMMOX reactors and the shower nozzle are in turn connected to form percolate and returned
Fill system；
Hydraulic axial pressue device, the hydraulic axial pressue device include pressure volume controller and with the pressure body
The hydraulic control hammer (10) of plot controller control connection, the hydraulic control hammer are connected with the balancing gate pit；
Gas reclaims detection means, and the gas recovery detection means includes gas export line (11), defeated in the gas
Go out and valve is provided with pipeline, the end of the gas export line is provided with test gas collection cups (12), in the examination
The gas analyzer (13) being provided with for being analyzed test gas is tested on gas collection cup；
Control system, the control system include control main frame (14) and adopted with the data that the control main frame signal is connected
Collect server (15), the data acquisition server connects with the first pressure sensor and the temperature sensor signal
Connect.
It is 2. according to claim 1 except ammonia nitrogen refuse soil degraded compression visualizer, it is characterised in that
Also include percolate analytical equipment (16), the percolate analytical equipment includes percolate analyzer, element determination
Instrument and PH meters, the percolate analyzer, the element determination instrument and test side possessed by PH meters may be contained within
In the leachate collection cup.
It is 3. according to claim 1 except ammonia nitrogen refuse soil degraded compression visualizer, it is characterised in that
Also include secondary buffer pond (17), the secondary buffer pond is arranged at the nitration reaction device and the ANAMMOX
Buffering between reactor, for percolate；
The bottom in the secondary buffer pond is connected by mud return line, the mud return line with the nitration reaction device,
In being provided with sludge reflux pump on the mud return line.
It is 4. according to claim 1 except ammonia nitrogen refuse soil degraded compression visualizer, it is characterised in that
Tail gas collecting device is provided with the UASB reactors and the ANAMMOX reactors.
It is 5. according to claim 1 except ammonia nitrogen refuse soil degraded compression visualizer, it is characterised in that
First flowmeter is provided between the ANAMMOX reactors and the shower nozzle；
In being provided with second flowmeter and air gauge on the gas export line.
It is 6. according to claim 1 except ammonia nitrogen refuse soil degraded compression visualizer, it is characterised in that
The bottom of the test cavity is provided with the filter element with filtering function.
It is 7. according to claim 1 except ammonia nitrogen refuse soil degraded compression visualizer, it is characterised in that
The nitration reaction device includes nitration reaction device framework, in being provided with first in the nitration reaction device framework
Agitating device and film carry nitrobacteria, and the bottom of the nitration reaction device framework is provided with the air pump for inflation.
It is 8. according to claim 1 except ammonia nitrogen refuse soil degraded compression visualizer, it is characterised in that
The ANAMMOX reactors include ANAMMOX reactor frameworks, are provided with the ANAMMOX reactors framework
ANAMMOX bacteria carriers and the second agitating device.
9. being degraded except ammonia nitrogen refuse soil according to any one of claim 1 to 8 compresses visualizer, it is characterised in that
In being provided with load sensor on the bottom surface of the balancing gate pit, the load sensor and the data acquisition server
Signal connects.
It is 10. according to claim 9 except ammonia nitrogen refuse soil degraded compression visualizer, it is characterised in that
It is provided with the outside of the load frame for being passed to the laser ranging that test material decrement is detected in test cavity
Sensor, the laser range sensor are connected with the data acquisition server signal.
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| CN201710445963.6A CN107421819A (en) | 2017-06-14 | 2017-06-14 | Degraded except ammonia nitrogen refuse soil and compress visualizer |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710445963.6A CN107421819A (en) | 2017-06-14 | 2017-06-14 | Degraded except ammonia nitrogen refuse soil and compress visualizer |
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| CN108801888A (en) * | 2018-05-25 | 2018-11-13 | 昆明理工大学 | It degrades in a kind of organic soil room simulator |
| CN110608996A (en) * | 2018-06-14 | 2019-12-24 | 天水红山试验机有限公司 | Solid waste physical simulation test system |
| CN114280271A (en) * | 2021-11-23 | 2022-04-05 | 中北大学 | Testing device and testing method for degradation rate of biodegradable high polymer material in soil |
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