CN107412024A - A kind of hydrogen-rich gel mask and preparation method thereof - Google Patents

A kind of hydrogen-rich gel mask and preparation method thereof Download PDF

Info

Publication number
CN107412024A
CN107412024A CN201710286537.2A CN201710286537A CN107412024A CN 107412024 A CN107412024 A CN 107412024A CN 201710286537 A CN201710286537 A CN 201710286537A CN 107412024 A CN107412024 A CN 107412024A
Authority
CN
China
Prior art keywords
parts
hydrogen
water
rich
gel mask
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201710286537.2A
Other languages
Chinese (zh)
Other versions
CN107412024B (en
Inventor
王天湶
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yu Yan
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201710286537.2A priority Critical patent/CN107412024B/en
Publication of CN107412024A publication Critical patent/CN107412024A/en
Application granted granted Critical
Publication of CN107412024B publication Critical patent/CN107412024B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/676—Ascorbic acid, i.e. vitamin C
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212—Face masks
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04—Dispersions; Emulsions
    • A61K8/042—Gels
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/20—Halogens; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/678—Tocopherol, i.e. vitamin E
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/731—Cellulose; Quaternized cellulose derivatives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Dermatology (AREA)
  • Emergency Medicine (AREA)
  • Inorganic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to medical products field, discloses a kind of hydrogen-rich gel mask and preparation method thereof.The facial mask is made by the raw material of following parts by weight：70 90 parts of seaweed extracted liquor, 150 400 parts of crosslinker solution, it is adsorbed with 15 25 parts of the water-soluble resin of hydrogen rich water, 13 parts of collagen peptide micro mist, 0.1 0.3 parts of B B-complex, 0.5 1.5 parts of cellulose gum, 13 parts of sodium carboxymethylcellulose, 30 50 parts of alcohol, 13 parts of sodium carbonate, 1.5 4.5 parts of citric acid.The facial mask of the present invention containing a variety of hydrogen rich waters and other a variety of anti-aging compositions, can desalinate color spot simultaneously, prevent skin aging, corrugation.And the facial mask of the present invention has preferable gas permeability, is advantageous to cutaneous respiration, comfort is strong.

Description

A kind of hydrogen-rich gel mask and preparation method thereof
Technical field
The present invention relates to medical products field, more particularly to a kind of hydrogen-rich gel mask and preparation method thereof.
Background technology
Facial mask species in the market is various, and the facial mask of gel-type vehicle is because of its good water-retaining property in recent years, it is easy to use and Obtain prevalence.And the function of current facial mask is also more and more, there are many products in the market.
Patent CN201610939286.9 discloses a kind of preparation method of sticking type hydrogel substrate facial mask：Prepare PVA The aqueous solution；Corresponding skin care ingredient is added in the PVA solution to stir；The mixed liquor prepared is poured into mould, instead Hydrogel facial mask is prepared after multiple freeze thawing.Hydrogel facial mask water content prepared by the invention is high, and surface smooth resilient is good, has Skin attachement；In addition, the preparation method of this hydrogel facial mask is simple, cost of material is low, it is adapted to large-scale production.
Although above-mentioned hydrogel facial mask has water retention, skin surface smooth resilient is enabled to, it does not have There is anti-aging effect.In addition, the gel mask, using Hydrogels as matrix, the gel gas permeability is poor, after laying by skin with Air is thoroughly isolated, and is unfavorable for the breathing of skin, influences the secreting function of cell, and comfort is poor.
The content of the invention
In order to solve the above-mentioned technical problem, the invention provides a kind of hydrogen-rich gel mask and preparation method thereof.The present invention Facial mask simultaneously containing a variety of hydrogen rich waters and other a variety of anti-aging compositions, color spot can be desalinated, prevent skin aging, corrugation. And the facial mask of the present invention has preferable gas permeability, is advantageous to cutaneous respiration, comfort is strong.
The present invention concrete technical scheme be：A kind of hydrogen-rich gel mask, is made by the raw material of following parts by weight：
Seaweed extracted liquor 70-90 parts, crosslinker solution 150-400 parts, water-soluble resin 15-25 parts of hydrogen rich water are adsorbed with, Collagen peptide micro mist 1-3 parts, B B-complex 0.1-0.3 parts, cellulose gum 0.5-1.5 parts, sodium carboxymethylcellulose 1-3 Part, alcohol 30-50 parts, sodium carbonate 1-3 parts, citric acid 1.5-4.5 parts.
The facial mask of the present invention be crosslinked using seaweed extracted liquor after gel as matrix, contain alginic acid in seaweed extracted liquor Sodium, algal polysaccharides isoreactivity material, transparent mucus shape, there is water conservation, wetting, antibacterial and other effects, after being laid on skin, parent Skin is good, and skin will not be made to produce allergy.
The present invention is in facial mask added with the water-soluble resin, collagen peptide micro mist and compound dimension life for being adsorbed with hydrogen rich water Element, wherein, hydrogen rich water has extremely strong reproducibility, can act as natural antioxidant, contains reactive hydrogen in hydrogen rich water, can be with The free radical in skin histology is effectively removed, is enhanced metabolism, delay skin aging, plays spot, corrugation.But in facial mask mistake processed Hydrogen rich water is easily lost in journey, therefore the present invention is adsorbed to it in advance from the water-soluble resin with high water absorption function, so as to There is preferable stability in facial mask preparation process.And collagen peptide micro mist and B B-complex also have anti-oxidant work( Effect, synergy is played with hydrogen rich water one.
In addition, sodium carboxymethylcellulose has thickening and peptizaiton, it is possible to increase the stickiness of gel and in gel Other components play dispersion effect.Cellulose gum plays viscosifying action, it is possible to increase the cohesive of gel and skin, in addition its be Natural materials, it is non-stimulated to skin.
Preferably, the hydrogen content of the hydrogen rich water is 1.0-1.5ppm.
Preferably, the water-soluble resin is water soluble acrylic resin, adsorbs the moisture content after hydrogen rich water and is 80-120wt%.
Preferably, the B B-complex is vitamin C and vitamin E.
Preferably, the crosslinker solution is 3-5wt% calcium chloride solution.
Preferably, the moisture content of the seaweed extracted liquor is 25-35wt%.
Preferably, the mean molecule quantity of the collagen peptide micro mist is 500-1000Da.In above-mentioned low molecule The collagen peptide micro mist good water solubility of scope is measured, is easily absorbed by the skin, and there is strong reducing power, prevents that skin is old Change.
A kind of preparation method of hydrogen-rich gel mask, step are as follows：
(a) collagen peptide micro mist, B B-complex, sodium carboxymethylcellulose are added in seaweed extracted liquor successively, Stir, obtain sticky mixing mucus.
(b) under conditions of stirring at low speed, 1-5 DEG C, sodium carbonate and citric acid are successively added into mixing mucus, until stirring Mix uniformly.
(c) mixing mucus is stirred vigorously and heating treatment simultaneously, sodium carbonate and citric acid is fully contacted concurrently The alveolate mucus of parcel is made after raw reaction, fully reaction.
(d) mucus of step (c) is transferred in pressure reduction vessel, alcohol is added under stirring at low speed, after stirring, taken Go out, drain unnecessary alcohol and water；Then the water-soluble resin and cellulose gum for being adsorbed with hydrogen rich water are added again, and stirring at low speed is equal It is even.
(e) mucus for obtaining step (d) is added in crosslinker solution, carries out cross-linking reaction, until after reaction terminates, mistake Filter, the jel product shaped, hydrogen-rich gel mask is made after cutting.
Although the gel-type vehicle after seaweed extracted liquor crosslinking has preferable moisture retention, its gas permeability still needs to be carried It is high.In facial mask preparation process, first collagen peptide micro mist, B B-complex are added in seaweed extracted liquor successively and mixed It is even, sodium carbonate and citric acid are then added, in the process, in order to prevent sodium carbonate and citric acid antedating response, it is necessary to be Under low stir speed (S.S.), cryogenic conditions, it is stirred vigorously and is heated up again after addition, sodium carbonate and citric acid is fully contacted And react, a large amount of bubbles are formed in matrix, the bubble is wrapped in matrix, and the meaning being stirred vigorously is while can The air in the external world is also mixed into matrix, and it can be the small of multiple small sizes by the bubble splitting of large volume to be stirred vigorously Bubble.Then mucus is transferred in pressure reduction vessel, under subnormal ambient, the gas in bubble is due to the generation of bubble inside and outside differential pressure Escape, adds alcohol, solubility very little of the seaweed extracted liquor in alcohol, therefore the alcohol in whipping process under stirring at low speed Can rapid osmotic enter bubble substitution gas.Then addition is adsorbed with the water-soluble resin and fibre of hydrogen rich water under stirring at low speed Plain glue is tieed up, the reason for cellulose gum adds at this moment is：If adding cellulose gum in advance, it will enter to be significantly greatly increased the viscous of matrix Property, it is unfavorable for scattered and reaction the progress of material.Finally mucus is added in crosslinker solution and carries out cross-linking reaction, is determined The jel product of property.After facial mask is made, packaging closures are carried out with aluminium film, aluminium film material can prevent the escape of hydrogen in hydrogen rich water. After facial mask is laid, due to gel-type vehicle and air bump contact, volatilize rapidly, come to skin tape refrigerant after alcohol heat absorption Sense, and it has Disinfection Effect.And be originally released after alcohol volatilization in matrix by the micro-bubble that alcohol is filled, formed a large amount of Capillary channel, therefore the gas permeability of facial mask is improved, and is advantageous to cutaneous respiration.
Preferably, the speed of stirring at low speed is 100-200r/min in step (b), is stirred vigorously in step (c) Speed be 800-1200r/min, the speed of stirring at low speed is 40-80r/min in step (d).
Preferably, 50-60 DEG C is warming up in step (c), crosslinker solution temperature is 20-30 DEG C in step (d).
In step (c), with the rise of temperature, sodium carbonate and citric acid gradually react.In step (d), in order to The loss of hydrogen in hydrogen rich water is prevented, it is necessary to which crosslinker solution is controlled in suitable temperature.
It is compared with the prior art, the beneficial effects of the invention are as follows：The facial mask of the present invention is simultaneously containing a variety of hydrogen rich waters and its His a variety of anti-aging compositions, can desalinate color spot, prevent skin aging, corrugation.And the facial mask of the present invention has preferably thoroughly Gas, is advantageous to cutaneous respiration, and comfort is strong.
Embodiment
With reference to embodiment, the invention will be further described.
Embodiment 1
A kind of hydrogen-rich gel mask, is made by the raw material of following parts by weight：
80 parts of seaweed extracted liquor (moisture content 30wt%), 250 parts of crosslinker solution (4wt% calcium chloride solution), absorption There are 20 parts of water soluble acrylic resin's (hydrogen content of hydrogen rich water is 1.2ppm, and resin aqueous rate is 100wt%) of hydrogen rich water, glue Former 2 parts of protein peptides micro mist (mean molecule quantity 800Da), 0.2 part of B B-complex (vitamin C and vitamin E), cellulose gum 1 part, 2 parts of sodium carboxymethylcellulose, 40 parts of alcohol, 2 parts of sodium carbonate, 3 parts of citric acid.
The preparation method of above-mentioned hydrogen-rich gel mask, step are as follows：
(a) collagen peptide micro mist, B B-complex, sodium carboxymethylcellulose are added in seaweed extracted liquor successively, Stir, obtain sticky mixing mucus.
(b) under conditions of stirring at low speed (150r/min), 3 DEG C, sodium carbonate and lemon are successively added into mixing mucus Acid, until stirring.
(c) (1000r/min) is stirred vigorously simultaneously to mixing mucus and is warming up to 55 DEG C, make sodium carbonate and citric acid Fully contact and react, the alveolate mucus of parcel is fully made after reaction.
(d) mucus of step (c) is transferred in pressure reduction vessel, alcohol is added under stirring at low speed (60r/min), stirred After uniformly, take out, drain unnecessary alcohol and water；Then the water-soluble resin and cellulose gum for being adsorbed with hydrogen rich water are added again, Stirring at low speed (60r/min) is uniform.
(e) mucus for obtaining step (d) is added in 25 DEG C of crosslinker solution, carries out cross-linking reaction, until reaction knot Shu Hou, filtering, the jel product shaped, hydrogen-rich gel mask is made after cutting.
Embodiment 2
A kind of hydrogen-rich gel mask, is made by the raw material of following parts by weight：
70 parts of seaweed extracted liquor (moisture content 25wt%), 150 parts of crosslinker solution (5wt% calcium chloride solution), absorption There are 25 parts of water soluble acrylic resin's (hydrogen content of hydrogen rich water is 1.0ppm, and resin aqueous rate is 120wt%) of hydrogen rich water, glue Former 1 part of protein peptides micro mist (mean molecule quantity 500Da), 0.3 part of B B-complex (vitamin C and vitamin E), cellulose gum 0.5 part, 3 parts of sodium carboxymethylcellulose, 30 parts of alcohol, 1 part of sodium carbonate, 1.5 parts of citric acid.
The preparation method of above-mentioned hydrogen-rich gel mask, step are as follows：
(a) collagen peptide micro mist, B B-complex, sodium carboxymethylcellulose are added in seaweed extracted liquor successively, Stir, obtain sticky mixing mucus.
(b) under conditions of stirring at low speed (100r/min), 1 DEG C, sodium carbonate and lemon are successively added into mixing mucus Acid, until stirring.
(c) (800r/min) is stirred vigorously simultaneously to mixing mucus and is warming up to 50 DEG C, make sodium carbonate and citric acid Fully contact and react, the alveolate mucus of parcel is fully made after reaction.
(d) mucus of step (c) is transferred in pressure reduction vessel, alcohol is added under stirring at low speed (40r/min), stirred After uniformly, take out, drain unnecessary alcohol and water；Then the water-soluble resin and cellulose gum for being adsorbed with hydrogen rich water are added again, Stirring at low speed (40r/min) is uniform.
(e) mucus for obtaining step (d) is added in 20 DEG C of crosslinker solution, carries out cross-linking reaction, until reaction knot Shu Hou, filtering, the jel product shaped, hydrogen-rich gel mask is made after cutting.
Embodiment 3
A kind of hydrogen-rich gel mask, is made by the raw material of following parts by weight：
90 parts of seaweed extracted liquor (moisture content 35wt%), 400 parts of crosslinker solution (3wt% calcium chloride solution), absorption There are 15 parts of water soluble acrylic resin's (hydrogen content of hydrogen rich water is 1.5ppm, and resin aqueous rate is 80wt%) of hydrogen rich water, glue Former 3 parts of protein peptides micro mist (mean molecule quantity 1000Da), 0.1 part of B B-complex (vitamin C and vitamin E), cellulose 1.5 parts of glue, 1 part of sodium carboxymethylcellulose, 50 parts of alcohol, 3 parts of sodium carbonate, 4.5 parts of citric acid.
The preparation method of above-mentioned hydrogen-rich gel mask, step are as follows：
(a) collagen peptide micro mist, B B-complex, sodium carboxymethylcellulose are added in seaweed extracted liquor successively, Stir, obtain sticky mixing mucus.
(b) under conditions of stirring at low speed (200r/min), 5 DEG C, sodium carbonate and lemon are successively added into mixing mucus Acid, until stirring.
(c) (1200r/min) is stirred vigorously simultaneously to mixing mucus and is warming up to 60 DEG C, make sodium carbonate and citric acid Fully contact and react, the alveolate mucus of parcel is fully made after reaction.
(d) mucus of step (c) is transferred in pressure reduction vessel, alcohol is added under stirring at low speed (80r/min), stirred After uniformly, take out, drain unnecessary alcohol and water；Then the water-soluble resin and cellulose gum for being adsorbed with hydrogen rich water are added again, Stirring at low speed (80r/min) is uniform.
(e) mucus for obtaining step (d) is added in 30 DEG C of crosslinker solution, carries out cross-linking reaction, until reaction knot Shu Hou, filtering, the jel product shaped, hydrogen-rich gel mask is made after cutting.
The facial mask of the facial mask of embodiment 1 and common hydrogel matrix (comparative example) on the market is contrasted.
Respectively the sensory evaluation of 20 women users of collection, statistics are as follows：
In addition, by recalling surveys, after being used continuously 30 days, user's facial colour spot has visual desalination phenomenon, and And skin of face more preferably water profit, gloss can be clearly felt that, it is flexible.
Raw materials used in the present invention, equipment, it is the conventional raw material, equipment of this area unless otherwise noted；In the present invention Method therefor, it is the conventional method of this area unless otherwise noted.
It is described above, only it is presently preferred embodiments of the present invention, not the present invention is imposed any restrictions, it is every according to the present invention Any simple modification, change and the equivalent transformation that technical spirit is made to above example, still fall within the technology of the present invention side The protection domain of case.

Claims (10)

  1. A kind of 1. hydrogen-rich gel mask, it is characterised in that：It is made by the raw material of following parts by weight：
    Seaweed extracted liquor 70-90 parts,
    Crosslinker solution 150-400 parts,
    Water-soluble resin 15-25 parts of hydrogen rich water are adsorbed with,
    Collagen peptide micro mist 1-3 parts,
    B B-complex 0.1-0.3 parts,
    Cellulose gum 0.5-1.5 parts,
    Sodium carboxymethylcellulose 1-3 parts,
    Alcohol 30-50 parts,
    Sodium carbonate 1-3 parts,
    Citric acid 1.5-4.5 parts.
  2. A kind of 2. hydrogen-rich gel mask as claimed in claim 1, it is characterised in that：The hydrogen content of the hydrogen rich water is 1.0- 1.5ppm。
  3. A kind of 3. hydrogen-rich gel mask as claimed in claim 2, it is characterised in that：The water-soluble resin is water soluble propene Acid resin, the moisture content adsorbed after hydrogen rich water is 80-120wt%.
  4. A kind of 4. hydrogen-rich gel mask as claimed in claim 1, it is characterised in that：The B B-complex be vitamin C and Vitamin E.
  5. A kind of 5. hydrogen-rich gel mask as claimed in claim 1, it is characterised in that：The crosslinker solution is 3-5wt% chlorine Change calcium solution.
  6. A kind of 6. hydrogen-rich gel mask as claimed in claim 5, it is characterised in that：The moisture content of the seaweed extracted liquor is 25-35wt%.
  7. A kind of 7. hydrogen-rich gel mask as claimed in claim 1, it is characterised in that：The average mark of the collagen peptide micro mist Son amount is 500-1000Da.
  8. 8. the preparation method of a kind of hydrogen-rich gel mask as described in claim 1-7 is any, it is characterised in that step is as follows：
    (a) collagen peptide micro mist, B B-complex, sodium carboxymethylcellulose are added in seaweed extracted liquor successively, stirred Uniformly, sticky mixing mucus is obtained；
    (b) under conditions of stirring at low speed, 1-5 DEG C, sodium carbonate and citric acid are successively added into mixing mucus, until stirring is equal It is even；
    (c) mixing mucus is stirred vigorously and heating treatment simultaneously, sodium carbonate and citric acid is fully contacted and occur anti- Should, the alveolate mucus of parcel is fully made after reaction；
    (d) mucus of step (c) is transferred in pressure reduction vessel, alcohol is added under stirring at low speed, after stirring, taken out, Drain unnecessary alcohol and water；Then the water-soluble resin and cellulose gum for being adsorbed with hydrogen rich water are added again, and stirring at low speed is uniform；
    (e) mucus for obtaining step (d) is added in crosslinker solution, carries out cross-linking reaction, until after reaction terminates, filtering, The jel product shaped, hydrogen-rich gel mask is made after cutting.
  9. A kind of 9. preparation method of hydrogen-rich gel mask as claimed in claim 8, it is characterised in that：Low speed stirs in step (b) The speed mixed is 100-200r/min, and the speed being stirred vigorously in step (c) is 800-1200r/min, and low speed stirs in step (d) The speed mixed is 40-80r/min.
  10. A kind of 10. preparation method of hydrogen-rich gel mask as claimed in claim 8, it is characterised in that：It is warming up in step (c) 50-60 DEG C, crosslinker solution temperature is 20-30 DEG C in step (d).
CN201710286537.2A 2017-04-27 2017-04-27 Hydrogen-rich gel mask and preparation method thereof Active CN107412024B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710286537.2A CN107412024B (en) 2017-04-27 2017-04-27 Hydrogen-rich gel mask and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710286537.2A CN107412024B (en) 2017-04-27 2017-04-27 Hydrogen-rich gel mask and preparation method thereof

Publications (2)

Publication Number Publication Date
CN107412024A true CN107412024A (en) 2017-12-01
CN107412024B CN107412024B (en) 2020-12-01

Family

ID=60425322

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710286537.2A Active CN107412024B (en) 2017-04-27 2017-04-27 Hydrogen-rich gel mask and preparation method thereof

Country Status (1)

Country Link
CN (1) CN107412024B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113502561A (en) * 2021-08-04 2021-10-15 河北云悦生物科技有限公司 Antibacterial health-care fiber and preparation method and application thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103417462A (en) * 2013-07-23 2013-12-04 陈俊杰 Facial mask for treating whelk and pigment patch and whitening skin
CN104042449A (en) * 2014-05-26 2014-09-17 诺斯贝尔(中山)无纺日化有限公司 High-temperature stable hydrogel mask
CN106562916A (en) * 2016-11-14 2017-04-19 广州蜜妆生物科技有限公司 Gel bubble mask

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103417462A (en) * 2013-07-23 2013-12-04 陈俊杰 Facial mask for treating whelk and pigment patch and whitening skin
CN104042449A (en) * 2014-05-26 2014-09-17 诺斯贝尔(中山)无纺日化有限公司 High-temperature stable hydrogel mask
CN106562916A (en) * 2016-11-14 2017-04-19 广州蜜妆生物科技有限公司 Gel bubble mask

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113502561A (en) * 2021-08-04 2021-10-15 河北云悦生物科技有限公司 Antibacterial health-care fiber and preparation method and application thereof

Also Published As

Publication number Publication date
CN107412024B (en) 2020-12-01

Similar Documents

Publication Publication Date Title
CN103494668B (en) Medical hydrogel moisturizing eye care mask and preparation method thereof
CN103861538B (en) A kind of gel ball and preparation method thereof
CN106619320A (en) Oil control and acne removal facial mask
CN106420368A (en) Preparation method of applying-type hydrogel-base facial mask
CN104721099A (en) Deep-purification black facial mask capable of generating bubbles and production method thereof
CN107412024A (en) A kind of hydrogen-rich gel mask and preparation method thereof
CN108815567A (en) A kind of preparation method of antiseptic dressing aquagel
CN107714631A (en) A kind of collagen peptide facial mask liquid and preparation method thereof
CN109908030A (en) A kind of manufacture craft of anhydrous facial mask
CN103407205B (en) Konjac glucomannan fiber wet tissue and method for preparing same
CN107189080A (en) A kind of preparation method of the regenerated silk fibroin hydrogel with graphene oxide
CN106978000A (en) Far infrared health care inner wall putty powder and preparation method thereof
CN108653054A (en) A kind of compound multiple-effect facial mask liquid
CN107625920A (en) Gynaecology's gel and preparation method thereof
CN108904874A (en) With membrane-like medical gel, manufacturing method and its application for promoting the effect of surface of a wound wet union
CN107080768A (en) A kind of dual effect type gel bring down a fever patch and preparation method thereof
CN103405374B (en) Freckle-removing and skin-whitening type gulcomannan particle facial mask and preparation method thereof
CN111281646A (en) Production process of medical cold compress patch
CN112516011A (en) Preparation method of D-phase emulsified emulsion
CN109718137A (en) A kind of production method of anhydrous facial mask and the anhydrous facial mask using the production of heat pump drying method
JP5556866B2 (en) Slaked lime mixture and method for producing the same
JPH0383555A (en) Vegetable juice-containing devil's-tongue jelly
CN112225855A (en) Formula and preparation process of hydrogel
CN107998040A (en) A kind of canna skin care item and preparation method thereof
CN114886784A (en) Water-refreshing soft film and preparation method and use method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
TA01 Transfer of patent application right
TA01 Transfer of patent application right

Effective date of registration: 20201113

Address after: 6-5, No.9, Huayu Plaza, Shapingba District, Chongqing

Applicant after: Yu Yan

Address before: 362141, Fujian, Quanzhou Province, Huian County, East Village, Heng Shan village, No. 98

Applicant before: Wang Tianquan

GR01 Patent grant
GR01 Patent grant