CN107406807B - 制备对映体混合物的方法和对映体混合物 - Google Patents

制备对映体混合物的方法和对映体混合物 Download PDF

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Publication number
CN107406807B
CN107406807B CN201680014500.8A CN201680014500A CN107406807B CN 107406807 B CN107406807 B CN 107406807B CN 201680014500 A CN201680014500 A CN 201680014500A CN 107406807 B CN107406807 B CN 107406807B
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mono
salts
mixtures
acid
mixture
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Chinese (zh)
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CN107406807A (zh
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C·弗兰兹克
M·莱诺索加西亚
R·巴曼
T·格赖因德尔
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/06—Preparation of carboxylic acid nitriles from N-formylated amino compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
    • C07C227/18—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions involving amino or carboxyl groups, e.g. hydrolysis of esters or amides, by formation of halides, salts or esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/26—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing carboxyl groups by reaction with HCN, or a salt thereof, and amines, or from aminonitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
    • C07C229/10—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C07C229/16—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of hydrocarbon radicals substituted by amino or carboxyl groups, e.g. ethylenediamine-tetra-acetic acid, iminodiacetic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/24—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one carboxyl group bound to the carbon skeleton, e.g. aspartic acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
    • C07C255/24—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms containing cyano groups and singly-bound nitrogen atoms, not being further bound to other hetero atoms, bound to the same saturated acyclic carbon skeleton
    • C07C255/25—Aminoacetonitriles
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Detergent Compositions (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201680014500.8A 2015-03-12 2016-03-02 制备对映体混合物的方法和对映体混合物 Active CN107406807B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP15158841.5 2015-03-12
EP15158841 2015-03-12
PCT/EP2016/054375 WO2016142228A1 (en) 2015-03-12 2016-03-02 Process for making mixtures of enantiomers, and mixtures of enantiomers

Publications (2)

Publication Number Publication Date
CN107406807A CN107406807A (zh) 2017-11-28
CN107406807B true CN107406807B (zh) 2021-03-23

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Family Applications (1)

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CN201680014500.8A Active CN107406807B (zh) 2015-03-12 2016-03-02 制备对映体混合物的方法和对映体混合物

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US (1) US10619125B2 (enExample)
EP (1) EP3268348B1 (enExample)
JP (1) JP6727225B2 (enExample)
KR (1) KR102694078B1 (enExample)
CN (1) CN107406807B (enExample)
BR (1) BR112017019108A2 (enExample)
CA (1) CA2976716A1 (enExample)
ES (1) ES2881309T3 (enExample)
MX (1) MX2017011725A (enExample)
MY (1) MY189265A (enExample)
RU (1) RU2722803C2 (enExample)
WO (1) WO2016142228A1 (enExample)

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RU2019138212A (ru) * 2017-04-27 2021-05-27 Басф Се Контейнер, содержащий композицию моющего средства, содержащую соли mgda и glda
CN113382980B (zh) * 2018-12-21 2024-06-21 诺力昂化学品国际有限公司 甲基甘氨酸n,n-二乙酸的易碎相组合物
US20230135390A1 (en) * 2020-03-03 2023-05-04 Basf Se Process for manufacture of a complexing agent
CN117658857B (zh) * 2022-08-25 2025-11-04 万华化学集团股份有限公司 存储稳定的甲基甘氨酸-n,n-二乙腈组合物、制备方法及其用途

Citations (4)

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WO2010139755A1 (en) * 2009-06-05 2010-12-09 Akzo Nobel Chemicals International B.V. Process to prepare a chelating agent or precursor thereof using a cyanide salt
WO2011080540A1 (en) * 2009-12-30 2011-07-07 Ecolab Inc. Phosphate substitutes for membrane-compatible cleaning and/or detergent compositions
WO2011100344A1 (en) * 2010-02-09 2011-08-18 Basf Se Detergent composition
WO2012150155A1 (de) * 2011-05-03 2012-11-08 Basf Se Verfahren zur herstellung eines kristallinen l-mgda-trialkalimetallsalzes

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US5837663A (en) 1996-12-23 1998-11-17 Lever Brothers Company, Division Of Conopco, Inc. Machine dishwashing tablets containing a peracid
DE19819187A1 (de) 1998-04-30 1999-11-11 Henkel Kgaa Festes maschinelles Geschirrspülmittel mit Phosphat und kristallinen schichtförmigen Silikaten
DE102005021055A1 (de) * 2005-05-06 2006-11-09 Basf Ag Verfahren zur Herstellung von nebenproduktarmen Methylglycin-N,N-diessigsäure-Trialkalimetallsalzen
GB0522659D0 (en) * 2005-11-07 2005-12-14 Reckitt Benckiser Nv Delivery cartridge
DE102007019458A1 (de) * 2007-04-25 2008-10-30 Basf Se Phosphatfreies Maschinengeschirrspülmittel mit ausgezeichneter Klarspülleistung
WO2009024518A1 (en) * 2007-08-17 2009-02-26 Akzo Nobel N.V. Alkali metal salt of glutamic acid n,n-diacetic acid, a process to prepare such salt, and the use thereof
GB0716228D0 (en) * 2007-08-20 2007-09-26 Reckitt Benckiser Nv Detergent composition
WO2010004798A1 (ja) * 2008-07-08 2010-01-14 シャープ株式会社 照明装置および液晶表示装置
CN102666828B (zh) 2009-12-24 2014-07-30 阿克佐诺贝尔化学国际公司 谷氨酸n,n-二乙酸盐螯合剂的涂覆颗粒
WO2011141566A2 (de) * 2010-05-14 2011-11-17 Compo Gmbh & Co. Kg Köderformulierungen zur bekämpfung von schnecken
AU2011200525B8 (en) 2010-12-17 2016-10-13 Akzo Nobel Chemicals International B.V. Environmentally friendly stimulation fluids, processes to create wormholes in carbonate reservoirs, and processes to remove wellbore damage in carbonate reservoirs
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JP5914632B2 (ja) * 2011-04-04 2016-05-11 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ メチルグリシン−ｎ，ｎ−二酢酸三アルカリ金属塩の水溶液の製造方法
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US9227915B2 (en) * 2011-05-03 2016-01-05 Basf Se Process for the preparation of a crystalline L-MGDA trialkali metal salt
DE102011084934A1 (de) 2011-10-21 2013-04-25 Henkel Ag & Co. Kgaa Klarspül- und Geschirrspülmittel
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EP2997121B1 (en) 2013-05-17 2018-12-05 Unilever N.V. Machine dishwash detergent composition
BR112015029557A2 (pt) * 2013-05-27 2020-03-10 Basf Se solução aquosa, processo para fabricação de uma solução aquosa, e, uso de uma solução aquosa
RU2659787C2 (ru) * 2013-05-27 2018-07-04 Басф Се Водные растворы, содержащие комплексообразующий агент в высокой концентрации
WO2015000744A1 (en) * 2013-07-04 2015-01-08 Basf Se Process for cleaning dishware
ES2655195T3 (es) 2013-09-09 2018-02-19 Ecolab Usa Inc. Eliminación sinérgica de manchas mediante una combinación de quelantes nuevos
ES2982202T3 (es) 2013-09-09 2024-10-15 Ecolab Usa Inc Método de lavado de vajilla basado en la eliminación sinérgica de manchas mediante una nueva combinación de quelantes
US9802884B2 (en) * 2013-09-13 2017-10-31 Basf Se Mixtures of MGDA enantiomers, and process for making such mixtures

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WO2010139755A1 (en) * 2009-06-05 2010-12-09 Akzo Nobel Chemicals International B.V. Process to prepare a chelating agent or precursor thereof using a cyanide salt
WO2011080540A1 (en) * 2009-12-30 2011-07-07 Ecolab Inc. Phosphate substitutes for membrane-compatible cleaning and/or detergent compositions
WO2011100344A1 (en) * 2010-02-09 2011-08-18 Basf Se Detergent composition
WO2012150155A1 (de) * 2011-05-03 2012-11-08 Basf Se Verfahren zur herstellung eines kristallinen l-mgda-trialkalimetallsalzes

Also Published As

Publication number Publication date
RU2017136081A3 (enExample) 2019-07-29
RU2017136081A (ru) 2019-04-12
JP6727225B2 (ja) 2020-07-22
US20180237728A1 (en) 2018-08-23
ES2881309T3 (es) 2021-11-29
BR112017019108A2 (pt) 2018-04-17
EP3268348A1 (en) 2018-01-17
JP2018507898A (ja) 2018-03-22
RU2722803C2 (ru) 2020-06-03
KR102694078B1 (ko) 2024-08-09
MY189265A (en) 2022-01-31
EP3268348B1 (en) 2021-05-12
MX2017011725A (es) 2017-11-13
CA2976716A1 (en) 2016-09-15
KR20170128398A (ko) 2017-11-22
US10619125B2 (en) 2020-04-14
WO2016142228A1 (en) 2016-09-15
CN107406807A (zh) 2017-11-28

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