CN107384617A - Low temperature high performance surface degreasing powder and preparation method thereof - Google Patents

Low temperature high performance surface degreasing powder and preparation method thereof Download PDF

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Publication number
CN107384617A
CN107384617A CN201710604750.3A CN201710604750A CN107384617A CN 107384617 A CN107384617 A CN 107384617A CN 201710604750 A CN201710604750 A CN 201710604750A CN 107384617 A CN107384617 A CN 107384617A
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China
Prior art keywords
parts
low temperature
high performance
temperature high
sodium
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CN201710604750.3A
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Chinese (zh)
Inventor
李林
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Wenzhou Yuhui New Mstar Technology Ltd
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Wenzhou Yuhui New Mstar Technology Ltd
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Priority to CN201710604750.3A priority Critical patent/CN107384617A/en
Publication of CN107384617A publication Critical patent/CN107384617A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/83Mixtures of non-ionic with anionic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/08Silicates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/10Carbonates ; Bicarbonates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2075Carboxylic acids-salts thereof
    • C11D3/2086Hydroxy carboxylic acids-salts thereof
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/39Organic or inorganic per-compounds
    • C11D3/3942Inorganic per-compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • C11D1/04Carboxylic acids or salts thereof
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/662Carbohydrates or derivatives

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention discloses a kind of low temperature high performance surface degreasing powder and preparation method thereof.The low temperature high performance surface degreasing powder includes the component of following parts by weight:25 parts of silicate, 12 18 parts of percarbonate, 15 20 parts of sodium carbonate, 8 15 parts of sodium gluconate.Beneficial effects of the present invention:In such as 25 DEG C of low temperature environment, the low temperature high performance surface degreasing powder still has good deoiling effect, without carrying out heating operation, so as to reduce the loss of the energy, increase the convenience of removal operation.

Description

Low temperature high performance surface degreasing powder and preparation method thereof
Technical field
The present invention relates to degreasing powder, more particularly to a kind of low temperature high performance surface degreasing powder and preparation method thereof.
Background technology
It is one of important procedure in industry that cleaning is carried out to workpiece.Workpiece is cleaned primarily directed to some heavy oil in industry The cleaning of stain workpiece, it directly influences the use function and aesthetic property of workpiece.Some heavy oil stain workpiece are all using organic at present Solvent is cleaned, but due to organic solvent component, content and preparation method the defects of, easily have to health larger Influence.
Degreasing powder is to be removed using refined low bubbles formed such as a variety of high-quality surfactants, detergent, bleeding agent, builders Oily degreasing agent, there is the abilities such as good wetting, emulsification, there is stronger ability of deoiling.Workpiece surface after cleaning is without visible oil Film or oil mark.It is mainly used in the cleaning of the alloy materials such as aluminium alloy, kirsite, magnesium alloy to degreaser, to workpiece not damaged Phenomenon.
Publication No. CN104451752A Chinese patent discloses a kind of degreasing powder for cleaning heavy oil stain and its preparation side Method.The deoiling effect of the degreasing powder is stronger, and service life is longer, improves the technological difficulties of counterweight oil stain multiple working procedure cleaning, has Effect improves operating efficiency.
But from embodiment it was found from, the degreasing powder needs to be used in temperature is 80 DEG C or so of environment.Change Yan Zhi, it is necessary to which the cleaning fluid that degreasing powder is configured to is heated to 80 DEG C or so when using the degreasing powder, it can reach preferable Deoiling effect.And the loss that this undoubtedly needs to increase the energy.As common knowledge, with the rise of temperature, degreasing powder removes Oily effect is typically stronger.Therefore, how preferable deoiling effect is maintained in such as 25 DEG C of low temperature environment, is urgently Solve the problems, such as.
The content of the invention
It is an object of the invention to provide a kind of low temperature high performance surface degreasing powder.In such as 25 DEG C of low temperature environment, this is low Temperature high-performance surface degreasing powder still has good deoiling effect, without carrying out heating operation, so as to reduce the loss of the energy, Increase the convenience of removal operation.
The present invention above-mentioned technical purpose technical scheme is that:
A kind of low temperature high performance surface degreasing powder, include the component of following parts by weight:
Silicate 2-5 parts
Percarbonate 12-18 parts
Sodium carbonate 15-20 parts
Sodium gluconate 8-15 parts.
By using above-mentioned technical proposal, silicate has the distinctive property of softening, dispersiveness, suspension and inorganic emulsibility With the strong attraction to greasy dirt.Percarbonate is the additive compound of carbonate and hydrogen peroxide, white particulate powder, water Solution alkaline.Percarbonate can be decomposed into sodium carbonate and hydrogen peroxide in water, hydrogen peroxide continue to be decomposed into again water and Oxygen.SODIUM PERCARBONATE is the unstable compound formed by sodium carbonate, hydrogen peroxide and water three compositions system using hydrogen bond, Easily decompose at high temperature.Sodium carbonate has stronger alkalescence, can promote the saponification of grease.Sodium gluconate is a kind of metal The highly effective chelating agent of surface treatment, it can be used in chelating the metal ions such as calcium, magnesium, softening of water.
The present invention is further arranged to:According to parts by weight, in addition to spaonin powder 15-20 parts.
By using above-mentioned technical proposal, spaonin powder is gleditsia sinensis grinds.Gleditsia sinensis is the peculiar hungry Caesalpiniaceae Chinese honey locust in China Belong to one of seeds.The main chemical compositions of gleditsia sinensis are Gleditschiasaponin, palmitic acid, stearic acid, oleic acid.Spaonin powder is a kind of plant table Face activating agent.Metal deoiling after spaonin powder is handled, blast is polished after plating.Using spaonin powder to metal surface without appoint What corrodes.
The present invention is further arranged to:According to parts by weight, in addition to ethylenediamine oleate 15-20 parts.
By using above-mentioned technical proposal, ethylenediamine oleate belongs to nonionic surfactant, with other surfaces activity Agent compatibility is good, and dissolving power is strong, does not produce oil slick, has certain deoiling effect, more preferably, persistence is longer for rust-proof effect.
The present invention is further arranged to:The silicate selects sodium metasilicate.
By using above-mentioned technical proposal, because the cation in sodium carbonate, grape grape acid sodium is sodium ion, therefore select Bringing into for variety classes cation can be reduced with sodium metasilicate.It is water-soluble preferable meanwhile the ionic radius of sodium ion is smaller.
The present invention is further arranged to:The percarbonate selects SODIUM PERCARBONATE.
By using above-mentioned technical proposal, because the cation in sodium carbonate, grape grape acid sodium is sodium ion, therefore select Bringing into for variety classes cation can be reduced with SODIUM PERCARBONATE.It is water-soluble preferable meanwhile the ionic radius of sodium ion is smaller.
Another goal of the invention of the present invention is to provide a kind of preparation method of low temperature high performance surface degreasing powder, including as follows Step:According to parts by weight, silicate 2-5 parts, percarbonate 12-18 parts, sodium carbonate 15-20 parts, sodium gluconate 8-15 are weighed Part, spaonin powder 15-20 parts, ethylenediamine oleate 15-20 parts, it is well mixed.
By using above-mentioned technical proposal, each component is sufficiently mixed, the low temperature with good deoiling effect is prepared High performance surface degreasing powder.
In summary, the invention has the advantages that:
1st, the present invention can have good deoiling effect under such as 25 DEG C of low temperature environment, without carrying out heating operation, so as to The loss of the energy is reduced, increases the convenience of removal operation;
2nd, SODIUM PERCARBONATE can produce oxygen in water, so as to realize the oxidation Decomposition to grease, promote the dissolving of grease;
3rd, spaonin powder and ethylenediamine oleate are used in conjunction with, and can cooperate with enhancing deoiling effect.
Embodiment
Embodiment 1
A kind of low temperature high performance surface degreasing powder, include the component of following parts by weight:
2 parts of sodium metasilicate, 18 parts of SODIUM PERCARBONATE, 20 parts of sodium carbonate, 8 parts of sodium gluconate, 16 parts of spaonin powder, ethylenediamine oleate 20 Part.
A kind of preparation method of low temperature high performance surface degreasing powder, comprises the following steps:
According to parts by weight, 2 parts of sodium metasilicate, 18 parts of SODIUM PERCARBONATE, 20 parts of sodium carbonate, 8 parts of sodium gluconate, spaonin powder 16 are weighed Part, 20 parts of ethylenediamine oleate, it is well mixed.
Embodiment 2
A kind of low temperature high performance surface degreasing powder, include the component of following parts by weight:
4 parts of sodium metasilicate, 17 parts of SODIUM PERCARBONATE, 19 parts of sodium carbonate, 10 parts of sodium gluconate, 17 parts of spaonin powder, ethylenediamine oleate 15 parts.
A kind of preparation method of low temperature high performance surface degreasing powder, comprises the following steps:
According to parts by weight, 4 parts of sodium metasilicate, 17 parts of SODIUM PERCARBONATE, 19 parts of sodium carbonate, 10 parts of sodium gluconate, spaonin powder 17 are weighed Part, 15 parts of ethylenediamine oleate, it is well mixed.
Embodiment 3
A kind of low temperature high performance surface degreasing powder, include the component of following parts by weight:
3 parts of sodium metasilicate, 16 parts of SODIUM PERCARBONATE, 15 parts of sodium carbonate, 12 parts of sodium gluconate, 18 parts of spaonin powder, ethylenediamine oleate 16 parts.
A kind of preparation method of low temperature high performance surface degreasing powder, comprises the following steps:
According to parts by weight, 3 parts of sodium metasilicate, 16 parts of SODIUM PERCARBONATE, 15 parts of sodium carbonate, 12 parts of sodium gluconate, spaonin powder 18 are weighed Part, 16 parts of ethylenediamine oleate, it is well mixed.
Embodiment 4
A kind of low temperature high performance surface degreasing powder, include the component of following parts by weight:
5 parts of sodium metasilicate, 15 parts of SODIUM PERCARBONATE, 16 parts of sodium carbonate, 15 parts of sodium gluconate, 15 parts of spaonin powder, ethylenediamine oleate 18 parts.
A kind of preparation method of low temperature high performance surface degreasing powder, comprises the following steps:
According to parts by weight, 5 parts of sodium metasilicate, 15 parts of SODIUM PERCARBONATE, 16 parts of sodium carbonate, 15 parts of sodium gluconate, spaonin powder 15 are weighed Part, 18 parts of ethylenediamine oleate, it is well mixed.
Embodiment 5
A kind of low temperature high performance surface degreasing powder, include the component of following parts by weight:
3 parts of sodium metasilicate, 18 parts of SODIUM PERCARBONATE, 17 parts of sodium carbonate, 11 parts of sodium gluconate, 20 parts of spaonin powder, ethylenediamine oleate 19 parts.
A kind of preparation method of low temperature high performance surface degreasing powder, comprises the following steps:
According to parts by weight, 3 parts of sodium metasilicate, 18 parts of SODIUM PERCARBONATE, 17 parts of sodium carbonate, 11 parts of sodium gluconate, spaonin powder 20 are weighed Part, 19 parts of ethylenediamine oleate, it is well mixed.
Embodiment 6
A kind of low temperature high performance surface degreasing powder, include the component of following parts by weight:
3 parts of sodium metasilicate, 16 parts of SODIUM PERCARBONATE, 15 parts of sodium carbonate, 12 parts of sodium gluconate.
A kind of preparation method of low temperature high performance surface degreasing powder, comprises the following steps:
According to parts by weight, 3 parts of sodium metasilicate, 16 parts of SODIUM PERCARBONATE, 15 parts of sodium carbonate, 12 parts of sodium gluconate are weighed, is well mixed .
Comparative example 1
From the embodiment 1 as a comparison case 1 of Publication No. CN104451752A Chinese patent.
Comparative example 2
Difference with embodiment 3 is, changes ethylenediamine oleate into trihydroxy ethylamine oleate soap, other are same as Example 3.
Comparative example 3
Difference with embodiment 3 is, removes spaonin powder, other are same as Example 3.
Comparative example 4
Difference with embodiment 3 is, changes ethylenediamine oleate into trihydroxy ethylamine oleate soap and removes spaonin powder, other with Embodiment 3 is identical.
Except oil test
By ready stainless steel test piece, hung up properly, be placed in constant temperature oven with hook, control temperature as 130 ± 2 DEG C of baking 20min Cooling is weighed afterwards, the degree of accuracy to 0.0001g, and the test piece after weighing is absorbed into artificial greasy dirt with small pieces uniformly coats, and will coat The test piece of oil is hung up properly with hook, is put into constant temperature oven, and temperature control is dried 2 hours at 130 ± 2 DEG C, is weighed after taking out cooling 8h.
In 500mL beakers, the degreasing powder according to embodiment 1-6 and comparative example 1-4 preparations is configured to 3wt% concentration The cleaning fluid of (15g → 500ml).It is 25 DEG C to control temperature, and the test piece for coating oil is placed in cleaning fluid, and then pendulum is washed 5 minutes, Pendulum takes out after washing and rinsed well, is put into 130 ± 2 DEG C of thermostatic drying chamber and dries 20 minutes, is weighed after cooling, calculates oil removing Rate.
Calculate:X1=(m1-m2)/(m1-m0) × 100%
In formula:X1- is oil removal rate/%;M0- is quality/g of test piece;M1- is test piece quality/g after oiling;After m2- is cleaning Test piece quality/g.
The embodiment 1-6 of table 1 and comparative example 1-4 oil removal rate record sheets
It can be drawn from table 1 to draw a conclusion:
Oil removal rate/%
Embodiment 1 93.21
Embodiment 2 95.54
Embodiment 3 97.64
Embodiment 4 93.21
Embodiment 5 92.16
Embodiment 6 75.34
Comparative example 1 67.34
Comparative example 2 83.42
Comparative example 3 80.14
Comparative example 4 80.17
Comparative example 1-6 and comparative example 1 understand that embodiment 1-6 oil removal rate is all higher than comparative example 1, it is seen that the present invention is right In being superior to comparative example 1 on the removal capacity of greasy dirt.
Comparative example 3 and comparative example 2-4 understand that, compared to embodiment 3, comparative example 2-4 oil removal rate is smaller.Its In, the oil removal rate of comparative example 2 is more than comparative example 3 and comparative example 4, and comparative example 3 is equal with the oil removal rate of comparative example 4.Therefore, it is single Solely change trihydroxy ethylamine oleate soap into ethylenediamine oleate, the oil removing performance of degreasing powder is constant.Individually increase spaonin powder, degreasing powder Oil removing performance increase.But when changing trihydroxy ethylamine oleate soap into ethylenediamine oleate simultaneously and increasing spaonin powder, oil removing Performance can further enhance.As can be seen here, ethylenediamine oleate and spaonin powder be used in conjunction with can further lift oil removing Performance.
This specific embodiment is only explanation of the invention, and it is not limitation of the present invention, people in the art Member can make the modification of no creative contribution to the present embodiment as needed after this specification is read, but as long as at this All protected in the right of invention by Patent Law.

Claims (6)

1. a kind of low temperature high performance surface degreasing powder, it is characterized in that:Include the component of following parts by weight:
Silicate 2-5 parts
Percarbonate 12-18 parts
Sodium carbonate 15-20 parts
Sodium gluconate 8-15 parts.
2. low temperature high performance surface degreasing powder according to claim 1, it is characterized in that:According to parts by weight, in addition to gleditsia sinensis Powder 15-20 parts.
3. low temperature high performance surface degreasing powder according to claim 1, it is characterized in that:According to parts by weight, in addition to second two Amine oleate 15-20 parts.
4. low temperature high performance surface degreasing powder according to claim 1, it is characterized in that:The silicate selects sodium metasilicate.
5. low temperature high performance surface degreasing powder according to claim 1, it is characterized in that:The percarbonate selects percarbonic acid Sodium.
6. a kind of preparation method of low temperature high performance surface degreasing powder, it is characterized in that:Comprise the following steps:According to parts by weight, claim Take silicate 2-5 parts, percarbonate 12-18 parts, sodium carbonate 15-20 parts, sodium gluconate 8-15 parts, spaonin powder 15-20 parts, second Diamines oleate 15-20 parts, it is well mixed.
CN201710604750.3A 2017-07-22 2017-07-22 Low temperature high performance surface degreasing powder and preparation method thereof Pending CN107384617A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107815691A (en) * 2017-12-20 2018-03-20 苏州德菱化学品有限公司 A kind of aluminium workpiece surface nano aperture processing method for nanometer injection
CN108485847A (en) * 2018-05-05 2018-09-04 深圳市竑鎏电子表面处理科技有限公司 A kind of room temperature degreasing powder
CN111057619A (en) * 2019-12-16 2020-04-24 青岛中科润美润滑材料技术有限公司 Cleaning agent for needle threading, coking and carbon deposition of artificial board equipment
CN112143576A (en) * 2020-10-21 2020-12-29 湖南澳美佳健康科技有限公司 Production process of sodium bicarbonate cleanser without damaging skin

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CN1087940A (en) * 1993-10-07 1994-06-15 柏绿山 A kind of multipurpose sterilizing detergent
CN103013688A (en) * 2011-09-20 2013-04-03 孙善家 Laundry grease stain cleaning agent
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107815691A (en) * 2017-12-20 2018-03-20 苏州德菱化学品有限公司 A kind of aluminium workpiece surface nano aperture processing method for nanometer injection
CN108485847A (en) * 2018-05-05 2018-09-04 深圳市竑鎏电子表面处理科技有限公司 A kind of room temperature degreasing powder
CN108485847B (en) * 2018-05-05 2020-10-20 深圳市竑鎏电子表面处理科技有限公司 Normal-temperature oil removing powder
CN111057619A (en) * 2019-12-16 2020-04-24 青岛中科润美润滑材料技术有限公司 Cleaning agent for needle threading, coking and carbon deposition of artificial board equipment
CN111057619B (en) * 2019-12-16 2021-07-30 青岛中科润美润滑材料技术有限公司 Cleaning agent for needle threading, coking and carbon deposition of artificial board equipment
CN112143576A (en) * 2020-10-21 2020-12-29 湖南澳美佳健康科技有限公司 Production process of sodium bicarbonate cleanser without damaging skin

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Application publication date: 20171124