CN107384119A - Color brilliant self-leveling floor coating of a kind of non-solvent epoxy and preparation method thereof - Google Patents
Color brilliant self-leveling floor coating of a kind of non-solvent epoxy and preparation method thereof Download PDFInfo
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- CN107384119A CN107384119A CN201710482431.XA CN201710482431A CN107384119A CN 107384119 A CN107384119 A CN 107384119A CN 201710482431 A CN201710482431 A CN 201710482431A CN 107384119 A CN107384119 A CN 107384119A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/50—Amines
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/50—Amines
- C08G59/5026—Amines cycloaliphatic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/36—Silica
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses color brilliant self-leveling floor coating of a kind of non-solvent epoxy and preparation method thereof, the floor coatings include component A and B component, and the mass ratio of component A and B component is 5:1~7:1；The component A is prepared by the raw material of following mass parts：25~33 parts of liquid-state epoxy resin, 2~5 parts of epoxy active diluent, 0.4~0.7 part of dispersant, 0.8~1.2 part of defoamer, 0.3~0.7 part of levelling agent, 48~54 parts of silicon powder, 12~18 parts of flashlight powder；The B component is amine curing agent.The floor coatings VOC content of the present invention is low, safety and environmental protection, preparation method is simple, and the terrace surface formed can produce diffusing reflection to light, and gloss is soft, comfort level is high, terrace third dimension is strong, ornamental strong, the excellent performance such as hardness, wear-resisting, resistance to compression and chemical resistance is easy to clean, service life is grown, and has a good application prospect and industrial production potential.
Description
Technical field
The present invention relates to color brilliant self-leveling floor coating of a kind of non-solvent epoxy and preparation method thereof, belong to coating technology neck
Domain.
Background technology
Developed rapidly as Chinese society economic level improves constantly with science and technology, people's living standard there has also been very big
Lifting, Process of Urbanization Construction scale constantly expands, and the interior decoration industry of building has good development space, requires simultaneously
Also it is higher, not only to accomplish decoration, more to defer to safety and environmental protection, save the energy, reduce the multinomial principles such as pollution.
Solvent based coating needs to use substantial amounts of volatile organic matter (VOC) in production, construction and solidification process, not only
The health of people is influenceed, and the atmospheric environment that people depend on for existence can be damaged, such as causes photochemical reaction, is produced
Third contact of a total solar or lunar eclipse chemical fumes, and then more serious harm is caused to human health.In recent years, many western developed countries had promulgated method
Order, discharge species, discharge capacity to organic matter are controlled, and China has also promulgated corresponding regulation.Traditional solvent based coating
Huge challenge is faced with, it has been trend of the times to develop no-solvent type coating or water paint.
Organic or inorganic toner is added in traditional solvent-free epoxy self-leveling terrace, such as titanium dioxide, carbon black, medium chrome yellow, lemon
Lemon Huang, phthalocyanine blue and dark green etc., required color is modulated by the way that they are used in combination, though smooth attractive in appearance, decoration
Property is inadequate.The color brilliant gravity flow self-leveling floor of non-solvent epoxy has selected flashlight powder lucuriant in design, and steamed bun spreads man-hour flashlight powder can companion
Epoxy flooring coating is evenly distributed on ground, and flashlight powder can float up to surface before coating surface drying, after solidification, flashlight powder just by
Fixation is embedded in epoxide terrace coating, not only smooth attractive in appearance, and also enhances the visual effect of coating, makes decorative parts recessed
It is convex to have levels, more third dimension.The color brilliant gravity flow self-leveling floor of non-solvent epoxy is a kind of seamless integrated novel decorative terrace, phase
Than in common epoxy self-leveling floor, the color brilliant terrace of non-solvent epoxy has more superior decoration functions and using function, no
Only seem graceful dignified, also there are a variety of advantages such as wear-resistant, resistance to compression, corrosion-resistant, anti-skidding, waterproof, be applied not only to industrial ground
Level ground, it can be used for again in business or civil construction thing.
The content of the invention
It is an object of the invention to provide color brilliant self-leveling floor coating of a kind of non-solvent epoxy and preparation method thereof.
The technical solution used in the present invention is：
A kind of quality of the color brilliant self-leveling floor coating of non-solvent epoxy, including component A and B component, component A and B component
Than for 5:1~7:1；The component A is prepared by the raw material of following mass parts：25~33 parts of liquid-state epoxy resin, epoxy are lived
2~5 parts of diluent of property, 0.4~0.7 part of dispersant, 0.8~1.2 part of defoamer, 0.3~0.7 part of levelling agent, silicon powder 48~
54 parts, 12~18 parts of flashlight powder；The B component is amine curing agent.
The liquid-state epoxy resin is in bisphenol A type epoxy resin, bisphenol f type epoxy resin, aliphatic epoxy resin
It is at least one.
The epoxy active diluent is butyl glycidyl ether, C12~C14Aliphatic polyol glycidol ether, benzyl
At least one of base glycidol ether.
The dispersant be BYK-104S, BYK-110, the modest Disponer 904 of moral, EFKA-405, EFKA-5065,
At least one of UNIQCHEM UNIQSPERSE 560S, UNIQCHEM UNIQSPERSE 765S.
The defoamer be moral is modest 5500, moral is modest 6800, in EFKA-2722, TEGO 900, Lenze LC-179 at least
It is a kind of.
The levelling agent is EFKA-3239, BYK-354, TEGO Glide B 1484, moral are modest 495, Lenze LC-178
At least one of.
The particle diameter of the silicon powder is 10~25 μm.
The particle diameter of the flashlight powder is 0.07~0.5mm.
The amine curing agent is one kind in modified aliphatic cyclic amine, modified polyether amine, modified mixed amine.
The preparation method of the color brilliant self-leveling floor coating of above-mentioned non-solvent epoxy comprises the following steps：
1) liquid-state epoxy resin and epoxy active diluent are well mixed, then sequentially add dispersant while stirring, disappears
Infusion and levelling agent, it is well mixed；
2) silicon powder is added while stirring, is well mixed, and is filtered with 80 mesh filter screens；
3) flashlight powder is added while stirring, is well mixed, is obtained component A；
4) it is when using that component A and B component is well mixed.
The beneficial effects of the invention are as follows：The color brilliant self-leveling floor coating VOC content of the non-solvent epoxy of the present invention is low, safety
Environmental protection, preparation method is simple, and the terrace surface formed can produce diffusing reflection to light, and gloss is soft, comfort level is high, and terrace is three-dimensional
Sense is strong, and ornamental strong, the excellent performance such as hardness, wear-resisting, resistance to compression and chemical resistance is easy to clean, service life length, has
Good application prospect and industrial production potential, it can be widely applied to the top grade entertainment place high to aesthetic, hotel, machine
Field, subway, megastore, Business Building, conference and exhibition center, office and laboratory etc..
1) present invention spreads man-hour flashlight powder from the conventional organic or inorganic toner of flashlight powder substitution lucuriant in design, steamed bun
It can be evenly distributed in company with epoxide terrace paint on ground, because flash of light powder density can gentlier float up to surface before coating surface drying,
Flashlight powder is just embedded in epoxide terrace coating by fixation after solidification, not only smooth attractive in appearance, and decorative parts bumps have levels, and is stood
Body-sensing is strong, and its height flasher characteristic make it that ornament is dazzlingly beautiful, adds brilliance doubly, and its color can freely allocate combination, and color is rich
Richness, good decorating effect, texture is strong, great Modern Decorative style, in addition, the flashlight powder for floating up to surface can be produced to light and overflow
Reflect and show soft gloss, overcome common epoxy self-leveling coating because of bloom mirror-reflection and caused by light stimulus,
Improve the comfort level of terrace；
2) present invention adds low oil absorption ferric and the good silicon powder of reservoir stability, obtained product in liquid-state epoxy resin
VOC content is low, meets environmental protection concept, harmless.
Embodiment
A kind of quality of the color brilliant self-leveling floor coating of non-solvent epoxy, including component A and B component, component A and B component
Than for 5:1~7:1；The component A is prepared by the raw material of following mass parts：25~33 parts of liquid-state epoxy resin, epoxy are lived
2~5 parts of diluent of property, 0.4~0.7 part of dispersant, 0.8~1.2 part of defoamer, 0.3~0.7 part of levelling agent, silicon powder 48~
54 parts, 12~18 parts of flashlight powder；The B component is amine curing agent.
Preferably, the liquid-state epoxy resin is bisphenol A type epoxy resin, bisphenol f type epoxy resin, aliphatic epoxy tree
At least one of fat.
It is further preferred that the liquid-state epoxy resin is bisphenol A type epoxy resin.
Still further preferably, the liquid-state epoxy resin is brominated bisphenol a type epoxy resin.
Preferably, the epoxy active diluent is butyl glycidyl ether, C12~C14Aliphatic polyol shrink it is sweet
At least one of oily ether, benzyl glycidyl ether.
Preferably, the dispersant is BYK-104S, BYK-110, the modest Disponer 904 of moral, EFKA-405, EFKA-
5065th, at least one of UNIQCHEM UNIQSPERSE 560S, UNIQCHEM UNIQSPERSE 765S.
Preferably, the defoamer is that moral is modest 5500, moral is modest 6800, EFKA-2722, TEGO 900, Lenze LC-179
At least one of.
Preferably, the levelling agent is EFKA-3239, BYK-354, TEGO Glide B 1484, moral are modest 495,
At least one of LenzeLC-178.
Preferably, the particle diameter of the silicon powder is 10~25 μm.
Preferably, the particle diameter of the flashlight powder is 0.07~0.5mm.
Preferably, the amine curing agent is one kind in modified aliphatic cyclic amine, modified polyether amine, modified mixed amine.
The preparation method of the color brilliant self-leveling floor coating of above-mentioned non-solvent epoxy comprises the following steps：
1) liquid-state epoxy resin and epoxy active diluent are well mixed, then sequentially add dispersant while stirring, disappears
Infusion and levelling agent, it is well mixed；
2) silicon powder is added while stirring, is well mixed, and is filtered with 80 mesh filter screens；
3) flashlight powder is added while stirring, is well mixed, is obtained component A；
4) it is when using that component A and B component is well mixed.
Preferably, the preparation method of the color brilliant self-leveling floor coating of above-mentioned non-solvent epoxy comprises the following steps：
1) liquid-state epoxy resin and epoxy active diluent are added into mixer, starts stirring, 300~500r/min's
Dispersant, defoamer and levelling agent are sequentially added under rotating speed, then rotating speed rises to 800~1000r/min, stirs 5~10min；
2) silicon powder is added under 300~500r/min rotating speed, then rotating speed rises to 800~1000r/min, stirring 30
~40min, filtered with 80 mesh filter screens；
3) flashlight powder is added under 300~500r/min rotating speed, then rotating speed rises to 500~800r/min, stirring 10
~15min, obtains component A；
4) it is when using that component A and B component is well mixed.
The present invention is made further explanation and description with reference to specific embodiment.
Embodiment 1：
A kind of color brilliant self-leveling floor coating of non-solvent epoxy, its raw material composition are as follows：
The raw material composition of component A is as shown in table 1：
The raw material composition table of table 1A components
| Component | The trade mark or component | Mass parts |
| Liquid-state epoxy resin | South Asia NPEL-128 | 28 |
| Epoxy active diluent | Benzyl glycidyl ether | 4 |
| Dispersant | UNIQSPERSE 560S | 0.4 |
| Dispersant | UNIQSPERSE 765S | 0.3 |
| Defoamer | TEGO 900 | 0.5 |
| Defoamer | Lenze LC-179 | 0.5 |
| Levelling agent | Lenze LC-178 | 0.3 |
| Silicon powder | 600 mesh active micro silicon powders | 51 |
| Flashlight powder | Dark green flashlight powder | 15 |
B component：Modified aliphatic cyclic amine G2109 curing agent；
In use, by component A and B component according to mass ratio 5:1~7:1 is well mixed.
Embodiment 2：
A kind of color brilliant self-leveling floor coating of non-solvent epoxy, its raw material composition are as follows：
The raw material composition of component A is as shown in table 2：
The raw material composition table of table 2A components
B component：Modified aliphatic cyclic amine G2107 curing agent；
In use, by component A and B component according to mass ratio 5:1~7:1 is well mixed.
Embodiment 3：
A kind of color brilliant self-leveling floor coating of non-solvent epoxy, its raw material composition are as follows：
The raw material composition of component A is as shown in table 3：
The raw material composition table of table 3A components
| Component | The trade mark or component | Mass parts |
| Liquid-state epoxy resin | South Asia NPEF-170 | 25 |
| Epoxy active diluent | Benzyl glycidyl ether | 5 |
| Dispersant | EFKA-4050 | 0.4 |
| Dispersant | EFKA-5065 | 0.3 |
| Defoamer | TEGO 900 | 0.5 |
| Defoamer | Moral modest 5500 | 0.5 |
| Levelling agent | TEGO Glide B 1484 | 0.3 |
| Levelling agent | Moral modest 495 | 0.3 |
| Silicon powder | 1250 mesh active micro silicon powders | 50.7 |
| Flashlight powder | Purple flashlight powder | 17 |
B component：Modified aliphatic cyclic amine G2108 curing agent；
In use, by component A and B component according to mass ratio 5:1~7:1 is well mixed.
Test case：
The color brilliant self-leveling floor coating of non-solvent epoxy prepared by embodiment 1 is according to component A：B component=6:1 is mixed
Close, stir, at 25 DEG C, the method applied using steamed bun is coated on the ground, then using the defoaming vertical and horizontal roller coating of roller coating, solidification
24h, the color brilliant gravity flow self-leveling floor of non-solvent epoxy is obtained, carries out performance test, test result is as shown in table 4.
The performance test results of the color brilliant gravity flow self-leveling floor of the non-solvent epoxy of table 4
Above-described embodiment is the preferable embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any Spirit Essences without departing from the present invention with made under principle change, modification, replacement, combine, simplification,
Equivalent substitute mode is should be, is included within protection scope of the present invention.
Claims (10)
- A kind of 1. color brilliant self-leveling floor coating of non-solvent epoxy, it is characterised in that：Including component A and B component, component A and B groups The mass ratio divided is 5:1~7:1；The component A is prepared by the raw material of following mass parts：Liquid-state epoxy resin 25~33 Part, 2~5 parts of epoxy active diluent, 0.4~0.7 part of dispersant, 0.8~1.2 part of defoamer, 0.3~0.7 part of levelling agent, silicon 48~54 parts of micro mist, 12~18 parts of flashlight powder；The B component is amine curing agent.
- 2. the color brilliant self-leveling floor coating of non-solvent epoxy according to claim 1, it is characterised in that：The liquid epoxy Resin is at least one of bisphenol A type epoxy resin, bisphenol f type epoxy resin, aliphatic epoxy resin.
- 3. the color brilliant self-leveling floor coating of non-solvent epoxy according to claim 1, it is characterised in that：The epoxy-reactive Diluent is butyl glycidyl ether, C12~C14Aliphatic polyol glycidol ether, in benzyl glycidyl ether at least It is a kind of.
- 4. the color brilliant self-leveling floor coating of non-solvent epoxy according to claim 1, it is characterised in that：The dispersant is The modest Disponer 904 of BYK-104S, BYK-110, moral, EFKA-405, EFKA-5065, UNIQCHEM UNIQSPERSE At least one of 560S, UNIQCHEM UNIQSPERSE 765S.
- 5. the color brilliant self-leveling floor coating of non-solvent epoxy according to claim 1, it is characterised in that：The defoamer is Moral is modest 5500, moral is modest 6800, at least one of EFKA-2722, TEGO 900, Lenze LC-179.
- 6. the color brilliant self-leveling floor coating of non-solvent epoxy according to claim 1, it is characterised in that：The levelling agent is EFKA-3239, BYK-354, TEGO Glide B 1484, moral are modest 495, at least one of Lenze LC-178.
- 7. the color brilliant self-leveling floor coating of non-solvent epoxy according to claim 1, it is characterised in that：The silicon powder Particle diameter is 10~25 μm.
- 8. the color brilliant self-leveling floor coating of non-solvent epoxy according to claim 1, it is characterised in that：The flashlight powder Particle diameter is 0.07~0.5mm.
- 9. the color brilliant self-leveling floor coating of non-solvent epoxy according to claim 1, it is characterised in that：The amine-type cure Agent is one kind in modified aliphatic cyclic amine, modified polyether amine, modified mixed amine.
- 10. the preparation method of the color brilliant self-leveling floor coating of non-solvent epoxy in claim 1~9 described in any one, its It is characterised by：Comprise the following steps：1) liquid-state epoxy resin and epoxy active diluent are well mixed, then sequentially add dispersant, defoamer while stirring And levelling agent, it is well mixed；2) silicon powder is added while stirring, is well mixed, and is filtered with 80 mesh filter screens；3) flashlight powder is added while stirring, is well mixed, is obtained component A；4) it is when using that component A and B component is well mixed.
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108342144A (en) * | 2018-03-09 | 2018-07-31 | 青岛舜捷通生物科技有限公司 | A kind of environment-friendly epoxy floor paint and preparation method thereof |
| CN108676460A (en) * | 2018-05-03 | 2018-10-19 | 广州挚业化工有限公司 | A kind of brilliant color terrace decorative paint and preparation method thereof |
| CN108929612A (en) * | 2018-05-29 | 2018-12-04 | 富思特新材料科技发展股份有限公司 | A kind of illusion-colour flash of light terrace finishing coat |
| CN109439171A (en) * | 2018-12-01 | 2019-03-08 | 金美云 | A kind of environment-friendly epoxy floor coatings and its preparation method and application |
| CN110003766A (en) * | 2019-03-20 | 2019-07-12 | 河北晨阳工贸集团有限公司 | A kind of environment-friendly solvent-free epoxy flash of light artistic floors paint and preparation method thereof |
| CN110144161A (en) * | 2019-06-11 | 2019-08-20 | 江苏绿带新材料科技有限公司 | A kind of solvent-free Self-leveling paint of water-base epoxy |
| CN110437705A (en) * | 2019-06-26 | 2019-11-12 | 河北晨阳工贸集团有限公司 | A kind of antibacterial and mouldproof floor paint and preparation method thereof |
| CN110614708A (en) * | 2019-10-22 | 2019-12-27 | 上海典跃建材科技有限公司 | Grindstone component and laying method thereof |
| CN110616024A (en) * | 2019-09-24 | 2019-12-27 | 东莞市东升地坪材料有限公司 | Wear-resistant floor coating and construction method thereof |
| CN111500017A (en) * | 2020-05-07 | 2020-08-07 | 上海博珥建材有限公司 | Epoxy resin floor material and preparation method thereof |
| CN111690232A (en) * | 2020-06-24 | 2020-09-22 | 雷帝(中国)建筑材料有限公司 | Solvent-free epoxy joint mixture and preparation method thereof |
| CN112063271A (en) * | 2020-09-11 | 2020-12-11 | 启东维度化工科技有限公司 | Solvent-free flash epoxy color sand self-leveling finish paint and preparation method thereof |
| CN112409833A (en) * | 2020-11-19 | 2021-02-26 | 广西帝品建材有限公司 | Decorative wear-resistant epoxy color paste-free high-definition colored sand self-leveling |
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| CN115700265A (en) * | 2022-10-09 | 2023-02-07 | 广东花王涂料有限公司 | Self-leveling coating and preparation method and application thereof |
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| CN108342144A (en) * | 2018-03-09 | 2018-07-31 | 青岛舜捷通生物科技有限公司 | A kind of environment-friendly epoxy floor paint and preparation method thereof |
| CN108676460A (en) * | 2018-05-03 | 2018-10-19 | 广州挚业化工有限公司 | A kind of brilliant color terrace decorative paint and preparation method thereof |
| CN108676460B (en) * | 2018-05-03 | 2020-06-30 | 广州挚业化工有限公司 | Crystal color floor decorative coating and preparation method thereof |
| CN108929612A (en) * | 2018-05-29 | 2018-12-04 | 富思特新材料科技发展股份有限公司 | A kind of illusion-colour flash of light terrace finishing coat |
| CN109439171A (en) * | 2018-12-01 | 2019-03-08 | 金美云 | A kind of environment-friendly epoxy floor coatings and its preparation method and application |
| CN110003766A (en) * | 2019-03-20 | 2019-07-12 | 河北晨阳工贸集团有限公司 | A kind of environment-friendly solvent-free epoxy flash of light artistic floors paint and preparation method thereof |
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