CN107375104B

CN107375104B - Production method of hydrogen-rich antioxidant anti-aging mask

Info

Publication number: CN107375104B
Application number: CN201710740832.0A
Authority: CN
Inventors: 刘士磊
Original assignee: Beijing Zhongqingyuan Engineering Technology Co ltd
Current assignee: Beijing Zhongqingyuan Engineering Technology Co ltd
Priority date: 2017-08-25
Filing date: 2017-08-25
Publication date: 2021-02-02
Anticipated expiration: 2037-08-25
Also published as: CN107375104A

Abstract

The invention relates to a production method of a hydrogen-rich anti-oxidation anti-aging mask, which comprises the following steps: and transferring the mask liquid into a hydrogenation kettle, carrying out hydrogenation for more than 0.5h under the condition that the pressure is 0.8-1 MPa and the stirring is carried out continuously, and filling. Hydrogen is introduced into the mask liquid for hydrogenation, and the technological parameters of hydrogenation are controlled, so that high-concentration hydrogen molecules can be dissolved into the mask liquid, and the hydrogen-rich mask liquid is prepared; the hydrogen-rich facial mask obtained after filling into facial mask has the effects of removing facial oxidation free radicals, beautifying, removing freckles, resisting aging and the like.

Description

Production method of hydrogen-rich antioxidant anti-aging mask

Technical Field

The invention relates to a production method of a mask, in particular to a production method of a hydrogen-rich anti-oxidation anti-aging mask.

Background

With the increase of the pace of life and the pressure of life of people, the problem of skin elasticity deficiency caused by skin aging is increased gradually, so that daily care and maintenance of the skin are required to be strengthened. The facial mask is an important content in skin care, and is applied regularly according to various skin characteristics, so that oily skin can be degreased, large pores can be converged, withered and wrinkled skin can recover luster, and inflammation of pimpled skin can be inhibited. The facial mask makes skin look fresh, smooth, white and tender after being used, because when the facial mask is applied to the skin, the facial mask generates affinity with the skin, the skin temperature rises along with the gradual drying of the facial mask, the blood circulation is accelerated, the skin is tightened and the tension is strengthened, sebum and moisture secreted by the skin reversely permeate into a horny layer, the epidermis is soft and stretched, pores are naturally opened, effective components in the facial mask permeate into the skin to be absorbed by the skin, meanwhile, the facial mask is tightly connected with the skin, and when the facial mask is removed, aged cutin on the skin and deep dirt in the pores are simultaneously leukorrhed, so that the skin is fresh and clean. The principle of the facial mask is that the facial mask is covered on the face for a short time, so that the external air and pollution are temporarily isolated, the skin temperature is increased, pores of the skin are expanded, the secretion and metabolism of sweat glands are promoted, the oxygen content of the skin is increased, products of metabolism of epidermal cells and accumulated grease substances are favorably removed from the skin, water in the facial mask permeates into the horny layer of the epidermis of the skin, the skin becomes soft, and the skin is naturally bright and elastic. However, oxygen-containing radicals are easily formed after the oxygen content of the skin increases, and aging of the skin is accelerated.

Disclosure of Invention

The invention aims to overcome the defects of the prior art and provide a production method of a hydrogen-rich anti-oxidation anti-aging mask.

In order to achieve the purpose, the technical scheme adopted by the invention is as follows: a production method of a hydrogen-rich anti-oxidation anti-aging mask comprises the following steps: and transferring the mask liquid into a hydrogenation kettle, carrying out hydrogenation for more than 0.5h under the condition that the pressure is 0.8-1 MPa and the stirring is carried out continuously, and filling.

Optimally, the hydrogenation is to introduce hydrogen into a hydrogen disperser in a hydrogenation kettle at a flow rate of 5-15L/min, so that the hydrogen is dissolved in the mask liquid in a micro-bubble manner.

Further, hydrogen-rich water balls accounting for 5-15% of the mask liquid are mixed in the mask liquid, and the diameter of each hydrogen-rich water ball is 2-5 mm; and filtering the mask liquid before filling.

Further, the mask liquid comprises the following raw material components in parts by weight: 40-50 parts of water, 10-15 parts of 2, 3-butanediol, 0.5-1 part of vitamin C, 0.1-0.5 part of vitamin E, 0.1-0.2 part of phenoxyethanol, 0.5-1 part of glycerol, 0.05-0.2 part of arbutin, 0.01-0.06 part of allantoin, 0.02-0.05 part of palmitoyl tripeptide-5, 1-5 parts of trehalose, 2-8 parts of sodium hyaluronate, 0.05-0.2 part of glycine, 1-5 parts of beta-glucan, 0.5-1 part of dipotassium glycyrrhizinate, 0.2-1 part of calendula officinalis extract and 0.2-0.5 part of austenitic seaweed extract.

Further, the preparation method of the facial mask liquid comprises the following steps:

(a) dissolving vitamin C in a formula amount in water, and then continuously adding allantoin, trehalose, sodium hyaluronate, glycine, beta-glucan, arbutin and dipotassium glycyrrhizinate in the formula amount under the condition of continuous stirring to obtain a first solution;

(b) dissolving phenoxyethanol with the formula amount in 2, 3-butanediol, continuously stirring, and continuously adding vitamin E, glycerol, palmitoyl tripeptide-5, calendula extract and austenitic seaweed extract with the formula amount at 40-60 ℃ to form a uniform second solution;

(c) and mixing the first solution and the second solution.

Due to the application of the technical scheme, compared with the prior art, the invention has the following advantages: according to the production method of the hydrogen-rich anti-oxidation anti-aging mask, hydrogen is introduced into the mask liquid for hydrogenation, and the technological parameters of hydrogenation are controlled, so that high-concentration hydrogen molecules can be dissolved into the mask liquid, and the hydrogen-rich mask liquid is prepared; the hydrogen-rich facial mask obtained after filling into facial mask has the effects of removing facial oxidation free radicals, beautifying, removing freckles, resisting aging and the like.

Detailed Description

The following detailed description of preferred embodiments of the invention is provided:

example 1

In example 1, the existing silk mask is selected and optimized, and specifically comprises the following components: 700g of water, 40g of 2, 3-butanediol, 60g of saturated caprylic triglyceride, 7.5g of aloe leaf extract, 20g of bioglycasin-1, 20g of oat beta-glucan, 30g of purslane extract, 3g of hyaluronic acid, 15g of vitamin C, 120g of hydrolyzed silk, 150g of hydroxyethyl cellulose, 10g of xanthan gum, 20g of snow lotus extract and 3g of phenoxyethanol; the preparation method comprises the following steps: (a) adding part of water, 2, 3-butanediol and saturated caprylic triglyceride into a first emulsifying pot, and continuously adding vitamin C, hyaluronic acid and oat beta-glucan in formula amount under the condition of continuously stirring to form uniform solution; (b) adding the rest water into a second emulsifying pot, and sequentially adding hydroxyethyl cellulose, hydrolyzed silk, xanthan gum and biogel-1 according to the formula ratio under the conditions of continuous stirring and 50-80 ℃ to uniformly disperse the materials; (c) adding the product obtained in the step (b) into the product obtained in the step (a) while the product is still hot under stirring, cooling to room temperature, continuously adding the aloe leaf extract, the purslane extract, the snow lotus herb extract and phenoxyethanol according to the formula, and filtering to obtain the facial mask liquid (refer to the Chinese patent with the application number of 201710092652.6).

The embodiment provides a production method for enriching hydrogen in the mask, which specifically comprises the following steps: transferring the mask liquid into a hydrogenation kettle, introducing hydrogen into a hydrogen disperser in the hydrogenation kettle at a flow rate of 5L/min under the condition of continuously stirring at a pressure of 0.8MPa, carrying out hydrogenation for 1h to dissolve the hydrogen in the mask liquid in a microbubble form, and filling.

Example 2

The embodiment provides a production method of a hydrogen-rich anti-oxidation and anti-aging mask, which basically conforms to the steps in the embodiment 1, and the difference is that: transferring the mask liquid into a hydrogenation kettle, introducing hydrogen into a hydrogen disperser in the hydrogenation kettle at a flow rate of 15L/min under the condition of continuous stirring at a pressure of 1MPa, carrying out hydrogenation for 0.5h to dissolve the hydrogen in the mask liquid in a microbubble form, and filling.

Example 3

The embodiment provides a production method of a hydrogen-rich anti-oxidation and anti-aging mask, which basically conforms to the steps in the embodiment 1, and the difference is that: and adding 5% of hydrogen-rich water balls (with average diameter of about 2mm, specifically refer to the Chinese patent with application number of 2014101662470) into the facial mask liquid, filtering, and filling.

Example 4

The embodiment provides a production method of a hydrogen-rich anti-oxidation and anti-aging mask, which basically conforms to the steps in the embodiment 1, and the difference is that: adding hydrogen-rich water ball (average diameter is about 2mm, specifically refer to Chinese patent application No. 2014101662470) 15% by mass into the facial mask solution, filtering, and packaging.

Example 5

The embodiment provides a production method of a hydrogen-rich anti-oxidation and anti-aging mask, which basically conforms to the steps in the embodiment 1, and the difference is that: and adding 10% of hydrogen-rich water balls (with average diameter of about 2mm, specifically refer to the Chinese patent with application number of 2014101662470) into the facial mask liquid, filtering, and filling.

Example 6

The embodiment provides a production method of a hydrogen-rich anti-oxidation and anti-aging mask, which basically conforms to the steps in the embodiment 1, and the difference is that: the components and the preparation method of the mask liquid are different, and specifically comprise the following steps: 40 parts of water, 15 parts of 2, 3-butanediol, 1 part of vitamin C, 0.1 part of vitamin E, 0.1 part of phenoxyethanol, 1 part of glycerol, 0.05 part of arbutin, 0.01 part of allantoin, 0.02 part of palmitoyl tripeptide-5, 1 part of trehalose, 8 parts of sodium hyaluronate, 0.05 part of glycine, 1 part of beta-glucan, 0.5 part of dipotassium glycyrrhizinate, 0.2 part of calendula extract and 0.2 part of austenitic seaweed extract;

the preparation method specifically comprises the following steps: (a) dissolving vitamin C in a formula amount in water, and then continuously adding allantoin, trehalose, sodium hyaluronate, glycine, beta-glucan, arbutin and dipotassium glycyrrhizinate in the formula amount under the condition of continuous stirring to obtain a first solution; (b) dissolving phenoxyethanol with the formula amount in 2, 3-butanediol, continuously stirring, and continuously adding vitamin E, glycerol, palmitoyl tripeptide-5, calendula extract and austenitic seaweed extract with the formula amount at 40-60 ℃ to form a uniform second solution; (c) and mixing the first solution and the second solution.

Example 7

The embodiment provides a production method of a hydrogen-rich anti-oxidation and anti-aging mask, which basically conforms to the steps in the embodiment 5, except that: the components of the mask liquid are different, and specifically comprise: 50 parts of water, 10 parts of 2, 3-butanediol, 0.5 part of vitamin C, 0.5 part of vitamin E, 0.2 part of phenoxyethanol, 0.5 part of glycerol, 0.2 part of arbutin, 0.06 part of allantoin, 0.05 part of palmitoyl tripeptide-5, 5 parts of trehalose, 2 parts of sodium hyaluronate, 0.2 part of glycine, 5 parts of beta-glucan, 1 part of dipotassium glycyrrhizinate, 1 part of calendula extract and 0.5 part of austenitic seaweed extract.

Example 8

The embodiment provides a production method of a hydrogen-rich anti-oxidation and anti-aging mask, which basically conforms to the steps in the embodiment 5, except that: the components of the mask liquid are different, and specifically comprise: 45 parts of water, 12 parts of 2, 3-butanediol, 0.8 part of vitamin C, 0.3 part of vitamin E, 0.15 part of phenoxyethanol, 0.8 part of glycerin, 0.1 part of arbutin, 0.05 part of allantoin, 0.03 part of palmitoyl tripeptide-5, 3 parts of trehalose, 5 parts of sodium hyaluronate, 0.1 part of glycine, 3 parts of beta-glucan, 0.8 part of dipotassium glycyrrhizinate, 0.5 part of calendula extract and 0.3 part of austenitic seaweed extract.

Comparative example 1

This example provides a method for producing an antioxidant anti-aging mask, which has a material formula and preparation steps substantially the same as those in example 1, except that: no hydrotreatment was performed.

Comparative example 2

This example provides a method for producing an antioxidant anti-aging mask, which has a material formula and preparation steps substantially the same as those in example 6, except that: sodium hyaluronate and glycerol are not contained.

Comparative example 3

This example provides a method for producing an antioxidant anti-aging mask, which has a material formula and preparation steps substantially the same as those in example 6, except that: all the raw materials are directly mixed.

Comparative example 4

This example provides a method for producing an antioxidant anti-aging mask, which has a material formula and preparation steps substantially the same as those in example 6, except that: hydrogenation is carried out for 0.5h under the pressure of 1.5MPa, and the hydrogen reaches 20L/min.

The masks obtained in examples 1 to 8 and comparative examples 1 to 3 were subjected to physicochemical tests, and the results thereof are shown in table 1.

TABLE 1 physicochemical test data of masks prepared in examples 1 to 3 and comparative examples 1 to 3

TABLE 1 continuation

While the present application has been described with examples, those of ordinary skill in the art will appreciate that there are numerous variations and permutations of the present application without departing from the spirit of the application, and it is intended that the appended claims encompass such variations and permutations without departing from the spirit of the application.

Claims

1. The production method of the hydrogen-rich mask is characterized by comprising the following steps of: transferring the mask liquid into a hydrogenation kettle, carrying out hydrogenation for more than 0.5h under the condition that the pressure is 0.8-1 MPa and the stirring is kept, filtering the mask liquid, and filling; the mask liquid comprises the following raw material components in parts by weight: 40-50 parts of water, 10-15 parts of 2, 3-butanediol, 0.5-1 part of vitamin C, 0.1-0.5 part of vitamin E, 0.1-0.2 part of phenoxyethanol, 0.5-1 part of glycerol, 0.05-0.2 part of arbutin, 0.01-0.06 part of allantoin, 0.02-0.05 part of palmitoyl tripeptide-5, 1-5 parts of trehalose, 2-8 parts of sodium hyaluronate, 0.05-0.2 part of glycine, 1-5 parts of beta-glucan, 0.5-1 part of dipotassium glycyrrhizinate, 0.2-1 part of calendula extract and 0.2-0.5 part of austenitic seaweed extract; the hydrogenation step is that hydrogen is introduced into a hydrogen disperser in a hydrogenation kettle at the flow rate of 5-15L/min, so that the hydrogen is dissolved in the mask liquid in the form of microbubbles; the mask liquid is also mixed with hydrogen-rich water balls accounting for 5-15% of the mask liquid in mass fraction, and the diameter of each hydrogen-rich water ball is 2-5 mm;

the preparation method of the facial mask liquid comprises the following steps:

(c) and mixing the first solution and the second solution.