CN107361403A - One kind contains Extracts of Tupistra chinensis additive in cigarette and preparation method thereof - Google Patents
One kind contains Extracts of Tupistra chinensis additive in cigarette and preparation method thereof Download PDFInfo
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- CN107361403A CN107361403A CN201710667679.3A CN201710667679A CN107361403A CN 107361403 A CN107361403 A CN 107361403A CN 201710667679 A CN201710667679 A CN 201710667679A CN 107361403 A CN107361403 A CN 107361403A
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- Prior art keywords
- cigarette
- additive
- tupistra
- extraction
- parts
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
A kind of cigarette containing Extracts of Tupistra chinensis additive in cigarette, its preparation method is the extraction of (1) Tupistra active principle, (2) preparation of additive in cigarette, (3) preparation of cigarette, wherein the composition containing Extracts of Tupistra chinensis additive in cigarette includes following components：Tupistra extracts 5 20 parts of medicinal extract, 50 150 parts of water, 23 parts of surfactant, 23 parts of additive, 48 parts of alcohol.The present invention has found the cigarette of addition Tupistra additive, can reduce the excitant of cigarette, improve cigarette mouthfeel using Extracts of Tupistra chinensis as cigarette additive.
Description
Technical field
The invention belongs to additive in cigarette field, and in particular to a kind of Extracts of Tupistra chinensis additive in cigarette.
Background technology
In recent years, in the World Health Organization (WHO)), under the actively promoting of many national governments and various Fan Yan groups, entirely
The anti-smoking campaign of ball grows to even greater heights, and the social pressures that tobacco business is subject to are increasing.Member's international politics that WHO is formulated, each
Mansion is signed《The Framework Convention on Tobacco Control》Not only define national governments to take and carry out effective legislation, it is administrative and its
Its measure prevents and reduced tobacco consumption, nicotine addiction and Exposure To Tobacco flue gas etc., but also requires to enter tobacco product composition
Row limitation.At present, some Main Developed Countries are also made that to the tar, nicotine and carbon monoxide of commercial cigarettes in succession in the world
Specific limitation, meanwhile, the health and environmental consciousness of consumer itself have also strengthened.In this context, World tobacco industry is
Reduce harm of the tobacco product to human health, preferably protect the health of consumer, including tobacco leaf production, processing and
Reducing tar and reducing harm new technology simultaneously successfully applies in production of cigarettes.Meanwhile accelerating to lower Jiao also occurs in international cigarette market
The trend of oil, nicotine and the development of low harmful components cigarette.
In China, investigation finds urban and rural residents' smoking rate, and 15 years old and above population smoking rate in male are 48.0%, and women inhales
Cigarette rate is 2.6%, is thus calculated, the current smoking population in China has 2.7 hundred million.Compared with 2003, smoking rate has declined, but inhales
The smoking capacity increase of cigarette person is obvious, and smoker's ratio of daily smoking 20 and the above was increased to 2008 by 2003 51%
62%.China is the native place of Chinese herbal medicine, and application of the Chinese herb feed additive in Chinese-style cigarette is that Chinese Tobacco Industry is incomparable
Peculiar advantage.At present, domestic existing more cigarette enterprises use advanced scientific and technological means, with China's extensive knowledge and profound scholarship
Herbal medicine is theoretical, and the cigarette for adding medicinal herb componentses is ground on the selection of Chinese herbal medicine, drug mechanism, drug study
Study carefully, developed the Chinese style brand cigarette of the mitigation to human body with certain curative effect, such as golden sage, rivers and mountains, five leaves
God etc..Countries tobacco office in the works, is also clearly proposed using development and usage Chinese herbal medicine advantage as in raising in countries tobacco
The important means of formula cigarette competitiveness and direction.China should make full use of tcm theory, and further exploitation contains and had to human body
The cigarette additive of the medicinal herb componentses of benefit, makes it have certain drug effect, alleviates the harm to human body caused by smoking, carry
The international competitiveness of high China's cigarette brand.
Tupistra (Tupistra) plant is under the jurisdiction of Liliaceae Convallarieae (Convallarieae).China's Tupistra
Floristics is various, aboundresources, is distributed mainly on the ground such as Sichuan, Yunnan, Zhejiang, Guangxi, Jiangxi, Fujian.This platymiscium is more
For ethnic group's medication among the people, traditional Chinese medical science traditional theory thinks that the platymiscium is bitter, pungent, cold in nature, poisonous.With clearing heat and detoxicating, wind-dispelling
Dehumidifying, dissipate addiction analgesic and other effects.Tujia is among the people to treat sphagitis, tonsillitis with its gargle, evident in efficacy.Meanwhile open
Mouth arrow is as shenlongjia forest zone Folk medicine, for pharynx-clearing throat-benefiting in West of Hubei Province existing centuries history among the people, its distinguishing feature
It is quick, action time is longer, efficacy stability, and high reputation is enjoyed in this area.
Primary Study shows, the main chemical compositions of Tupistra are steroid saponin or sapogenin, carbohydrate, volatile oil etc., but
It treats the active site or the medical mechanism of unit and pharynx-clearing throat-benefiting of sphagitis, is still further being studied at present.
Studied confirmation, Tupistra have to bottleneck throat common pathogen such as staphylococcus aureus, beta hemolytic streptococcus etc. compared with
Good bacteriostasis, so as to effectively antagonize the sphagitis as caused by infection.Tupistra can also mitigate throat local inflammation oedema, ooze
Go out, and there is eliminating the phlegm and bacteriostasis, so as to alleviate or even remove the symptom of sphagitis.Separately by acute viral experimental study table
It is bright, the toxicity very little of Tupistra, it can be also suitably used for as tobacco additive agent.
It is the Pharmacological result of study of Tupistra below, experimental data is all from technical literature.Le Kaili etc. was once
Pharmacological research was carried out to congener palpus valve opening.So as to the tupistrin got in the rhizome of valve Tupistra, in cardiac glycoside
Chromogenic chemical reacts.Typical digitalis sample ECG change is produced to cat and cavy, it was demonstrated that palpus valve Tupistra has cardiac stimulant work
With.And judge that tupistrin belongs to quick-acting cardiac glycoside using Zhou Yefa, prove that its is accumulative minimum according to family Honda method measure.Poplar
Spring, the gorgeous auricle acute inflammation for waiting research to find that Tupistra (149.75g.kg-1) paraxylene induces had significant suppress
Effect；But to DNCB induced mices DTH without obvious effect；Antibacterial experiment in vitro shows that Tupistra is to staphylococcus aureus, table
The false single armful of bacterium of skin staphylococcus, verdigris has obvious bacteriostasis, MIC 125gL-1；Acute toxicity testing shows, mouse
IgLD50 is 1487gL-1, toxicity very little.Qiu's religion etc. have studied Tupistra active ingredient and experimental colitis of rats controlled
Treat Function and its mechanisms.TNB rat colitis model is established, (main component is steroidal soap with Tupistra alcohol extract
Glycosides) enema treatment 2 weeks, pretherapy and post-treatment Injured colonic mucosa index (CMDI) and histological score (HS) are calculated, determines its colon
Organize superoxide dismutase (SOD) activity, neutrophil leucocyte myeloperoxidase (MPO), MDA (MDA), blood platelet table
Face palatelet-selectin (palatelet-selectin) and maximum platelet aggregation rate (PagT) change.Rat CMDI and HS are reduced after treatment, MDA
Reduce, MPO activity is reduced, and PagT and palatelet-selectin are counted and declined, SOD activity increases.Prompt Tupistra alcohol extract real to rat
The property tested colitis has therapeutic action, its mechanism may be scavenging activated oxygen, mitigate damage of the MDA to tissue with
And suppress hematoblastic aggregation and activation, reduce the release of inflammatory factor.Qu Shaoshuan etc. using Tupistra as main ingredient be aided with Chinese atropanthe root,
The medicines such as blackberry lily, vinegar form compound gargle, treat sphagitis 45, the results showed that recovery from illness 37, account for 92%, effective 8, account for
8%.Nearest 2 years, it is multi-party that antitumor, anti-inflammatory, platelet aggregation-against and immunoregulatory activity etc. have been carried out to Extracts of Tupistra chinensis
The pharmaceutical research in face, find that there is significant antineoplastic action at the saponin extraction position of Tupistra first.It is antitumor in vivo to grind
Study carefully and show, S-180 tumor-bearing mice 0.5g/kg and 1.5g/kg Tupistra total saposins gavages respectively can to the inhibiting rate of tumour growth
Up to 34.5% and 52.2%；The discovery Tupistra total saposins of in vitro cytotoxic effect measure have stronger cell levisticum, right
The IC50 of HepG2 growth of tumour cell is 4.92 μ g/ml.These results indicate that Rhizoma Tupistrae Chinensis saponin have it is safe and effective anti-swollen
Knurl acts on, and is worth further research.
There is more research in terms of the anticancer to Tupistra and sterilization in the prior art, but Tupistra is used for cigarette
Field, the research for improving cigarette mouthfeel are rarely reported.
The present invention has found the cigarette of addition Tupistra additive, can dropped using Extracts of Tupistra chinensis as cigarette additive
The excitant of low cigarette, improve cigarette mouthfeel.
The content of the invention
New there is eliminating the phlegm, anti-inflammatory, antibacterial and prevention breathing problem cigarette it is an object of the invention to provide a kind of
It additive and preparation method, can significantly improve the excitant of cigarette using this additive in cigarette, improve the body of smoker
Test sense.
Realized especially by following methods, mainly including following three steps, the extraction of (1) Tupistra active principle,
(2) preparation of additive in cigarette, the preparation of (3) cigarette.
The wherein extraction of (1) Tupistra active principle, comprises the following steps：
1-1：Tupistra is dried；
1-2：Organic solvent soak extraction；The organic solvent can be：Methanol, ethanol, acetone, n-butanol, acetic acid second
Ester, ether, chloroform, hexamethylene, petroleum ether and methanol, ethanol, acetone and a certain proportion of mixed solution of water；By above-mentioned immersion
24h Tupistra medicinal material is extracted 3 times with appropriate extracting method, collects extract solution.The extracting method used can be:Dipping
Method, percolation, decocting method, reflux extraction, soxhlet extraction, ultrasonic extraction, microwave loss mechanisms, Smashing extraction method.
1-3：Concentrated extracting solution；The extract solution obtained in step 1-2 is transferred to after being evaporated under reduced pressure on Rotary Evaporators
On evaporating dish, heating evaporation removes excessive moisture, is concentrated into without pure taste；
1-4：Prepare medicinal extract；After concentrated extracting solution is measured into distilled water diluting dissolving with 2-4 times, have with 1/4-1/2 volumes
Solvent extracts 2-4 times.The organic solvent used can be：N-butanol, ethyl acetate, ether, chloroform, hexamethylene, petroleum ether.
Extract part is transferred on evaporating dish after being evaporated under reduced pressure on Rotary Evaporators, the heating removing residual under 100 DEG C of water-baths
Organic solvent, it is concentrated into medicinal extract.Or aqueous fraction is transferred on evaporating dish after being evaporated under reduced pressure on Rotary Evaporators after extraction, in
Heating evaporation removes the organic solvent and excessive moisture of residual under 100 DEG C of water-baths, is concentrated into medicinal extract.
The wherein preparation of step (2) additive in cigarette, additive include medicinal extract 5-20 parts that step (1) is prepared, water
50-150 parts, surfactant 2-3 parts, additive 2-3 parts, alcohol 4-8 parts, mixing, obtain additive in cigarette.
The surfactant is triethyl group hexyl phosphoric acid, lauryl sodium sulfate；
Surfactant is added in additive in cigarette, the interface performance in additive can be improved so that Tupistra carries
Taking thing can quickly dissolve and dispersed, can be that Tupistra is evenly distributed when being finally applied in pipe tobacco.
The additive is alum, zeolite, montmorillonite kind, calgon, the one or more of sodium pyrophosphate；
The alcohol be C1-C5 alcohol, preferred alcohol.
Because additive is to add in liquid form, a certain amount of alcohol can improve the dispersiveness of each material in additive
Can, while additive in cigarette, when being sprayed onto on pipe tobacco, ethanol can quickly be volatilized, volatilized due to readily volatilized characteristic
During can take away partial moisture, so as to shorten color drying time, improve production efficiency.
The wherein preparation of step (3) cigarette, specifically carried out according to following operation.
The additive in cigarette and the mass ratio 1-10 of pipe tobacco being prepared according to step (2):100, additive in cigarette is sprayed
It is spread across on pipe tobacco, stirs, dry, by pipe tobacco winding, assembling, the cigarette containing Tupistra composition is prepared.
The cigarette prepared by the present invention, the excitant of cigarette can be significantly reduced, improve cigarette mouthfeel.
Embodiment
Embodiment 1
The 1000g Tupistra medicinal materials dried are fitted into the mono- neck flasks of 3000ml, carried with being flowed back after 65% ethanol immersion 24h
Take 3 times, every time 3 hours.Filtering, merging filtrate.Extract solution is transferred on evaporating dish after being evaporated under reduced pressure on Rotary Evaporators, in
Heating evaporation removes excessive moisture under 100 DEG C of water-baths, is concentrated into without pure taste medicinal extract.Gained medicinal extract is diluted with 4 times of volume water
Dissolving, then with 1/3 amount extracting n-butyl alcohol 3 times.Extract part is transferred to evaporating dish after being evaporated under reduced pressure on Rotary Evaporators
On, heating evaporation removes the n-butanol solvent of residual under 100 DEG C of water-baths, and concentration is caused without n-butanol taste medicinal extract.Aqueous fraction in
It is transferred to after being evaporated under reduced pressure on Rotary Evaporators on evaporating dish, it is molten to remove the n-butanol remained for heating evaporation under 100 DEG C of water-baths
Agent and excessive moisture, are concentrated into medicinal extract, and two parts medicinal extract is mixed, and obtain medicinal extract and are used for tobacco additive agent.
Embodiment 2
10 parts of medicinal extract obtained by weighing in embodiment 1,100 parts of water, 2 parts of lauryl sodium sulfate, 2 parts of alum, ethanol 5
Part, mixing, obtain additive in cigarette.
Embodiment 3
20 parts of medicinal extract obtained by weighing in embodiment 1,100 parts of water, 2 parts of lauryl sodium sulfate, 2 parts of alum, ethanol 5
Part, mixing, obtain additive in cigarette.
Embodiment 4
15 parts of medicinal extract obtained by weighing in embodiment 1,100 parts of mixing of water, obtains additive in cigarette.
Embodiment 5
15 parts of medicinal extract obtained by weighing in embodiment 1,100 parts of mixing of water, 2 parts of lauryl sodium sulfate, 2 parts of alum,
1 part of calgon, obtains additive in cigarette.
Embodiment 6
It is respectively 5 according to mass ratio with pipe tobacco by the preparation-obtained additive in cigarette containing Tupistra of embodiment 2-5:100,
Pipe tobacco is sprayed onto, pipe tobacco is well mixed, and is dried afterwards, obtains the pipe tobacco containing Tupistra additive in cigarette, by the pipe tobacco system of drying
It is standby to obtain cigarette.Wherein, it is respectively labeled as using the preparation-obtained cigarettes containing Tupistra additive in cigarette of embodiment 2-5
A, B, C, D.
Comparative example 1
A kind of cigarette, any additive in cigarette is not added, is prepared by pipe tobacco.
Comparative example 2
A kind of cigarette, Tupistra pulverized particles are mixed in pipe tobacco, thus raw material prepares cigarette.
The cigarette that the additive in cigarette containing Tupistra that embodiment 2-6 is prepared is prepared prepares with comparative example 1-2
Obtained cigarette carries out sensory test.
Method of testing and standard, wherein 20 volunteers, the people of male 10, the people of women 20, age 22-35 year, to sucking reality
The cigarette that example and comparative example are prepared is applied, and cigarette is graded.
Mainly from mouthfeel whether alcohol just, if stimulate, fragrance it is whether pure three aspect evaluated, be classified as simultaneously
Five grades, specific division are as follows：
One-level：Mouthfeel is good, alcohol just, stingless excitation, aroma of pure.
Two level：Mouthfeel is good, and just, a little to stimulate, fragrance is just for alcohol.
Three-level：Mouthfeel is general, can feel alcohol just, a little to stimulate, and fragrance is general.
Level Four：Mouthfeel is general, stimulates.
Pyatyi：Poor taste, stimulate.
Wherein count the number of every kind of cigarette grading, the final mouthfeel for judging cigarette.Statistical result is shown in Table 1
Table 1：Volunteer grades to different cigarettes
| A | B | C | D | Comparative example 1 | Comparative example 2 | |
| One-level | 15 | 13 | 12 | 16 | 8 | 3 |
| Two level | 5 | 6 | 5 | 4 | 8 | 5 |
| Three-level | 0 | 1 | 3 | 0 | 3 | 5 |
| Level Four | 0 | 0 | 0 | 0 | 1 | 3 |
| Pyatyi | 0 | 0 | 0 | 0 | 0 | 4 |
Extracts of Tupistra chinensis is added for Tupistra powder is directly added into from statistics as can be seen that working as, energy
Enough significant mouthfeels for improving cigarette, the experience of smoker is improved, is targetedly to extract mainly due to extraction medicinal extract, and be open
Arrow powder contains substantial amounts of impurity, can reduce and suck experience.It can be seen that simultaneously from the comparison between embodiment and with the addition of surface
Activating agent and additive, such as alum, which can also improve, sucks mouthfeel, and possible cause is that alum can be inhaled in cigarette combustion
Mouthfeel is sucked in attached a certain amount of pungent, raising.
Claims (8)
- A kind of 1. additive in cigarette containing Extracts of Tupistra chinensis, it is characterised in that in parts by mass, including following components：Open Mouth arrow extraction medicinal extract 5-20 parts, water 50-150 parts, surfactant 2-3 parts, alcohol 4-8 parts.
- 2. a kind of additive in cigarette containing Extracts of Tupistra chinensis as claimed in claim 1, it is characterised in that live on the surface Property agent be triethyl group hexyl phosphoric acid, the one or two of lauryl sodium sulfate kind.
- A kind of 3. additive in cigarette containing Extracts of Tupistra chinensis as claimed in claim 1, it is characterised in that additive in cigarette Also include 2-3 part additives, additive is alum, zeolite, montmorillonite kind, calgon, the one or more of sodium pyrophosphate.
- 4. a kind of additive in cigarette containing Extracts of Tupistra chinensis as claimed in claim 1, alcohol is C1-C5 alcohol.
- 5. a kind of additive in cigarette containing Extracts of Tupistra chinensis as claimed in claim 4, alcohol is ethanol.
- A kind of 6. cigarette of additive in cigarette containing Extracts of Tupistra chinensis as described in claim any one of 1-5.
- A kind of 7. preparation side of the cigarette of additive in cigarette containing Extracts of Tupistra chinensis as described in claim any one of 1-5 Method, it is characterised in that comprise the following steps the extraction of (1) Tupistra active principle；(2) preparation of additive in cigarette；(3) cigarette Preparation, the additive in cigarette and the mass ratio 1-10 of pipe tobacco that step (2) is prepared:100, additive in cigarette is sprayed onto On pipe tobacco, stir, dry, by pipe tobacco winding, assembling, the cigarette containing Tupistra composition is prepared.
- 8. a kind of preparation method of the cigarette of the additive in cigarette containing Extracts of Tupistra chinensis as claimed in claim 7, it is special Sign is, the extraction of step (1) Tupistra active principle, comprises the following steps：1-1：Tupistra is dried；1-2：Organic solvent soak extraction；The organic solvent is：Methanol, ethanol, acetone, n-butanol, ethyl acetate, ether, One or more and a certain proportion of mixed solution of water in chloroform, hexamethylene, petroleum ether and methanol, ethanol, acetone；Will be above-mentioned The Tupistra medicinal material of immersion is extracted 3 times with appropriate extracting method, collects extract solution；The extracting method used is yes:Infusion process, percolation, decocting method, reflux extraction, soxhlet extraction, ultrasonic extraction, One kind in microwave loss mechanisms, Smashing extraction method；1-3：Concentrated extracting solution；The extract solution obtained in step 1-2 is transferred to evaporation after being evaporated under reduced pressure on Rotary Evaporators On ware, heating evaporation removes excessive moisture, is concentrated into without pure taste；1-4：Prepare medicinal extract；It is organic molten with 1/4-1/2 volumes after concentrated extracting solution is measured into distilled water diluting dissolving with 2-4 times Agent extracts 2-4 times；The organic solvent used is one kind in n-butanol, ethyl acetate, ether, chloroform, hexamethylene, petroleum ether； Extract part is transferred on evaporating dish after being evaporated under reduced pressure on Rotary Evaporators, the heating removing residual under 100 DEG C of water-baths Organic solvent, it is concentrated into medicinal extract；Or aqueous fraction is transferred on evaporating dish after being evaporated under reduced pressure on Rotary Evaporators after extraction, in Heating evaporation removes the organic solvent and excessive moisture of residual under 100 DEG C of water-baths, is concentrated into medicinal extract.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710667679.3A CN107361403B (en) | 2017-08-07 | 2017-08-07 | A kind of cigarette of additive in cigarette and preparation method thereof containing Extracts of Tupistra chinensis |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710667679.3A CN107361403B (en) | 2017-08-07 | 2017-08-07 | A kind of cigarette of additive in cigarette and preparation method thereof containing Extracts of Tupistra chinensis |
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| Publication Number | Publication Date |
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| CN107361403A true CN107361403A (en) | 2017-11-21 |
| CN107361403B CN107361403B (en) | 2018-09-18 |
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| CN201710667679.3A Expired - Fee Related CN107361403B (en) | 2017-08-07 | 2017-08-07 | A kind of cigarette of additive in cigarette and preparation method thereof containing Extracts of Tupistra chinensis |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108041674A (en) * | 2017-11-29 | 2018-05-18 | 武汉纺织大学 | A kind of impermeable capsule and preparation method thereof that efficiently blocks water |
| CN108851179A (en) * | 2018-08-07 | 2018-11-23 | 武汉纺织大学 | One kind containing Herba Dendrobii extract additive in cigarette and preparation method thereof |
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| JPH05236926A (en) * | 1991-03-13 | 1993-09-17 | T Hasegawa Co Ltd | Improver of taste of tobacco flavor |
| CN1686241A (en) * | 2005-04-08 | 2005-10-26 | 三峡大学 | Tupistra Chinensis Bak extract medicinal composition, and its preparation method and use same |
| CN1775267A (en) * | 2005-11-03 | 2006-05-24 | 南方医科大学 | Kaikoujian extract, Its preparing method and use |
| CN104757703A (en) * | 2014-12-31 | 2015-07-08 | 贵州中烟工业有限责任公司 | Tobacco distillate, and preparation and application thereof |
| CN105505580A (en) * | 2015-12-14 | 2016-04-20 | 长江大学 | Microcapsule and preparation method thereof |
| CN106509281A (en) * | 2016-12-21 | 2017-03-22 | 神农架林区中医医院 | campylandra chinensis sore-throat relieving tea and preparation method thereof |
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2017
- 2017-08-07 CN CN201710667679.3A patent/CN107361403B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05236926A (en) * | 1991-03-13 | 1993-09-17 | T Hasegawa Co Ltd | Improver of taste of tobacco flavor |
| CN1686241A (en) * | 2005-04-08 | 2005-10-26 | 三峡大学 | Tupistra Chinensis Bak extract medicinal composition, and its preparation method and use same |
| CN1775267A (en) * | 2005-11-03 | 2006-05-24 | 南方医科大学 | Kaikoujian extract, Its preparing method and use |
| CN104757703A (en) * | 2014-12-31 | 2015-07-08 | 贵州中烟工业有限责任公司 | Tobacco distillate, and preparation and application thereof |
| CN105505580A (en) * | 2015-12-14 | 2016-04-20 | 长江大学 | Microcapsule and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108041674A (en) * | 2017-11-29 | 2018-05-18 | 武汉纺织大学 | A kind of impermeable capsule and preparation method thereof that efficiently blocks water |
| CN108041674B (en) * | 2017-11-29 | 2020-12-18 | 武汉纺织大学 | Efficient water-blocking anti-seepage capsule and preparation method thereof |
| CN108851179A (en) * | 2018-08-07 | 2018-11-23 | 武汉纺织大学 | One kind containing Herba Dendrobii extract additive in cigarette and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN107361403B (en) | 2018-09-18 |
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