CN107320578A - A kind of glucomannan hydrogel of konnjaku infant bring down a fever patch and preparation method thereof - Google Patents
A kind of glucomannan hydrogel of konnjaku infant bring down a fever patch and preparation method thereof Download PDFInfo
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- CN107320578A CN107320578A CN201710601133.8A CN201710601133A CN107320578A CN 107320578 A CN107320578 A CN 107320578A CN 201710601133 A CN201710601133 A CN 201710601133A CN 107320578 A CN107320578 A CN 107320578A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/534—Mentha (mint)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/484—Glycyrrhiza (licorice)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/539—Scutellaria (skullcap)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/63—Oleaceae (Olive family), e.g. jasmine, lilac or ash tree
- A61K36/634—Forsythia
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/752—Citrus, e.g. lime, orange or lemon
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/82—Theaceae (Tea family), e.g. camellia
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/70—Web, sheet or filament bases ; Films; Fibres of the matrix type containing drug
- A61K9/7007—Drug-containing films, membranes or sheets
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
Abstract
The present invention relates to a kind of glucomannan hydrogel of konnjaku infant bring down a fever patch and preparation method thereof.A kind of glucomannan hydrogel of konnjaku infant brings down a fever the preparation method of patch, including medicinal material infusion, carries that prepared by medicinal gel and prepared by glucomannan hydrogel of konnjaku infant patch of bringing down a fever.The present invention is with natural biological polysaccharide --- konjaku glucomannan（KGM）Hydrogel is prepared as carrier, with very high retentiveness, dilatancy, thickening property and gelation, its performance foodstuff glue conventional better than agar, carragheen and gelatin etc.；From the wholefoods such as peppermint, green tea, dried orange peel, radix glycyrrhizae, honeysuckle and swap buffers and Chinese herbal medicine, with fall fire and the effect of bringing down a fever.The present invention prepares synthetic material using natural plant polyose as raw material, using the distinctive retentiveness of konjaku glucomannan, dilatancy, thickening property and gelation, it is swelled by stirring and gel has been made all preferable glucomannan hydrogel of konnjaku infant of performance and drug effect and brought down a fever patch.
Description
Technical field
Brought down a fever paster and preparation method thereof the present invention relates to a kind of external application physics, and in particular to a kind of konjak portuguese gansu polyose syrup
Gel infant bring down a fever patch and preparation method thereof, belong to pharmaceutical technology field.
Background technology
Heating refers to that body temperature exceedes normal range (NR) high limit, is a kind of children's very common symptom.Normal children armpit table body
Temperature is 36 DEG C~37 DEG C（The body temperature that anus thermometre is measured is higher than oral thermometer about 0.3 DEG C, and the body temperature that oral thermometer is measured is higher than armpit table about 0.4 DEG C）,
Armpit table is such as regarded as heating more than 37.4 DEG C.As a rule, heating is a kind of protectiveness that body-defence invades cause of disease
Reaction, is the process that human body is starting immune system fight to infect.Heating be infant period some common diseases at first
The symptom showed, respiratory tract, infection of digestive canal and some infectious diseases etc. can all cause heating.The influence generated heat to body
It is ambilateral.On the one hand, a certain degree of heating is the defense reaction of body resist the disease, can strengthen body to disease
Resistance；If another aspect body temperature is too high and the various regulatory functions of body can be made to get muddled.Therefore, infant brings down a fever production
Product become the necessity of each family.
Traditional antipyretic is that after being absorbed by oral stomach, physiological function reaches cooling purpose, medicine in regulation human body
The internal vital organs of the human body are reached into branch;And defervescence plaster used is exterior patch, body surface is attached to, is entirely external Physical temperature-lowering side
Formula, reach the effect of zero side effect, it is to avoid the first pass effect of liver.At present, note of bringing down a fever on the market, usually utilizes the world
Popular TDDS technologies make moisture and drug transdermal enter skin, and the physical change then absorbed heat by water vapor reaches reduction body
A kind of drug paste of temp effect.Patch of bringing down a fever belongs to Physical temperature-lowering articles for use, is widely used in fever in children fever, passes the summer in a leisurely way and high temperature work
Situations such as industry.Recently some occurred also have low security, complex process, material expensive etc. to lack for the patch of bringing down a fever of infant
Point.
The patent of Application No. 201320768829.7 be " a kind of octadecyl methacrylate homopolymer phase-change material
Preparation method, application process and paster of bringing down a fever "（The applying date：2013.11.26）, describe octadecyl methacrylate equal
The preparation method of polymers phase-change material, the method is purified octadecyl methacrylate homopolymer and suction filtration, then
It is dried in vacuo, obtains octadecyl methacrylate homopolymer phase-change material and applied to paster of bringing down a fever.This patch of bringing down a fever
Piece has the advantages that reusable, good cooling effect, cost are low, but is related to some industrial monomers and polymerization in material
, there is potential safety issue in thing.
" pure Chinese medicine for infantile hyperpyrexia is brought down a fever pastes and its preparation side the patent of invention of Application No. 201510274341.2
Method "（The applying date：2015.05.27）, describe a kind of small to be used for made from Chinese medicine in folium isatidis, the capsule of weeping forsythia, radix glycyrrhizae etc. 12
The patch of bringing down a fever of youngster's hyperpyrexia, the pure Chinese medicine, which is brought down a fever, pastes to infantile hyperpyrexia effect significantly, not only patient is preferably treated infantile hyperpyrexia,
It can also treat because high thermally-induced pneumonia, but its traditional Chinese medicine ingredients contained is various, manufacture technology is complicated.
The patent of invention " one kind bring down a fever patch " of Application No. 201420549051.5（The applying date：2014.09.23）, introduce
It is a kind of include cold and hot, heat dissipating layer, heat-sink shell, the patch of bringing down a fever of water bag and thermal insulation layer.By cold and hot, be close to cold and hot
The heat-sink shell and water bag of heat-absorbent surface, to cause the patch of bringing down a fever can closely be applied to skin surface progress cooling to bring down a fever, environmental protection, side
Just use, to cause the patch of bringing down a fever can closely be applied to skin surface temperature controllable, environmental protection, convenient use.But this product is set
Meter structure is more complicated, and cost is higher.
Hydrogel is the gel using water as decentralized medium.One is introduced in water soluble polymer with cross-linked network
Divide hydrophobic grouping and hydrophilic residue, hydrophilic residue and water molecules, hydrone is connected to netted inside, and hydrophobic residue is met
Water swellable cross-linked polymer.It is a kind of macromolecule network system, property is soft, can keep certain shape, can absorbs a large amount of
Water.As a kind of high water-keeping material of high water absorption, hydrogel can be widely used for multiple fields, such as：The drought resisting of arid area, is changing
It is stifled in facial mask, defervescence plaster used, pain easing plaster, agricultural film in cosmetic, the condensation preventing agent in building, conditioning agent, petrochemical industry
Water is adjusted, the dehydration of crude oil or product oil, the dust suppressant in mining industry, antistaling agent, thickener in food, the medicine in medical treatment
Carrier etc..
The content of the invention
Brought down a fever it is an object of the invention to provide a kind of glucomannan hydrogel of konnjaku infant different from existing patch of bringing down a fever
Patch and preparation method thereof.The present invention using glucomannan hydrogel of konnjaku as main carriers, addition peppermint, green tea, dried orange peel, radix glycyrrhizae,
The medicinal material such as honeysuckle and swap buffers is made infant and brought down a fever patch.Using the water conservation and slow releasing function of hydrogel, edible material
Cooling effect, and the pure natural security of konjaku glucomannan, are made good cooling effect, the simple baby of safe, technique
Child brings down a fever patch.
The purpose of the present invention is achieved through the following technical solutions.
The glucomannan hydrogel of konnjaku infant of the present invention brings down a fever the preparation method of patch, it is characterised in that preparation process is such as
Under：
（1）Medicinal material infusion：Component, takes 9-15 parts of dried peppermint leaf, 10-14 parts of green tea, 2-4 parts of dried orange peel, 3-9 parts of radix glycyrrhizae, gold by weight
3-9 parts of 3-9 parts of honeysuckle flower and swap buffers, are put into 80-100 DEG C of hot water and soak 20-24 hours, and filtering, filtrate is standby；
（2）Medicinal gel is carried to prepare：Take step（1）In 97-99 parts of filtrate, under 50-70 DEG C of water-bath, 500rpm rotating speeds stir,
1-3 parts of konjaku glucomannan is added simultaneously, is stirred 3-5 hours, pH8-10 is adjusted with aqueous slkali, is formed and is carried liquid medicine gel, it is standby；
（3）Glucomannan hydrogel of konnjaku infant, which brings down a fever to paste, to be prepared：By step（2）The load liquid medicine gel of acquisition pours into mould
In, it is put into refrigeration solidification sizing in 1-4 DEG C of refrigerator and is no less than 24 hours, glucomannan hydrogel of konnjaku infant is made and brings down a fever
Patch.
The present invention is with natural biological polysaccharide --- konjaku glucomannan（KGM）Hydrogel is prepared as carrier, with very high
Retentiveness, dilatancy, thickening property and gelation, and the performance foodstuff glue conventional better than agar, carragheen and gelatin etc.；Choosing
With the wholefoods such as peppermint, green tea, dried orange peel, radix glycyrrhizae, honeysuckle and swap buffers and Chinese herbal medicine, with fall fire and the effect of bringing down a fever.This
Invention prepares synthetic material using natural plant polyose as raw material, utilizes the distinctive retentiveness of konjaku glucomannan, dilatancy, increasing
Consistence and gelation, are swelled by stirring and all preferable glucomannan hydrogel of konnjaku baby children of performance and drug effect has been made in gel
Youngster brings down a fever patch.Glucomannan hydrogel of konnjaku has very big application potential in field of medicaments.The konjaku glucomannan of the present invention
Hydrogel infant bring down a fever patch with the market it is existing bring down a fever paste correlated performance test comparison result it is as shown in table 1.
The glucomannan hydrogel of konnjaku infant of the present invention of table 1 brings down a fever to paste to survey with patch correlated performance of having brought down a fever on the market
Try comparing result
By above-mentioned test comparison, glucomannan hydrogel of konnjaku infant of the invention bring down a fever the temperature reduction performance of patch, security,
The index such as cost of material and potential market, all other patches of bringing down a fever are more excellent more on the market, can turn into the high-quality that consumers in general select
Bring down a fever patch.
Embodiment
Pasted and preparation method thereof in order to which fully open glucomannan hydrogel of konnjaku infant of the present invention brings down a fever, with reference to
Embodiment is described in further detail to the present invention.
Embodiment 1, a kind of glucomannan hydrogel of konnjaku infant are brought down a fever the preparation method of patch, are comprised the following steps：
（1）Medicinal material infusion：9 parts of 9 parts of dried peppermint leaf, 14 parts of green tea, 2 parts of dried orange peel, 9 parts of radix glycyrrhizae, 3 parts of honeysuckle and swap buffers are taken, are put
Enter after being soaked 20 hours in 80 DEG C of hot water, filtering, filtrate is standby；
（2）Medicinal gel is carried to prepare：Take step（1）In 97 parts of filtrate, under 70 DEG C of water-baths, 500rpm rotating speeds stirring, while plus
Enter 3 parts of konjaku glucomannan, stir 3 hours, adjust pH to be 9 with aqueous slkali, formed and carry liquid medicine gel, it is standby；
（3）Glucomannan hydrogel of konnjaku infant, which brings down a fever to paste, to be prepared：By step（2）The load liquid medicine gel of acquisition pours into rectangle
In mould, it is put into 4 DEG C of refrigerator after refrigerating solidification sizing 24 hours, glucomannan hydrogel of konnjaku infant is made and brings down a fever
Patch.
Embodiment 2, a kind of glucomannan hydrogel of konnjaku infant are brought down a fever the preparation method of patch, are comprised the following steps：
（1）Medicinal material infusion：3 parts of 15 parts of dried peppermint leaf, 10 parts of green tea, 4 parts of dried orange peel, 3 parts of radix glycyrrhizae, 9 parts of honeysuckle and swap buffers are taken, are put
Enter and filtered after being soaked 24 hours in 100 DEG C of hot water, filtrate is standby；
（2）Medicinal gel is carried to prepare：Take step（1）In 99 parts of filtrate, under 50 DEG C of water-baths, 500rpm rotating speeds stir, while plus
Enter 1 part of konjaku glucomannan, stir 5 hours, adjust pH to be 9 with aqueous slkali, form load liquid medicine gel stand-by；
（3）Glucomannan hydrogel of konnjaku infant, which brings down a fever to paste, to be prepared：By step（2）The load liquid medicine gel of acquisition pours into rectangle
After refrigeration solidification sizing being put into 4 DEG C of refrigerator in mould 24 hours, glucomannan hydrogel of konnjaku infant is made and brings down a fever patch.
Embodiment 3, a kind of glucomannan hydrogel of konnjaku infant are brought down a fever the preparation method of patch, are comprised the following steps：
（1）Medicinal material infusion：6 parts of 12 parts of dried peppermint leaf, 12 parts of green tea, 3 parts of dried orange peel, 6 parts of radix glycyrrhizae, 6 parts of honeysuckle and swap buffers are taken, are put
Enter and filtered after being soaked 22 hours in 80-100 DEG C of hot water, filtrate is standby；
（2）Medicinal gel is carried to prepare：Take step（1）In 98 parts of filtrate, under 60 DEG C of water-baths, 500rpm rotating speeds stir, while plus
Enter 2 parts of konjaku glucomannan, stir 4 hours, adjust pH to be 9 with aqueous slkali, formed and carry liquid medicine gel, it is standby；
（3）Glucomannan hydrogel of konnjaku infant, which brings down a fever to paste, to be prepared：By step（2）The load liquid medicine gel of acquisition pours into rectangle
After refrigeration solidification sizing being put into 4 DEG C of refrigerator in mould 24 hours, glucomannan hydrogel of konnjaku infant is made and brings down a fever patch.
The foregoing is only presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with
Modification, should all belong to the covering scope of the present invention.
Claims (4)
- The preparation method of patch 1. a kind of glucomannan hydrogel of konnjaku infant brings down a fever, it is characterised in that preparation process is as follows：（1）Medicinal material infusion：Component, takes 9-15 parts of dried peppermint leaf, 10-14 parts of green tea, 2-4 parts of dried orange peel, 3-9 parts of radix glycyrrhizae, gold by weight 3-9 parts of 3-9 parts of honeysuckle flower and swap buffers, are put into 80-100 DEG C of hot water and soak 20-24 hours, and filtering, filtrate is standby；（2）Medicinal gel is carried to prepare：Take step（1）In 97-99 parts of filtrate, under 50-70 DEG C of water-bath, 500rpm rotating speeds stir, 1-3 parts of konjaku glucomannan is added simultaneously, is stirred 3-5 hours, pH8-10 is adjusted with aqueous slkali, is formed and is carried liquid medicine gel, it is standby；（3）Glucomannan hydrogel of konnjaku infant, which brings down a fever to paste, to be prepared：By step（2）The load liquid medicine gel of acquisition pours into mould In, it is put into refrigeration solidification sizing in 1-4 DEG C of refrigerator and is no less than 24 hours, glucomannan hydrogel of konnjaku infant is made and brings down a fever Patch.
- The preparation method of patch, its feature 2. a kind of glucomannan hydrogel of konnjaku infant according to claim 1 brings down a fever It is the medicinal material infusion：9 parts of 9 parts of dried peppermint leaf, 14 parts of green tea, 2 parts of dried orange peel, 9 parts of radix glycyrrhizae, 3 parts of honeysuckle and swap buffers are taken, are put Enter after being soaked 20 hours in 80 DEG C of hot water, filtering, filtrate is standby.
- The preparation method of patch, its feature 3. a kind of glucomannan hydrogel of konnjaku infant according to claim 1 brings down a fever It is prepared by the load medicinal gel：Take step（1）In 97 parts of filtrate, under 70 DEG C of water-baths, 500rpm rotating speeds stir, while plus Enter 3 parts of konjaku glucomannan, stir 3 hours, adjust pH to be 9 with aqueous slkali, formed and carry liquid medicine gel.
- 4. patch of being brought down a fever as glucomannan hydrogel of konnjaku infant prepared by the either method described in claim 1-3.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710601133.8A CN107320578A (en) | 2017-07-21 | 2017-07-21 | A kind of glucomannan hydrogel of konnjaku infant bring down a fever patch and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710601133.8A CN107320578A (en) | 2017-07-21 | 2017-07-21 | A kind of glucomannan hydrogel of konnjaku infant bring down a fever patch and preparation method thereof |
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| CN107320578A true CN107320578A (en) | 2017-11-07 |
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| CN201710601133.8A Pending CN107320578A (en) | 2017-07-21 | 2017-07-21 | A kind of glucomannan hydrogel of konnjaku infant bring down a fever patch and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109820839A (en) * | 2019-04-04 | 2019-05-31 | 广东泰宝医疗科技股份有限公司 | It is a kind of medical defervescence plaster used and preparation method thereof |
| CN110447967A (en) * | 2019-07-10 | 2019-11-15 | 武汉力诚生物科技有限公司 | A kind of heating of plant polyose aeroge is not burnt electronic cigarette mouth stick temperature descending section and preparation method thereof |
| CN116617342A (en) * | 2023-01-18 | 2023-08-22 | 渤海大学 | Preparation method of atomization spray for armyworm virus infection |
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| CN102319142A (en) * | 2011-05-26 | 2012-01-18 | 谭波 | Antipyretic gel |
| CN104337796A (en) * | 2014-10-12 | 2015-02-11 | 浙江欧洁科技股份有限公司 | Polymeric hydrogel fever cooling patch for children and preparation method thereof |
| CN104922058A (en) * | 2015-07-03 | 2015-09-23 | 福建农林大学 | Anti-beriberi konjac glucomannan gelata and preparation method thereof |
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2017
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| CN102319142A (en) * | 2011-05-26 | 2012-01-18 | 谭波 | Antipyretic gel |
| CN104337796A (en) * | 2014-10-12 | 2015-02-11 | 浙江欧洁科技股份有限公司 | Polymeric hydrogel fever cooling patch for children and preparation method thereof |
| CN104922058A (en) * | 2015-07-03 | 2015-09-23 | 福建农林大学 | Anti-beriberi konjac glucomannan gelata and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109820839A (en) * | 2019-04-04 | 2019-05-31 | 广东泰宝医疗科技股份有限公司 | It is a kind of medical defervescence plaster used and preparation method thereof |
| CN110447967A (en) * | 2019-07-10 | 2019-11-15 | 武汉力诚生物科技有限公司 | A kind of heating of plant polyose aeroge is not burnt electronic cigarette mouth stick temperature descending section and preparation method thereof |
| CN116617342A (en) * | 2023-01-18 | 2023-08-22 | 渤海大学 | Preparation method of atomization spray for armyworm virus infection |
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Application publication date: 20171107 |