CN107296274A - A kind of lipid rose powder and preparation method thereof - Google Patents
A kind of lipid rose powder and preparation method thereof Download PDFInfo
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- CN107296274A CN107296274A CN201710672120.XA CN201710672120A CN107296274A CN 107296274 A CN107296274 A CN 107296274A CN 201710672120 A CN201710672120 A CN 201710672120A CN 107296274 A CN107296274 A CN 107296274A
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- rose
- lipid
- powder
- particulate
- water
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- 241000220317 Rosa Species 0.000 title claims abstract description 136
- 239000000843 powder Substances 0.000 title claims abstract description 73
- 150000002632 lipids Chemical class 0.000 title claims abstract description 56
- 238000002360 preparation method Methods 0.000 title claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 44
- 239000012071 phase Substances 0.000 claims abstract description 31
- 239000008346 aqueous phase Substances 0.000 claims abstract description 25
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 19
- 239000003223 protective agent Substances 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 238000001694 spray drying Methods 0.000 claims abstract description 6
- 238000001816 cooling Methods 0.000 claims abstract description 5
- 238000000034 method Methods 0.000 claims description 13
- 150000003904 phospholipids Chemical group 0.000 claims description 13
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims description 12
- 229940083466 soybean lecithin Drugs 0.000 claims description 12
- 239000008236 heating water Substances 0.000 claims description 11
- UKMSUNONTOPOIO-UHFFFAOYSA-N docosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCC(O)=O UKMSUNONTOPOIO-UHFFFAOYSA-N 0.000 claims description 10
- 238000000227 grinding Methods 0.000 claims description 10
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 claims description 9
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 claims description 9
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 claims description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 8
- 125000005456 glyceride group Chemical group 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 7
- 244000068988 Glycine max Species 0.000 claims description 7
- 235000010469 Glycine max Nutrition 0.000 claims description 7
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 claims description 6
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 claims description 6
- 239000002270 dispersing agent Substances 0.000 claims description 6
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 6
- 150000003431 steroids Chemical class 0.000 claims description 6
- DUXYWXYOBMKGIN-UHFFFAOYSA-N trimyristin Chemical compound CCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCC DUXYWXYOBMKGIN-UHFFFAOYSA-N 0.000 claims description 6
- PVNIQBQSYATKKL-UHFFFAOYSA-N tripalmitin Chemical compound CCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCC PVNIQBQSYATKKL-UHFFFAOYSA-N 0.000 claims description 6
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims description 5
- 235000021357 Behenic acid Nutrition 0.000 claims description 5
- 229940116226 behenic acid Drugs 0.000 claims description 5
- 235000009508 confectionery Nutrition 0.000 claims description 5
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 5
- 229930195729 fatty acid Natural products 0.000 claims description 5
- 239000000194 fatty acid Substances 0.000 claims description 5
- 150000004665 fatty acids Chemical class 0.000 claims description 5
- 238000000265 homogenisation Methods 0.000 claims description 5
- 235000010445 lecithin Nutrition 0.000 claims description 5
- 239000000787 lecithin Substances 0.000 claims description 5
- 229940067606 lecithin Drugs 0.000 claims description 5
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims description 4
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 4
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims description 4
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 4
- 210000002969 egg yolk Anatomy 0.000 claims description 4
- 239000008103 glucose Substances 0.000 claims description 4
- 239000008101 lactose Substances 0.000 claims description 4
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 claims description 4
- FLPJVCMIKUWSDR-UHFFFAOYSA-N 2-(4-formylphenoxy)acetamide Chemical compound NC(=O)COC1=CC=C(C=O)C=C1 FLPJVCMIKUWSDR-UHFFFAOYSA-N 0.000 claims description 3
- 239000005632 Capric acid (CAS 334-48-5) Substances 0.000 claims description 3
- WQZGKKKJIJFFOK-QTVWNMPRSA-N D-mannopyranose Chemical compound OC[C@H]1OC(O)[C@@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-QTVWNMPRSA-N 0.000 claims description 3
- 235000021314 Palmitic acid Nutrition 0.000 claims description 3
- 235000021355 Stearic acid Nutrition 0.000 claims description 3
- 229940074979 cetyl palmitate Drugs 0.000 claims description 3
- 235000012000 cholesterol Nutrition 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 3
- 150000002148 esters Chemical class 0.000 claims description 3
- 235000011187 glycerol Nutrition 0.000 claims description 3
- PXDJXZJSCPSGGI-UHFFFAOYSA-N hexadecanoic acid hexadecyl ester Natural products CCCCCCCCCCCCCCCCOC(=O)CCCCCCCCCCCCCCC PXDJXZJSCPSGGI-UHFFFAOYSA-N 0.000 claims description 3
- VMPHSYLJUKZBJJ-UHFFFAOYSA-N lauric acid triglyceride Natural products CCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCC)COC(=O)CCCCCCCCCCC VMPHSYLJUKZBJJ-UHFFFAOYSA-N 0.000 claims description 3
- 239000003595 mist Substances 0.000 claims description 3
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 3
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 3
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical group CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims description 3
- 239000008117 stearic acid Substances 0.000 claims description 3
- 229960001947 tripalmitin Drugs 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims 4
- 239000005639 Lauric acid Substances 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000007513 acids Chemical class 0.000 claims 1
- 239000004519 grease Substances 0.000 claims 1
- 235000019658 bitter taste Nutrition 0.000 abstract description 15
- 239000003921 oil Substances 0.000 description 22
- 239000002245 particle Substances 0.000 description 17
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 16
- 238000001035 drying Methods 0.000 description 15
- 239000007788 liquid Substances 0.000 description 9
- 230000008569 process Effects 0.000 description 8
- 239000004576 sand Substances 0.000 description 6
- 238000010008 shearing Methods 0.000 description 6
- 239000007921 spray Substances 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 5
- 235000013305 food Nutrition 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- -1 pH value Inorganic materials 0.000 description 5
- 230000008901 benefit Effects 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 235000013325 dietary fiber Nutrition 0.000 description 4
- 238000004945 emulsification Methods 0.000 description 4
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000686 essence Substances 0.000 description 3
- 235000019197 fats Nutrition 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 238000003306 harvesting Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 235000019640 taste Nutrition 0.000 description 3
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 2
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 2
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 235000014633 carbohydrates Nutrition 0.000 description 2
- 229910021645 metal ion Inorganic materials 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 150000008442 polyphenolic compounds Chemical class 0.000 description 2
- 235000013824 polyphenols Nutrition 0.000 description 2
- 230000014860 sensory perception of taste Effects 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 235000019605 sweet taste sensations Nutrition 0.000 description 2
- 235000018553 tannin Nutrition 0.000 description 2
- 229920001864 tannin Polymers 0.000 description 2
- 239000001648 tannin Substances 0.000 description 2
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 150000003722 vitamin derivatives Chemical class 0.000 description 2
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 1
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 1
- GLZPCOQZEFWAFX-JXMROGBWSA-N Nerol Natural products CC(C)=CCC\C(C)=C\CO GLZPCOQZEFWAFX-JXMROGBWSA-N 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 230000035603 choleresis Effects 0.000 description 1
- BHQCQFFYRZLCQQ-OELDTZBJSA-N cholic acid Chemical class C([C@H]1C[C@H]2O)[C@H](O)CC[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CC[C@H]([C@@H](CCC(O)=O)C)[C@@]2(C)[C@@H](O)C1 BHQCQFFYRZLCQQ-OELDTZBJSA-N 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000012041 food component Nutrition 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 150000008131 glucosides Chemical class 0.000 description 1
- 125000005908 glyceryl ester group Chemical group 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 235000020778 linoleic acid Nutrition 0.000 description 1
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 206010025482 malaise Diseases 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229920000136 polysorbate Polymers 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000008844 regulatory mechanism Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- OABYVIYXWMZFFJ-ZUHYDKSRSA-M sodium glycocholate Chemical compound [Na+].C([C@H]1C[C@H]2O)[C@H](O)CC[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CC[C@H]([C@@H](CCC(=O)NCC([O-])=O)C)[C@@]2(C)[C@@H](O)C1 OABYVIYXWMZFFJ-ZUHYDKSRSA-M 0.000 description 1
- JAJWGJBVLPIOOH-IZYKLYLVSA-M sodium taurocholate Chemical compound [Na+].C([C@H]1C[C@H]2O)[C@H](O)CC[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CC[C@H]([C@@H](CCC(=O)NCCS([O-])(=O)=O)C)[C@@]2(C)[C@@H](O)C1 JAJWGJBVLPIOOH-IZYKLYLVSA-M 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/10—Foods or foodstuffs containing additives; Preparation or treatment thereof containing emulsifiers
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/30—Encapsulation of particles, e.g. foodstuff additives
- A23P10/35—Encapsulation of particles, e.g. foodstuff additives with oils, lipids, monoglycerides or diglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Nutrition Science (AREA)
- Molecular Biology (AREA)
- Mycology (AREA)
- Biophysics (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a kind of lipid rose powder and preparation method thereof, the lipid rose powder includes the raw material of following percentage by weight：Rose Ultramicro-powder 1 20%, lipid carrier 6 20%, emulsifying agent 1 15%, scattered protective agent 1 15%, remaining be water.The preparation method includes：An oil phase is provided, the oil phase includes rose Ultramicro-powder and lipid carrier；An aqueous phase is provided, the aqueous phase includes emulsifying agent, scattered protective agent and water；By the oil phase and aqueous phase is blended, homogeneous, cooling, lipid rose powder is made after spray drying.Formula of the present invention and preparation method effectively shield the bitter taste of rose, and the rose powder without bitter taste, stable in physicochemical property is made.
Description
Technical field
The invention belongs to food technology field, more particularly to a kind of lipid rose powder and preparation method thereof.
Background technology
The historical origin of rose medicine-food two-purpose is the diet good food that a kind of quality-high and inexpensive, nutrition and health care has both for a long time.Rose
Rare flower is rich in protein, fat, starch, several amino acids and vitamin, also abundant macroelement and trace element et al.
The essential multiple nutritional components of body.
Modern pharmacology analysis finds that rose contains volatile oil, esters, benzyl carbinol, nerol, organic acid, haematochrome, Huang
Tens kinds of pigment, wax, carrotene etc. composition beneficial to human body.Skin glucoside, tannin, fat oil contained by rose etc. are to be used as medicine
Composition.Rose also containing abundant Polyphenols and Flavonoid substances, abundant trace element and vitamin and linoleic acid and
Dietary fiber.There is rose toxin-expelling and face nourishing, the promoting flow of qi and blood circulation, having one's ideas straightened out to become silted up, soothing the liver to be amusing, and promotes choleresis, helps digest,
The effect of regulation mechanism.
In field of food, directly using rose as raw material, rose beverage, rose paste, rose cake etc. can be made into, but due to
Contain the materials such as Polyphenols, glycoside and tannin in rose so that rose food carries offending bitter taste, although adding sweet tea
Taste agent can reduce bitter taste to a certain degree, but be different taste areas, bitter taste and sweet taste because people experience bitter taste and sweet taste
While exist, especially rear taste is had a significant effect, allows people to have unwell sensation after eat up or finish off, to a certain degree
On have impact on rose food popularization and application.
The content of the invention
For the drawbacks described above of prior art, it is a primary object of the present invention to provide a kind of lipid rose powder and its preparation
Method, the preparation method effectively shields the bitter taste of rose, and the rose powder without bitter taste, stable in physicochemical property is made.
In order to achieve the above object, the present invention is adopted the following technical scheme that：
A kind of lipid rose powder, specifically includes the raw material of following percentage by weight：
Rose Ultramicro-powder 1-20%
Lipid carrier 6-20%
Emulsifying agent 1-15%
Scattered protective agent 1-15%
Remaining is water.
As the preferred of the present embodiment, the lipid carrier is selected from glyceride type, fatty acid, steroid and wax
Class；The emulsifying agent is selected from phospholipid；The scattered protective agent is selected from sorbierite, PEARLITOL 25C, glucose, mannose, lactose
And trehalose.
As the preferred of the present embodiment, the glyceride type be selected from caprylic/capric triglyceride, laurin,
Tripalmitin, glyceryl tristearate, myristin, glycerin monostearate and behenic acid list,
Double, glyceryl ester mixture；The fatty acid is selected from stearic acid, palmitic acid, capric acid and behenic acid；The steroid
Selected from cholesterol, the wax class is selected from cetyl palmitate；The phospholipid is selected from soybean lecithin, yolk phospholipid and lecithin
Fat.
As the preferred of the present embodiment, the list of Trivent OCG and 5-15% of the lipid carrier including 1-5% is hard
Glycerol, the emulsifying agent includes soybean lecithin, and the scattered protective agent includes trehalose.
The embodiment of the present invention provides a kind of preparation method of lipid rose powder, and specific method includes：
A, one oil phase of offer, the oil phase include rose Ultramicro-powder and lipid carrier；
B, one aqueous phase of offer, the aqueous phase include emulsifying agent, scattered protective agent and water；
C, by the oil phase and aqueous phase be blended, homogeneous, cooling, lipid rose powder is made after spray drying.
As the preferred of the present embodiment, the lipid carrier and rose Ultramicro-powder are mixed, heating water bath to 80-90 DEG C,
It is used as the oil phase；Emulsifying agent, scattered protective agent and water are mixed, heating water bath is used as the aqueous phase to 80-90 DEG C.
As the preferred of the present embodiment, the oil phase it is mixed with water including：The oil phase is poured into the aqueous phase, stirred
Mix to uniform, speed of agitator is 6000-9000rpm, temperature of charge is 85-95 DEG C.
As the preferred of the present embodiment, the homogeneous includes：By mixed oil phase thing homogeneous mixed with water, homogeneous pressure
10~40Mpa of power, homogenizing temperature is 85-95 DEG C, is cooled to room temperature after homogeneous.
The embodiment of the present invention provides a kind of preparation method of rose Ultramicro-powder, specifically includes following steps：
(1) new fresh-rose is cleaned up；
(2) by the fresh rose flower coarse crushing after cleaning, the thick particulate of rose is obtained, water is added during the coarse crushing；
(3) the thick particulate of the rose is subjected to Crushing of Ultrafine, obtains rose particulate, before Crushing of Ultrafine and during micro mist essence
Add water；
(4) the rose particulate is subjected to ultramicro grinding, obtains rose ultra micron, added during ultramicro grinding scattered
Agent；
(5) the rose ultra micron is spray-dried, obtains rose Ultramicro-powder.
As the preferred of the present embodiment, the thick particulate of rose is diameter 0.5-5mm particulate；The rose particulate is straight
The particulate in 50-100 μm of footpath；The rose ultra micron is a diameter of 0.1-1 μm of particulate.
The invention has the advantages that：
1st, the present invention uses lipid carrier, and the rose Ultramicro-powder is wrapped in lipid carrier, of the present invention to prepare
Method is also an embedding process, and embedding can cover the bitter taste of rose to a certain extent.
2nd, the present invention can also reduce impression of the sense of taste to bitter taste to a certain extent using phospholipid as emulsifying agent.
3rd, the rose Ultramicro-powder that the present invention is used, its raw material fresh rose flower directly uses soybean dietary fiber without drying,
It is spray-dried into powder, greatly reduce the loss of rose nutriment and functional component.
4th, the present invention carries out soybean dietary fiber to fresh rose flower, and the attached of ultramicron can be effectively prevented after adding dispersant
It is poly-.
5th, the present invention in rose nutriment and functional component be difficult light, heat, oxygen, pH value, metal ion etc. because
Element influence and cause damage, improve the stability of nutriment and functional component in rose.
Embodiment
In order that the purpose, technical scheme and advantage of the embodiment of the present invention are clearer, below in conjunction with present invention implementation
Technical scheme in example carries out clear, complete description, it is clear that described embodiment is the section Example of the present invention, and
It is not all of embodiment.Based on embodiments of the invention, those of ordinary skill in the art are not before creative work is paid
The every other embodiment obtained is put, protection scope of the present invention is belonged to.
The embodiment of the present invention provides a kind of lipid rose powder and preparation method thereof, specifically includes the original of following percentage by weight
Material：
Rose Ultramicro-powder 1-20%
Lipid carrier 6-20%
Emulsifying agent 1-15%
Scattered protective agent 1-15%
Remaining is water.
Lipid carrier can be the biodegradable natural or synthetic lipoid of PHYSIOLOGICALLY COMPATIBLE, such as glyceride in the present invention
Class, fatty acid, steroid and wax class；The emulsifying agent is selected from phospholipid；The scattered protective agent be selected from sorbierite,
PEARLITOL 25C, glucose, mannose, lactose and trehalose.
Wherein, glyceride type be selected from caprylic/capric triglyceride, it is laurin, tripalmitin, three hard
Glycerol, myristin, the mixture of glycerin monostearate and behenic acid single, double, triple glyceride；
The fatty acid is selected from stearic acid, palmitic acid, capric acid and behenic acid；The steroid is selected from cholesterol, the wax
Class is selected from cetyl palmitate；The phospholipid is selected from soybean lecithin, yolk phospholipid and lecithin.
Wherein, lipid carrier includes 1-5% Trivent OCG and 5-15% glycerin monostearate, the emulsification
Agent includes soybean lecithin, and the scattered protective agent includes trehalose.
Wherein, conventional emulsifying agent has phospholipid such as soybean lecithin, yolk phospholipid, lecithin；Nonionic surfactants
Such as tween, sapn；Cholic acid salt such as sodium taurocholate, sodium glycocholate, natrium taurocholicum, deoxidation natrium taurocholicum；Short-chain alcohols such as fourth
Alcohol, butyric acid etc..
With some carbohydrate (such as sorbierite, PEARLITOL 25C, glucose, sweet dew in preparation process of the embodiment of the present invention
Sugar, lactose and trehalose) for scattered protective agent, can be dried during spraying drying powder-forming and adhesion good graininess powder
End, and required particulate can be obtained after disperseing again.Increase carbohydrate concentration can improve the protective effect to SLN.
The embodiment of the present invention provides a kind of preparation method of lipid rose powder, specifically includes：
A, one oil phase of offer, the oil phase include rose Ultramicro-powder and lipid carrier；
B, one aqueous phase of offer, the aqueous phase include emulsifying agent, scattered protective agent and water；
C, by the oil phase and aqueous phase be blended, homogeneous, cooling, lipid rose powder is made after spray drying.
Wherein, lipid carrier and rose Ultramicro-powder are mixed, heating water bath is used as oil phase to 80-90 DEG C；By emulsifying agent, divide
Protective agent and water mixing are dissipated, heating water bath is used as aqueous phase to 80-90 DEG C.
Wherein, oil phase process mixed with water is：The oil phase is poured into the aqueous phase, is stirred until homogeneous, is stirred
Rotating speed is 6000-9000rpm, and temperature of charge is 85-95 DEG C.By mixed oil phase thing homogeneous mixed with water, homogenization pressure
10~40Mpa, homogenizing temperature is 85-95 DEG C, is cooled to room temperature after homogeneous.
Wherein, oil phase and the spray drying process of aqueous phase are：Liquefied mixture after cooling is dried to powder, spraying is dry
Dry EAT is 150~180 DEG C, and leaving air temp is 60~80 DEG C, and atomising head rotating speed is 20000~25000rpm.
The embodiment of the present invention, which also provides a kind of preparation method of rose Ultramicro-powder, to be included：
(1) new fresh-rose is cleaned up；
(2) by the fresh rose flower coarse crushing after cleaning, the thick particulate of rose is obtained, water is added during the coarse crushing；
(3) the thick particulate of the rose is subjected to Crushing of Ultrafine, obtains rose particulate, before Crushing of Ultrafine and during micro mist essence
Add water；
(4) the rose particulate is subjected to ultramicro grinding, obtains rose ultra micron, added during ultramicro grinding scattered
Agent；
During manufactured in the present embodiment, a diameter of 0.5-5mm of the thick particulate of rose, a diameter of 50- of rose particulate
100 μm, a diameter of 0.1-1 μm of particulate of rose ultra micron；During ultra micro is smashed, the temperature of rose particulate is protected all the time
Hold as 20-40 DEG C.
Further optimize the present embodiment, the dispersant is lecithin, and the consumption of the dispersant accounts for rose mixture
The 0.5%~3% of quality.
Wherein, the process of ultramicro grinding is：The rose particulate is first ground with the zirconia media of 1mm particle diameters, is ground
Mill rotating speed is 1800~2500rpm；Add after dispersant, then be ground with the zirconia media of 0.5mm particle diameters, grind rotating speed
2500~3500rpm.
Wherein, during the spray drying, EAT is 150~180 DEG C, and leaving air temp is 60~80 DEG C；Atomising head turns
15000~20000rpm of speed, above-mentioned rose ultra micron is spray-dried, rose Ultramicro-powder is obtained.
In order to which above and other purpose, feature and the advantage of the present invention can be become apparent, number cited below particularly is implemented
Example, to illustrate lipid rose powder of the present invention and preparation method thereof.
Embodiment 1：
The preparation method of rose Ultramicro-powder includes in the embodiment of the present invention 1：
1st, after rose harvesting, cleaned up in time with pure water.
2nd, coarse crushing
Clean fresh rose flower is crushed with miniature high-speed pulverizer (ZN-08 types, Zhong Kenaichi Co., Ltds), is pressed during crushing
Feed liquid weight compares 1:1 adds pure water, and fresh rose flower is crushed to the particulate less than 5mm.
3rd, Crushing of Ultrafine
With high speed rotating disintegrator (GY100 types, Five continents Ding Chuan Science and Technology Ltd.s) by the thick particle comminution of rose to being less than
100 μm of particulate.The pure water of 15 parts by weight is added with during before Crushing of Ultrafine, to increase mobility, is easy to operation.
4th, ultramicro grinding
Above-mentioned rose particulate is further crushed to sand mill (the resistance to MiniCer sand mills of speeding of Germany) super less than 1 μm
Particulate.Rough lapping is first carried out with the zirconia media of 1mm particle diameters, 1800~2500rpm of rotating speed is ground, temperature of charge is less than 40
℃.2% oil-in-water type soybean phosphatide is weighed, is added after first soybean lecithin is dissolved with a small amount of hot water, and stir.Use again
The zirconia media of 0.5mm particle diameters is ground, and grinds 2500~3500rpm of rotating speed, and temperature of charge is less than 40 DEG C.Examined with laser
Instrument (LS13320 type laser diffraction particle size analyzers, Beckman Coulter Inc. of the U.S.) detection particle diameter is surveyed, is as a result D90
For 0.82 μm.
5th, it is spray-dried
Rose ultra micro liquid is sprayed with drying machine with centrifugal spray (LPG-5 types, Changzhou Ding Zhuo drying equipments Co., Ltd) dry
It is dry into powder.175~180 DEG C of EAT, leaving air temp is controlled at 70~80 DEG C by charging rate.Charging rate 50ml/
It is stirred continuously in min, fill process, atomising head rotating speed 20000rpm.
The preparation method of lipid rose powder is in the embodiment of the present invention 1：
1st, 2% Trivent OCG, 8% glycerin monostearate and 5% rose Ultramicro-powder are mixed into combination according to quantity,
Heating water bath is used as oil phase to 85 DEG C.
2nd, 10% soybean lecithin, 5% trehalose and water are combined according to quantity, heating water bath is used as aqueous phase to 85 DEG C.
3rd, step 1 oil phase is poured slowly into step 2 aqueous phase, while being emulsified with high speed emulsification cutter, shearing speed
Degree is not less than 6000rpm, shears 2~5min, temperature of charge is not less than 85 DEG C during shearing.
4th, by the material of step 3 high pressure homogenizer homogeneous, 10~40Mpa of homogenization pressure, homogenizing temperature is not less than 85 DEG C.
5th, step 4 homogenizing fluid is rapidly cooled to room temperature with frozen water.
6th, with drying machine with centrifugal spray (LPG-5 types, Changzhou Ding Zhuo drying equipments Co., Ltd) by liquid made from step 4
Rose lipid carrier is dried to powder.150~180 DEG C of EAT, 60~80 DEG C of leaving air temp.Atomising head rotating speed 20000~
25000rpm。
Lipid rose powder in the embodiment of the present invention 1 is evaluated：
1st, embedding rate >=91%；
2nd, lipid rose powder is without bitter taste.
Embodiment 2：
The preparation method of rose Ultramicro-powder includes in the embodiment of the present invention 2：
1st, after rose harvesting, cleaned up in time with pure water.
2nd, coarse crushing
Clean fresh rose flower is crushed with miniature high-speed pulverizer (ZN-08 types, Zhong Kenaichi Co., Ltds), is pressed during crushing
Feed liquid weight compares 1:5 add pure water, and fresh rose flower is crushed to the particulate less than 5mm.
3rd, Crushing of Ultrafine
With high speed rotating disintegrator (GY100 types, Five continents Ding Chuan Science and Technology Ltd.s) by the thick particle comminution of rose to being less than
100 μm of particulate.The pure water of 50 parts by weight is added with during before Crushing of Ultrafine, to increase mobility, is easy to operation.
4th, ultramicro grinding
Above-mentioned rose particulate is further crushed to sand mill (the resistance to MiniCer sand mills of speeding of Germany) super less than 1 μm
Particulate.Rough lapping is first carried out with the zirconia media of 1mm particle diameters, 1800~2500rpm of rotating speed is ground, temperature of charge is less than 40
℃.3% oil-in-water type soybean phosphatide is weighed, is added after first soybean lecithin is dissolved with a small amount of hot water, and stir.Use again
The zirconia media of 0.5mm particle diameters is ground, and grinds 2500~3500rpm of rotating speed, and temperature of charge is less than 40 DEG C.Examined with laser
Instrument (LS13320 type laser diffraction particle size analyzers, Beckman Coulter Inc. of the U.S.) detection particle diameter is surveyed, is as a result D90
For 0.86 μm.
5th, it is spray-dried
Rose ultra micro liquid is sprayed with drying machine with centrifugal spray (LPG-5 types, Changzhou Ding Zhuo drying equipments Co., Ltd) dry
It is dry into powder.150~175 DEG C of EAT, leaving air temp is controlled at 60~70 DEG C by charging rate.Charging rate 50ml/
It is stirred continuously in min, fill process, atomising head rotating speed 15000rpm.
The preparation of lipid rose powder in the embodiment of the present invention 2：
1st, 5% Trivent OCG, 5% glycerin monostearate and 20% rose Ultramicro-powder are mixed into group according to quantity
Close, heating water bath is used as oil phase to 90 DEG C.
2nd, 15% soybean lecithin, 15% trehalose and water are combined according to quantity, heating water bath is used as aqueous phase to 90 DEG C.
3rd, step 1 oil phase is poured slowly into step 2 aqueous phase, while being emulsified with high speed emulsification cutter, shearing speed
Degree is not less than 6000rpm, shears 2~5min, temperature of charge is not less than 85 DEG C during shearing.
4th, by the material of step 3 high pressure homogenizer homogeneous, 10~40Mpa of homogenization pressure, homogenizing temperature is not less than 85 DEG C.
5th, step 4 homogenizing fluid is rapidly cooled to room temperature with frozen water.
6th, with drying machine with centrifugal spray (LPG-5 types, Changzhou Ding Zhuo drying equipments Co., Ltd) by liquid made from step 4
Rose lipid carrier is dried to powder.175~180 DEG C of EAT, 70~80 DEG C of leaving air temp.Atomising head rotating speed 20000~
25000rpm。
Lipid rose powder in the embodiment of the present invention 2 is evaluated：
1st, embedding rate >=92%；
2nd, lipid rose powder is without bitter taste.
Embodiment 3：
The preparation method of rose Ultramicro-powder includes in the embodiment of the present invention 3：
1st, after rose harvesting, cleaned up in time with pure water.
2nd, coarse crushing
Clean fresh rose flower is crushed with miniature high-speed pulverizer (ZN-08 types, Zhong Kenaichi Co., Ltds), is pressed during crushing
Feed liquid weight compares 1:3 add pure water, and fresh rose flower is crushed to the particulate less than 5mm.
3rd, Crushing of Ultrafine
With high speed rotating disintegrator (GY100 types, Five continents Ding Chuan Science and Technology Ltd.s) by the thick particle comminution of rose to being less than
100 μm of particulate.The pure water of 10 parts by weight is added with during before Crushing of Ultrafine, to increase mobility, is easy to operation.
4th, ultramicro grinding
Above-mentioned rose particulate is further crushed to sand mill (the resistance to MiniCer sand mills of speeding of Germany) super less than 1 μm
Particulate.Rough lapping is first carried out with the zirconia media of 1mm particle diameters, 1800~2500rpm of rotating speed is ground, temperature of charge is less than 40
℃.0.5% oil-in-water type soybean phosphatide is weighed, is added after first soybean lecithin is dissolved with a small amount of hot water, and stir.Use again
The zirconia media of 0.5mm particle diameters is ground, and grinds 2500~3500rpm of rotating speed, and temperature of charge is less than 40 DEG C.Examined with laser
Instrument (LS13320 type laser diffraction particle size analyzers, Beckman Coulter Inc. of the U.S.) detection particle diameter is surveyed, is as a result D90
For 0.78 μm.
5th, it is spray-dried
Rose ultra micro liquid is sprayed with drying machine with centrifugal spray (LPG-5 types, Changzhou Ding Zhuo drying equipments Co., Ltd) dry
It is dry into powder.175~180 DEG C of EAT, leaving air temp is controlled at 70~80 DEG C by charging rate.Charging rate 50ml/
It is stirred continuously in min, fill process, atomising head rotating speed 18000rpm.
The preparation of the lipid rose powder of the embodiment of the present invention 3：
1st, 1% Trivent OCG, 15% glycerin monostearate and 1% rose Ultramicro-powder are mixed into group according to quantity
Close, heating water bath is used as oil phase to 80 DEG C.
2nd, 1% soybean lecithin, 1% trehalose and water are combined according to quantity, heating water bath is used as aqueous phase to 80 DEG C.
3rd, step 1 oil phase is poured slowly into step 2 aqueous phase, while being emulsified with high speed emulsification cutter, shearing speed
Degree is not less than 6000rpm, shears 2~5min, temperature of charge is not less than 85 DEG C during shearing.
4th, by the material of step 3 high pressure homogenizer homogeneous, 10~40Mpa of homogenization pressure, homogenizing temperature is not less than 85 DEG C.
5th, step 4 homogenizing fluid is rapidly cooled to room temperature with frozen water.
6th, with drying machine with centrifugal spray (LPG-5 types, Changzhou Ding Zhuo drying equipments Co., Ltd) by liquid made from step 4
Rose lipid carrier is dried to powder.150~160 DEG C of EAT, 60~70 DEG C of leaving air temp.Atomising head rotating speed 20000~
25000rpm。
The lipid rose powder of the embodiment of the present invention 3 is evaluated：
1st, embedding rate >=90%；
2nd, lipid rose powder is without bitter taste.
Technical scheme in above-mentioned the embodiment of the present application, at least has the following technical effect that or advantage：
(1) present invention uses lipid carrier, and the rose Ultramicro-powder is wrapped in lipid carrier, of the present invention to prepare
Method is also an embedding process, and embedding can eliminate the bitter taste of rose to a certain extent.
(2) present invention can also reduce impression of the sense of taste to bitter taste to a certain extent using phospholipid as emulsifying agent.
(3) the rose Ultramicro-powder that the present invention is used, its raw material fresh rose flower directly uses wet method Ultramicro-powder without drying
It is broken, it is spray-dried into powder, greatly reduce the loss of rose nutriment and functional component.
(4) present invention carries out soybean dietary fiber to fresh rose flower, and ultramicron can be effectively prevented after adding dispersant
Agglomeration.
(5) present invention in rose nutriment and functional component be difficult light, heat, oxygen, pH value, metal ion etc. because
Element influence and cause damage, improve the stability of nutriment and functional component in rose.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
God is with principle, and any modification, equivalent substitution and improvements made etc. should be included in the scope of the protection.
Claims (10)
1. a kind of lipid rose powder, it is characterised in that include the raw material of following percentage by weight：
Rose Ultramicro-powder 1-20%
Lipid carrier 6-20%
Emulsifying agent 1-15%
Scattered protective agent 1-15%
Remaining is water.
2. lipid rose powder according to claim 1, it is characterised in that：The lipid carrier is selected from glyceride type, fat
Acids, steroid and wax class；The emulsifying agent is selected from phospholipid；The scattered protective agent is selected from sorbierite, D- sweet dews
Alcohol, glucose, mannose, lactose and trehalose.
3. lipid rose powder according to claim 2, it is characterised in that：The glyceride type is selected from caprylic/capric glycerine
Three esters, laurin, tripalmitin, glyceryl tristearate, myristin, monostearate are sweet
The mixture of grease and behenic acid single, double, triple glyceride；The fatty acid is selected from stearic acid, palmitic acid, capric acid and two
Lauric acid/dodecanoic acid；The steroid is selected from cholesterol, and the wax class is selected from cetyl palmitate；The phospholipid is selected from soybean
Phosphatide, yolk phospholipid and lecithin.
4. lipid rose powder according to claim 3, it is characterised in that：The lipid carrier includes the sad sweet of 1-5%
The glycerin monostearate of oily three esters and 5-15%, the emulsifying agent includes soybean lecithin, and the scattered protective agent includes marine alga
Sugar.
5. a kind of preparation method of lipid rose powder as described in claim any one of 1-4, it is characterised in that methods described bag
Include：
A, one oil phase of offer, the oil phase include rose Ultramicro-powder and lipid carrier；
B, one aqueous phase of offer, the aqueous phase include emulsifying agent, scattered protective agent and water；
C, by the oil phase and aqueous phase be blended, homogeneous, cooling, lipid rose powder is made after spray drying.
6. the preparation method of lipid rose powder according to claim 5, it is characterised in that：By the lipid carrier and rose
Ultramicro-powder is mixed, and heating water bath is used as the oil phase to 80-90 DEG C；Emulsifying agent, scattered protective agent and water are mixed, water-bath
80-90 DEG C is heated to, the aqueous phase is used as.
7. the preparation method of lipid rose powder according to claim 5, it is characterised in that：Oil phase bag mixed with water
Include：The oil phase is poured into the aqueous phase, is stirred until homogeneous, speed of agitator is 6000-9000rpm, temperature of charge is 85-95
℃。
8. the preparation method of lipid rose powder according to claim 5, it is characterised in that：, the homogeneous includes：Will mixing
Oil phase thing homogeneous mixed with water afterwards, 10~40Mpa of homogenization pressure, homogenizing temperature is 85-95 DEG C, is cooled to room after homogeneous
Temperature.
9. a kind of preparation method of rose Ultramicro-powder according to claim 5, it is characterised in that comprise the following steps：
(1) new fresh-rose is cleaned up；
(2) by the fresh rose flower coarse crushing after cleaning, the thick particulate of rose is obtained, water is added during the coarse crushing；
(3) the thick particulate of the rose is subjected to Crushing of Ultrafine, obtains rose particulate, added before Crushing of Ultrafine and during micro mist essence
Water；
(4) the rose particulate is subjected to ultramicro grinding, obtains rose ultra micron, dispersant is added during ultramicro grinding；
(5) the rose ultra micron is spray-dried, obtains rose Ultramicro-powder.
10. the preparation method of rose Ultramicro-powder according to claim 9, it is characterised in that：The thick particulate of rose is straight
Footpath 0.5-5mm particulate；The rose particulate is the particulate of 50-100 μm of diameter；The rose ultra micron is a diameter of 0.1-1 μ
M particulate.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109805407A (en) * | 2019-03-01 | 2019-05-28 | 江苏一号农场科技股份有限公司 | A kind of dry-forming method of food and drink rose local flavor coarse cereal solid beverage |
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| CN104116643A (en) * | 2014-07-10 | 2014-10-29 | 上海应用技术学院 | Nanometer solid lipid carrier covering kojic acid dipalmitate and preparing method thereof |
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| CN104116643A (en) * | 2014-07-10 | 2014-10-29 | 上海应用技术学院 | Nanometer solid lipid carrier covering kojic acid dipalmitate and preparing method thereof |
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| CN109805407A (en) * | 2019-03-01 | 2019-05-28 | 江苏一号农场科技股份有限公司 | A kind of dry-forming method of food and drink rose local flavor coarse cereal solid beverage |
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Application publication date: 20171027 |