CN107267315A - A kind of cinnamomum camphora soap and preparation method thereof - Google Patents
A kind of cinnamomum camphora soap and preparation method thereof Download PDFInfo
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- CN107267315A CN107267315A CN201710406366.2A CN201710406366A CN107267315A CN 107267315 A CN107267315 A CN 107267315A CN 201710406366 A CN201710406366 A CN 201710406366A CN 107267315 A CN107267315 A CN 107267315A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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Abstract
The invention discloses a kind of cinnamomum camphora soap and preparation method thereof, mainly the raw material including following parts by weight is constituted cinnamomum camphora soap：90 ~ 100 parts of cinnamomum camphora seed oil, 27 ~ 29 parts of potassium hydroxide, 46 ~ 58 parts of deionized water, 6 ~ 10 parts of cinnamomum camphora seed pericarp powder, 3 ~ 5 parts of Sweet Almond Oil, the invention belongs to household chemicals technical field, obtained cinnamomum camphora soap uses natural and green safety cinnamomum camphora seed oil and Sweet Almond Oil for raw material, compared with commercially available chemical industry perfumed soap, the natural plant grease of raw material 100%, very abundant of originating and category renewable resource, it is nontoxic gentle material, no added chemical composition, it is without any side effects to human body, and sterilization, cleaning effect is good, do not stimulate skin, it is gentle to moisten, foaming abundancy and it is fine and smooth, use safety.
Description
Technical field
The invention belongs to household chemicals technical field, and in particular to a kind of cinnamomum camphora soap and preparation method thereof.
Background technology
Perfumed soap is indispensable washing and nursing article in daily life, and the function of perfumed soap is cleaning dirt, skin secretion
Thing, chemical substance or bacterium etc., perfumed soap it is more be sodium soap and other surfaces activity be raw material Cake-shape soap, although
With preferable cleaning capacity and easy washability, but pH value is high, and human body skin can not be resistant to for a long time, can be to the sebum of human body skin
Film is destroyed, and skin can feel dry and astringent, stimulate, and intolerant to hard water, incrustation scale can be produced during washing, forms calcium and magnesium soap.
And in the modern times for pursuing cosmetic result, also require that perfumed soap has whitening, moisturizing, antibacterial etc. multi-functional, in order to
Multi-functional effect is reached, various additives, such as chemical blowing agent, active interface agent and preservative are added in its composition
Deng, although it can play certain maintenance skin effect, but the foam that these chemical compositions are produced, in the same of cleaning spot itself
When, also pollute the environment, and after people's long-term use, some meetings produce allergy, itch and the symptoms such as whelk that easily trigger,
Cure the symptoms, not the disease.
And the pH value that plant weak base soap contains is low, human skin can be resistant to for a long time, and contain various nutrition in plant
Material, there is skin care, therefore, researches and develops a kind of former material added, made containing natral plant ingredients, without chemical composition
Material is abundant, turns into a kind of with maintenance skin-care effect and cheap perfumed soap and needs.
Many oil plants that perfumed soap is produced using coconut oil, but the country hardly produces coconut oil in the prior art, every year
Country will expend substantial amounts of foreign exchange import few hundred thousand tonnes of coconut oil, and camphor tree seed oil is compared phase with the various aspects of performance of coconut oil
Seemingly, the Camphor resources of China are again relatively abundant, and its root, stem, leaf, branch and fruit are rich in grease, but relevant utilize camphor tree seed oil system
The research for making perfumed soap is seldom reported.
The content of the invention
To solve the above problems, the present invention provides a kind of cinnamomum camphora soap and preparation method thereof, obtained cinnamomum camphora soap is using natural
It is raw material with green safety cinnamomum camphora seed oil and Sweet Almond Oil, compared with commercially available chemical industry perfumed soap, the natural plant grease of raw material 100% comes
Source very abundant and category renewable resource, are nontoxic gentle material, no added chemical composition, to human body without the secondary work of any poison
With, and sterilization, cleaning effect are good, do not stimulate skin, gentle to moisten, foaming abundancy and it is fine and smooth, use safety.
The present invention is achieved through the following technical solutions：
A kind of cinnamomum camphora soap, includes the raw material composition of following parts by weight：90 ~ 100 parts of cinnamomum camphora seed oil, 27 ~ 29 parts of potassium hydroxide, go
46 ~ 58 parts of ionized water, 6 ~ 10 parts of cinnamomum camphora seed pericarp powder, 3 ~ 5 parts of Sweet Almond Oil.
It is preferred that, described cinnamomum camphora seed oil and the preparation method of cinnamomum camphora seed pericarp powder comprise the following steps：
A, cinnamomum camphora seed is cleaned with 15 ~ 25 DEG C of water drained；
B, by clean drain after cinnamomum camphora seed peel off pericarp, make pericarp at a temperature of 40 ~ 50 DEG C air-dry, after crushing cross 50 ~ 70
Mesh sieve, obtains cinnamomum camphora seed pericarp powder, standby；
C, separated with nut cracker and peel off the shell and kernel of the cinnamomum camphora seed after pericarp, by kernel at a temperature of 60 ~ 80 DEG C
Air-dry, 50 ~ 70 mesh sieves are crossed after crushing, cinnamomum camphora kernel powder is obtained；
D, by cinnamomum camphora kernel powder add supercritical CO2In abstraction instrument, gained extract is cinnamomum camphora seed oil.
It is preferred that, set in step d extracting pressure as 20~35Mpa, extraction temperature be 30 ~ 40 DEG C, extraction time be 50 ~
70min, fixed CO2Flow is 30L/h.
It is preferred that, a kind of preparation method of cinnamomum camphora soap comprises the following steps：
A, cinnamomum camphora seed oil, potassium hydroxide, deionized water, cinnamomum camphora seed pericarp powder and Sweet Almond Oil are weighed by above-mentioned parts by weight,
It is standby；
B, potassium hydroxide is slowly added in the stainless steel or heatproof glass container equipped with 18 ~ 28 parts of deionized waters, stirring is to complete
Fully dissolved, obtains potassium hydroxide solution；
C, cinnamomum camphora seed oil is put into stainless steel or heatproof glass container, 30 ~ 35 DEG C is heated to, by the potassium hydroxide solution of configuration
It is slowly added into cinnamomum camphora seed oil, it is stirring while adding, it is uniformly mixed, obtain soap lye；
D, cinnamomum camphora seed pericarp powder added in soap lye obtained by step c, while remaining deionized water is added, it is stirring while adding to make
It is well mixed with soap lye, untill thick state occurs in stirring to soap lye, adds Semen pruni armeniacae quintessence oil, stirs；
E, soap lye obtained by step d poured into after mould, insulation is stripped after 1 ~ 2 day at a temperature of 25 ~ 30 DEG C, is then placed on 15
Lucifuge, aeration-drying are deposited 5 ~ 6 weeks at a temperature of ~ 20 DEG C, you can obtain cinnamomum camphora soap.
It is preferred that, mixing time is 20 ~ 30min in step c.
The beneficial effects of the present invention are：
1st, it is perfumed soap made from raw material that the present invention, which uses camphor tree seed oil and Sweet Almond Oil, and Camphor Tree Seeds are by pericarp, shell and fruit
The part of benevolence 3 is constituted, and wherein Camphor Tree Seeds kernel contains aliphatic acid in abundant grease, grease and constituted with C10, C12 series fatty acid
Based on, up to 90% or so, capric acid content is up to more than 40%, also containing laurate, oleic acid, myristic acid, linoleic acid, palmitin
Acid and octanoic acid, based on capric acid and laurate, cinnamomum camphora seed oil is colourless or faint yellow to rufous oily liquids in appearance, with height
The inoxidizability of degree, appropriate dissolubility preferably shows activity, efficient foaminess and soil release performance, can replace import coconut
Oil etc. manufactures table people's activating agent, can make that skin is warm, encourages, urges sweat, expelling parasite, controls wound, is the good material of soapmaking；
2nd, kernel of the grease from pure plant of the invention passes through supercritical CO2Extraction is made, with solvability it is strong, carry
Take that speed is fast, bioactivity retain it is complete, without residual solvent the features such as, and obtained cinnamomum camphora seed oil yield is high, and impurity contains
Low, lighter color is measured, does not have any injury to the natural environment of human body, security is greatly improved；
3rd, Sweet Almond Oil of the invention, can soft flesh rich in materials such as polybasic unsaturated fatty acid, vitamin D, E and protein
Skin, moisturizing, quality is relaxed and comfortable soft, moist and non-greasy, and skin can be made to recover smooth soft and fine, and having all can be complementary with any plant
Characteristic, the also effect with isolation ultraviolet；
4th, the perfumed soap that the present invention makes, fine proportioning is carried out to raw material, is reduced production cost, is made it have good sterilization clear
Clean effect, foam is fine and smooth, has effects that skin care, also ensure that the security of cinnamomum camphora soap；
5th, the present invention make cinnamomum camphora soap when, by cinnamomum camphora seed pericarp powder add gained soap lye in, while add it is remaining go from
Sub- water, stirring while adding it is well mixed with soap lye, there is thick state in stirring to soap lye, and the pericarp of Camphor Tree Seeds has clearing damp
Effect, in wetter air ambient, or so half a year adds cinnamomum camphora seed pericarp powder not only all without going mouldy, therefore in soap lye
Energy clearing damp, moreover it is possible to ensure the stability of cinnamomum camphora soap.
Embodiment
With reference to specific embodiment, the invention will be further described：
Embodiment 1：
A kind of cinnamomum camphora soap, includes the raw material composition of following parts by weight：90 parts of cinnamomum camphora seed oil, 27 parts of potassium hydroxide, deionized water
46 parts, 6 parts of cinnamomum camphora seed pericarp powder, 3 parts of Sweet Almond Oil.
Described cinnamomum camphora seed oil and the preparation method of cinnamomum camphora seed pericarp powder comprise the following steps：
A, the cinnamomum camphora seed of intact unbroken is cleaned with 15 DEG C of water drained；
B, by clean drain after cinnamomum camphora seed peel off pericarp, make pericarp at a temperature of 40 DEG C air-dry, after crushing cross 50 mesh sieves, obtain
It is standby to cinnamomum camphora seed pericarp powder；
C, separated with nut cracker and peel off the shell and kernel of the cinnamomum camphora seed after pericarp, oil content is extremely low in shell, during liquefaction
It is not only not fuel-displaced, grease can be adsorbed on the contrary, causes oil yield to reduce, liquefaction after shell is gone, and reduced grease loss, improved fuel-displaced
Rate, therefore shell is peelled off, kernel is air-dried at a temperature of 60 DEG C, after kernel is preserved 1 day under 5 ~ 10MPa after air-drying,
Kernel is fully fuel-displaced when being conducive to extracting after crushing, then carries out segmentation frying, and the water content for controlling kernel is 6%；
Segmentation frying is first progress first paragraph frying processing, then carries out second segment frying processing, then carries out the 3rd section of frying, the
The temperature of one section of frying is 70 DEG C, and the frying time is 30min, and the temperature of second segment frying is 90 DEG C, and the frying time is 20min,
The temperature of 3rd section of frying is 110 DEG C, and the frying time is 10min, and the multiple frying of different temperatures finally controls the water content of kernel
For 6%, this water content makes kernel more broken, and moisture is too low will to increase fines content, and powder is excessive, easy conglomeration, moisture mistake
Height, oil plant do not allow it is broken and easily it is fuel-displaced, and to cinnamomum camphora seed kernel carry out segmentation frying can preferably change oil plant cell membrane
Structure, expand grease passage, improve extraction when oil yield, passivation cinnamomum camphora seed kernel in lipoxidase, improve cinnamomum camphora
The oxidation stability of seed oil；
Size-reduced machine is crushed again after frying, is then crossed 50 mesh sieves and is obtained cinnamomum camphora kernel powder, it is ensured that the granularity of cinnamomum camphora kernel powder is favourable
In subsequent operation, granularity is excessive, loss of extractant can be caused to increase, the reduction of grease yield, and particle size after cracking is too small can cause oil
The color and luster of fat is aggravated and extraction is difficult, equally adds the loss increase of extractant；
D, by cinnamomum camphora kernel powder add supercritical CO2In abstraction instrument, gained extract be cinnamomum camphora seed oil, set extracting pressure as
20Mpa, extraction temperature are 30 DEG C, extraction time is 50min, fixed CO2Flow is 30L/h, supercritical CO2The extraction that extraction is obtained
Take liquid yield high, impurity content is low, lighter color, the size of extracting pressure is influenceed than more significant on extraction yield, it is necessary to strict control
Extracting pressure, it is ensured that higher extraction efficiency.
Wherein the preparation method of cinnamomum camphora soap, comprises the following steps：
A, cinnamomum camphora seed oil, potassium hydroxide, deionized water, cinnamomum camphora seed pericarp powder and Sweet Almond Oil are weighed by above-mentioned parts by weight,
It is standby；
B, potassium hydroxide is slowly added in the stainless steel or heatproof glass container equipped with 18 parts of deionized waters, stirring is to completely molten
Solution, obtains potassium hydroxide solution；
C, cinnamomum camphora seed oil is put into stainless steel or heatproof glass container, is heated to 30 DEG C and maintains in this temperature, by configuration
Potassium hydroxide solution is slowly added into cinnamomum camphora seed oil, and stirring while adding, mixing time is 20min, it is uniformly mixed, and is obtained
Soap lye；
D, cinnamomum camphora seed pericarp powder added in soap lye obtained by step c, while remaining deionized water is added, it is stirring while adding to make
It is well mixed with soap lye, observes container condition, water-oil separating occurs, be just again stirring for, until it is well mixed, stirring to soap
Untill thick state occurs in liquid, Semen pruni armeniacae quintessence oil is added, is stirred；
E, soap lye obtained by step d poured into after mould, insulation is stripped after 1 day at a temperature of 25 DEG C, is then placed on 15 DEG C of temperature
The lower lucifuge of degree, aeration-drying are deposited 5 weeks, you can obtain cinnamomum camphora soap.
Embodiment 2：
A kind of cinnamomum camphora soap, includes the raw material composition of following parts by weight：95 parts of cinnamomum camphora seed oil, 278 parts of potassium hydroxide, deionized water
50 parts, 8 parts of cinnamomum camphora seed pericarp powder, 4 parts of Sweet Almond Oil.
Described cinnamomum camphora seed oil and the preparation method of cinnamomum camphora seed pericarp powder comprise the following steps：
A, the cinnamomum camphora seed of intact unbroken is cleaned with 20 DEG C of water drained；
B, by clean drain after cinnamomum camphora seed peel off pericarp, make pericarp at a temperature of 45 DEG C air-dry, after crushing cross 60 mesh sieves, obtain
It is standby to cinnamomum camphora seed pericarp powder；
C, separated with nut cracker and peel off the shell and kernel of the cinnamomum camphora seed after pericarp, oil content is extremely low in shell, during liquefaction
It is not only not fuel-displaced, grease can be adsorbed on the contrary, causes oil yield to reduce, liquefaction after shell is gone, and reduced grease loss, improved fuel-displaced
Rate, therefore shell is peelled off, kernel is air-dried at a temperature of 70 DEG C, after kernel is preserved 2 days under 5 ~ 10MPa after air-drying,
Kernel is fully fuel-displaced when being conducive to extracting after crushing, then carries out segmentation frying, and the water content for controlling kernel is 10%；
Segmentation frying is first progress first paragraph frying processing, then carries out second segment frying processing, then carries out the 3rd section of frying, the
The temperature of one section of frying is 60 DEG C, and the frying time is 30min, and the temperature of second segment frying is 80 DEG C, and the frying time is 20min,
The temperature of 3rd section of frying is 100 DEG C, and the frying time is 10min；
The multiple frying of different temperatures finally controls the water content of kernel to be 10%, and this water content makes kernel more broken, moisture mistake
Low to increase fines content, powder is excessive, and easy conglomeration, moisture is too high, oil plant do not allow it is broken and easily fuel-displaced, and to cinnamomum camphora seed
Kernel, which carries out segmentation frying, can preferably change the structure of oil plant cell membrane, expand grease passage, improve oil yield during extraction,
The lipoxidase in cinnamomum camphora seed kernel is passivated, the oxidation stability of cinnamomum camphora seed oil is improved；
Size-reduced machine is crushed again after frying, is then crossed 60 mesh sieves and is obtained cinnamomum camphora kernel powder, it is ensured that the granularity of cinnamomum camphora kernel powder is favourable
In subsequent operation, granularity is excessive, loss of extractant can be caused to increase, the reduction of grease yield, and particle size after cracking is too small can cause oil
The color and luster of fat is aggravated and extraction is difficult, equally adds the loss increase of extractant；
D, by cinnamomum camphora kernel powder add supercritical CO2In abstraction instrument, gained extract be cinnamomum camphora seed oil, set extracting pressure as
30Mpa, extraction temperature are 35 DEG C, extraction time is 60min, fixed CO2Flow is 30L/h.
The preparation method of one of which cinnamomum camphora soap, comprises the following steps：
A, cinnamomum camphora seed oil, potassium hydroxide, deionized water, cinnamomum camphora seed pericarp powder and Sweet Almond Oil are weighed by above-mentioned parts by weight,
It is standby；
B, potassium hydroxide is slowly added in the stainless steel or heatproof glass container equipped with 25 parts of deionized waters, stirring is to completely molten
Solution, obtains potassium hydroxide solution；
C, cinnamomum camphora seed oil is put into stainless steel or heatproof glass container, is heated to 32 DEG C and maintains in this temperature, by configuration
Potassium hydroxide solution is slowly added into cinnamomum camphora seed oil, and stirring while adding, mixing time is 25min, it is uniformly mixed, and is obtained
Soap lye；
D, cinnamomum camphora seed pericarp powder added in soap lye obtained by step c, while remaining deionized water is added, it is stirring while adding to make
It is well mixed with soap lye, observes container condition, water-oil separating occurs, be just again stirring for, until it is well mixed, stirring to soap
Untill thick state occurs in liquid, Semen pruni armeniacae quintessence oil is added, is stirred；
E, soap lye obtained by step d poured into after mould, insulation is stripped after 1 day at a temperature of 28 DEG C, is then placed on 18 DEG C of temperature
The lower lucifuge of degree, aeration-drying are deposited 5 weeks, you can obtain cinnamomum camphora soap.
Embodiment 3：
A kind of cinnamomum camphora soap, includes the raw material composition of following parts by weight：100 parts of cinnamomum camphora seed oil, 29 parts of potassium hydroxide, deionized water
58 parts, 10 parts of cinnamomum camphora seed pericarp powder, 5 parts of Sweet Almond Oil.
It is preferred that, described cinnamomum camphora seed oil and the preparation method of cinnamomum camphora seed pericarp powder comprise the following steps：
A, cinnamomum camphora seed is cleaned with 25 DEG C of water drained；
B, by clean drain after cinnamomum camphora seed peel off pericarp, make pericarp at a temperature of 50 DEG C air-dry, after crushing cross 70 mesh sieves, obtain
It is standby to cinnamomum camphora seed pericarp powder；
C, separated with nut cracker and peel off the shell and kernel of the cinnamomum camphora seed after pericarp, oil content is extremely low in shell, during liquefaction
It is not only not fuel-displaced, grease can be adsorbed on the contrary, causes oil yield to reduce, liquefaction after shell is gone, and reduced grease loss, improved fuel-displaced
Rate, therefore shell is peelled off, kernel is air-dried at a temperature of 80 DEG C, after kernel is preserved 3 days under 5 ~ 10MPa after air-drying,
Kernel is fully fuel-displaced when being conducive to extracting after crushing, then carries out segmentation frying, and the water content for controlling kernel is 15%；
Segmentation frying is first progress first paragraph frying processing, then carries out second segment frying processing, then carries out the 3rd section of frying, the
The temperature of one section of frying is 50 DEG C, and the frying time is 30min, and the temperature of second segment frying is 60 DEG C, and the frying time is 20min,
The temperature of 3rd section of frying is 80 DEG C, and the frying time is 10min, and the multiple frying of different temperatures finally controls the water content of kernel to be
15%, this water content makes kernel more broken, and moisture is too low will to increase fines content, and powder is excessive, and easy conglomeration, moisture is too high,
Oil plant do not allow it is broken and easily it is fuel-displaced, and to cinnamomum camphora seed kernel carry out segmentation frying can preferably change the knot of oil plant cell membrane
Structure, expands grease passage, improves the lipoxidase in oil yield during extraction, passivation cinnamomum camphora seed kernel, improves cinnamomum camphora seed oil
Oxidation stability；
Size-reduced machine is crushed again after frying, is then crossed 70 mesh sieves and is obtained cinnamomum camphora kernel powder, it is ensured that the granularity of cinnamomum camphora kernel powder is favourable
In subsequent operation, granularity is excessive, loss of extractant can be caused to increase, the reduction of grease yield, and particle size after cracking is too small can cause oil
The color and luster of fat is aggravated and extraction is difficult, equally adds the loss increase of extractant；
D, by cinnamomum camphora kernel powder add supercritical CO2In abstraction instrument, gained extract is setting extraction in cinnamomum camphora seed oil, step d
Pressure be 35Mpa, extraction temperature be 40 DEG C, extraction time be 70min, fixed CO2Flow 30L/h.
A kind of preparation method of cinnamomum camphora soap, comprises the following steps：
A, cinnamomum camphora seed oil, potassium hydroxide, deionized water, cinnamomum camphora seed pericarp powder and Sweet Almond Oil are weighed by above-mentioned parts by weight,
It is standby；
B, potassium hydroxide is slowly added in the stainless steel or heatproof glass container equipped with 28 parts of deionized waters, stirring is to completely molten
Solution, obtains potassium hydroxide solution；
C, cinnamomum camphora seed oil is put into stainless steel or heatproof glass container, is heated to 35 DEG C and maintains in this temperature, by configuration
Potassium hydroxide solution is slowly added into cinnamomum camphora seed oil, and stirring while adding, mixing time is 30min, it is uniformly mixed, and is obtained
Soap lye；
D, cinnamomum camphora seed pericarp powder added in soap lye obtained by step c, while remaining deionized water is added, it is stirring while adding to make
It is well mixed with soap lye, observes container condition, water-oil separating occurs, be just again stirring for, until it is well mixed, stirring to soap
Untill thick state occurs in liquid, Semen pruni armeniacae quintessence oil is added, is stirred；
E, soap lye obtained by step d poured into after mould, insulation is stripped after 2 days at a temperature of 30 DEG C, is then placed on 20 DEG C of temperature
The lower lucifuge of degree, aeration-drying are deposited 6 weeks, you can obtain cinnamomum camphora soap.
The basic principles, principal features and advantages of the present invention have been shown and described above, the technical staff of the industry should
Understand, the present invention is not limited to the above embodiments, the original for simply illustrating the present invention described in above-described embodiment and specification
Reason, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes and improvements
It all fall within the protetion scope of the claimed invention, the claimed scope of the invention is by appended claims and its equivalent circle
It is fixed.
Claims (5)
1. a kind of cinnamomum camphora soap, it is characterised in that：Raw material composition including following parts by weight：90 ~ 100 parts of cinnamomum camphora seed oil, hydrogen-oxygen
Change 27 ~ 29 parts of potassium, 46 ~ 58 parts of deionized water, 6 ~ 10 parts of cinnamomum camphora seed pericarp powder, 3 ~ 5 parts of Sweet Almond Oil.
2. a kind of cinnamomum camphora soap according to claim 1, it is characterised in that：Described cinnamomum camphora seed oil and cinnamomum camphora seed pericarp powder
Preparation method comprise the following steps：
A, cinnamomum camphora seed is cleaned with 15 ~ 25 DEG C of water drained；
B, by clean drain after cinnamomum camphora seed peel off pericarp, make pericarp at a temperature of 40 ~ 50 DEG C air-dry, after crushing cross 50 ~ 70
Mesh sieve, obtains cinnamomum camphora seed pericarp powder, standby；
C, separated with nut cracker and peel off the shell and kernel of the cinnamomum camphora seed after pericarp, by kernel at a temperature of 60 ~ 80 DEG C
Air-dry, 50 ~ 70 mesh sieves are crossed after crushing, cinnamomum camphora kernel powder is obtained；
D, by cinnamomum camphora kernel powder add supercritical CO2In abstraction instrument, gained extract is cinnamomum camphora seed oil.
3. a kind of cinnamomum camphora soap according to claim 2, it is characterised in that：Set in step d extracting pressure as 20~
35Mpa, extraction temperature are 30 ~ 40 DEG C, extraction time is 50 ~ 70min, fixed CO2Flow is 30L/h.
4. a kind of preparation method of cinnamomum camphora soap according to claim 1, it is characterised in that：Comprise the following steps：
A, cinnamomum camphora seed oil, potassium hydroxide, deionized water, cinnamomum camphora seed pericarp powder and Sweet Almond Oil are weighed by above-mentioned parts by weight,
It is standby；
B, potassium hydroxide is slowly added in the stainless steel or heatproof glass container equipped with 18 ~ 28 parts of deionized waters, stirring is to complete
Fully dissolved, obtains potassium hydroxide solution；
C, cinnamomum camphora seed oil is put into stainless steel or heatproof glass container, 30 ~ 35 DEG C is heated to, by the potassium hydroxide solution of configuration
It is slowly added into cinnamomum camphora seed oil, it is stirring while adding, it is uniformly mixed, obtain soap lye；
D, cinnamomum camphora seed pericarp powder added in soap lye obtained by step c, while remaining deionized water is added, it is stirring while adding to make
It is well mixed with soap lye, untill thick state occurs in stirring to soap lye, adds Semen pruni armeniacae quintessence oil, stirs；
E, soap lye obtained by step d poured into after mould, insulation is stripped after 1 ~ 2 day at a temperature of 25 ~ 30 DEG C, is then placed on 15
Lucifuge, aeration-drying are deposited 5 ~ 6 weeks at a temperature of ~ 20 DEG C, you can obtain cinnamomum camphora soap.
5. a kind of preparation method of cinnamomum camphora soap according to claim 4, it is characterised in that：In step c mixing time be 20 ~
30min。
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102517174A (en) * | 2011-11-27 | 2012-06-27 | 郴州邦尔泰苏仙油脂有限公司 | Camellia facial soap |
| CN103589535A (en) * | 2013-11-27 | 2014-02-19 | 骆志明 | Skin-care honeysuckle liquid soap |
| CN103589536A (en) * | 2013-11-27 | 2014-02-19 | 骆志明 | Licorice-containing skin moistening liquid soap |
| CN104099198A (en) * | 2014-07-03 | 2014-10-15 | 广西大学 | Pure natural plant acne-removing facial soap |
| CN104629899A (en) * | 2014-12-30 | 2015-05-20 | 广州白云山汉方现代药业有限公司 | Method for extracting malania oleifera oil by virtue of supercritical CO2 fluid |
| CN104629895A (en) * | 2015-02-09 | 2015-05-20 | 吴海军 | Cucumis metuliferus fruit seed oil and preparation method thereof |
| CN105238551A (en) * | 2015-10-09 | 2016-01-13 | 福建天斯顿生物科技有限公司 | Method for supercritical CO2 extraction and purification of camellia seed oil |
-
2017
- 2017-06-02 CN CN201710406366.2A patent/CN107267315A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102517174A (en) * | 2011-11-27 | 2012-06-27 | 郴州邦尔泰苏仙油脂有限公司 | Camellia facial soap |
| CN103589535A (en) * | 2013-11-27 | 2014-02-19 | 骆志明 | Skin-care honeysuckle liquid soap |
| CN103589536A (en) * | 2013-11-27 | 2014-02-19 | 骆志明 | Licorice-containing skin moistening liquid soap |
| CN104099198A (en) * | 2014-07-03 | 2014-10-15 | 广西大学 | Pure natural plant acne-removing facial soap |
| CN104629899A (en) * | 2014-12-30 | 2015-05-20 | 广州白云山汉方现代药业有限公司 | Method for extracting malania oleifera oil by virtue of supercritical CO2 fluid |
| CN104629895A (en) * | 2015-02-09 | 2015-05-20 | 吴海军 | Cucumis metuliferus fruit seed oil and preparation method thereof |
| CN105238551A (en) * | 2015-10-09 | 2016-01-13 | 福建天斯顿生物科技有限公司 | Method for supercritical CO2 extraction and purification of camellia seed oil |
Non-Patent Citations (2)
| Title |
|---|
| 科普小组: "《中国学生成长必读书—草木奇葩》", 31 October 2006, 吉林电子出版社 * |
| 马振友 等: "《皮肤美容化妆品制剂手册》", 31 March 2001, 中医古籍出版社 * |
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