CN106190609A - The preparation method of high active ingredient tea cake powder detergent and tea cake powder detergent - Google Patents
The preparation method of high active ingredient tea cake powder detergent and tea cake powder detergent Download PDFInfo
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- CN106190609A CN106190609A CN201610522603.7A CN201610522603A CN106190609A CN 106190609 A CN106190609 A CN 106190609A CN 201610522603 A CN201610522603 A CN 201610522603A CN 106190609 A CN106190609 A CN 106190609A
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- tea
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- powder detergent
- cake powder
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- 239000000843 powder Substances 0.000 title claims abstract description 102
- 239000003599 detergent Substances 0.000 title claims abstract description 86
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000004480 active ingredient Substances 0.000 title claims abstract description 14
- 241001122767 Theaceae Species 0.000 title claims abstract 27
- 210000000582 semen Anatomy 0.000 claims abstract description 37
- 238000000034 method Methods 0.000 claims abstract description 23
- 239000001397 quillaja saponaria molina bark Substances 0.000 claims abstract description 19
- 229930182490 saponin Natural products 0.000 claims abstract description 19
- 150000007949 saponins Chemical class 0.000 claims abstract description 19
- 235000018597 common camellia Nutrition 0.000 claims abstract description 17
- 239000000835 fiber Substances 0.000 claims abstract description 15
- 239000012535 impurity Substances 0.000 claims abstract description 10
- 238000000926 separation method Methods 0.000 claims abstract description 9
- 238000001035 drying Methods 0.000 claims abstract description 6
- 241000209507 Camellia Species 0.000 claims abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- 235000019750 Crude protein Nutrition 0.000 claims description 10
- 230000006835 compression Effects 0.000 claims description 10
- 238000007906 compression Methods 0.000 claims description 10
- 238000005406 washing Methods 0.000 claims description 9
- 229910052785 arsenic Inorganic materials 0.000 claims description 8
- 229910001385 heavy metal Inorganic materials 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- 239000000725 suspension Substances 0.000 claims description 7
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 229910052745 lead Inorganic materials 0.000 claims 1
- 239000003921 oil Substances 0.000 abstract description 55
- 238000005187 foaming Methods 0.000 abstract description 14
- 230000000694 effects Effects 0.000 abstract description 8
- 102000004169 proteins and genes Human genes 0.000 abstract description 7
- 108090000623 proteins and genes Proteins 0.000 abstract description 7
- 230000008569 process Effects 0.000 abstract description 6
- 238000005202 decontamination Methods 0.000 abstract description 5
- 230000003588 decontaminative effect Effects 0.000 abstract description 5
- 230000001804 emulsifying effect Effects 0.000 abstract description 5
- 239000000284 extract Substances 0.000 abstract description 5
- 239000000203 mixture Substances 0.000 abstract description 4
- 235000014593 oils and fats Nutrition 0.000 abstract description 4
- 238000010008 shearing Methods 0.000 abstract description 4
- 244000269722 Thea sinensis Species 0.000 description 136
- 235000019198 oils Nutrition 0.000 description 54
- 239000000047 product Substances 0.000 description 28
- 238000004851 dishwashing Methods 0.000 description 13
- 240000001548 Camellia japonica Species 0.000 description 12
- 239000010779 crude oil Substances 0.000 description 11
- 239000002994 raw material Substances 0.000 description 11
- 235000005593 Camellia sinensis f parvifolia Nutrition 0.000 description 10
- 244000041840 Camellia sinensis f. parvifolia Species 0.000 description 10
- 230000001236 detergent effect Effects 0.000 description 9
- 238000004140 cleaning Methods 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 8
- 239000000463 material Substances 0.000 description 8
- 238000007670 refining Methods 0.000 description 7
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 238000001556 precipitation Methods 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- 238000000605 extraction Methods 0.000 description 5
- 230000036541 health Effects 0.000 description 5
- 241000526900 Camellia oleifera Species 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 244000294611 Punica granatum Species 0.000 description 3
- 235000014360 Punica granatum Nutrition 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- 238000005520 cutting process Methods 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000009434 installation Methods 0.000 description 3
- 229930014626 natural product Natural products 0.000 description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 description 3
- 235000021419 vinegar Nutrition 0.000 description 3
- 239000000052 vinegar Substances 0.000 description 3
- HPVKSGLGOKNQON-UHFFFAOYSA-N 3-O-(beta-D-galactopyranosyl-(1->3)-beta-D-glucopyranosyl)serjanic acid 28-O-beta-D-glucopyranoside Natural products COC(=O)C1(C)CCC2(CCC3(C)C(=CCC4C5(C)CCC(OC6OC(CO)C(O)C(OC7OC(CO)C(O)C(O)C7O)C6O)C(C)(C)C5CCC34C)C2C1)C(=O)OC8OC(CO)C(O)C(O)C8O HPVKSGLGOKNQON-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
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- 239000012141 concentrate Substances 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 230000008030 elimination Effects 0.000 description 2
- 238000003379 elimination reaction Methods 0.000 description 2
- 239000003925 fat Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 238000012216 screening Methods 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- 244000147058 Derris elliptica Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 240000007817 Olea europaea Species 0.000 description 1
- AOILXFWEUKCKQQ-UHFFFAOYSA-N Saponin 8 Natural products COC(=O)C1(C)CCC2(CCC3(C)C(=CCC4C5(C)CCC(OC6OC(CO)C(O)C(O)C6OC7OC(CO)C(O)C(O)C7O)C(C)(C)C5CCC34C)C2C1)C(=O)OC8OC(CO)C(O)C(O)C8O AOILXFWEUKCKQQ-UHFFFAOYSA-N 0.000 description 1
- 235000006468 Thea sinensis Nutrition 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000001139 anti-pruritic effect Effects 0.000 description 1
- -1 antiinflammatory Substances 0.000 description 1
- 239000003908 antipruritic agent Substances 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000010495 camellia oil Substances 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 230000007850 degeneration Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000003505 heat denaturation Methods 0.000 description 1
- 230000002949 hemolytic effect Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 229930182493 triterpene saponin Natural products 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C11D2111/14—
Abstract
The invention discloses preparation method and the tea cake powder detergent of a kind of high active ingredient tea cake powder detergent.The present invention will clear up after remove impurity Semen Camelliae or tea-seed at a temperature of 70～80 DEG C through repeated drying, the moisture making Semen Camelliae or tea-seed controls to be 7%～8%, then use stranding to tear the shearing mode of peeling off to peel off and make Kernel-hull separation, control rate of hull in kernel 5%～8%, the moisture adjusting the camellia seed kernel after shelling or tea-seed core again is 4%～5%, squeeze fuel-displaced under conditions of temperature is not higher than 60 DEG C, control cake temperature and be not higher than 90 DEG C, residual oil of tea cakes rate 5%～6%, tea cake after fuel-displaced for squeezing is pulverized, take and i.e. obtain tea cake detergent by the fine powder of 150～200 mesh sieves.The present invention is gained tea cake after specific shelling squeezing process extracts oils and fats, maintain the activity of the composition such as protein and tea saponin well, and the crude fibre containing reasonable amount, be have excellent emulsifying, disperse, moisten, decontamination, the natural detergent of foaming isoreactivity function, it is achieved that complete feed, the whole part of tea cake is utilized.
Description
Technical field
The present invention relates to the preparation method of daily cleaning product, wash more particularly, to a kind of high active ingredient tea cake powder
Wash preparation method and the tea cake powder detergent of agent.
Background technology
The detergent relevant to camellia oleosa seed, because natural, becomes the focus of research.
Camellia oleosa seed powder, rich in natural tea saponin powder, can go rapidly to degrease in theory, bowls and chopsticks capable of washing, plate, bowl, vegetable,
Fruit etc., deoil, dirt-removing power very strong, good punching is washed the best, does not hurts hands, can decompose the remaining pesticide in vegetables and fruits.It is exclusive
Sterilization, removing toxic substances, antiinflammatory, antipruritic pharmacological function, be a pure natural wash clean product, at our ancient Chinese, had
Ancients begin to use camellia oleosa seed powder.
The method having several making camellia oleosa seed powder at present: a kind of is directly to be squeezed out by the oil in Camellia by high temperature squeezing
Come (deoiling treatment), then pulverize the shell of Camellia and grind pressure, lappingout and become dark brown powder, another without take off
Oil is directly pulverized as off-white powder.
It is more to utilize tea cake, tea cake is crushed to certain fineness and uses as detergent.Tea cake is also known as Oil-tea-cake
It is the grouts after Property of Tea oil Tree Fruit oil expression, aboundresources, low price.
China is the country finding and utilizing Camellia sinensis the most the earliest, is also the country cultivating oil tea the most the earliest, tool
There is the plantation history of 2000 or three thousand years.Folium Camelliae sinensis and oil tea are same mesh, equal, the plant that belongs to together, are the different tree species of Camellia.According to system
Meter, China's oil tea cultivated area has reached 4,000,000 hm the most2, gross annual output Semen Camelliae more than 60 ten thousand t, wherein with Hunan, Jiangxi provinces
Yield most, account for more than the 60% of the total Semen Camelliae yield in the whole nation.It addition, also there is bigger yield in Hubei, Guangxi, Anhui, Zhejiang.
According to another statistics, China existing tea place area about 213.33 ten thousand hm2(32,000,000 mu), produce tea-seed about 1,000,000 t per year.
Obtain accounting for the tea cake of raw material more than 50%, current domestic most employings after Semen Camelliae or tea-seed shelling squeezing liquefaction
Traditional Semen Camelliae or tea-seed squeezing oil-producing technique, peel off and after Kernel-hull separation, and usual rate of hull in kernel, more than 15%, makes
The ratio of raw material shared by tea cake that obtains is also possible to higher.About moisture content 4%～5% in tea cake, fat 5%～6%, crude protein 12%
～15%, crude fibre 8%～10%, tea saponin 10%～15%, saccharide 30%～35%.The utilization of tea cake at present is mainly used as
The extraction raw material of tea saponin, conventional extraction process mainly has flooding and alcohol two kinds of techniques of extraction.Flooding: be by tea cake powder
Broken, hot-water soak, cross extracting solution after elimination residue and concentrate, reconcentration after decolouring, then carry out decolouring and obtain tea saponin.Alcohol extracts:
Being tea cake steaming stir-fry to be pulverized, use ethanol solution alcohol extraction, after crossing elimination residue, extracting solution concentrates, then through decolouring, refining (such as ultrafilter membrane
Separate) obtain tea saponin.Although it is higher that above two method obtains product purity, but complex technical process, yield is relatively low, equipment
Investment is raw and product cost is the highest, is not suitable with medium and small Semen Camelliae or the needs of tea-seed processing factory comprehensive utilization.Extraction has
After the tea saponin of hemolytic, although tea cake is containing a certain amount of fat and crude protein, can be as animal feed, but due to water
Or alcoholic solution extracts tea saponin and makes tea cake contain large quantity of moisture, must dry to store use, this will consume substantial amounts of heat
Energy.So existing tea cake recycling mode is not suitable for most of manufacturing enterprise of China, recycling effect is the most poor.Additionally adopt
With hot moulding technique obtained tea cake brown color, the tea cake pink colour being ground into this tea cake is deep and emulsibility and washability relatively
Difference, it is impossible to bubble or foam is not enough.
Summary of the invention
The technical problem to be solved in the present invention is the deficiency utilizing technology for existing tea cake, makes after especially being pulverized
The technical deficiency of the detergent become, it is provided that the preparation method of a kind of high active ingredient tea cake powder detergent.
Another that the invention solves the problems that technical problem is that based on a kind of tea cake powder detergent of described preparation method offer.
The purpose of the present invention is achieved by the following technical programs:
The preparation method of a kind of high active ingredient tea cake powder detergent is provided, Semen Camelliae or tea-seed are shelled through specific
Squeezing process extracts gained tea cake complete feed after oils and fats and is crushed to certain fineness and prepares, and this squeezing process that specifically shells can ensure that institute
The detergent prepared has good foaming characteristic, emulsibility and oil stain eluting power.
Specifically, it is provided that the preparation method of a kind of high active ingredient tea cake powder detergent, comprise the following steps:
S1. after clearing up remove impurity, Semen Camelliae or tea-seed are dried through 2～3 times at a temperature of 70～80 DEG C, make aqueous
Dividing content to control is 7%～8%；
S2. use stranding to tear-shear the mode of peeling off to peel off and make Kernel-hull separation, control rate of hull in kernel 5%～8%；
S3. the moisture adjusting the camellia seed kernel after shelling or tea-seed core is down to 4%～5% by 7%～8%,
Under conditions of temperature is not higher than 60 DEG C, it is fed directly into twin screw or single screw spiral oil press squeezing is fuel-displaced, control cake temperature
Not higher than 90 DEG C；Obtain squeezing fuel-displaced after tea cake；
S4. tea cake is pulverized, take and i.e. obtain tea cake detergent by the fine powder of 150～200 mesh sieves.
Product of the present invention can use automatic gauge, irrigate, that the small packer that seals is distributed into 50g and 100g is packed.
First Semen Camelliae after cleaning remove impurity or tea-seed are dried at a temperature of 70～80 DEG C by the present invention through 2～3 times,
Making moisture content content control is 7%～8%, and the technological parameter of this step strictly controls, by being dried under special parameter
Processing, it is achieved two purposes, first is to avoid Semen Camelliae well in dry run or tea-seed is excessively heated and leads
Cause protein heat denaturation in raw material, ensured the surface activity of protein in tea cake, finally ensure that product detergent active and
Good foaming characteristic；Second be control Semen Camelliae or tea-seed be dried to moisture be accurate scope, this moisture
Condition is that important basis is established in the follow-up requirement that reaches preferably to peel off.Preferably, dry described in step S1 is to dry 40 every time
～60 minutes.
Research summary of the present invention, can help dirt dirt rubbing although crude fibre contained by tea cake is in the suds
Eluting, but in cake, the too high meeting of crude fiber content causes tea cake powder detergent coarse and water solublity is deteriorated, and this is also to use tea equally
Cake is crushed to certain fineness, but the one of the main reasons that the mass difference of Betengent product is the most remote.The present invention set peel off and
After Kernel-hull separation, rate of hull in kernel, 5%～8%, can effectively solve this problem, both ensure that in tea cake powder detergent certain
Crude fiber content, in turn ensure that the exquisiteness of tea cake powder detergent and good water solublity.Specifically, do in special process parameter
On the basis of dry step S1, technique of peeling off is optimized by the present invention, use stranding tear-shearing-type Fructus Camelliae sinensis decorticator is to oil tea
Seed or tea-seed are peeled off, and tea core is separated by the machine for separating kernel and shell combined with sieve wind with Camellia oleifera Abel, controls rate of hull in kernel and exists
5%～8%.Fructus Camelliae sinensis decorticator has dividing of centrifugal collision type and crowded stranding type etc., and the present invention passes through numerous studies and Test Summary,
Under the conditions of moisture is 7%～8%, use rub with the hands tear-shearing-type Fructus Camelliae sinensis decorticator combines with the sieve machine for separating kernel and shell that is combined of wind,
It is best suitable for reaching the requirement of relatively low rate of hull in kernel.
The present invention shell further after camellia seed kernel or tea-seed core in quality-adjusting device by its contained humidity by 7%～
8% is down to 4%～5%, and at this particular range temperature and moisture condition, and raw material contained oil is divided and contains the mutual work of shell amount
With, making possess the plasticity and elasticity matched with oil press pressure into squeezing material, squeezing is fuel-displaced continuously, go out cake, and crude oil is through precipitation
Refining procedure is delivered to after filtration.The residual oil content of Semen Camelliae or tea-seed press cake is 5%～6%.
Carry out squeezing and control cake temperature at this particular range temperature and moisture condition, oils and fats contained in raw material to the greatest extent
Piezometric is squeezed out, it is ensured that rational residual oil content in tea cake, not only increases crude oil yield, and in tea cake, Residual oil reduction makes
The water solublity obtaining tea cake powder detergent is significantly improved, and improves its emulsifiability and frothing capacity, and uses compression ratio
The twin screw high, squeezing breech pressure is big or single screw spiral oil press squeezing are fuel-displaced, reach for residual oil content in press cake further
5%～6% requires the guarantee in terms of offer equipment.Meanwhile, the further research summary of the present inventor, tea saponin is a class olive
Alkane type pentacyclic triterpene saponin compound, when pressing temperature is too high, the contained heated denaturalization such as pectin, protein, tea soap in tea cake
Element is wrapped in degeneration condensation product, causes the tea cake powder detergent of preparation in use, and tea saponin is difficult to be discharged into cleaning mixture
In, affect this natural nonionic surfactant of tea saponin emulsifying, disperse, moisten, decontamination, the surface activity such as foaming,
Pressing temperature is set as 60 DEG C and goes out cake temperature and be set as not higher than 90 DEG C by step S3 the most of the present invention, it is thus achieved that excellent crude oil
Save the activity of tea saponin while quality well, and protect the surface activity of protein in tea cake powder the most further, eventually
Product tea cake powder detergent have good emulsifying, disperse, moisten, decontamination, the some surface active property such as foaming.
Preferably, the compression ratio of single-screw oil press described in step S3 is 17, and machine breech pressure is 25.5MPa.
Preferably, the compression ratio of twin-screw press described in step S3 is 17.3, and machine breech pressure is 23.5MPa.
Preferably, pulverizing described in step S4 is to use turbine whirlwind (WFJ) type micronizing unit.The present invention accurately determines
The smashing fineness scope of tea cake powder is by 150～200 mesh sieves, in this range, and beneficially tea cake powder fine dispersion in water
And form suspension, it is also beneficial to ingredient in cake and preferably dissolves in water or spread.
Present invention simultaneously provides obtained tea cake powder detergent.Betengent product outward appearance of the present invention is that light coffee color is thin
Powder, fatty 5%～6%, moisture 4%～5%, crude fibre 5%～8%.Active principals: crude protein 12%～15%, tea
Saponin 10%～15%.Fineness crosses 150～200 mesh sieves.Heavy metal: arsenic (in 1% solution in terms of As), mg/kg≤0.05 lead
(in 1% solution in terms of Pb), mg/kg≤1.
During use, cutting off packed by product of the present invention, tea cake cleanser is poured in the hot water of 40～50 DEG C, and stirring is i.e. formed
Having the emulsified suspension of soapy feeling, wash for tableware etc., clean result is excellent.
The method have the advantages that
The present invention will clear up after remove impurity Semen Camelliae or tea-seed at a temperature of 70～80 DEG C through repeated drying, make oil tea
It is 7%～8% that the moisture of seed or tea-seed controls, and then uses stranding to tear-shear the mode of peeling off and peels off and make Kernel-hull separation, control
Rate of hull in kernel processed 5%～8%, then adjust the camellia seed kernel after shelling or the moisture of tea-seed core be 4%～5%,
Squeeze fuel-displaced under conditions of temperature is not higher than 60 DEG C, control cake temperature and be not higher than 90 DEG C, residual oil of tea cakes rate 5%～6%, will
Squeeze fuel-displaced after tea cake pulverize, take and i.e. obtain tea cake detergent by the fine powder of 150～200 mesh sieves.The present invention is through specific de-
Shell squeezing process extracts gained tea cake after oils and fats, maintains the activity of the composition such as protein and tea saponin well, and containing closing
The crude fibre of reason amount, be have excellent emulsifying, disperse, moisten, decontamination, the natural detergent of foaming isoreactivity function, it is achieved
Complete feed, the whole part of tea cake is utilized.
Contained protein in the tea cake powder detergent obtained by the inventive method is used to have good surface activity, it is possible to
Make fatty and moisture when being dissolved in the hot water of 40～50 DEG C, under rubbing somewhat and agitation, form oil-in-water type (O/
W) stable emulsion, and bubbling, tea saponin content is higher, product have emulsifying, disperse, moisten, decontamination, foaming etc. multiple
Surface-active property；Product is fine and smooth and contained crude fibre amount is relatively more reasonable, is in the suds and dirt can be formed the rubbing of appropriateness,
Helping the eluting of dirt, product fineness ensures its fine dispersion form suspension in water further, is also beneficial in cake institute
Dissolve in water containing composition or spread.Tea cake powder detergent of the present invention has above-mentioned excellent wash characteristics, pour into during use 40～
In the hot water of 50 DEG C, the tableware being then placed in washing i.e. can be by the oil stain on tableware and dirt eluting, with existing tea cake powder
Product compares, it is not necessary to rubbing energetically.Rinse tableware with clear water after having washed, the washing on tableware can be will attach to
Agent is rinsed well, owing to this detergent is natural component, thus pollution-free to wash environment.
The present invention is that the tea cake after oil expression provides feasible reutilization technology means.
Detailed description of the invention
The present invention is further illustrated below in conjunction with specific embodiment.Following embodiment being merely cited for property explanation, it is impossible to reason
Solve as limitation of the present invention.Unless stated otherwise, the raw material used in following embodiment obtains for conventional commercial or commercial sources
The raw material obtained, unless stated otherwise, the method and apparatus used in following embodiment is method commonly used in the art and sets
Standby.
Embodiment 1
S1. after clearing up remove impurity, Semen Camelliae or tea-seed are dried through 3 times at a temperature of 70 DEG C, make moisture content content control
It is made as 8%；
S2. use stranding to tear-shear the mode of peeling off to peel off and make Kernel-hull separation, control rate of hull in kernel 5%；Described stranding tears-
Shearing is peeled off to use and is produced YTTK.100 type decorticator by Scientia Agricultura Sinica academy Wuhan oil crop institute, also
Other manufacturer production of this area, other models similar decorticator can be used.Camellia oleifera Abel is delivered to shell storehouse.
S3. adjust the moisture of the camellia seed kernel after shelling or tea-seed core by 8% being down to 4% (by camellia seed kernel or
Tea-seed core carries out steam heating in being placed in quality-adjusting device, discharge steam), under conditions of temperature reaches 60 DEG C.It is fed directly into double spiral shell
(such as SYZX.12 type, TianXing, city of Anlu Hubei grain and oil machinery equipment company limited producing, this machine compression ratio 17.3, in press chamber for bar
Pressure 23.5MPa) screw oil expeller, control cake temperature less than 90 DEG C.At this particular range temperature and moisture condition, with
And raw material contained oil divides and contain the reciprocal action of shell amount, make possess the plasticity and bullet matched with oil press pressure into squeezing material
Property.Squeezing is fuel-displaced continuously, go out cake, and crude oil delivers to refining procedure after precipitation filters.Semen Camelliae or tea-seed press cake residual oil content
It is 5%.
S4., tea cake is sent into turbine whirlwind micronizing unit, and (WFJ-60 type, by the limited public affairs of Jiangyin City's health and machine-building
Department produces), it is ground into and is tea cake detergent by the fine powder of 200 mesh sieves.
Product appearance is light coffee color fine powder, fatty 5%, and moisture 4%, crude fibre 5%.Active principals: crude protein
15%, tea saponin 15%.Fineness crosses 200 mesh sieves.Heavy metal: arsenic (in 1% solution in terms of As), (1% is molten for mg/kg≤0.05 lead
In liquid in terms of Pb), mg/kg≤1.
It is packed that the small packer can be measured through (automatically) by gained, irrigate, sealed is distributed into 50g and 100g.During use, cut
Opening in the packed hot water that tea cake cleanser is poured into 40～50 DEG C, stirring i.e. forms the emulsified suspension with soapy feeling, is used for
Dishwashing detergent.Compared with the present embodiment tea cake powder detergent washes essence alive with " vertical white " new Fructus Fortunellae Margaritae of board, its 2g is to dishwashing detergent effect
Essence of living is washed equal with 2mL.But when rinsing, owing to " vertical white " new Fructus Fortunellae Margaritae of board washes the adhesive force of essence of living by force, need to repeatedly rush with clear water
Wash and could clean, and tea cake powder detergent only rinses can clean with a clear water.By the present embodiment tea cake powder detergent and Korea Spro
State's " long green elegant hands " Punica granatum L. vinegar detergent compares, and its 2g is equal to this Korea S's detergent of dishwashing detergent effect and 2mL, and clear water floats
The time of washing is about 5 seconds, and this product is natural product, not residual.By the present embodiment tea cake powder and sale on existing network
Camellia oleosa seed powder cleaning product compares, and the foaming characteristic of the present embodiment tea cake powder, emulsibility and oil stain eluting power are significantly superior to
Existing camellia oleosa seed powder product.
Meanwhile, the present embodiment gained crude oil color is shallower, reaches camellia seed oil national standard after conventional refinery
(GB11765-2003)。
Embodiment 2
S1. after clearing up remove impurity, Semen Camelliae or tea-seed are dried through 2 times at a temperature of 80 DEG C, make moisture content content control
It is made as 7%；
S2. use stranding to tear-shear the mode of peeling off to peel off and make Kernel-hull separation, control rate of hull in kernel 8%；Described stranding tears-
Shearing is peeled off to use and is produced YTTK.100 type decorticator by Scientia Agricultura Sinica academy Wuhan oil crop institute, also
Other manufacturer production of this area, other models similar decorticator can be used.Camellia oleifera Abel is delivered to shell storehouse.
S3. adjust the moisture of the camellia seed kernel after shelling or tea-seed core by 8% being down to 4% (by camellia seed kernel or
Tea-seed core carries out steam heating in being placed in quality-adjusting device, discharge steam), temperature single screw rod under conditions of reaching 50 DEG C (as
KQZX.18 type, is produced by TianXing, city of Anlu Hubei grain and oil machinery equipment company limited, this machine compression ratio 17, machine breech pressure
25.5MPa) screw oil expeller, controls cake temperature less than 80 DEG C.At this particular range temperature and moisture condition, Yi Jiyuan
Material contained oil is divided and contains the reciprocal action of shell amount, makes possess the plasticity and elasticity matched with oil press pressure into squeezing material.Even
Continuous squeezing is fuel-displaced, go out cake, and crude oil delivers to refining procedure after precipitation filters.Semen Camelliae or tea-seed press cake residual oil content are 6%；
S4., tea cake is sent into turbine whirlwind micronizing unit, and (WFJ-60 type, by the limited public affairs of Jiangyin City's health and machine-building
Department produces), it is ground into and is tea cake detergent by the fine powder of 150 mesh sieves.
Product appearance is light coffee color fine powder, fatty 6%, and moisture 5%, crude fibre 8%.Active principals: crude protein
12%, tea saponin 10%.Fineness crosses 150 mesh sieves.Heavy metal: arsenic (in 1% solution in terms of As), (1% is molten for mg/kg≤0.05 lead
In liquid in terms of Pb), mg/kg≤1.
It is packed that the small packer can be measured through (automatically) by gained, irrigate, sealed is distributed into 50g and 100g.During use, cut
Opening in the packed hot water that tea cake cleanser is poured into 40～50 DEG C, stirring i.e. forms the emulsified suspension with soapy feeling, is used for
Dishwashing detergent.Compared with the present embodiment tea cake powder detergent washes essence alive with " vertical white " new Fructus Fortunellae Margaritae of board, its 2g is to dishwashing detergent effect
Essence of living is washed equal with 2mL.But when rinsing, owing to " vertical white " new Fructus Fortunellae Margaritae of board washes the adhesive force of essence of living by force, need to repeatedly rush with clear water
Wash and could clean, and tea cake powder detergent only rinses can clean with a clear water.By the present embodiment tea cake powder detergent and Korea Spro
State's " long green elegant hands " Punica granatum L. vinegar detergent compares, and its 2g is equal to this Korea S's detergent of dishwashing detergent effect and 2mL, and clear water floats
The time of washing is about 5 seconds, and this product is natural product, not residual.By the present embodiment tea cake powder and sale on existing network
Camellia oleosa seed powder cleaning product compares, and the foaming characteristic of the present embodiment tea cake powder, emulsibility and oil stain eluting power are significantly superior to
Existing camellia oleosa seed powder product.
Meanwhile, the present embodiment gained crude oil color is shallower, reaches camellia seed oil national standard after conventional refinery
(GB11765-2003)。
Embodiment 3
S1. after clearing up remove impurity, Semen Camelliae or tea-seed are dried through 3 times at a temperature of 75 DEG C, make moisture content content control
It is made as 7%；
S2. use stranding to tear-shear the mode of peeling off to peel off and make Kernel-hull separation, control rate of hull in kernel 6%；Described stranding tears-
Shearing is peeled off to use and is produced YTTK.100 type decorticator by Scientia Agricultura Sinica academy Wuhan oil crop institute, also
Other manufacturer production of this area, other models similar decorticator can be used.Camellia oleifera Abel is delivered to shell storehouse.
S3. adjust the moisture of the camellia seed kernel after shelling or tea-seed core by 7% being down to 4% (by camellia seed kernel or
Tea-seed core carries out steam heating in being placed in quality-adjusting device, discharge steam), temperature reach 50 DEG C under conditions of the single screw rod of feeding (as
KQZX.18 type, is produced by TianXing, city of Anlu Hubei grain and oil machinery equipment company limited, this machine compression ratio 17, machine breech pressure
25.5MPa) screw oil expeller, controls cake temperature less than 80 DEG C.At this particular range temperature and moisture condition, Yi Jiyuan
Material contained oil is divided and contains the reciprocal action of shell amount, makes possess the plasticity and elasticity matched with oil press pressure into squeezing material.Even
Continuous squeezing is fuel-displaced, go out cake, and crude oil delivers to refining procedure after precipitation filters.Semen Camelliae or tea-seed press cake residual oil content are 6%；
S4., tea cake is sent into turbine whirlwind micronizing unit, and (WFJ-60 type, by the limited public affairs of Jiangyin City's health and machine-building
Department produces), it is ground into and is tea cake detergent by the fine powder of 180 mesh sieves.
Product appearance is light coffee color fine powder, fatty 6%, and moisture 5%, crude fibre 8%.Active principals: crude protein
12%, tea saponin 10%.Fineness crosses 180 mesh sieves.Arsenic (in 1% solution in terms of As), mg/kg≤0.05 heavy metal is (in 1% solution
In terms of Pb), mg/kg≤1.
It is packed that the small packer can be measured through (automatically) by gained, irrigate, sealed is distributed into 50g and 100g.During use, cut
Opening in the packed hot water that tea cake cleanser is poured into 40～50 DEG C, stirring i.e. forms the emulsified suspension with soapy feeling, is used for
Dishwashing detergent.Compared with the present embodiment tea cake powder detergent washes essence alive with " vertical white " new Fructus Fortunellae Margaritae of board, its 2g is to dishwashing detergent effect
Essence of living is washed equal with 2mL.But when rinsing, owing to " vertical white " new Fructus Fortunellae Margaritae of board washes the adhesive force of essence of living by force, need to repeatedly rush with clear water
Wash and could clean, and tea cake powder detergent only rinses can clean with a clear water.By the present embodiment tea cake powder detergent and Korea Spro
State's " long green elegant hands " Punica granatum L. vinegar detergent compares, and its 2g is equal to this Korea S's detergent of dishwashing detergent effect and 2mL, and clear water floats
The time of washing is about 5 seconds, and this product is natural product, not residual.By the present embodiment tea cake powder and sale on existing network
Camellia oleosa seed powder cleaning product compares, and the foaming characteristic of the present embodiment tea cake powder, emulsibility and oil stain eluting power are significantly superior to
Existing camellia oleosa seed powder product.
Meanwhile, the present embodiment gained crude oil color is shallower, reaches camellia seed oil national standard after conventional refinery
(GB11765-2003)。
Comparative example 1
S1. Semen Camelliae or tea-seed raw material use screening installation cleaning remove impurity；
S2. Semen Camelliae or tea-seed use tea-seed (Semen Camelliae) dehydrator of band arrangements for speed regulation, and at 70 DEG C, circulation is dried
Dry, make the internal contained humidity of seed gradually diffuse to the surface, make material moisture content drop to 13%；
S3. dried Semen Camelliae or tea-seed use plane centrifugal impact decorticator to peel off, and are then hung down by adjustable
Straight suction channel, makes Renhe shell separate according to the floating velocity difference of Renhe shell, according to the different needs of tea cake, controls in core containing shell
Rate is 13%, by shell suction and conveying to shell storehouse；
S4. Semen Camelliae or tea-seed core use drying machine to make its moisture be down to 7%；
S5. Semen Camelliae or tea-seed core are at 70 DEG C, and moisture is fed directly into single screw rod for 7% time (such as KQZX.18 type, by Hubei
Tianxing Grain & Oil Machinery Equipment Co., Ltd., Anlu City produces, this machine compression ratio 17, machine breech pressure 25.5MPa) screw oil expeller,
Control cake temperature less than 90 DEG C.Squeezing is fuel-displaced continuously, and crude oil delivers to refining procedure after precipitation filters, and tea cake delivers to tea cake
Powder detergent manufacturing procedure.
Semen Camelliae or tea-seed squeezing residual oil content are 7%.
S4., tea cake is sent into turbine whirlwind micronizing unit, and (WFJ-60 type, by the limited public affairs of Jiangyin City's health and machine-building
Department produces), it is ground into the fine powder by 180 mesh sieves and is i.e. obtained tea cake detergent.
Product appearance is dark brown fine powder, fatty 9%, and moisture 8%, crude fibre 13%.Active principals: crude protein
8%, tea saponin 7%.Fineness crosses 180 mesh sieves.Heavy metal: arsenic (in 1% solution in terms of As), mg/kg=0.10, lead (1% solution
In in terms of Pb), mg/kg=1.5 or higher.The small packer subpackage that gained tea cake powder can be measured through (automatically), irrigates, seals
Become 50g and 100g packed.During use, cutting off in the packed hot water that tea cake detergent is poured into 40～50 DEG C, stirring, for tableware
Washing.Compared with the present embodiment tea cake powder detergent example arbitrary with embodiment 1 to 3 tea cake powder detergent, feel is coarse, and bubble is not
And embodiment 1 to 3 arbitrary example gained detergent, compared with the present embodiment tea cake powder detergent washes essence alive with " vertical white " new Fructus Fortunellae Margaritae of board
Relatively, dishwashing detergent effect is washed alive smart equal by its 2.5g with 2mL.Foaming characteristic, emulsibility and the oil stain of the present embodiment tea cake powder are washed
De-ability is all inferior to the tea cake powder detergent of embodiment 1 to 3 gained.
Comparative example 2
S1. Semen Camelliae or tea-seed raw material use screening installation cleaning remove impurity；
S2. Semen Camelliae or tea-seed use tea-seed (Semen Camelliae) dehydrator of band arrangements for speed regulation, and at 80 DEG C, circulation is dried
Dry, make the internal contained humidity of seed gradually diffuse to the surface, make material moisture content drop to 10%；
S3. dried Semen Camelliae or tea-seed use stranding to tear-shear Fructus Camelliae sinensis decorticator (such as YTTK.100 type, by China's agriculture
Industry research institute Wuhan oil crop institute produces) Semen Camelliae or tea-seed to be peeled off, rate of hull in kernel is 15%,
Shell is delivered to shell storehouse；
S4. Semen Camelliae or tea-seed core use drying machine to make its moisture be down to 7%；
S5. Semen Camelliae or tea-seed core are at 80 DEG C, and moisture is fed directly into single screw rod for 7% time (such as KQZX.18 type, by Hubei
Tianxing Grain & Oil Machinery Equipment Co., Ltd., Anlu City produces, this machine compression ratio 17, machine breech pressure 25.5MPa) screw oil expeller,
Control cake temperature less than 90 DEG C.Squeezing is fuel-displaced continuously, and crude oil delivers to refining procedure after precipitation filters, and tea cake delivers to tea cake
Powder detergent manufacturing procedure.
Semen Camelliae or tea-seed squeezing residual oil content are 7%.
S4., tea cake is sent into turbine whirlwind micronizing unit, and (WFJ-60 type, by the limited public affairs of Jiangyin City's health and machine-building
Department produces), it is ground into the fine powder by 180 mesh sieves and is i.e. obtained tea cake detergent.
Product appearance is dark brown fine powder, fatty 8%, and moisture 9%, crude fibre 15%.Active principals: crude protein
7%, tea saponin 8%.Fineness crosses 180 mesh sieves.Heavy metal: arsenic (in 1% solution in terms of As), mg/kg=0.10, lead (1% solution
In in terms of Pb), mg/kg=1.5 or higher.The small packer subpackage that gained tea cake powder can be measured through (automatically), irrigates, seals
Become 50g and 100g packed.During use, cutting off in the packed hot water that tea cake cleanser is poured into 40～50 DEG C, stirring, for tableware
Washing.Compared with the present embodiment tea cake powder detergent example arbitrary with embodiment 1 to 3 tea cake powder detergent, feel is coarse, and bubble is not
And embodiment 1 to 3 arbitrary example gained detergent, compared with the present embodiment tea cake powder detergent washes essence alive with " vertical white " new Fructus Fortunellae Margaritae of board
Relatively, dishwashing detergent effect is washed alive smart equal by its 2.5g with 2mL.Foaming characteristic, emulsibility and the oil stain of the present embodiment tea cake powder are washed
De-ability is all inferior to the tea cake powder detergent of embodiment 1 to 3 gained.
Comparative example 3
Other are with comparative example 2, and except for the difference that the present embodiment enters to squeeze temperature is 90 DEG C, and going out cake temperature is 110 DEG C.
Product appearance is dark brown extremely shallow brown fine powder, fatty 8%, and moisture 8%, crude fibre 13%.Active principals:
Crude protein 8%, tea saponin 7%.Fineness crosses 180 mesh sieves.Heavy metal: arsenic (in 1% solution in terms of As), mg/kg=0.10, lead
(in 1% solution in terms of Pb), mg/kg=1.5 or higher.The parcel that gained tea cake powder can be measured through (automatically), irrigates, seals
It is packed that installation is distributed into 50g and 100g.During use, cut off in the packed hot water that tea cake cleanser is poured into 40～50 DEG C, stirring,
For dishwashing detergent.Compared with the present embodiment tea cake powder detergent example arbitrary with embodiment 1 to 3 tea cake powder detergent, feel is thick
Rough, bubble is washed with " vertical white " new Fructus Fortunellae Margaritae of board not as good as embodiment 1 to 3 arbitrary example gained detergent, the present embodiment tea cake powder detergent
Essence of living compares, and dishwashing detergent effect is washed alive smart equal by its 2.5g with 2mL.The foaming characteristic of the present embodiment tea cake powder, emulsibility
With the tea cake powder detergent that oil stain eluting power is all inferior to embodiment 1 to 3 gained.This comparative example and comparative example 1 and comparative example 2 phase
Relatively, the foaming characteristic of tea cake powder, emulsibility and oil stain eluting power are more weaker, and clean result is not as good as comparative example 1 and contrast
Example 2.
Claims (10)
1. the preparation method of a high active ingredient tea cake powder detergent, it is characterised in that comprise the following steps:
S1. after general clears up remove impurity, Semen Camelliae or tea-seed are through repeated drying at a temperature of 70～80 DEG C, make Semen Camelliae or tea
It is 7%～8% that the moisture of leaf seed controls；
S2. use stranding to tear-shear the mode of peeling off to peel off and make Kernel-hull separation, control rate of hull in kernel 5%～8%；
S3. the moisture adjusting the camellia seed kernel after shelling or tea-seed core is down to 4%～5%, in temperature by 7%～8%
Under conditions of not higher than 60 DEG C, it is fed directly into twin screw or single screw spiral oil press squeezing is fuel-displaced, control cake temperature the highest
In 90 DEG C；Obtain squeezing fuel-displaced after tea cake；
S4. tea cake is pulverized, take and i.e. obtain tea cake detergent by the fine powder of 150～200 mesh sieves.
The preparation method of high active ingredient tea cake powder detergent the most according to claim 1, it is characterised in that described in step S1
The number of times dried is 2～3 times.
The preparation method of high active ingredient tea cake powder detergent the most according to claim 1, it is characterised in that described in step S1
Drying is to dry 40～60 minutes every time.
The preparation method of high active ingredient tea cake powder detergent the most according to claim 1, it is characterised in that described in step S3
The residual oil content of tea cake is 5%～6%.
The preparation method of high active ingredient tea cake powder detergent the most according to claim 1, it is characterised in that described in step S3
The compression ratio of single-screw oil press is 17, and machine breech pressure is 25.5MPa.
The preparation method of high active ingredient tea cake powder detergent the most according to claim 1, it is characterised in that described in step S3
The compression ratio of twin-screw press is 17.3, and machine breech pressure is 23.5MPa.
The preparation method of high active ingredient tea cake powder detergent the most according to claim 1, it is characterised in that described in step S4
Pulverizing is to use turbine whirlwind type micronizing unit.
8. tea cake powder detergent obtained by preparation method described in any one of claim 1 to 7.
Tea cake powder detergent the most according to claim 8, it is characterised in that the outward appearance of described tea cake powder detergent is shallow coffee
Coffee color fine powder, fatty 5%～6%, moisture 4%～5%, crude fibre 5%～8%；In Active principals, crude protein 12%～
15%, tea saponin 10%～15%；Fineness crosses 150～200 mesh sieves；Heavy metal is with in 1% solution in terms of As, mg/kg≤
0.05, in 1% solution in terms of Pb, mg/kg≤1.
The using method of tea cake powder detergent the most according to claim 8 or claim 9, it is characterised in that by appropriate described tea
Cake detergent is poured in the hot water of 40～50 DEG C, and stirring i.e. forms the emulsified suspension with soapy feeling, is used for washing tableware.
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| CN108486715A (en) * | 2018-05-03 | 2018-09-04 | 广东护康宝农林生物科技有限公司 | A kind of Tea Saponin washes clean bag and its application method |
| CN111019756A (en) * | 2019-12-20 | 2020-04-17 | 仲恺农业工程学院 | Industrial production and processing method of camellia seeds |
| CN113621017A (en) * | 2021-08-25 | 2021-11-09 | 青岛职业技术学院 | Comprehensive utilization method of camellia seed meal |
| CN113881520A (en) * | 2021-09-29 | 2022-01-04 | 贵州省林业科学研究院 | Processing method of green and efficient camellia oleifera washing powder |
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| CN105219517A (en) * | 2015-09-25 | 2016-01-06 | 潜山县经汇农业综合发展有限公司 | A kind of organic tea oil production technique |
| CN105670815A (en) * | 2016-01-13 | 2016-06-15 | 浙江农林大学 | Camellia seed cleaning powder and preparation technology thereof |
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| CN103409225A (en) * | 2013-07-29 | 2013-11-27 | 中国林业科学研究院亚热带林业研究所 | Processing method for camellia seed oil with aromatic flavor and nutrition |
| CN105219517A (en) * | 2015-09-25 | 2016-01-06 | 潜山县经汇农业综合发展有限公司 | A kind of organic tea oil production technique |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108486715A (en) * | 2018-05-03 | 2018-09-04 | 广东护康宝农林生物科技有限公司 | A kind of Tea Saponin washes clean bag and its application method |
| CN108486715B (en) * | 2018-05-03 | 2019-04-26 | 广东护康宝农林生物科技有限公司 | A kind of Tea Saponin washes clean bag and its application method |
| CN111019756A (en) * | 2019-12-20 | 2020-04-17 | 仲恺农业工程学院 | Industrial production and processing method of camellia seeds |
| CN113621017A (en) * | 2021-08-25 | 2021-11-09 | 青岛职业技术学院 | Comprehensive utilization method of camellia seed meal |
| CN113881520A (en) * | 2021-09-29 | 2022-01-04 | 贵州省林业科学研究院 | Processing method of green and efficient camellia oleifera washing powder |
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