CN107266935A - A kind of dyestuff, dye composite and dye material composition - Google Patents
A kind of dyestuff, dye composite and dye material composition Download PDFInfo
- Publication number
- CN107266935A CN107266935A CN201710509422.5A CN201710509422A CN107266935A CN 107266935 A CN107266935 A CN 107266935A CN 201710509422 A CN201710509422 A CN 201710509422A CN 107266935 A CN107266935 A CN 107266935A
- Authority
- CN
- China
- Prior art keywords
- dye
- monomer
- composite
- material composition
- dyestuff
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000975 dye Substances 0.000 title claims abstract description 97
- 239000002131 composite material Substances 0.000 title claims abstract description 26
- 239000000203 mixture Substances 0.000 title claims abstract description 23
- 239000000463 material Substances 0.000 title claims abstract description 22
- 239000000178 monomer Substances 0.000 claims abstract description 43
- 239000012752 auxiliary agent Substances 0.000 claims description 15
- 238000002156 mixing Methods 0.000 claims description 11
- 241000288027 Chrysolophus pictus Species 0.000 claims description 10
- 108091060290 Chromatid Proteins 0.000 claims description 9
- 210000004756 chromatid Anatomy 0.000 claims description 9
- 239000000843 powder Substances 0.000 claims description 4
- 239000002270 dispersing agent Substances 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 239000000243 solution Substances 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 230000002708 enhancing effect Effects 0.000 abstract description 8
- 230000000052 comparative effect Effects 0.000 description 6
- 239000004744 fabric Substances 0.000 description 5
- 238000004043 dyeing Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 239000000985 reactive dye Substances 0.000 description 4
- QOSTVEDABRQTSU-UHFFFAOYSA-N 1,4-bis(methylamino)anthracene-9,10-dione Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C(NC)=CC=C2NC QOSTVEDABRQTSU-UHFFFAOYSA-N 0.000 description 3
- 241000083869 Polyommatus dorylas Species 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 2
- 229920000297 Rayon Polymers 0.000 description 2
- 239000001045 blue dye Substances 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000007405 data analysis Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000009725 powder blending Methods 0.000 description 2
- YXZRCLVVNRLPTP-UHFFFAOYSA-J turquoise blue Chemical compound [Na+].[Na+].[Na+].[Na+].[Cu+2].NC1=NC(Cl)=NC(NC=2C=C(NS(=O)(=O)C3=CC=4C(=C5NC=4NC=4[N-]C(=C6C=CC(=CC6=4)S([O-])(=O)=O)NC=4NC(=C6C=C(C=CC6=4)S([O-])(=O)=O)NC=4[N-]C(=C6C=CC(=CC6=4)S([O-])(=O)=O)N5)C=C3)C(=CC=2)S([O-])(=O)=O)=N1 YXZRCLVVNRLPTP-UHFFFAOYSA-J 0.000 description 2
- YIWGJFPJRAEKMK-UHFFFAOYSA-N 1-(2H-benzotriazol-5-yl)-3-methyl-8-[2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carbonyl]-1,3,8-triazaspiro[4.5]decane-2,4-dione Chemical compound CN1C(=O)N(c2ccc3n[nH]nc3c2)C2(CCN(CC2)C(=O)c2cnc(NCc3cccc(OC(F)(F)F)c3)nc2)C1=O YIWGJFPJRAEKMK-UHFFFAOYSA-N 0.000 description 1
- 229920003043 Cellulose fiber Polymers 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- -1 it includes Substances 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 239000010981 turquoise Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0034—Mixtures of two or more pigments or dyes of the same type
- C09B67/0035—Mixtures of phthalocyanines
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/004—Mixtures of two or more reactive dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0092—Dyes in solid form
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of dyestuff, dye composite and dye material composition.The invention provides a kind of dye material composition, it includes, the dye monomer A as shown in formula (1), the dye monomer B as shown in formula (2), wherein, a+b=3.5；X+Y+Z=3.5~4.0；Described dye monomer A and described dye monomer B, 1.1 are calculated as with parts by weight:1~8.7:1.The invention also discloses a kind of dye composite containing the dye material composition, the dyestuff that the dye composite is prepared, with higher enhancing, excellent color fastness, high performance-price ratio.
Description
Technical field
The present invention relates to a kind of dyestuff, dye composite and dye material composition.
Background technology
With the increasingly raising of living standard, requirement of the people to textile product also more and more higher, thereby using in weaving
Requirement of the reactive dye of product dyeing on properties is increasingly harsh.Reactive dye not only will have excellent dyefastness and
Dyeability, and to meet environmental requirement.
The dye monomer of bright blue kind, is generally used for the stamp of cellulose fibre in the market, and enhancing is inadequate, often
More than 30g/kg consumptions, with the increase of dye strength, stamp cloth cover depth can not but increase therewith, reach saturation depth,
Therefore some deeper turquoise blues can not accomplish；Or predominantly normal dyeing is used, depth is splendid during for stamp, but coloured light
Greener dark, every fastness has been short of.
The content of the invention
The present invention is in order to overcome bright blue dye printing enhancing in the prior art and the defect such as fastness ability is not good, so as to carry
A kind of dyestuff, dye composite and dye material composition are supplied.The dye composite of the present invention, using compounded technology, compounding
Reactive turquoise blue dye product out, is used on stamp, there is excellent enhancing, and each side fastness is excellent, with more apparent
Advantage.
The invention provides a kind of dye material composition, it includes, and the dye monomer A as shown in formula (1) is (bright blue
14#)：
Dye monomer B (bright blue 21#) as shown in formula (2)：
Wherein, a+b=3.5；X+Y+Z=3.5~4.0；
Described dye monomer A and described dye monomer B, 1.1 are calculated as with parts by weight:1~8.7:1.
Described dye material composition can be made up of described dye monomer A with described dye monomer B.
Described dye monomer A and described dye monomer B, is preferably calculated as 1.4 with parts by weight:1~5:1.
Wherein, the dye monomer A and dye monomer B can independently of one another preferably with powdery, synthetic solvent or
Its aqueous solution form is present.
(the bright blue K-GL of golden pheasant (Jiangsu golden pheasant industry) or the bright blue K- of good enlightening may be selected in bright blue 14) to described dye monomer A
GL (praises Dihua work in Shaoxing), the preferably bright blue K-GL of golden pheasant.
(the bright blue KN-G of golden pheasant (Jiangsu golden pheasant industry) or the bright blue G of good enlightening may be selected in bright blue 21) to described dye monomer B
266% (praising Dihua work in Shaoxing), the preferably bright blue KN-G of golden pheasant.
As needed, the component form that dye material composition of the present invention can mix for all the components, also may be used
Independently or by each composition it is divided into some groups of many component nested forms for each composition.
Present invention also offers a kind of dye composite, it includes, dye material composition and auxiliary agent as described above.
Described dye composite can by described dye monomer A, described dye monomer B is constituted and auxiliary agent is constituted.
The auxiliary agent can be the conventional auxiliary agent of this area, such as Dispersant MF and/or dispersing agent NNO.
The auxiliary agent exists preferably in the form of powder and/or solution.The auxiliary agent can use commercially available prod.
In described dye composite, it may include following components by percentage to the quality：For example, described chromatid
A is 87%, 80%, 75%, 70%, 65%, 60%, 55% or 50%；Described chromatid B be 10%, 16%, 20%,
25%th, 32%, 36%, 40% or 45%.
Described dye composite is preferably comprised following components by percentage to the quality：Dye described in 50%~87%
Chromophoric monomer A, the chromatid B described in 10%~45%, the auxiliary agent described in 3~5%；More preferably, described dye composite bag
Include following components by percentage to the quality：Chromatid A described in 65%~80%, the chromatid described in 16%~32%
B, the auxiliary agent described in 3~5%.
As needed, the component form that dye composite of the present invention can mix for all the components, or respectively
Composition is independent or each composition is divided into some groups of many component nested forms.
The present invention's additionally provides a kind of dyestuff, and it is mixed with by the dye composite and obtained.Described mixing can
This area conventional mixing method is used, ratio mechanically mixed dye monomer A, dye monomer B and auxiliary agent, or with ability such as needed for
Mode known to domain carries out blending；More preferably, described dye composite is spray-dried again using liquid slurry blending, or
The mode of monomer powders blending is prepared；The liquid slurry blending time is 3 hours；At present mouth material is returned the powder blending
Material suitable for reading 3 times, total incorporation time 3 hours.
Present invention also offers the dyestuff cellulosic material dyeing in application, the preferred cotton of cellulosic material,
Fiber crops or viscose fiber, more preferably viscose fiber.
Without prejudice to the field on the basis of common sense, above-mentioned each optimum condition, can be combined, and produce the present invention each preferably
Example.
Dye monomer A and dye monomer B can use commercially available prod, it would however also be possible to employ method system well known in the art
It is standby.
The positive effect of the present invention is：The invention provides a kind of dye material composition and containing the dye material
The dye composite of composition, the dyestuff that the dye composite is prepared has excellent dyefastness and dyeability, and
It is highly suitable for the dyeing of cellulosic material, with excellent enhancing, excellent every color fastness, thick in color.
Brief description of the drawings
Fig. 1 is enhancing curve comparison.
Embodiment
The present invention is further illustrated below by the mode of embodiment, but does not therefore limit the present invention to described reality
Apply among a scope.The experimental method of unreceipted actual conditions in the following example, conventionally and condition, or according to business
Product specification is selected.
Embodiment 1~8 and comparative example 1~9
(bright blue 14) are the bright blue K-GL of golden pheasant to dye monomer A；(bright blue 21) are the bright blue KN-G of golden pheasant to dye monomer B.
Dye monomer A, dye monomer B can be prepared using method well known in the art, the compound being known in the art.
Embodiment 1-8 and comparative example 1~9 use monomer dry powder blending, using the taper blending device that dye industry is common,
Blending 3 hours, once, totally 3 times, abundant blending is uniform for feed back per hour, no more than 2% be with Sampling Intensity difference up and down up to
Mark.
Table 1
Turquoise reactive dyestuffs made from above-described embodiment are subjected to stamp test using the printing with reactive dye method of standard
(measure of GB/T2388-2003 chemically-reactive dyes stamp coloured light and intensity), obtains its corresponding performance data, is shown in Table 2.
Table 2 (stamp depth 30g/kg, pure cotton plain cloth)
Reactive turquoise blue dyestuff effect detection uses standard for wear resistance made from above-described embodiment：ISO 105X12；It is resistance to
Perspiration fastness：ISO 105 E04；Soaping fastness：ISO 105 C03.
Data analysis is detected by the embodiment 1-8 of table 2, the compound bright blue dyestuff that the present invention is obtained can be according to market need
Ask, proportioning is adjusted according to different form and aspect and depth, every fastness can reach standard requirement.
Data analysis is detected by the comparative example 1-9 of table 2, when component B ratios are higher than component A, fastness can decline；When
When being compounded using bright blue 72# and bright blue 25# combination, fastness is not as the effect of component A and component B compoundings.
Stamp enhancing contrast is carried out by embodiment 3 and comparative example 1 and comparative example 2,10/20/30/40/50/ is printed respectively
60/70/80g/kg cloth specimens, with embodiment 3, stamp depth 80g/kg cloth specimen is surveyed using colour photometer respectively as reference depth
Other cloth specimen depth are tried, and draw following enhancing curve comparison Fig. 1.It will be seen from figure 1 that embodiment 3 is carried compared to comparative example 2
The rate of liter is substantially high.
Claims (10)
1. a kind of dye material composition, it is characterised in that including the dye monomer A as shown in formula (1)：
Dye monomer B as shown in formula (2)：
Wherein, a+b=3.5；X+Y+Z=3.5~4.0；
Described dye monomer A and described dye monomer B, 1.1 are calculated as with parts by weight:1~8.7:1.
2. dye material composition as claimed in claim 1, it is characterised in that it is bright blue that described dye monomer A is selected from golden pheasant
The bright blue K-GL of K-GL or good enlightening；Described dye monomer B is selected from the bright blue G 266% of golden pheasant bright blue KN-G or good enlightening.
3. dye material composition as claimed in claim 1 or 2, it is characterised in that the dye monomer A and described dyestuff
Monomer B is each independent to be existed with powdery, synthetic solvent or its aqueous solution form；
And/or, described dye monomer A and described dye monomer B is calculated as 1.4 with parts by weight:1~5:1.
4. a kind of dye composite, it is characterised in that including the dye material composition as described in any one of claims 1 to 3
And auxiliary agent.
5. dye composite as claimed in claim 4, it is characterised in that the auxiliary agent is Dispersant MF and/or diffusant
NNO。
6. dye composite as claimed in claim 4, it is characterised in that the auxiliary agent is deposited in the form of powder and/or solution
.
7. dye composite as claimed in claim 4, it is characterised in that described dye composite includes following with quality hundred
Divide the component than meter：Chromatid A described in 50%~87%, the chromatid B described in 10%~45%, described in 3~5%
Auxiliary agent.
8. dye composite as claimed in claim 7, it is characterised in that described dye composite includes following with quality hundred
Divide the component than meter：Chromatid A described in 65%~80%, the chromatid B described in 16%~32%, described in 3~5%
Auxiliary agent.
9. a kind of dyestuff, it is characterised in that will be mixed with and obtained by any one of claim 4~8 dye composite.
10. dyestuff as claimed in claim 9, it is characterised in that described to be mixed into described dye monomer A, described
Dye monomer B and described auxiliary agent are spray-dried again using liquid slurry blending, or monomer powders blending.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710509422.5A CN107266935B (en) | 2017-06-28 | 2017-06-28 | A kind of dyestuff, dye composite and dye material composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710509422.5A CN107266935B (en) | 2017-06-28 | 2017-06-28 | A kind of dyestuff, dye composite and dye material composition |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107266935A true CN107266935A (en) | 2017-10-20 |
| CN107266935B CN107266935B (en) | 2019-04-12 |
Family
ID=60071047
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710509422.5A Expired - Fee Related CN107266935B (en) | 2017-06-28 | 2017-06-28 | A kind of dyestuff, dye composite and dye material composition |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107266935B (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002097393A (en) * | 2000-09-26 | 2002-04-02 | Mitsubishi Chemicals Corp | Ink set for ink jet recording and method for ink jet recording |
| CN1444634A (en) * | 2000-07-26 | 2003-09-24 | 日本化药株式会社 | Cyan dye mixture, water-based cyan ink composition and method of ink-jet recording |
| CN1445297A (en) * | 2003-04-10 | 2003-10-01 | 孙德锁 | Complex reactive turquoise blue dye |
| CN1810891A (en) * | 2005-01-25 | 2006-08-02 | 京仁洋行 | Novel reactive dye composition with three-color combination |
| CN104478887A (en) * | 2014-12-11 | 2015-04-01 | 吴江桃源染料有限公司 | Reactive turquoise blue dye semifinished product, and preparation method and application thereof |
| CN106049105A (en) * | 2016-06-08 | 2016-10-26 | 山东黄河三角洲纺织科技研究院有限公司 | Method of improving printing dye uniformity of active jade blue |
-
2017
- 2017-06-28 CN CN201710509422.5A patent/CN107266935B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1444634A (en) * | 2000-07-26 | 2003-09-24 | 日本化药株式会社 | Cyan dye mixture, water-based cyan ink composition and method of ink-jet recording |
| JP2002097393A (en) * | 2000-09-26 | 2002-04-02 | Mitsubishi Chemicals Corp | Ink set for ink jet recording and method for ink jet recording |
| CN1445297A (en) * | 2003-04-10 | 2003-10-01 | 孙德锁 | Complex reactive turquoise blue dye |
| CN1810891A (en) * | 2005-01-25 | 2006-08-02 | 京仁洋行 | Novel reactive dye composition with three-color combination |
| CN104478887A (en) * | 2014-12-11 | 2015-04-01 | 吴江桃源染料有限公司 | Reactive turquoise blue dye semifinished product, and preparation method and application thereof |
| CN106049105A (en) * | 2016-06-08 | 2016-10-26 | 山东黄河三角洲纺织科技研究院有限公司 | Method of improving printing dye uniformity of active jade blue |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107266935B (en) | 2019-04-12 |
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Effective date of registration: 20190809 Address after: 201703 Shanghai city Qingpu District Songhua Road No. 881 Co-patentee after: YANTAI ANOKY FINE CHEMICALS Co.,Ltd. Patentee after: SHANGHAI ANOKY GROUP Co.,Ltd. Co-patentee after: SHANGHAI ANOKY DIGITAL TECHNOLOGY Co.,Ltd. Co-patentee after: DONGYING ANOKY TEXTILE MATERIALS Co.,Ltd. Co-patentee after: SHANGHAI SHANGHU DIGITAL TECHNOLOGY Co.,Ltd. Co-patentee after: Yantai Shangyu Digital Technology Co.,Ltd. Address before: 224631 North of Weiliu Road, Chenjiagang Town, Xiangshui County, Yancheng City, Jiangsu Province Co-patentee before: SHANGHAI ANOKY GROUP Co.,Ltd. Patentee before: JIANGSU ANOKY CHEMICALS Co.,Ltd. Co-patentee before: SHANGHAI ANOKY DIGITAL TECHNOLOGY Co.,Ltd. Co-patentee before: YANTAI ANOKY FINE CHEMICALS Co.,Ltd. Co-patentee before: DONGYING ANOKY TEXTILE MATERIALS Co.,Ltd. |
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Effective date of registration: 20201228 Address after: 265601 Hairun Road, BEIGOU Town, Penglai District, Yantai City, Shandong Province Patentee after: YANTAI ANOKY FINE CHEMICALS Co.,Ltd. Patentee after: SHANGHAI ANOKY GROUP Co.,Ltd. Patentee after: SHANGHAI ANOKY DIGITAL TECHNOLOGY Co.,Ltd. Patentee after: DONGYING ANOKY TEXTILE MATERIALS Co.,Ltd. Patentee after: SHANGHAI SHANGHU DIGITAL TECHNOLOGY Co.,Ltd. Patentee after: Yantai Shangyu Digital Technology Co.,Ltd. Patentee after: Shandong annuoqi Fine Chemical Co.,Ltd. Address before: No. 881, Songhua Road, Qingpu District, Shanghai City, Shanghai Patentee before: SHANGHAI ANOKY GROUP Co.,Ltd. Patentee before: YANTAI ANOKY FINE CHEMICALS Co.,Ltd. Patentee before: SHANGHAI ANOKY DIGITAL TECHNOLOGY Co.,Ltd. Patentee before: DONGYING ANOKY TEXTILE MATERIALS Co.,Ltd. Patentee before: SHANGHAI SHANGHU DIGITAL TECHNOLOGY Co.,Ltd. Patentee before: Yantai Shangyu Digital Technology Co.,Ltd. |
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Granted publication date: 20190412 |
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