CN107260586A - A kind of makeup removing breast gel and preparation method thereof - Google Patents
A kind of makeup removing breast gel and preparation method thereof Download PDFInfo
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- CN107260586A CN107260586A CN201710504241.3A CN201710504241A CN107260586A CN 107260586 A CN107260586 A CN 107260586A CN 201710504241 A CN201710504241 A CN 201710504241A CN 107260586 A CN107260586 A CN 107260586A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
Abstract
A kind of makeup removing breast gel, is made up of following component：The caprylic/capric glyceryl esters of PEG 6,4.0~8.0 parts by weight；Water-soluble olive oil, 0.8~1.0 parts by weight；The copolymers of PEG/PPG 25/30,0.1~0.5 parts by weight；Polyol complex, 3.0~8.0 parts by weight；Saualane, 0.3~1.0 parts by weight and the parts by weight of acrylic resin 0.15~0.5；Water, 80~88 parts by weight.Its preparation method is：By the caprylic/capric glyceryl esters of PEG 6, water-soluble olive oil and the copolymers of PEG/PPG 25/30 formation ternary detersive micro-capsule cladding, microemulsion is then prepared with saualane, then uses acrylic resin stabilising system, translucent makeup removing breast gel is formed.Makeup removing gel makeup removing ability is strong, safe, small to eye irritation, easily rinses, and with rear moisturizing, moistens non-greasy.
Description
Technical field
The present invention relates to a kind of makeup removal products and preparation method thereof, belong to cosmetics color make-up technical field.
Background technology
Current makeup removal products are roughly divided into the makeup remover removed ornaments and formal dress by grease, the makeup remover removed ornaments and formal dress by surfactant
(makeup removing jelly), multilayer make up remover, makeup removing breast or the make-up remover removed ornaments and formal dress by oil and water etc..In makeup removing ability, washability side
Face, each formulation makeup removal products have his own strong points, and also respectively have deficiency.Makeup remover, make-up remover are rapid molten by the principle of " with oily molten oil "
Color make-up is solved, by wiping removal color make-up, needs the color make-up makeup removing effect for soaking again removal poor mascara etc., moreover, pigment
Diffusion causes pigment redeposited, and the excessive washability of grease is poor, easily causes clogging of pores.Make up remover, makeup-removing wet tissue, pass through " performance
Activating agent decontamination " principle, removal color make-up and facial spot, such product are similar to dairy products of washing one's face, and exist and unload decapacitation to heavy make-up
The problem of power is weak, toner floats the poor, skin irritation of support property and big eye irritation.Makeup removing breast (frost), mainly by " former with the molten oil of oil
Reason ", using the polarity grease of good dispersion, by oil-in-water (O/W) or Water-In-Oil (W/O) formation emulsified body, this kind of product is fitted
Face makeup removing is closed, is not suitable for eye makeup removing, because the type product emulsified particles is relatively stablized, it is impossible to rapid water oil separation,
And have impact on oil, water and directly act on color make-up, spot, it have impact on makeup removing effect.Meanwhile, there is also the problems such as washability difference.
Raw material generally selected by makeup removing class product mainly has grease type, water-soluble grease class, surfactant-based, solvent
Class etc., wherein, water-soluble grease has water-soluble plant oil and water-soluble Synthetic Oil, and water-soluble plant oil is relatively mild, such as water
Dissolubility olive oil, water-soluble babassu oil etc., are all that vegetable fat is carried out into PEGylation water solubility processing, improve grease in water
In dissolubility, but makeup removing ability.The caprylic/capric glyceryl ester commonly used in class product of removing ornaments and formal dress is subjected to PEGylation water-soluble
Processing, makeup removing ability performance is excellent, but excitant is larger.
Because makeup removal products using position are generally eye, lip, therefore it is required that makeup removal products have good makeup removing ability, and
And it is gentle non-stimulated.
The content of the invention
In view of the shortcomings of the prior art, the present invention provides a kind of makeup removing breast gel, and it has stronger makeup removing ability, simultaneously
Moisture retention is good, gentle non-stimulated.
To achieve the above object, the present invention includes following technical scheme：
A kind of makeup removing breast gel, it is made up of following raw material：PEG-6 caprylic/capric glyceryl esters, 4.0~8.0 weight
Part；Water-soluble olive oil, 0.8~1.0 parts by weight；PEG/PPG-25/30 copolymers, 0.1~0.5 parts by weight；Polyalcohol is compounded
Thing, 3.0~8.0 parts by weight；Saualane, 0.3~1.0 parts by weight；The parts by weight of acrylic resin 0.15~0.5 and the weight of water 80~88
Measure part.
Makeup removing breast gel as described above, it is preferable that the polyol complex is glycerine, dipropylene glycol, 1,3- fourths two
Alcohol, according to (5~6): (2~4): the weight of (0.8~1.2) is than composition.
Makeup removing breast gel as described above, it is preferable that the polyol complex is glycerine, dipropylene glycol, 1,3- fourths two
Alcohol, according to 6: 3: 1 weight than constituting.
Makeup removing breast gel as described above, it is preferable that the PEG-6 caprylic/caprics glyceryl ester, 4 parts by weight；It is water-soluble
Olive oil, 0.8 parts by weight；PEG/PPG-25/30 copolymers, 0.2 parts by weight；Polyol complex, 3.75 parts by weight；Spiny dogfish
Alkane, 0.31 parts by weight and the parts by weight of acrylic resin 0.25；Water, 85.0 parts by weight.
Makeup removing breast gel as described above, it is preferable that the moisturizing eye shadow also includes auxiliary material, auxiliary material is spices and anti-corrosion
Agent.
On the other hand, the present invention provides the preparation method of makeup removing breast gel as described above, and this method comprises the following steps：
Step I：PEG-6 caprylic/caprics glyceryl ester, water-soluble olive oil are mixed with PEG/PPG-25/30 copolymers
Ternary detersive micro-capsule cladding is made in heating；
Step II：By water, polyol complex and ternary detersive micro-capsule cladding Hybrid Heating, saualane is then added,
Interval homogeneous is carried out to system and fades to the semi-transparent state of micro emulsion to system from emulsus, microemulsion is obtained；Wherein, water is compounded with polyalcohol
The weight ratio of thing is 60: (3.0~8.0)；
Step III：Acrylic resin (0.15~0.5 parts by weight) is pre-dispersed in water (40.0~45.0 parts by weight),
The microemulsion that step II is obtained is added in acrylic resin aqueous dispersions, is subsequently added KOH solution to pH5.5~7.0, is obtained
Translucent makeup removing breast gel.
Preparation method as described above, it is preferable that the step I is：
A. PEG-6 caprylic/caprics glyceryl ester, water-soluble olive oil and PEG/PPG-25/30 copolymers are added and sterilized
In vacuum reaction kettle, stirring is heated to 80-85 DEG C, is incubated 15~20min；
B. 70-75 DEG C is cooled to, is evacuated to more than -0.08Mpa, stirs 15-20min, to micelle forma-tion, feed liquid is transparent
It is limpid, form homogeneous phase body；
C. 45 DEG C are cooled to bottom discharge, ternary detersive micro-capsule cladding is obtained.
Preparation method as described above, it is preferable that the step II is：Water, polyol complex and ternary detersive is micro-
Capsule cladding is mixed and heated to 70~80 DEG C, then adds saualane, to system carry out 8~15min of interval homogeneous to system from
Emulsus fades to the semi-transparent state of micro emulsion, obtains microemulsion；
Another aspect, the present invention provides a kind of makeup removing breast gel, and it is prepared using method as described above.
Present invention application is " with oily molten oil ", " surfactant detersive ", the principle such as " polyalcohol wetting " raising makeup removal products
Comprehensive makeup removing effect.Its advantage is embodied in the following aspects：
1. contain in makeup removing breast gel by PEG-6 caprylic/caprics glyceryl ester, water-soluble olive oil and PEG/PPG-25/
The ternary detersive micro-capsule cladding of 30 copolymers formation, these three materials mutually form micella in micro-capsule cladding, and PEG-6 is pungent
Acid/capric acid glyceryl ester, water-soluble olive oil form interior phase, and PEG/PPG-25/30 copolymers are foreign minister, reduce PEG-6 pungent
Stimulation of the acid/capric acid glyceryl ester directly to skin and eye mucosa, the decontamination without influenceing PEG-6 caprylic/capric glyceryl esters
Ability, belongs to non-stimulated rank through Eye irritation test.
2. the polyol component in makeup removing breast gel has wetting action.1,3-BDO wetting and dispersing ability is most strong, but
Eye irritation and bitter taste substantially, are not suitable for largely being used in makeup removal products, have compounded the good dipropylene glycol synergy of wetting and dispersing effect
Its wetting effect, and glycerine mitigation bitter taste is compounded, so that the product is applied to lip makeup removing and eye makeup removing.
Removing solid capacity is unloaded to oiliness color make-up 3. adding fat-soluble saualane in makeup removing breast gel and improving, polyalcohol is answered
Prepared with thing, ternary detersive micro-capsule cladding and saualane and to form microemulsion formulation and can make the rapid release of product reclaimed water oil, simultaneously
The advantage of water-soluble grease and the makeup removing of fat-soluble grease is played, is rapidly separated beneficial to oil, water, makeup removing speed is improved and synthesis is unloaded
Adornment effect, the polymorphic type color make-up such as the oiliness that can remove ornaments and formal dress color make-up and aqueous color make-up.
4. polyol complex, ternary detersive micro-capsule cladding and saualane pass through the compounding with acrylic acid solution, lifting
Product stability, forms translucent makeup removing breast gel, and plays the floating support effect to toner, prevents toner, soil re-deposition,
Use rear skin moisturizing, moisturizing non-greasy.
5. makeup removing gel makeup removing ability is strong, safe, small to eye irritation, easily rinse, with rear moisturizing, moisten not
It is greasy.
Brief description of the drawings
Fig. 1 is a kind of process chart of preferred embodiment of the invention.
The test zone that Fig. 2 is the eyeliner of experimental example 1, mascara is formed on cape skin.
Fig. 3 is the makeup removing ability evaluation and test experimental result photo of experimental example 1.
Fig. 4 is the situation of change block diagram that the sample of experimental example 1 uses rear tested region moisture.
Fig. 5 is the situation of change block diagram that the sample of experimental example 1 uses rear tested region hydration rate.
Fig. 6 is the sample wash evaluation experimental result photo of experimental example 1.
Embodiment
With reference to specific embodiment, the present invention is expanded on further, preparation technology flow is referring to Fig. 1.It should be understood that these realities
Example is applied to be only illustrative of the invention and is not intended to limit the scope of the invention.
Embodiment 1 prepares makeup removing breast gel (one)
1. prepare component 1-- ternary detersive micro-capsule cladding
(1) by PEG-6 caprylic/caprics glyceryl ester (40kg), water-soluble olive oil (8.0kg) and PEG/PPG-25/30
Copolymer (2kg) is added in sterilizing vacuum reaction kettle, opens stirring, is heated to 80 DEG C, is incubated 15min；
(2) 70 DEG C are cooled to, -0.08Mpa is evacuated to, 15min is stirred, to micelle forma-tion, feed liquid is transparent limpid, is formed
Homogeneous phase body；
(3) be cooled to 45 DEG C it is standby with bottom discharge.
2. prepare component 2 --- micro emulsion body
(1) component 1 (8kg), polyol complex (are specifically comprised into glycerine 6kg, dipropylene glycol 3kg, 1,3-BDO
1kg) add in purified water (60kg), open stirring, be heated to 80 DEG C；
(2) saualane (0.5kg) is added into system, interval homogeneous 8min fades to the semi-transparent state of micro emulsion to system from emulsus,
Form component 2；
3. prepare curdling glue
Acrylic resin soln (concentration 1wt%, 20kg) is added in component 2, is stirred, KOH solution (concentration is added
3wt%, 0.5kg), continue stirring and obtain translucent makeup removing breast gel.
Embodiment 2 prepares makeup removing breast gel (two)
1. prepare component 1 --- ternary detersive micro-capsule cladding
(1) by PEG-6 caprylic/caprics glyceryl ester (80.0kg), water-soluble olive oil (10kg) and PEG/PPG-25/30
Copolymer (5.0kg) is added in sterilizing vacuum reaction kettle, opens stirring, is heated to 80 DEG C, is incubated 15min；
(2) 70 DEG C are cooled to, -0.08Mpa is evacuated to, 15min is stirred, to micelle forma-tion, feed liquid is transparent limpid, is formed
Homogeneous phase body；
(3) 45 DEG C of dischargings are cooled to standby.
2. prepare component 2 --- micro emulsion body
(1) component 1 (9.0kg), polyol complex (are specifically comprised into glycerine 6kg, dipropylene glycol 3kg, 1,3- fourths two
Alcohol 1kg) add in purified water (60kg), stirring is opened, 70 DEG C are heated to；
(2) saualane (0.3kg) is added into system, interval homogeneous 8min fades to the semi-transparent state of micro emulsion to system from emulsus,
Form component 2；
3. prepare curdling glue
Acrylic acid solution (concentration 0.75wt%, 20kg) is added in component 2, is stirred, KOH solution (concentration is added
3.0wt%, 0.35kg), continue stirring and obtain translucent makeup removing breast gel.
Embodiment 3 prepares makeup removing breast gel (three)
1. prepare component 1 --- ternary detersive micro-capsule cladding
(1) by PEG-6 caprylic/caprics glyceryl ester (50.0kg), water-soluble olive oil (9kg) and PEG/PPG-25/30
Copolymer (3.0kg) is added in sterilizing vacuum reaction kettle, opens stirring, is heated to 85 DEG C, is incubated 15min；
(2) 75 DEG C are cooled to, -0.08Mpa is evacuated to, 20min is stirred, to micelle forma-tion, feed liquid is transparent limpid, is formed
Homogeneous phase body；
(3) 45 DEG C of dischargings are cooled to standby.
2. prepare component 2 --- micro emulsion body
(1) component 1 (6.0kg), polyol complex (are specifically comprised into glycerine 6kg, dipropylene glycol 3kg, 1,3- fourths two
Alcohol 1kg) add in purified water (60kg), stirring is opened, 78 DEG C are heated to；
(2) saualane (0.5kg) is added into system, interval homogeneous 8min fades to the semi-transparent state of micro emulsion to system from emulsus,
Form component 2；
3. prepare curdling glue
Acrylic acid solution (concentration 2.5wt%, 20kg) is added in component 2, is stirred, KOH solution (concentration is added
3.0wt%, 0.65kg), continue stirring and obtain translucent makeup removing breast gel.
The henchnmrk test of experimental example 1
(1) makeup removing ability evaluation and test
(1) evaluating method
Makeup removing power test is carried out with commercially available different dosage forms representative products.Eyeliner and mascara are smeared on cape skin (such as
Fig. 2), sample is applied to test zone, looped with same dynamics, it is ensured that the number of turns is consistent.Dipped with cotton pads equivalent 1#~
6# makeup removal products wipe the eyeliner and mascara on cape skin.
1# is the double-deck make up remover of U.S.'s brand；
2# is certain French brand makeup removing breast；
3# is U.S.'s brand makeup removing gel；
4# is certain Japanese brand makeup remover；
5# is the clean face cream of Chinese certain brand makeup removing；
6# is formulation makeup removing breast gel of the present invention.
(2) evaluation result
Test result is as shown in figure 3, formulation makeup removing breast gel 6# of the present invention is to oiliness color make-up (eyeliner) and aqueous color make-up
The comprehensive effect adornment effect of (mascara) is better than double-deck make up remover, makeup removing breast, makeup remover and make-up remover.
(2) moisture retention evaluation
(1) instrument and equipment
Moisture content of skin tester Corneometer CM825 (German CK companies).
(2) test index
A) skin moisture content MMV values
The probe of moisture of skin tester (Cornemeter CM825) is that the principle based on electric capacity is measured.Jie of water
Electric constant is 81, and the dielectric constant of other materials is typically smaller than 7, and water is the maximum material of dielectric constant on skin.When moisture contains
Amount is when changing, and the capacitance of skin also changes, thus can by determining skin pricktest capacitance, analyzing skin surface it is aqueous
Amount.Measured value is a relative value.
B) skin oil and fat content value
Oil content test uses universally acknowledged SEBUMETER methods, and it is to be based on photometer principle, and a kind of 0.1mm is thick
Special delustring adhesive tape absorb human body skin on grease after, a kind of translucent adhesive tape will be become, its light transmission capacity will
Change absorption grease it is more, light transmission capacity will be bigger, can thus measure the content of skin oil and fat.
(3) evaluating method
The left and right inboard arm specific region of selection subject is marked successively：Tested region samples group and blank control region；
Technical staff is using the Corneometer CM825 moisture content test probe measurement subject of MPA9 Multi-functional skin testers through clear
The tested region that water was cleaned and marked, averages, is designated as blank value.Given the test agent is smeared in the Test sites of subject
After 1min, with makeup removing cotton wipe samples, the data after 1min and 1h after tested region is wiped then are tested.
(4) tested sample：
Makeup removing breast gel of the present invention, commercially available Japanese certain brand makeup removing honey.
(5) evaluation result
Moisture content change was reflected in test period, and Experimental Area moisture changes over time rule.Its value is bigger,
Moisture is bigger, conversely, moisture is smaller.
Hydration rate=(sample sets moisture-starting moisture content)/starting moisture content, this value is higher, moisturizing effect
It is more obvious.
The result of variations of moisture is as shown in Figure 4, it can be seen that makeup removing breast gel of the present invention is smeared within test period
Recipient site wipe 1 minute after and wipe 1 hour after moisture be above blank value；Certain commercially available Japanese brand is smeared to unload
The recipient site of adornment honey is below blank value after testing 1 minute with the moisture after wiping 1 hour.
The change of hydration rate is as shown in Figure 5, it can be seen that the tested of makeup removing breast gel of the present invention is smeared within test period
Hydration rate after position is wiped 1 minute and after wiping 1 hour is on the occasion of illustrating that test sample has certain moisturizing effect；
Smear commercially available Japanese certain brand makeup removing honey recipient site test 1 minute after and the hydration rate after wiping 1 hour be negative value, say
Bright test sample moisturizing effect is poor.
Comprehensive moisture and hydration rate situation：
Within test period, smear moisture after the recipient site of makeup removing breast gel of the present invention, wipe samples and be higher than sky
White value, hydration rate is on the occasion of illustrating that test sample has certain moisturizing effect；Smear commercially available Japanese certain brand makeup removing honey by
Try moisture after position, wipe samples and be less than blank value, hydration rate is in negative value, illustrates that test sample does not possess moisturizing effect.
(3) acute ocular irritation test
Shanghai Disease Prevention and Control Centre is entrusted to carry out acute ocular irritation test and multiple Skin Irritation Test.
Acute ocular irritation test conclusion is：Experiment is under not washing condition, and tested material is accumulated to rabbit eye irritation highest
It is 0 to be divided into average cornea, and iris is 0, and conjunctiva is 0, is belonged to nonirritant.
Repeatedly Skin Irritation Test conclusion is：Tested material is in the multiple skin irritation test of rabbit, daily every animal
Skin wound repair integral mean value is 0, is belonged to nonirritant.
(4) washability
(1) evaluation method：Foundation cream cream is applied to the back of the hand, is applied to respectively using different makeup removal products on foundation cream cream, is seen
Examine scattered toner effect；Then rinsed with clear water, observe developing result.
1# is the double-deck make up remover of U.S.'s brand；
2# is certain French brand makeup removing breast；
3# is U.S.'s brand makeup removing gel；
4# is certain Japanese brand makeup remover；
5# is formulation makeup removing breast gel of the present invention.
(2) evaluation result：
As a result as shown in fig. 6, a is scattered toner effect photo after each makeup removal products sample is applied on foundation cream cream, b is
The effect photo then rinsed with clear water.As a result show：
U.S. brand bilayer make up remover 1# is preferable to the dispersion force of toner, but is difficult to rinse；
Certain brand makeup removing breast 2# of France is bad to powder dispersion effect, it is difficult to rinse；
U.S. brand makeup removing gel 3# is general to powder dispersion effect, there is obvious residual after flushing；
Japanese certain brand makeup remover 4# is preferable to powder dispersity, overcomes the shortcoming of conventional makeup remover washability difference, meets
Water and milk is melted into off-white color, easily rinses, but wash rear greasy feeling weight；
Makeup removing breast gel 5# of the present invention quickly floats support toner, easily rinses, salubrious water profit, no greasy feeling after.
By test, formulation makeup removing breast gel of the present invention has significantly floating support effect to toner, and easily rinses, skin
It is clear pleasant, washability and it is better than the formulation makeup removal products such as double-deck make up remover, makeup removing breast, makeup removing gel, makeup remover with rear skin sense.
Claims (9)
1. a kind of makeup removing breast gel, it is characterised in that it is made up of following raw material：PEG-6 caprylic/capric glyceryl esters, 4.0
~8.0 parts by weight；Water-soluble olive oil, 0.8~1.0 parts by weight；PEG/PPG-25/30 copolymers, 0.1~0.5 parts by weight；It is many
First alcohol compound, 3.0~8.0 parts by weight；Saualane, 0.3~1.0 parts by weight；The parts by weight of acrylic resin 0.15~0.5 and water
80~88 parts by weight.
2. makeup removing breast gel as claimed in claim 1, it is characterised in that the polyol complex be glycerine, dipropylene glycol,
1,3-BDO, according to (5~6): (2~4): the weight of (0.8~1.2) is than composition.
3. makeup removing breast gel as claimed in claim 2, it is characterised in that the polyol complex be glycerine, dipropylene glycol,
1,3-BDO, according to 6: 3: 1 weight than constituting.
4. makeup removing breast gel as claimed in claim 3, it is characterised in that the PEG-6 caprylic/caprics glyceryl ester, 4 weight
Part；Water-soluble olive oil, 0.8 parts by weight；PEG/PPG-25/30 copolymers, 0.2 parts by weight；Polyol complex, 3.75 weight
Part；Saualane, 0.31 parts by weight and the parts by weight of acrylic resin 0.25；Water, 85.0 parts by weight.
5. the makeup removing breast gel as any one of claim 1-4, it is characterised in that the moisturizing eye shadow also includes auxiliary
Material, auxiliary material is spices and preservative.
6. the preparation method of the makeup removing breast gel as any one of claim 1-5, it is characterised in that this method is included such as
Lower step：
Step I：By PEG-6 caprylic/caprics glyceryl ester, water-soluble olive oil and PEG/PPG-25/30 copolymer Hybrid Heatings
Ternary detersive micro-capsule cladding is made；
Step II：By water, polyol complex and ternary detersive micro-capsule cladding Hybrid Heating, saualane is then added, to body
System carries out interval homogeneous and fades to the semi-transparent state of micro emulsion to system from emulsus, obtains microemulsion；Wherein, water and polyol complex
Weight ratio is 60: (3.0~8.0)；
Step III：Acrylic resin (0.15~0.5 parts by weight) is pre-dispersed in water (40.0~45.0 parts by weight), it will walk
The microemulsion that rapid II is obtained is added in acrylic resin aqueous dispersions, is subsequently added KOH solution to pH5.5~7.0, is obtained semi-transparent
Bright makeup removing breast gel.
7. preparation method as claimed in claim 6, it is characterised in that the step I is：
A. PEG-6 caprylic/caprics glyceryl ester, water-soluble olive oil and PEG/PPG-25/30 copolymers are added into sterilizing vacuum
In reactor, stirring is heated to 80-85 DEG C, is incubated 15~20min；
B. 70-75 DEG C is cooled to, is evacuated to more than -0.08Mpa, stirs 15-20min, to micelle forma-tion, feed liquid is transparent clear
It is clear, form homogeneous phase body；
C. 45 DEG C are cooled to bottom discharge, ternary detersive micro-capsule cladding is obtained.
8. preparation method as claimed in claim 6, it is characterised in that the step II is：By water, polyol complex and three
First decontamination micro-capsule cladding is mixed and heated to 70~80 DEG C, then adds saualane, and 8~15min of interval homogeneous is carried out to system
The semi-transparent state of micro emulsion is faded to system from emulsus, microemulsion is obtained.
9. a kind of makeup removing breast gel, it is characterised in that it is prepared using the method as any one of claim 6-8.
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