CN107259561A - Flower of Panax ginseng glue drink and preparation method thereof - Google Patents
Flower of Panax ginseng glue drink and preparation method thereof Download PDFInfo
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- CN107259561A CN107259561A CN201710342679.6A CN201710342679A CN107259561A CN 107259561 A CN107259561 A CN 107259561A CN 201710342679 A CN201710342679 A CN 201710342679A CN 107259561 A CN107259561 A CN 107259561A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 20
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Mycology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Botany (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention provides a kind of flower of Panax ginseng glue drink, and the raw material matched by following weight is made：5 10 parts of ginseng, 5 10 parts of jujube, 5 10 parts of matrimony vine, 5 10 parts of longan, 8 20 parts of glue of flower, 900 950 parts of water.The present invention also provides the preparation method of the flower of Panax ginseng glue drink, and its method contains following steps：Step：(1) ginseng is extracted, Ginseng extract is made；(2) jujube, matrimony vine and longan are mixed and extracted, herbal extract is made；(3) will flower glue digested, deodorization, colored glue enzymolysis liquid after deodorization is made；(4) flower glue enzymolysis liquid after the Ginseng extract, herbal extract and deodorization is merged, adds auxiliary material, mixing.The effects such as obtained flower of Panax ginseng glue drink has relieving fatigue, increase body immunity, beautifying face and moistering lotion.
Description
Technical field
The invention belongs to field of health care food, it is related to a kind of natural health drink and preparation method thereof, it is more particularly to a kind of
Flower of Panax ginseng glue drink and preparation method thereof.
Background technology
In recent years, with the improvement of living standards, the popularization of health knowledge, people are to the health of itself, diet-therapy health-preserving, guarantor
It is strong increasingly to pay attention to and be concerned about.Thus to natural, the healthy positive continuous enlargement of plant extracts product demand.Along with people couple
The lifting of " back to nature ", " green consumption " degree of recognition, it is time saving, laborsaving, uncap ready-to-drink natural health drink in the world
Interior to be praised highly energetically, conventional medicament is also by the concern and accreditation of broad masses.
Ginseng tonifying middle-Jiao and Qi, blood-nourishing of promoting the production of body fluid, tranquilize the mind and promote the intelligence, can adjust nervous centralis, regulation immunity of organism, regulation painstaking effort
Guard system.
Flower glue tool effectively improves immunity, suppresses cancer cell, activating cell, prevents skin aging from removing wrinkle, activation muscle
Bone slows down arthritis and the effect such as ache, especially enriching blood, stop blooding, enriching yin, moisturize in terms of more have obvious effect；But flower glue
It is difficult directly to be absorbed by body and skin, it is necessary to which it is hydrolyzed into amino acid and polypeptide can just be absorbed by organisms.
At present, in other beverage formulations containing medicinal materials such as ginseng, flower glue, it, which is formulated, constitutes all more complicated, and
Substantially preparation technology is that whole components crush extraction together, causes the shortcoming of medicinal material active ingredient loss.
The content of the invention
In order to overcome deficiency of the prior art, the present invention provide it is a kind of have relieving fatigue, increase body immunity with
The flower of Panax ginseng glue drink of beauty functions, present invention also offers the method for preparing flower of Panax ginseng glue drink.
To solve the above problems, the technical scheme used is as follows：A kind of flower of Panax ginseng glue drink, the original matched by following weight
Material is made：5-10 parts of ginseng, 5-10 parts of jujube, 5-10 parts of matrimony vine, 5-10 parts of longan, 8-20 parts of glue of flower, 900-950 parts of water.
It is preferred that, a kind of flower of Panax ginseng glue drink, the raw material matched by following weight is made：8 parts of ginseng, 8 parts of jujube, matrimony vine
8 parts, 8 parts of longan, flower 15 parts of glue, 908 parts of water.
Present invention also offers a kind of preparation method of flower of Panax ginseng glue drink, including：
(1) ginseng is extracted, Ginseng extract is made；
(2) jujube, matrimony vine and longan are mixed and extracted, herbal extract is made；
(3) will flower glue digested, deodorization, colored glue enzymolysis liquid after deodorization is made；
(4) flower glue enzymolysis liquid after the Ginseng extract, herbal extract and deodorization is merged, adds auxiliary material, mixing.
The step (1) includes：It is 1: 65- by weight that people is participated in into the ethanol that concentration of volume percent is 70-80%
85 mixing, soak 20-50 minutes；Circumfluence distillation is carried out, extraction time is 2-3 times, each 1.5-2.5 hours；Filtering, merges
Filtrate, reclaims ethanol, and Ginseng extract is made.
It is preferred that, in step (1), it is 1: 75 mixed by weight that people is participated in into the ethanol that concentration of volume percent is 75%
Close, soak 30 minutes.
It is preferred that, in step (1), the extraction time of the circumfluence distillation 2 times, every time 2 hours.
Present inventor has found, ginseng is taken into ethanol for solvent circumfluence distillation and separately extracted with other medicinal materials,
The total Ginsenosides Content extracted is maximum.
The step (2) includes：Jujube, matrimony vine and longan are mixed, added equivalent to 65-85 times of total weight of the mixture
Water infiltration 30-40 minutes；Circumfluence distillation is carried out, extraction time is 2-3 times, each 1.5-2.5 hours；Filtering, merging filtrate,
Concentration, is made concentrate；
Concentrate is subjected to alcohol precipitation, supernatant 1 and sediment is obtained；It is with concentration of volume percent by gained sediment
60-70% ethanol washing, standing, obtain supernatant 2；Merge supernatant 1 and supernatant 2, herbal extract is made.
It is preferred that, in step (2), the extraction time of the circumfluence distillation is 2 times, every time 2 hours.
It is preferred that, in step (2), the alcohol precipitation comprises the following steps：Percent by volume is slowly added into concentrate dense
Spend for 90-98% ethanol, it is stirring while adding, the concentrate concentration of volume percent containing ethanol is reached 45-55%, stop stirring
Mix, stand 24 ± 3 hours.
Particularly preferred, in step (2), the alcohol precipitation comprises the following steps：Volume basis is slowly added into concentrate
Specific concentration is 95% ethanol, stirring while adding, the concentrate concentration of volume percent containing ethanol is reached 50%, stops stirring
Mix, stand 24 ± 3 hours.
It is preferred that, in step (2), the concentration comprises the following steps：Filtered fluid will be extracted to be concentrated into relative density and be
0.95-1.15(20℃)。
Particularly preferred, in step (2), the concentration comprises the following steps：Filtered fluid will be extracted and pass through Multi-effect concentration extremely
Relative density is 1.05.
The step (3) includes：Flower glue is mixed with water by weight for 1: 55-65, temperature is 50-60 DEG C, soaks 20-
30 minutes；Mashing processing is carried out, flower rubber cement liquid is made；
To flower rubber cement liquid, the papain of the 0.4-2% equivalent to flower glue weight is added, enzymolysis pH value is 6.5-7.5,
Under the conditions of temperature is 55-65 DEG C, digest 2-5 hours, enzymolysis liquid is made；
Enzymolysis liquid is heated to 90-110 DEG C, inactivation time is 3-5min, filtered, enzymolysis inactivation liquid is made；
Into enzymolysis inactivation liquid, the 2-3% yeast equivalent to flower glue weight is added, under the conditions of temperature is 33-37 DEG C, hair
Ferment 25-35min, is made enzymatic hydrolysis and fermentation liquid；
Into enzymatic hydrolysis and fermentation liquid, the 2-3% cycloheptaamyloses equivalent to flower glue weight are added, are 60-70 DEG C of bar in temperature
25-35min is reacted under part, is filtered, flower glue enzymolysis liquid after deodorization is made.
It is preferred that, in step (3), flower glue is mixed with water by weight for 1: 60 amount.
It is preferred that, in step (3), add 1.2% papain equivalent to flower glue weight.
It is preferred that, in step (3), enzymolysis liquid is heated to 100 DEG C and inactivated.
It is preferred that, in step (3), into the enzymolysis filtered fluid, 2.5% yeast equivalent to flower glue weight is added,
Temperature is the 30min that under the conditions of 35 DEG C, ferments, and enzymatic hydrolysis and fermentation liquid is made.
It is preferred that, in step (3), into the enzymatic hydrolysis and fermentation liquid, add 2.5% β-ring-type paste equivalent to flower glue weight
Essence, under the conditions of temperature is 65 DEG C, reacts 30min, flower glue enzymolysis liquid after deodorization is made in filtering.
Present inventor find by by flower glue separately extract, can be effectively improved finished product Chinese medicine it is effective into
Divide content.Because flower glue is animal class material, rich in colloid, its extract solution somewhat viscous.If flower glue and medicinal material are extracted together,
Medicinal material can be wrapped up after flower peptization solution, influence the dissolution of medicinal material active ingredient, and larger resistance can be formed to filter material during filtering
And it is not easy filtering, cause medicinal material active ingredient to be lost in.Flower glue is separately extracted, it is to avoid medicinal material active ingredient is lost in；Therefore,
Improve the active constituent content of finished product Chinese medicine.
The present invention to flower glue digest the processing of deodorization, and reaction condition is gentle, nutrient component damages are few, and the used time is short, receive
Rate is high, and pollution-free, and the enzymolysis product of gained is amino acid and peptide material, directly can be digested by body with absorbing, while gram
Clothes flower glue protein the product bitter taste and fishy smell that are brought, obtain it is a kind of it is yellowish, without flower glue protein solution of the bitter taste without fishy smell.
It is preferred that, in step (4), the auxiliary material includes white granulated sugar and resistant dextrin.
The step (4) includes：Herbal extract is mixed with flower glue enzymolysis liquid after deodorization, water is added, adds white sand
Sugar and resistant dextrin solution, dissolving, filtering, packing.
It is preferred that, in step (4), the preparation method of the resistant dextrin solution, including resistant dextrin is added 65-75 DEG C
Hot water dissolving, filtering.
Beneficial effects of the present invention：
The invention provides a kind of health, safety, eutrophy and can beautifying face and moistering lotion pure natural Chinese herbal medicine health drink.This
Invention uses integration of drinking and medicinal herbs medicinal material ginseng, matrimony vine, longan, jujube.Life is mended into the enriching yin of ginseng, solid original, the nourishing of longan is helped
Enrich blood, QI invigorating calming heart, the kidney-tonifying sperm-generating of matrimony vine, nourish the liver to improve visual acuity, the tonifying middle-Jiao and Qi of jujube, the fusion of nourishing blood and tranquilization effect together, and
It is equipped with the precious good merchantable brand flower glue of nourishing dietotherapy；By scientific and reasonable proportioning, each component share can reach raising body immunity and
Effect of beautifying face and moistering lotion.Present invention is especially suited for rhythm of life is fast, working strength big, through conventional brain, daily life is irregular, body is empty
The crowd that weak, immunologic hypofunction or body are in sub-health state takes, being capable of relieving fatigue, raising work effect after use
Rate, increase body immunity, have more had the effect of beautifying face and moistering lotion concurrently.
The present invention is individually taken ginseng using ethanol as solvent circumfluence distillation, improves the yield of ginseng effective component,
The waste of ginseng resource is reduced, cost-effective effect can be played in terms of the consumption of ginseng.The present invention is to jujube, matrimony vine
Circumfluence distillation is used with longan, and is purified using alcohol precipitation after first water extraction, each medicinal material active ingredient yield is effectively raised, obtains
Obtain the higher required material of purity.The present invention takes independent processing to flower glue, after being digested with papain, then passes through hair
After ferment deodorization, mixed preparing is carried out under optimum conditions with herbal extract.This not only avoids the loss of medicinal material active ingredient,
Also obtain that a mouthfeel is unique, pure taste, it is long-term drink have no side effect, various people's all suitable health drinks.
Embodiment
With reference to specific embodiment, the present invention is further described, but illustrated embodiment does not make limitation of the invention.
Various raw materials used are commercial goods in following examples, are that can buy to obtain by commercial sources.
A kind of flower of Panax ginseng glue drink, the raw material matched by following weight is made：5-10 parts of ginseng, 5-10 parts of jujube, matrimony vine
5-10 parts, 5-10 parts of longan, flower 8-20 parts of glue, 900-950 parts of water.
Above-mentioned each component has following effect and effect respectively：
Ginseng：The dry root of araliaceae ginseng plant, be described as from ancient times " kings of hundred grass, enriching yin mend raw, strengthen the body resistance to consolidate the constitution " it
Superfine product.Ginseng tonifying middle-Jiao and Qi, blood-nourishing of promoting the production of body fluid, tranquilize the mind and promote the intelligence, can adjust nervous centralis, regulation immunity of organism, regulation angiocarpy
System.Ginseng contains a variety of saponin(es and polysaccharide constituents, and leachate can expand skin by skin slow-absorbing and without pessimal stimulation
Capillary, promote skin blood circulation, increase skin-nourishing, adjust skin water and oil balance, prevent skin dehydration, hardening,
Corrugation, ginseng active material suppresses the reducing property of melanin, makes skin pure white smooth, can strengthen skin elasticity, obtain cell
Obtain newborn, be the superfine product improved looks.
Jujube：Rich in protein, fat, carbohydrate, carrotene, B family vitamin, vitamin C, citrin and calcium, phosphorus,
The nutritional ingredient such as iron and CAMP, with enhancing body immunity, enhancing muscular strength, protection liver, antiallergy, menstruation regulating, goes
Constipation, tonifying spleen, nourishing blood and tranquilization, nti-freckle of preserving youthful looks, vigorous and graceful rich flesh effect.
Matrimony vine：Rich in multiple nutritional components such as matrimony vine proteoglycan, vitamin C, phosphorus, iron, with qi-restoratives production of sperm, nourishing liver
Kidney, except irascibility, improving eyesight the effects such as, can play enhancing immunologic function, beneficial to sleep, beauty face-whitening-nourishing, anti-oxidant, anti-aging, drop
Low blood-fat and blood sugar effect.
Longan：Contain abundant protein, fat, carbohydrate, organic acid, crude fibre, iron and multivitamin and mineral matter etc.
Various nutrients, can promote hemoglobin regeneration to enrich blood again while improving heat energy, supplementing the nutrients；Also have simultaneously
Brain tonic and intelligence development, takes a tonic or nourishing food to build up one's health heart spleen, calms the nerves, control insomnia, it is forgetful, the effects such as palpitate with fear.
Flower glue：The main component of flower glue is senior collagen and mucopolysaccharide material, multivitamin and calcium, zinc, iron, selenium
Etc. various trace elements, its protein content is up to 84.2%, and fat is only 0.2%.Contain a large amount of large biological molecule glue in flower glue
Former albumen, is human body supplement, the raw material of synthetic protein, and be easy to absorb and utilize.Immunity, suppression cancer can be effectively improved thin
Born of the same parents, activating cell, prevent that skin aging from removing wrinkle, activation muscles and bones is slowed down arthritis and ached, especially enriching blood, stop blooding, grow
It is cloudy, moisturize in terms of more have obvious effect.But protein is difficult directly to be absorbed by body and skin, it is necessary to which it is hydrolyzed into ammonification
Base acid and polypeptide can be just absorbed by organisms.
A kind of flower of Panax ginseng glue drink that the present invention is provided, including following examples：
Embodiment 1
A kind of flower of Panax ginseng glue drink, the raw material matched by following weight is made：8 parts of ginseng, 8 parts of jujube, 8 parts of matrimony vine, osmanthus
8 parts of circle, 15 parts of glue of flower, 908 parts of water.
Above-mentioned flower of Panax ginseng glue drink includes following preparation method：
(1) ginseng is extracted
1.1) it is 1: 75 mixing by weight people to be participated in into the ethanol that concentration of volume percent is 70-80%, soaks 30 points
Clock；
1.2) circumfluence distillation is carried out to ginseng, extraction time is 2 times, and 2 hours every time, filtering merged filtrate twice；
1.3) ethanol is recovered under reduced pressure, Ginseng extract is obtained.
(2) jujube, matrimony vine and longan are extracted
2.1) jujube, matrimony vine and longan are mixed, adds water of 75 times equivalent to total weight of the mixture, infiltrated 30 minutes；
2.2) circumfluence distillation is carried out to mixture, extraction time is 2 times, and 2 hours every time, filtering merged filtrate twice；
2.3) it is 1.05 extract solution to be concentrated into relative density by Multi-effect concentration evaporator；
2.4) concentration of volume percent is slowly added into concentrate for 95% ethanol, it is stirring while adding, contain concentrate
Ethanol concentration of volume percent reaches 50%, stops stirring, and cream liquid stands 24 ± 3 hours.
2.5) supernatant 1 of standing is taken to reclaim ethanol, precipitation is that 65% ethanol washs standing with concentration of volume percent, is taken
Supernatant 2 reclaims ethanol, merges supernatant 1 and supernatant 2, obtains herbal extract.
(3) flower glue enzymolysis deodorization：
3.1) flower glue is mixed with water by weight for 1: 60, infiltrated 20-30 minutes at 50-60 DEG C, carry out mashing processing,
Flower rubber cement liquid is made；
3.2) to flower rubber cement liquid, the 0.4-2.0% papains equivalent to flower glue weight are added, pH6.5-7.5 is adjusted,
Stir evenly after keeping 2-5 hours progress enzyme digestion reactions in 60 DEG C of water-baths, enzymolysis process need to be stirred repeatedly, and enzymolysis liquid is made；
3.3) enzymolysis liquid is heated to 95-100 DEG C and boils 3-5 minutes by enzyme-deactivating, enzymolysis reaction；Filtering, is made
Enzymolysis inactivation liquid；
3.4) into enzymolysis inactivation liquid, 2.5% yeast equivalent to flower glue weight is added, under the conditions of temperature is 35 DEG C,
Ferment 30min, and enzymatic hydrolysis and fermentation liquid is made；
3.5) to enzymatic hydrolysis and fermentation liquid, 2.5% cycloheptaamylose equivalent to flower glue weight is added, is 65 DEG C of conditions in temperature
Under, 30min is reacted, filtering obtains flower glue enzymolysis liquid after deodorization.
(4) prepare：
4.1) 0.3-0.5% resistant dextrins 70 DEG C of hot water dissolvings, the filtering equivalent to raw material gross weight are added, is made anti-
Property dextrin liquid；
4.2) herbal extract is mixed with flower glue enzymolysis liquid, adds 45 portions of white granulated sugars, above-mentioned resistant dextrin liquid, added
After preparation is mixed with water in right amount, filter, dispense, sterilizing, packaging obtain flower of Panax ginseng glue drink.
Embodiment 2：Investigate the method that ginseng is extracted
2.1 using water as solvent, takes ginseng independent extraction, and circumfluence distillation number of times is 1 time：
The water for taking ginseng 2g to add 75 times equivalent to ginseng gross weight, soaks 30 minutes, circumfluence distillation 1 time, during extraction
Between be respectively 1.5 hours, 2.5 hours, 3.5 hours, filtering, obtain sample；The detection of total saponin content is carried out to sample.Experiment
It the results are shown in Table 1.
2.2 using water as solvent, takes ginseng independent extraction, and circumfluence distillation number of times is 2 times：
Ginseng 2g is taken, water of 75 times equivalent to ginseng gross weight is added, soaked 30 minutes, circumfluence distillation 2 times is carried every time
It is respectively 1.5 hours, 2.5 hours, 3.5 hours to take the time, filtering, obtains sample；The detection of total saponin content is carried out to sample.
Experimental result is shown in Table 1.
2.3 using water as solvent, takes ginseng, jujube, matrimony vine and longan mixing to extract, and circumfluence distillation number of times is 1 time：
Ginseng 2g, jujube 2g, matrimony vine 2g and longan 2g are taken, water of 75 times equivalent to total weight of the mixture, immersion 30 is added
Minute, circumfluence distillation 1 time, extraction time is respectively 1.5 hours, 2.5 hours, 3.5 hours, filtering, obtains sample；To sample
Carry out the detection of total saponin content.Experimental result is shown in Table 1.
2.4 using water as solvent, takes ginseng, jujube, matrimony vine and longan mixing to extract, and circumfluence distillation number of times is 2 times：
Ginseng 2g, jujube 2g, matrimony vine 2g and longan 2g are taken, water of 75 times equivalent to total weight of the mixture, immersion 30 is added
Minute, circumfluence distillation 2 times, each extraction time is respectively 1.5 hours, 2.5 hours, 3.5 hours, filtering, obtains sample；It is right
Sample carries out the detection of total saponin content.Experimental result is shown in Table 1.
2.5 using concentration of volume percent be 75% ethanol as solvent, take ginseng independent extraction, circumfluence distillation
Number is 1 time：
Ginseng 2g is taken, the ethanol that the concentration of volume percent for adding 75 times equivalent to ginseng gross weight is 75%, immersion 30
Minute, circumfluence distillation 1 time, extraction time is respectively 1.5 hours, 2.5 hours, 3.5 hours, filtering, obtains sample；To sample
Carry out the detection of total saponin content.Experimental result is shown in Table 1.
2.6 using concentration of volume percent be 75% ethanol as solvent, mixing is taken to ginseng, jujube, matrimony vine and longan
Extract, circumfluence distillation number of times is 1 time：
Ginseng 2g, jujube 2g, matrimony vine 2g and longan 2g are taken, percent by volume of 75 times equivalent to total weight of the mixture is added
Concentration is 75% ethanol, is soaked 30 minutes, circumfluence distillation 1 time, extraction time is respectively 1.5 hours, 2.5 hours, it is 3.5 small
When, filtering obtains sample；The detection of total saponin content is carried out to sample.Experimental result is shown in Table 1.
2.7 using concentration of volume percent be 75% ethanol as solvent, mixing is taken to ginseng, jujube, matrimony vine and longan
Extract, circumfluence distillation number of times is 1 time：
Ginseng 2g, jujube 2g, matrimony vine 2g and longan 2g are taken, percent by volume of 75 times equivalent to total weight of the mixture is added
Concentration is 75% ethanol, is soaked 30 minutes, circumfluence distillation 1 time, extraction time is respectively 1.5 hours, 2.5 hours, it is 3.5 small
When, filtering obtains sample；The detection of total saponin content is carried out to sample.Experimental result is shown in Table 1.
2.8 using concentration of volume percent be 75% ethanol as solvent, mixing is taken to ginseng, jujube, matrimony vine and longan
Extract, circumfluence distillation number of times is 2 times：
Ginseng 2g, jujube 2g, matrimony vine 2g and longan 2g are taken, percent by volume of 75 times equivalent to total weight of the mixture is added
Concentration is 75% ethanol, is soaked 30 minutes, circumfluence distillation 2 times, each extraction time is respectively 1.5 hours, 2.5 hours,
3.5 hours, filtering obtained sample；The detection of total saponin content is carried out to sample.Experimental result is shown in Table 1.
Table 1
As shown in Table 1, using concentration of volume percent by 75% ethanol as solvent extract general ginsenoside content
It is much more than amount using water as solvent extraction.Ginseng individually extracts the dissolution extracted than mixing and be more beneficial for general ginsenoside,
And yield is higher.Meanwhile, the total Ginsenosides Content of gained is higher 1 time than extracting after being extracted through 2 times, after 2 times are extracted, energy
Being extracted completely for the composition of extraction, the waste of resource is not resulted in.Therefore, final choice individually extracts ginseng, and
Use using ethanol as solvent circumfluence distillation, extraction time is 2 times；The loss brought during mixing is extracted, energy can so be reduced
The waste of ginseng is reduced, cost-effective effect can be played in terms of the consumption of ginseng.
It is attached：
(1) experiment reagent：Ginsenoside Re's standard items (content 98%) --- carried by Nat'l Pharmaceutical ＆ Biological Products Control Institute
For, methanol (analysis is pure), ethanol (analysis is pure)；
(2) laboratory apparatus：High performance liquid chromatograph (LC-20AT Shimadzus are sweet), electronic balance (sensibility reciprocal is 0.0001g)；
(3) assay method of total ginsenoside Re's content：
Measure according to People's Republic of China's agricultural industry criteria NY/T 1842-2010 ginsenosides
A. laboratory apparatus condition：
Chromatographic column：C18(4.6mm×300mm×0.5um)
Mobile phase：Methanol+water
Column temperature：47℃
Flow velocity：0.5~0.8ml/min
Detection wavelength：202nm
Sample size：10ul
B. the preparation of standard solution：
Precision weighs ginsenoside Re standard items 0.183g, puts in 100ml volumetric flask, plus methanol makes it dissolve and dilute
To scale, shake up, produce.
C. the drafting of standard curve：
Precision is drawn standard solution 0ml, 2ml, 4ml, 6ml, 8ml, 10ml and put in 10ml measuring bottles, with methanol dilution to quarter
Degree, takes 10ul to inject liquid chromatograph respectively, records peak area.Standard is drawn to its peak area with the mass concentration of saponin(e bent
Line.
D. sample is determined：
Accurate 10ul sample solutions of drawing inject liquid chromatograph, qualitative with retention time, with prepare liquid peak area and mark
Quasi- solution peak area ratio is more quantitative.
E. result is calculated：
The total Ginsenosides Content that the content of ginsenoside is represented with mass fraction w in sample is by formula：
In formula
m1The quality of-ginsenoside, unit is gram (g)；
m2The quality of-sample, unit is gram (g)；
V1The sampling volume of-sample, unit is milliliter (ml)；
V2The constant volume of-sample, unit is milliliter (ml).
The above described is only a preferred embodiment of the present invention, any formal limitation not is done to the present invention, therefore
All contents without departing from technical solution of the present invention, the technical spirit according to the present invention any is simply repaiied to made for any of the above embodiments
Change, equivalent variations and modification, in the range of still falling within technical solution of the present invention.
Claims (10)
1. a kind of flower of Panax ginseng glue drink, it is characterised in that the raw material matched including following weight is made：5-10 parts of ginseng, jujube
5-10 parts, 5-10 parts of matrimony vine, 5-10 parts of longan, flower 8-20 parts of glue, 900-950 parts of water.
2. a kind of flower of Panax ginseng glue drink according to claim 1, it is characterised in that the raw material matched by following weight is made：
8 parts of ginseng, 8 parts of jujube, 8 parts of matrimony vine, 8 parts of longan, 15 parts of glue of flower, 908 parts of water.
3. a kind of preparation method of flower of Panax ginseng glue drink as claimed in claim 1 or 2, it is characterised in that this method contains following
Step：
(1) ginseng is extracted, Ginseng extract is made；
(2) jujube, matrimony vine and longan are mixed and extracted, herbal extract is made；
(3) will flower glue digested, deodorization, colored glue enzymolysis liquid after deodorization is made；
(4) flower glue enzymolysis liquid after the Ginseng extract, herbal extract and deodorization is merged, adds auxiliary material, mixing.
4. a kind of preparation method of flower of Panax ginseng glue drink according to claim 3, it is characterised in that the step (1) includes：
It is 1: 65-85 mixing by weight that people is participated in into the ethanol that concentration of volume percent is 70-80%, is soaked 20-50 minutes；Carry out
Circumfluence distillation, extraction time is 2-3 times, each 1.5-2.5 hours；Filtering, merging filtrate reclaims ethanol, and obtained ginseng is carried
Take liquid.
5. a kind of preparation method of flower of Panax ginseng glue drink according to claim 3, it is characterised in that the step (2) includes：
Jujube, matrimony vine and longan are mixed, water of 65-85 times equivalent to total weight of the mixture is added, infiltrated 20-50 minutes；Carry out heat
Refluxing extraction, extraction time is 2-3 times, each 1.5-2.5 hours；Concentrate is made in filtering, merging filtrate, concentration；
Concentrate is subjected to alcohol precipitation, supernatant 1 and sediment is obtained；With concentration of volume percent it is 60- by gained sediment
70% ethanol is washed, stood, and obtains supernatant 2；Merge supernatant 1 and supernatant 2, herbal extract is made.
6. a kind of preparation method of flower of Panax ginseng glue drink according to claim 5, it is characterised in that in step (2), the alcohol
It is heavy, comprise the following steps：The ethanol that concentration of volume percent is 90-98% is added into concentrate, it is stirring while adding, make mixing
Contained ethanol concentration of volume percent reaches 45-55% in liquid, stops stirring, stands 24 ± 3 hours.
7. a kind of preparation method of flower of Panax ginseng glue drink according to claim 3, it is characterised in that the step (3) includes：
Flower glue is mixed with water by weight for 1: 55-65, soaked 20-30 minutes under the conditions of temperature is 50-60 DEG C；Carry out at mashing
Reason, is made flower rubber cement liquid；
To flower rubber cement liquid, the papain of the 0.4-2% equivalent to flower glue weight is added, enzymolysis pH value is 6.5-7.5, in temperature
Spend under the conditions of 55-65 DEG C, to digest 2-5 hours, enzymolysis liquid is made；
Enzymolysis liquid is heated to 90-110 DEG C, inactivation time is 3-5min, filtered, enzymolysis inactivation liquid is made；
Into enzymolysis inactivation liquid, the 2-3% yeast equivalent to flower glue weight is added, under the conditions of temperature is 33-37 DEG C, fermentation
25-35min, is made enzymatic hydrolysis and fermentation liquid；
Into enzymatic hydrolysis and fermentation liquid, the 2-3% cycloheptaamyloses equivalent to flower glue weight are added, under the conditions of temperature is 60-70 DEG C
25-35min is reacted, flower glue enzymolysis liquid after deodorization is made in filtering.
8. a kind of preparation method of flower of Panax ginseng glue drink according to claim 3, it is characterised in that described auxiliary in step (4)
Material includes white granulated sugar and resistant dextrin.
9. a kind of preparation method of flower of Panax ginseng glue drink according to claim 8, it is characterised in that the step (4) includes：
Ginseng extract, herbal extract are mixed with flower glue enzymolysis liquid after deodorization, water is added, adds white granulated sugar and resistant dextrin is molten
Liquid, dissolving, filtering, packing.
10. a kind of preparation method of flower of Panax ginseng glue drink according to claim 9, it is characterised in that described in step (4)
The preparation method of resistant dextrin solution, including the water that resistant dextrin is added into 65-75 DEG C dissolves, filtering.
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| CN115211562A (en) * | 2022-08-07 | 2022-10-21 | 南京中医药大学 | Traditional Chinese medicine flower gel composition for maintaining beauty and keeping young and preparation method thereof |
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Application publication date: 20171020 |
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