CN107235704A - A kind of preparation method of big ball mud underglaze colour high-temperature double-layer cup - Google Patents

A kind of preparation method of big ball mud underglaze colour high-temperature double-layer cup Download PDF

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Publication number
CN107235704A
CN107235704A CN201710465094.3A CN201710465094A CN107235704A CN 107235704 A CN107235704 A CN 107235704A CN 201710465094 A CN201710465094 A CN 201710465094A CN 107235704 A CN107235704 A CN 107235704A
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cup
mud
glaze
double layer
temperature
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CN201710465094.3A
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CN107235704B (en
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滕召华
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Hunan Dague Clay Porcelain Art Group Co ltd
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Hunan Great Qiu Nici Skill Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/04Clay; Kaolin
    • AHUMAN NECESSITIES
    • A47FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47GHOUSEHOLD OR TABLE EQUIPMENT
    • A47G19/00Table service
    • A47G19/22Drinking vessels or saucers used for table service
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B1/00Producing shaped prefabricated articles from the material
    • B28B1/26Producing shaped prefabricated articles from the material by slip-casting, i.e. by casting a suspension or dispersion of the material in a liquid-absorbent or porous mould, the liquid being allowed to soak into or pass through the walls of the mould; Moulds therefor ; specially for manufacturing articles starting from a ceramic slip; Moulds therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B11/00Apparatus or processes for treating or working the shaped or preshaped articles
    • B28B11/001Applying decorations on shaped articles, e.g. by painting
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B11/00Apparatus or processes for treating or working the shaped or preshaped articles
    • B28B11/04Apparatus or processes for treating or working the shaped or preshaped articles for coating or applying engobing layers
    • B28B11/044Apparatus or processes for treating or working the shaped or preshaped articles for coating or applying engobing layers with glaze or engobe or enamel or varnish
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B3/00Producing shaped articles from the material by using presses; Presses specially adapted therefor
    • B28B3/12Producing shaped articles from the material by using presses; Presses specially adapted therefor wherein one or more rollers exert pressure on the material
    • B28B3/123Producing shaped articles from the material by using presses; Presses specially adapted therefor wherein one or more rollers exert pressure on the material on material in moulds or on moulding surfaces moving continuously underneath or between the rollers, e.g. on an endless belt
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/24Manufacture of porcelain or white ware
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/28Slip casting
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3418Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • C04B2235/3463Alumino-silicates other than clay, e.g. mullite
    • C04B2235/3472Alkali metal alumino-silicates other than clay, e.g. spodumene, alkali feldspars such as albite or orthoclase, micas such as muscovite, zeolites such as natrolite

Abstract

The present invention provides a kind of preparation method of big ball mud underglaze colour high-temperature double-layer cup, comprises the following steps:The first step, making moulded pottery not yet put in a kiln to bake and glaze;Second step, making outer cup cup body, cup lid, interior cup, cup handle and cup lid top;Colored drawing operation is carried out after interior cup moulded pottery not yet put in a kiln to bake shaping;Complete Double layer cup moulded pottery not yet put in a kiln to bake is made again after the completion of 3rd step, the operation of interior cup colored drawing;4th step, obtained Double layer cup mud biscuit;5th step, the obtained Double layer cup base with outer glaze layer;6th step, obtained Double layer cup glaze biscuit;7th step, the obtained Double layer cup base with picture;8th step, the Double layer cup base that colored drawing glaze spraying is made;9th step, obtained Double layer cup first product;Tenth step, obtained Double layer cup finished product.Using the preparation method of the present invention, can produce with exquisite sparkling and crystal-clear moist, with more preferably robustness and brilliance the resistance to chilling of bright, glaze generous, bright in colour, emergency heat and cooling property resistance, resistance to anti-impact force, it is non-friable, environmentally friendly, be not only incubated but it is heat-insulated the features such as double-layer ceramic cup.

Description

A kind of preparation method of big ball mud underglaze colour high-temperature double-layer cup
Technical field
The present invention relates to technical field of ceramic technology, especially, it is related to a kind of system of big ball mud underglaze colour high-temperature double-layer cup Make method.
Background technology
The history of porcelain, of long standing and well established in China, from ancient times to the present, China has been handed down many ceramic fine work and skill.
The preparation method of ceramic cup has a variety of in the prior art, as follows:
The patent application of Application No. 201510673391.8 discloses a kind of ceramic cup of hanging cup and ceramic cup handle one Body firing process, the hanging cup includes cup, handle and base, and the cup is connected and cup and bottom by handle with base Gap is left between seat, firing process includes making hanging cup, making and mounting bracket successively, applies last layer antitack agent, drying, element Burning, glazing, burn till.
The patent of invention of Application No. 201210041991.9 discloses a kind of ceramic cup and its production technology with glass holder, Including cup and glass holder.The production technology of the described ceramic cup with glass holder, comprises the following steps:Cup is made in ceramic material Body, and to upper cup body and cup inner surface glazing, be then fired in kiln;In the bottom of cup groove glue baked Affix sheet metal;Glue is done, and sheet metal is fixed on after bottom of cup groove, the cushion rubber in upper cup body and lower cup body contact position set, then Put glass holder;Glass holder and cushion rubber are clinged, align the raised screw hole of sheet metal and the screw hole of glass holder bottom, uses a screw locking It is fixed;Polyurethanes filler is filled with toward any through hole in glass holder bottom, is foamed;The heelpiece on glass holder bottom outer set.
The patent of invention of Application No. 201010140107.8 discloses a kind of manufacture craft of ceramic vacuum thermos cup, bag Include following processing step:Ceramic material is made to the cup body of thermos cup, cup body is divided into interior cup and outer cup;Then it is fired, Bottom is heated to from the top of cup body in 90~120 minutes, while temperature rises to 350~400 DEG C;When reaching 350~400 DEG C Stop heating, temperature is reduced by 20~50 DEG C, then keep temperature 10~25 minutes;Finally it is again heated to 1200~1300 DEG C Fire 7~9 hours, semi-finished product are made;Semi-finished product progress polishing is scraped and air-dried again, glazing then is carried out to cup body, and It is fired at a temperature of 1050~1150 DEG C 5.5~7.5 hours, the cup body of the present invention is made.
In addition, other techniques make ceramic cup, but existing process can not produce exquisite generous, color and luster Bright-coloured sparkling and crystal-clear moist, with more preferably robustness and brilliance the resistance to chilling of bright, glaze, emergency heat and cooling property resistance, resistance to anti-impact force, it is difficult It is broken, environmentally friendly, be not only incubated but it is heat-insulated the features such as double-layer ceramic cup.
Therefore, a kind of method that double-layer ceramic cup can be made is designed significant.
The content of the invention
Being made it is an object of the invention to provide one kind has the sparkling and crystal-clear moist, tool of exquisite bright, glaze generous, bright in colour Have more preferably robustness and remarkable resistance to chilling, emergency heat and cooling property resistance, resistance to anti-impact force, it is non-friable, environmentally friendly, be not only incubated but it is heat-insulated the features such as Double-layer ceramic cup method, concrete technical scheme is as follows:
A kind of preparation method of big ball mud underglaze colour high-temperature double-layer cup, comprises the following steps:
The first step, making moulded pottery not yet put in a kiln to bake and glaze, be specifically:It will contain big ball mud 35-45%, kaolin in terms of mass fraction Moulded pottery not yet put in a kiln to bake is made in 25-30%, potassium feldspar 15-25%, quartz 15-25% pug;By feldspar 55-60%, cunning in terms of mass fraction Glaze is made in stone 10-15%, quartz 25-35% and clay 5-8%;
Second step, making outer cup cup body, cup lid, interior cup, cup handle and cup lid top;Colored drawing behaviour is carried out after interior cup moulded pottery not yet put in a kiln to bake shaping Make;
Complete Double layer cup moulded pottery not yet put in a kiln to bake is made again after the completion of 3rd step, the operation of interior cup colored drawing;
4th step, first time biscuiting will be carried out after the smart base of Double layer cup moulded pottery not yet put in a kiln to bake obtained by the 3rd step, and be subsequently cooled to room temperature, obtain Double layer cup mud biscuit;
5th step, will Double layer cup mud biscuit outer surface immersion the first step in glaze in carry out nature absorption, obtain Double layer cup base with outer glaze layer;
6th step, by with outer glaze layer Double layer cup base carry out second of biscuiting, be cooled to room temperature, obtain Double layer cup glaze element Sintering briquette;
7th step, Double layer cup glaze biscuit is subjected to glaze in upper, after picture creation is carried out to outer cup, obtain with picture Double layer cup base;
8th step, the glaze that will be sprayed on the picture of the Double layer cup base with picture in the first step, form glaze layer, obtain coloured silk Paint the Double layer cup base of glaze spraying;
9th step, the Double layer cup base of colored drawing glaze spraying is subjected to high temperature burnt till, be cooled to room temperature, obtain Double layer cup first product;
Tenth step, by Double layer cup first product carry out reclaim;Double layer cup first product after reclaim is subjected to the multiple fire of high temperature, room is cooled to Temperature, produces Double layer cup finished product.
Preferred in above technical scheme, second step is specifically:Mud bar has been taken according to outer cup specification, thickness degree, Outer cup cup body and cover are made using roll forming legal system, interior cup, cup handle and cup lid top are made using slip casting;
Mud bar is specifically:Tissue is uniform, fine and smooth, no visible foreign;Mass percent shared by moisture is less than or equal to 26%.
Preferred in above technical scheme, the process for making outer cup cup body and cup lid using roll forming legal system is specifically: Whether a1, the vacuum for checking pug, moisture reach blank forming requirement;A2, that the mud bar perfected cut into 250g is important Mud sticks together, and then by remaining mud bar good seal, prevents secondary pollution;A3, Jiang Nituo are put into wheel mould, and start machine passes through The quick revolving-rolling of machine milled head is into base substrate;A4, blank forming take base i.e. in the mould of outer cup cup body mould and cup lid Obtain outer cup cup body and cover.
It is preferred in above technical scheme, using slip casting make in cup, cup and cup lid top be specifically:b1、 Check the mobility and fineness of mud;Inside and outside b2, cleaning mould;B3, by model by fan close to getting up, leave no gaps and tie up jail Gu;B4, the slurry in mud cylinder stirred well even, obtain the mud that Baume concentration is 50-55 degree;B5, mud sieved, except iron, it is ensured that Free from admixture in mud;B6, the interior cup model that the mud injection being sieved excessively is got togather, cup are noted in model and cup lid backform type By on model placing rotary disk after the completion of slurry, and several circles are gently rotated, exclude bubble;After slip casting two hours, base is taken to produce interior cup, cup And cup lid top.
Preferred in above technical scheme, making complete Double layer cup moulded pottery not yet put in a kiln to bake in the 3rd step is specifically:Use joint Mud, which is manually operated, turns into an overall cup body by outer cup cup body is Nian Jie with interior cup, after again by overall cup body and cup, cup lid with And cup lid jacking row bonding;
The sticking clay is made up of mud, and the mud includes big ball mud 70-80%, feldspar 5- in terms of mass fraction 15%th, talcum 5-10%, quartz 5-15% and stone flour 5-10%.
Preferred in above technical scheme, the first time biscuiting is specifically:770 DEG C -820 DEG C, burning are increased to by room temperature It it is 5-6 hours into the cycle;
Second of biscuiting be specifically:770 DEG C -820 DEG C are increased to by room temperature, firing period is 5-6 hours;
The high temperature is burnt till specifically:1370 DEG C -1400 DEG C are increased to by room temperature;25-35 is incubated under the conditions of 1400 DEG C Minute;Firing period is 15-16 hours;
Fire is specifically the high temperature again:1350 DEG C -1380 DEG C are increased to by room temperature;25-35 is incubated under the conditions of 1380 DEG C Minute;Firing period is 13-14 hours.
Preferred in above technical scheme, the Baume concentration of the glaze is 39-43 degree.
Preferred in above technical scheme, the burning decrement of the big ball mud is 12.0%-14.0%, and it is with mass fraction Meter includes following Main chemical component:SiO2For 48.76%, Al2O3For 36.94%, Fe2O3Be 0.86% for 0.09%, CaO, MgO is 0.08%, K2O is 0.25%, Na2O is 0.42%, TiO2For 0.04%.
Preferred in above technical scheme, the burning decrement of the glaze is 1.5%-2%, and it is included in terms of mass fraction Following Main chemical component:SiO2For 73-75%, Al2O3For 13-14%, Fe2O3For 0.05-0.1%, CaO be 1-1.5%, MgO is 4-5%, K2O is 4-5%, Na2O is 3-4%.It is preferred in above technical scheme, in the 9th step and the tenth step Room temperature is cooled to for Temperature fall, temperature fall time is 20-26 hours.
The present invention makes two with small one and large one moulded pottery not yet put in a kiln to bake of device shape respectively using roll forming method and slip casting, by creating Make to admire design and creation including great master elder generation on cup moulded pottery not yet put in a kiln to bake, chisel and carve meticulously, be then bonded two glasss in the case of base substrate is undried Into an entirety;After after biscuiting, then by creation great master created in outer cup after formed through high-temperature firing, one integral piece works are big It is also extremely strong to poikilothermism while big reduction cup body thermal conductivity, it is difficult explosion;Skill is made by consummate bonding Skill, inside cup presented with being painted in outer cup, even more and the different visual impact of common one cup;Its manufacture craft The consummate exquisiteness in conjunction with big ball mud porcelain, the extremely strong characteristic of the soft and translucency of whiteness, even more present with it is common single The unusual visual enjoyment of cup, is the fashion production that a great scientific and technological content is combined with artistic taste, sight with practicality Product, this glass is not only the optimal tea set that drinking-water is made tea, and great sight.
In addition to objects, features and advantages described above, the present invention also has other objects, features and advantages. Below with reference to embodiment, the present invention is further detailed explanation.
Embodiment
Embodiments of the invention are described in detail with reference to embodiments, but the present invention can be according to claim Limit and the multitude of different ways of covering is implemented.
Embodiment 1:
A kind of big ball mud underglaze colour high-temperature double-layer cup manufacture craft, comprises the following steps:
The first step, making moulded pottery not yet put in a kiln to bake and glaze, be specifically:In terms of mass fraction by containing big ball mud contain big ball mud 40%, Moulded pottery not yet put in a kiln to bake is made in kaolin 28%, potassium feldspar 16%, the pug of quartz 16%, and the burning decrement (LOI) of the big ball mud is 12.5%, it, which is calculated in mass percent the Main chemical component included, is:SiO2For 48.76%, Al2O3For 36.94%, Fe2O3 It is that 0.86%, MgO is 0.08%, K for 0.09%, CaO2O is 0.25%, Na2O is 0.42%, TiO2For 0.04%.
Glaze is made by feldspar 58%, talcum 12%, quartz 25% and clay 5% in terms of mass fraction.The glaze Baume concentration be 39 degree, the burning decrement (LOI) of the glaze is 1.5%, and it is calculated in mass percent mainization included Learning component is:SiO2For 74%, Al2O3For 13%, Fe2O3It is that 1.2%, MgO is 4.5%, K for 0.05%, CaO2O be 4.5%, Na2O is 3.5%.
Second step, making outer cup cup body, cup lid, interior cup, cup handle and cup lid top, be specifically:According to the specification chi of outer cup Very little, thickness degree has taken mud bar, and outer cup cup body and cup lid are made using roll forming legal system, makes interior using slip casting Cup, cup handle and cup lid top, wherein:
The process for making outer cup cup body and cup lid using roll forming legal system is specifically:A1, the vacuum for checking pug, water Divide and whether reach blank forming requirement;A2, the mud bar perfected is cut into the important mud of 250g sticked together, then seal remaining mud bar It is good, prevent secondary pollution;A3, Jiang Nituo are put into wheel mould, start machine, by the quick revolving-rolling of machine milled head into Base substrate;A4, blank forming take base to produce outer cup cup body and cover in the mould of outer cup cup body mould and cup lid.
Making interior cup, cup handle and cup lid top using slip casting is specifically:B1, the mobility for checking mud and thin Degree;Inside and outside b2, cleaning mould;B3, model closed to getting up by fan, leave no gaps and tie up firmly;B4, the slurry in mud cylinder stirred Uniformly, the mud that Baume concentration is 50-55 degree is obtained;B5, mud sieved, except iron, it is ensured that free from admixture in mud;B6, mistake The mud being sieved injects the interior cup model got togather, cup in model and cup lid backform type, turns model placement after the completion of slip casting On disk, and several circles (3-6 circles) are gently rotated, exclude bubble;After slip casting two hours, base is taken to produce interior cup, cup handle and cup lid top. Colored drawing operation is carried out after interior cup moulded pottery not yet put in a kiln to bake shaping.
Complete Double layer cup moulded pottery not yet put in a kiln to bake is made again after the completion of 3rd step, the operation of interior cup colored drawing, is specifically:Handled using sticking clay Work operation turns into an overall cup body by outer cup cup body is Nian Jie with interior cup, after again by overall cup body and cup, cup lid and cup lid Jacking row is bonded.Painted at once after the completion of bonding, it is therefore intended that:Its interior cup moulded pottery not yet put in a kiln to bake is kept abundant humidity, thus reach with Humidity when outer cup moulded pottery not yet put in a kiln to bake is bonded is consistent, shrink consistent, finally realizes the sintering qualified rate of product.The sticking clay passes through mud Slurry is made, and the mud includes big ball mud 70%, feldspar 8%, talcum 6%, quartz 8% and stone flour 8% in terms of mass fraction.
4th step, (smooth to its surface) after the smart base of Double layer cup moulded pottery not yet put in a kiln to bake obtained by the 3rd step is put into kiln carried out for the first time Biscuiting, is subsequently cooled to room temperature, obtains Double layer cup mud biscuit.First time biscuiting is specifically:770 DEG C, burning are increased to by room temperature It it is 5 hours into the cycle.
5th step, will Double layer cup mud biscuit outer surface immersion the first step in glaze in carry out nature absorption, formed Glaze layer thick 0.3mm, obtains the Double layer cup base with outer glaze layer.
6th step, the Double layer cup base with outer glaze layer is put into kiln carries out second of biscuiting, be cooled to room temperature, obtain Double layer cup glaze biscuit.Second of biscuiting be specifically:770 DEG C are increased to by room temperature, firing period is 5 hours.
7th step, Double layer cup glaze biscuit is subjected to glaze in upper, after picture creation is carried out to outer cup, obtain with picture Double layer cup base, be specifically:Double layer cup base with outer glaze layer is stood upside down and places foot-operated glazing machine " tap " middle position implementation Spray in glaze, after glaze flows to end, from " tap " middle position remove blank removing corner more than glaze;Qualified blank is delivered into skill afterwards Art colored drawing portion carries out picture creation to outer cup.
8th step, the glaze that will be sprayed on the picture of the Double layer cup base with picture in the first step, form 0.05mm thickness Glaze layer, obtains the Double layer cup base of colored drawing glaze spraying.
9th step, by the Double layer cup base of colored drawing glaze spraying be put into kiln carry out high temperature burn till, be cooled to room temperature, obtain bilayer Cup first product, wherein:High temperature is burnt till specifically:1370 DEG C -1380 DEG C are increased to by room temperature, 30 minutes are incubated;Firing period is 15 Hour;Temperature fall is cooled to, temperature fall time is 24 hours.
Tenth step, Double layer cup first product is subjected to reclaim (be usually by its peristoma carry out reclaim);By the Double layer cup after reclaim First product, which is put into kiln, carries out the multiple fire of high temperature, is cooled to room temperature (temperature fall time is 24 hours), produces Double layer cup product, wherein: Fire is specifically high temperature again:1350 DEG C -1380 DEG C are increased to by room temperature, 25-35 minutes are incubated;Firing period is 13-14 hours.
The big ball mud Double layer cup made using above-mentioned steps is in not only the sparkling and crystal-clear moist, porcelain of specious generous, glaze is white General blue or green, the vivid aestheticism of picture, and it is both environmentally friendly, and heat-insulation and heat-preservation, the pearl connection wall conjunction of its quality and picture, not only with high-end Scientific and technological content and artistic taste, and be the trendy product that a great sight is combined with practicality.
Double layer cup product obtained by this implementation passes through the heat stability testing under the conditions of 20 DEG C -180 DEG C.
Embodiment 2-3:
Embodiment 2-3 difference from Example 1 is only that table 1.
Double layer cup product obtained by embodiment 2-3 passes through the heat stability testing under the conditions of 20 DEG C -180 DEG C.
The manufacture craft parametric statistics table of comparisons of 1 embodiment 1- embodiments of table 3
Porcelain cup is mostly individual layer on the market, and existing Double layer cup is also commonly cup in metal and is combined with porcelain outer cup, is led to Cross colloid filler interior cup is Nian Jie with outer cup filling as an entirety, because colloid filler is when meeting high temperature, have one Fixed chemical analysis is discharged, so simultaneously not environmentally.And the interior cup and outer cup and bonding sticking clay of the Double layer cup of the present invention Be made using the top rare big ball mud of raw material, it is not only environmentally friendly, and the resistance to chilling than common list porcelain cup, emergency heat and cooling property resistance, Resistance to anti-impact force will get well, and insulation, effect of heat insulation will be more preferably.Picture on cup including particularly, passes through penetrating, gentle porcelain and reflects It is even more out the enjoyment for giving U.S..
The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, for the skill of this area For art personnel, the present invention can have various modifications and variations.Within the spirit and principles of the invention, that is made any repaiies Change, equivalent substitution, improvement etc., should be included in the scope of the protection.

Claims (10)

1. a kind of preparation method of big ball mud underglaze colour high-temperature double-layer cup, it is characterised in that:Comprise the following steps:
The first step, making moulded pottery not yet put in a kiln to bake and glaze, be specifically:It will contain big ball mud 35-45%, kaolin 25- in terms of mass fraction 30%th, moulded pottery not yet put in a kiln to bake is made in potassium feldspar 15-25%, quartz 15-25% pug;By feldspar 55-60%, talcum in terms of mass fraction Glaze is made in 10-15%, quartz 25-35% and clay 5-8%;
Second step, making outer cup cup body, cup lid, interior cup, cup handle and cup lid top;Colored drawing operation is carried out after interior cup moulded pottery not yet put in a kiln to bake shaping;
Complete Double layer cup moulded pottery not yet put in a kiln to bake is made again after the completion of 3rd step, the operation of interior cup colored drawing;
4th step, first time biscuiting will be carried out after the smart base of Double layer cup moulded pottery not yet put in a kiln to bake obtained by the 3rd step, and be subsequently cooled to room temperature, obtain bilayer Cup mud biscuit;
5th step, will Double layer cup mud biscuit outer surface immersion the first step in glaze in carry out nature absorption, carried The Double layer cup base of outer glaze layer;
6th step, by with outer glaze layer Double layer cup base carry out second of biscuiting, be cooled to room temperature, obtain Double layer cup glaze biscuiting Base;
7th step, Double layer cup glaze biscuit is subjected to glaze in upper, after picture creation is carried out to outer cup, obtain the bilayer with picture Cup base;
8th step, the glaze that will be sprayed on the picture of the Double layer cup base with picture in the first step, form glaze layer, obtain colored drawing spray The Double layer cup base of glaze;
9th step, the Double layer cup base of colored drawing glaze spraying is subjected to high temperature burnt till, be cooled to room temperature, obtain Double layer cup first product;
Tenth step, by Double layer cup first product carry out reclaim;Double layer cup first product after reclaim is subjected to the multiple fire of high temperature, room temperature is cooled to, Produce Double layer cup finished product.
2. the preparation method of big ball mud underglaze colour high-temperature double-layer cup according to claim 1, it is characterised in that:Described second Step is specifically:Mud bar has been taken according to the specification of outer cup, thickness degree, outer cup cup body and cup are made using roll forming legal system Lid, interior cup, cup handle and cup lid top are made using slip casting;
The mud bar is specifically:Tissue is uniform, fine and smooth, no visible foreign;Mass percent shared by moisture is less than or equal to 26%.
3. the preparation method of big ball mud underglaze colour high-temperature double-layer cup according to claim 2, it is characterised in that:Using rolling The method of forming makes outer cup cup body and the process of cup lid is specifically:A1, check the vacuum of pug, moisture whether reach blank into Type requirement;A2, the mud bar perfected is cut into the important mud of 250g sticked together, then by remaining mud bar good seal, prevent secondary pollution; A3, Jiang Nituo are put into wheel mould, start machine, by the quick revolving-rolling of machine milled head into base substrate;A4, blank forming In in the mould of outer cup cup body mould and cup lid, base is taken to produce outer cup cup body and cover.
4. the preparation method of big ball mud underglaze colour high-temperature double-layer cup according to claim 2, it is characterised in that:Using slip casting The method of forming makes interior cup, cup handle and cup lid top:B1, the mobility and fineness for checking mud;In b2, cleaning mould Outside;B3, model closed to getting up by fan, leave no gaps and tie up firmly;B4, the slurry in mud cylinder stirred well even, obtain Baume dense Spend for the mud of 50-55 degree;B5, mud sieved, except iron, it is ensured that free from admixture in mud;B6, the mud that mistake is sieved inject and closed Good interior cup model, cup by model placing rotary disk after the completion of slip casting, and are gently rotated several in model and cup lid backform type Circle, excludes bubble;After slip casting two hours, base is taken to produce interior cup, cup handle and cup lid top.
5. the preparation method of big ball mud underglaze colour high-temperature double-layer cup according to claim 1, it is characterised in that:Described 3rd Complete Double layer cup moulded pottery not yet put in a kiln to bake is made in step is specifically:Manually operated using sticking clay outer cup cup body is Nian Jie with interior cup as one Individual overall cup body, after it is again that overall cup body and cup is Nian Jie, cup lid and cup lid jacking row;
The sticking clay is made up of mud, the mud in terms of mass fraction comprising big ball mud 70-80%, feldspar 5-15%, Talcum 5-10%, quartz 5-15% and stone flour 5-10%.
6. the preparation method of the big ball mud underglaze colour high-temperature double-layer cup according to claim 1-5 any one, its feature exists In:The first time biscuiting is specifically:770 DEG C -820 DEG C are increased to by room temperature, firing period is 5-6 hours;
Second of biscuiting be specifically:770 DEG C -820 DEG C are increased to by room temperature, firing period is 5-6 hours;
The high temperature is burnt till specifically:1370 DEG C -1400 DEG C are increased to by room temperature, 25-35 minutes are incubated;Firing period is 15- 16 hours;
Fire is specifically the high temperature again:1350 DEG C -1380 DEG C are increased to by room temperature, 25-35 minutes are incubated;Firing period is 13- 14 hours.
7. the preparation method of big ball mud underglaze colour high-temperature double-layer cup according to claim 6, it is characterised in that:The glaze Baume concentration be 39-43 degree.
8. the preparation method of big ball mud underglaze colour high-temperature double-layer cup according to claim 6, it is characterised in that:The big ball The burning decrement of mud is 12.0%-14.0%, and it includes following Main chemical component in terms of mass fraction:SiO2For 48.76%, Al2O3For 36.94%, Fe2O3It is that 0.86%, MgO is 0.08%, K for 0.09%, CaO2O is 0.25%, Na2O be 0.42%, TiO2For 0.04%.
9. the preparation method of big ball mud underglaze colour high-temperature double-layer cup according to claim 6, it is characterised in that:The glaze Burning decrement be 1.5%-2%, its in terms of mass fraction include following Main chemical component:SiO2For 73-75%, Al2O3For 13-14%, Fe2O3It is that 1-1.5%, MgO are 4-5%, K for 0.05-0.1%, CaO2O is 4-5%, Na2O is 3-4%.
10. the preparation method of big ball mud underglaze colour high-temperature double-layer cup according to claim 6, it is characterised in that:Described Room temperature is cooled to for Temperature fall in nine steps and the tenth step, and temperature fall time is 20-26 hours.
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CN108164248A (en) * 2018-01-09 2018-06-15 湖南大球泥瓷艺有限公司 A kind of production method of porcelain plate
CN108298954A (en) * 2018-03-02 2018-07-20 徐林燕 A kind of ceramic preparation method flow
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CN111892386A (en) * 2020-08-21 2020-11-06 湖南大球泥瓷艺有限公司 Method for manufacturing high-temperature large-block embossed porcelain plate
CN112062541A (en) * 2020-09-07 2020-12-11 福建泉州顺美集团有限责任公司 White porcelain wine cup and integrated manufacturing process thereof
CN112336142A (en) * 2020-09-30 2021-02-09 湖南省醴陵市环宇陶瓷实业有限公司 Ceramic round-bottom cup and production and manufacturing process
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CN109704738A (en) * 2017-10-26 2019-05-03 湖南省醴陵市创客中小企业服务中心有限公司 A kind of heat-insulating ceramic cup and its processing technology with handle
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CN111892386A (en) * 2020-08-21 2020-11-06 湖南大球泥瓷艺有限公司 Method for manufacturing high-temperature large-block embossed porcelain plate
CN111892386B (en) * 2020-08-21 2022-04-22 湖南大球泥瓷艺有限公司 Method for manufacturing high-temperature large-block embossed porcelain plate
CN112062541A (en) * 2020-09-07 2020-12-11 福建泉州顺美集团有限责任公司 White porcelain wine cup and integrated manufacturing process thereof
CN112336142A (en) * 2020-09-30 2021-02-09 湖南省醴陵市环宇陶瓷实业有限公司 Ceramic round-bottom cup and production and manufacturing process
CN114349474A (en) * 2022-01-27 2022-04-15 南平市建阳区紫玉瓯茶盏文化传播有限公司 Regenerated building cup and manufacturing method thereof

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