CN105801176A - Once-fired metal glaze surface deep-processing method - Google Patents

Once-fired metal glaze surface deep-processing method Download PDF

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CN105801176A
CN105801176A CN201610147996.8A CN201610147996A CN105801176A CN 105801176 A CN105801176 A CN 105801176A CN 201610147996 A CN201610147996 A CN 201610147996A CN 105801176 A CN105801176 A CN 105801176A
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glaze
once
metal glaze
working method
printing
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CN105801176B (en
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范柏良
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FOSHAN CITY SANSHUI KAILELAI CRAFT PRODUCT Co Ltd
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FOSHAN CITY SANSHUI KAILELAI CRAFT PRODUCT Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81—Coating or impregnation
    • C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/14—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201—Alkali metal oxides or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3206—Magnesium oxides or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/327—Iron group oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3272—Iron oxides or oxide forming salts thereof, e.g. hematite, magnetite

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  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
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Abstract

The invention discloses a once-fired metal glaze surface deep-processing method.The method is characterized by comprising the following steps of 1, metal glaze making; 2, glaze spraying on the surface of a green body in a glaze throwing mode, wherein the thickness of a glaze material layer is controlled to range from 0.3 mm to 0.5 mm; 3, medium printing, wherein a layer of medium is printed through a screen mesh; 4, ink-jet printing or screen mesh and rubber roller printing; 5, mica sheet spraying, wherein the particle size of a mica sheet ranges from 10 meshes to 20 meshes; 6, convex glaze semi-polished layer printing, wherein a semi-polished material and a printing paste are mixed to be uniform, subjected to ball milling and then printed into a 70-90-mesh screen mesh which is thickened three times; 7, polishing, grading and packing, wherein after the sixth process is completed, the obtained product enters a kiln furnace to be fired, and the fired product is subjected to polishing, grading and packing.According to the once-fired metal glaze surface deep-processing method, operation is convenient, and the produced product is high in stereoscopic impression, attractive and elegant.

Description

Once burn metal glaze deep working method
Technical field
The present invention relates to Wall or floor tile production technical field, the metal glaze of a kind of ceramic tile adds Work method.
Background technology
Metal glaze is the special artistic glaze of the one in china industry glaze, mainly imposes on Antique Imitation Tiles ceramic tile On, also have on the Bottle & Can imposing on daily decorative ceramics, on vase or artistic porcelain.Such as Chinese patent application Number it is 200710035665.6, the manufacture method of invention entitled a kind of golden metal glaze material, It includes that formula dispensing makes frit ball milling and sieves operation.During glazing, control glazed thickness and exist About 0.15mm, enters in rapidity sintering roller kiln and fires in the oxidizing atmosphere of 1160～1200 DEG C After, prepare metal glaze face brick, there is certain metal effect.But, use this technique manufacture Metal glaze face brick to there is also metallic luster effect unsatisfactory, portioned product have rubescent, blackout is existing As, around medium, even have curling cracking phenomena, without problems such as third dimensions.
Summary of the invention
The one that the purpose of the present invention is contemplated to solve the deficiency of prior art and provides not only operates Simply, the resultant metal luster effect of preparation is good, the once burning metal glaze deep processing that third dimension is strong Method.
The present invention is to use following technical solution to be attained in that once burning metal glaze Deep working method, it is characterised in that it comprises the steps:
A, making metal glaze, the raw material of employing includes: Kaolin, Anhydrite, quartz and burning Thing, ball milling after being mixed by raw material, fineness controls at 0.4-0.6%；
B, using and get rid of the mode of glaze and drench glaze in billet surface, glaze layer THICKNESS CONTROL is at 0.3- 0.5mm；
C, print medium, by one layer of medium of screen printing, the raw material of employing include Anhydrite, Zirconium orthosilicate., Burning Talcum, overprint cream ball milling after certain proportion mixes, specific gravity control is at 1.55g/cm3- 1.60g/cm3；
D, inkjet printing or silk screen, rubber roll stamp；
E, spray mica sheet, the granule size of mica sheet is 10-20 mesh, by with print cream, water by than Example mixes, and uses the mode getting rid of glaze to be sprayed at equably and has printed or the brick surface of stamp；
F, printing convex glaze and partly throw layer, throw material and print cream mixing ball milling with half, specific gravity control is at 1.5- 1.7g/cm3, then print 70-90 mesh thickeies the silk screen of 3 times；
G, polishing classification packing, step f operation i.e. enters kiln after completing and burns till, product out It is polished classification packing.
Further illustrating as such scheme, in described step b, base substrate powder is imitative Old china material, temperature firing range is at 1150-1185 DEG C, and water absorption rate requires as 1-3%, its powder Composition: silicon dioxide 68-79%, aluminium sesquioxide 15-19%, iron sesquioxide 0.6-1.1%, Calcium oxide 0.7-0.9%, magnesium oxide 0.8-1.2%, potassium oxide 2.5-4%, sodium oxide 1.5-2.5%, Titanium dioxide 0.2-0.3%, igloss 3.8%, the percentage ratio sum of described composition is 100%.
Preferably, in described step b, base substrate powder is Imitative Ancient Porcelains material, and temperature is burnt till Scope is at 1150-1185 DEG C, and water absorption rate requires as 1-3%, its powder composition: silicon dioxide 70.16%, aluminium sesquioxide 17.91%, iron sesquioxide 0.96%, calcium oxide 0.86%, magnesium oxide 0.97%, potassium oxide 3.1%, sodium oxide 2.0%, titanium dioxide 0.24%, igloss 3.8%, described The percentage ratio sum of composition is 100%.
Further, described print cream be mainly composed of methyl, ethylene glycol and water.
Further, the firing temperature of described medium must be controlled well, and firing temperature controls 1160 1185 DEG C, if firing temperature is the lowest, metal glaze cover incessantly, produces co-melting, has rubescent, blackout Phenomenon, even has curling cracking phenomena around medium；If initial melting temperature is the highest, then burn not Ripe.
Further, in described step e, mica sheet is 0.5:10 with print cream, the ratio of water: 40。
Preferably, in described step f, specific gravity control is at 1.6g/cm3If proportion is too low, then Without third dimension, stick with paste net, stick into a piece of.
In described step g, the grinding head of polishing machine of polishing process uses the Pilus Caprae seu Ovis of 5 group of 2 head Wheel, mesh number is 1500-3000 mesh.
The present invention uses above-mentioned technical solution can reach to provide the benefit that:
The present invention uses the metal glaze of the matched expansion coefficient with base substrate, uses the mode getting rid of glaze to drench Glaze, and its thickness is strictly controlled, make metallic luster effect more preferable；Further, drenched By one layer of medium of screen printing after glaze, control the firing temperature of medium well, and once spray mica sheet and Print convex glaze and partly throw layer so that the third dimension of product is strong, more elegant in appearance.
Detailed description of the invention
Below in conjunction with specific embodiment, the technical program is explained in detail.
Embodiment 1
The present invention is once burning metal glaze deep working method, it is characterised in that it includes walking as follows Rapid:
A, making metal glaze, the raw material of employing includes: Kaolin, Anhydrite, quartz and burning Thing, ball milling after being mixed by raw material, fineness controls 0.4-0.6% (crossing 325 mesh sieves)；
B, using and get rid of the mode of glaze and drench glaze in billet surface, glaze layer THICKNESS CONTROL is at 0.3- 0.5mm, if glaze layer is the thickest or the thinnest, metallic luster effect is the most undesirable；
C, print medium, by one layer of medium of screen printing, the raw material of employing include Anhydrite, Zirconium orthosilicate., Burning Talcum, overprint cream ball milling after certain proportion mixes, specific gravity control is at 1.55g/cm3- 1.60g/cm3；The firing temperature of medium must be controlled well, if initial melting temperature is the lowest, metal glaze cover is not Live, produce co-melting, have rubescent, blackout phenomenon, around medium, even have curling cracking existing As；If initial melting temperature is the highest, then burn not yet done；
D, inkjet printing or silk screen, rubber roll stamp；This operation depends on the performance of medium, and medium is wanted Meet the color development of ink, if the ink color development of certain color is poor or sends out outstanding, to whole pattern Will be impacted, and design aspect is also had great limitation；The most just Can only be with silk screen, roller printing or changing medium solves；
E, spray mica sheet, the granule size of mica sheet is 10-20 mesh, by with print cream, water by than Example mixes, and uses the mode getting rid of glaze to be sprayed at equably and has printed or the brick surface of stamp；
F, printing convex glaze and partly throw layer, throw material and print cream mixing ball milling with half, specific gravity control exists 1.6g/cm3If proportion is too low, then without third dimension, stick with paste net, stick into a piece of, then print 70-90 Mesh thickeies the silk screen of 3 times；
G, polishing classification packing, step f operation i.e. enters kiln after completing and burns till, product out It is polished classification packing.
In described step b, base substrate powder is Imitative Ancient Porcelains material, and temperature firing range exists 1150-1185 DEG C, water absorption rate requires as 1-3%, its powder composition: silicon dioxide 70.16%, three Al 2 O 17.91%, iron sesquioxide 0.96%, calcium oxide 0.86%, magnesium oxide 0.97%, oxygen Change potassium 3.1%, sodium oxide 2.0%, titanium dioxide 0.24%, igloss 3.8%, the percentage of described composition It is 100% than sum.The performance of metal glaze need to meet above-mentioned technological parameter, and will swollen with base substrate Swollen coefficient matches, and the biggest or the least flatness being all unfavorable for adobe, the biggest adobe is curved, the least Adobe is stuck up.
Further, described print cream be mainly composed of methyl, ethylene glycol and water；Described medium Firing temperature must be controlled well, and initial melting temperature controls at 1,160 1185 DEG C, in described step e, Mica sheet is 0.5:10:40 with print cream, the ratio of water.In described step g, polishing process Grinding head of polishing machine use the Pilus Caprae seu Ovis of 5 group of 2 head to take turns, mesh number is 1500-3000 mesh.
Embodiment 2
In the present embodiment, in described step b, base substrate powder is Imitative Ancient Porcelains material, its powder Material composition: silicon dioxide 72.2%, aluminium sesquioxide 15.8%, iron sesquioxide 0.88%, oxidation Calcium 0.79%, magnesium oxide 0.9%, potassium oxide 3.4%, sodium oxide 1.98%, titanium dioxide 0.25%, Igloss 3.8%, the percentage ratio sum of described composition is 100%.
The technical program compared with prior art, uses the metal with the matched expansion coefficient of base substrate Glaze, uses the mode getting rid of glaze to drench glaze, and strictly controls its thickness, make metallic luster effect More preferable；Further, having drenched after glaze by one layer of medium of screen printing, that controls medium well burns till temperature Degree, and once spray mica sheet and the convex glaze of print partly throw layer so that the third dimension of product is strong, more attractive in appearance Generous.
Above-described is only the preferred embodiment of the present invention, it is noted that for this area For those of ordinary skill, without departing from the concept of the premise of the invention, it is also possible to if making Dry deformation and improvement, these broadly fall into protection scope of the present invention.

Claims (8)

  1. The most once burn metal glaze deep working method, it is characterised in that it comprises the steps:
    A, making metal glaze, the raw material of employing includes: Kaolin, Anhydrite, quartz and burning Thing, ball milling after being mixed by raw material, fineness controls at 0.4-0.6%；
    B, using and get rid of the mode of glaze and drench glaze in billet surface, glaze layer THICKNESS CONTROL is at 0.3- 0.5mm；
    C, print medium, by one layer of medium of screen printing, the raw material of employing include Anhydrite, Zirconium orthosilicate., Burning Talcum, overprint cream ball milling after certain proportion mixes, specific gravity control is at 1.55g/cm3- 1.60g/cm3；
    D, inkjet printing or silk screen, rubber roll stamp；
    E, spray mica sheet, the granule size of mica sheet is 10-20 mesh, by with print cream, water by than Example mixes, and uses the mode getting rid of glaze to be sprayed at equably and has printed or the brick surface of stamp；
    F, printing convex glaze and partly throw layer, throw material and print cream mixing ball milling with half, specific gravity control is at 1.4- 1.7g/cm3, then print 70-90 mesh thickeies the silk screen of 3 times；
    G, polishing classification packing, step f operation i.e. enters kiln after completing and burns till, product out It is polished classification packing.
  2. Once burning metal glaze deep working method the most according to claim 1, its feature exists In, in described step b, base substrate powder is Imitative Ancient Porcelains material, and temperature firing range exists 1150-1185 DEG C, water absorption rate requires as 1-3%, its powder composition: silicon dioxide 68-79%, three Al 2 O 15-19%, iron sesquioxide 0.6-1.1%, calcium oxide 0.7-0.9%, magnesium oxide 0.8- 1.2%, potassium oxide 2.5-4%, sodium oxide 1.5-2.5%, titanium dioxide 0.2-0.3%, igloss 3.8%, the percentage ratio sum of described composition is 100%.
  3. Once burning metal glaze deep working method the most according to claim 1, its feature exists In, in described step b, base substrate powder is Imitative Ancient Porcelains material, and temperature firing range exists 1150-1185 DEG C, water absorption rate requires as 1-3%, its powder composition: silicon dioxide 70.16%, three Al 2 O 17.91%, iron sesquioxide 0.96%, calcium oxide 0.86%, magnesium oxide 0.97%, oxygen Change potassium 3.1%, sodium oxide 2.0%, titanium dioxide 0.24%, igloss 3.8%, the percentage of described composition It is 100% than sum.
  4. Once burning metal glaze deep working method the most according to claim 1, its feature exists It is mainly composed of methyl, ethylene glycol and water in, described print cream.
  5. Once burning metal glaze deep working method the most according to claim 1, its feature exists In, the firing temperature of described medium must be controlled well, and initial melting temperature controls at 1,160 1185 DEG C.
  6. Once burning metal glaze deep working method the most according to claim 1, its feature exists In, in described step e, mica sheet is 0.5:10:40 with print cream, the ratio of water.
  7. Once burning metal glaze deep working method the most according to claim 1, its feature exists In, in described step f, specific gravity control is at 1.6g/cm3。
  8. Once burning metal glaze deep working method the most according to claim 1, its feature exists In, in described step g, the grinding head of polishing machine of polishing process uses the Pilus Caprae seu Ovis of 5 group of 2 head Wheel, mesh number is 1500-3000 mesh.
CN201610147996.8A 2016-03-15 2016-03-15 It is primary to burn metal glaze paint deep working method Expired - Fee Related CN105801176B (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107382061A (en) * 2017-07-14 2017-11-24 东莞市唯美陶瓷工业园有限公司 A kind of anti-skidding glaze, anti-skid brick and preparation method thereof
CN107814587A (en) * 2017-09-22 2018-03-20 山东狮子王陶瓷科技有限公司 The preparation method of seven bright cloud ink stones
CN109456048A (en) * 2018-12-06 2019-03-12 佛山市玉矶材料科技有限公司 A kind of metal tile and preparation method thereof
CN114014698A (en) * 2021-10-26 2022-02-08 蒙娜丽莎集团股份有限公司 Flaky silver luster ceramic rock plate and preparation method thereof

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CN101654378A (en) * 2008-08-19 2010-02-24 郑水泉 Ceramic glaze pattern-glazed brick and production method thereof
CN102503566A (en) * 2011-10-12 2012-06-20 上海高诚艺术包装有限公司 Metal-like glaze as well as preparation method and using method thereof
CN103467134A (en) * 2012-06-06 2013-12-25 湖南泰鑫瓷业有限公司 Preparation method of beige high brightness metal glaze
CN103664236A (en) * 2013-12-18 2014-03-26 广东金意陶陶瓷有限公司 Metal fancy glaze as well as whole cast glaze ceramic tile with metal effect and production technology thereof
CN104446668A (en) * 2014-11-14 2015-03-25 佛山市三水凯利莱工艺制品有限公司 Production process of gold-plated brick

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Publication number Priority date Publication date Assignee Title
CN101654378A (en) * 2008-08-19 2010-02-24 郑水泉 Ceramic glaze pattern-glazed brick and production method thereof
CN102503566A (en) * 2011-10-12 2012-06-20 上海高诚艺术包装有限公司 Metal-like glaze as well as preparation method and using method thereof
CN103467134A (en) * 2012-06-06 2013-12-25 湖南泰鑫瓷业有限公司 Preparation method of beige high brightness metal glaze
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CN107382061A (en) * 2017-07-14 2017-11-24 东莞市唯美陶瓷工业园有限公司 A kind of anti-skidding glaze, anti-skid brick and preparation method thereof
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