CN107200638A - A kind of micro- charing marine alga is combined the preparation method of kaolin fleshiness anti-biotic material - Google Patents
A kind of micro- charing marine alga is combined the preparation method of kaolin fleshiness anti-biotic material Download PDFInfo
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- CN107200638A CN107200638A CN201710497667.0A CN201710497667A CN107200638A CN 107200638 A CN107200638 A CN 107200638A CN 201710497667 A CN201710497667 A CN 201710497667A CN 107200638 A CN107200638 A CN 107200638A
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- Prior art keywords
- charing
- micro
- marine alga
- kaolin
- fleshiness
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D1/00—Fertilisers containing potassium
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Inorganic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Molecular Biology (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses the preparation method that a kind of micro- charing marine alga is combined kaolin fleshiness anti-biotic material, using after marine alga crushing/dewatering then with hydrogenperoxide steam generator, after being reacted after sodium hydroxide regulation pH, after hydrochloric acid is neutralized after stirring to formation slurries, kaolin and starch are added into plant ash solution immersion simultaneously to be aged, bio-fermentation agent fermentation is added after centrifugal drying grinding and gained marine alga slurries are well mixed, it is then placed in high temperature furnace and is carried out the drying after the rear heating for dissolving such as urea using temperature change after micro- charing, granulation, by the material and clay of micro- charing, bamboo charcoal grain is mixed with and obtained, anti-biotic material prepared by the present invention, the nutriment of abundance can be provided for the growth of succulent by possessing the colleague of antibiotic property, improve survival rate, and material source is wide, cost is low.
Description
Technical field
The invention belongs to technical field of slow release fertilizer, and in particular to a kind of micro- charing marine alga is combined kaolin fleshiness anti-biotic material
Preparation method.
Background technology
Marine alga is the original producer of marine organisms, with powerful adsorption capacity, can concentrate equivalent to itself 44
Equilibrium is extremely enriched in ten thousand times of ocean material, nutrition.Contain protein, polysaccharide, food fiber, vitamin, inorganic member in marine alga
The materials such as element, amino acid, aliphatic acid, are all widely used in the field such as industry, agricultural, medicine, beauty, also with very high
Food therapy value.Alga fertilizer be it is a kind of using the production and processing of marine brown class or mix again a number of N P and K and in
A kind of fertilizer that trace element is processed.Using marine algae extract as the fertilizer of core substance, the production of crops can be significantly improved
Amount, and with certain resistant effect.Because the product comes from natural seaweed active component, the safe mass of agricultural product is being improved
Play an important roll.In marine algae extract in addition to containing organic nutrition and mineral nutrition composition, enhancing development is rich in again
Plant endogenous hormones, active material.Therefore alga fertilizer is considered as the fertilizer that forth generation updates, with wide development
Prospect.With the strict implement of national arable land policy, the administration of organic fertilizer is also increasingly paid attention to by governments at all levels.People's people's livelihood
Running water is flat to be improved constantly, and what high yield and high quality agricultural product and hygiene and health food had turned into current social and agricultural production urgent is essential
Ask.Nuisanceless green agricultural product are produced, scientifically fertilising, medication are maximally effective means.
In recent years, with the adjustment of agricultural planting structure, agriculture multiple crop index is improved constantly, the increase of crop yield,
China's agricultural infrastructure condition, crop allocation, planting system, fertilization structure, farming etc. there occurs larger change, soil nutrient
Larger change also occurs with farmland quality.Because soil bottom is unclear, blindly fertilising causes crop yield and quality to reduce, and applies
Fertile decline in benefits, farmland quality is degenerated, and corps diseases generally occur, and a large amount of N and P losses cause agricultural non-point source pollution to aggravate,
Some areas body eutrophication degree of progress speed, the deterioration of the ecological environment, overall agricultural productivity reduction seriously governs agriculture life
The sustainable development and raising of production.
The content of the invention
The present invention provides the preparation method that a kind of micro- charing marine alga is combined kaolin fleshiness anti-biotic material, prepared by the present invention
Anti-biotic material, the nutriment of abundance can be provided for the growth of succulent by possessing the colleague of antibiotic property, improve succulent
Survival rate, and material source is wide, cost is low.
The present invention is achieved by the following technical solutions：
A kind of micro- charing marine alga is combined the preparation method of kaolin fleshiness anti-biotic material, it is characterised in that comprise the following steps：
（1）The preparation of marine alga homogenate
Exposure under sunlight is placed in after 30-40 parts by weight marine alga is crushed, progress extrusion dehydration is standby, then adds 60-80 weight
In part hydrogenperoxide steam generator, pH is adjusted to 9-9.5 with 20-40% sodium hydroxides, 1-2 hours are stirred in 60-80 DEG C, after cooling extremely
After room temperature, the hydrochloric acid for then adding appropriate 10-40% be neutralized to after neutrality, and high-speed stirred is stand-by to being formed after slurries；
（2）Fermentation reactor system
The kaolin of 5-15 parts by weight is added with 5-15 weight starch and is well mixed in 50-80 parts by weight plant ash solutions
Afterwards, immersion ageing 24-48 hours, the hydrochloric acid for then adding appropriate 10-40% be neutralized to after neutrality, is dried after being centrifuged,
Then after ground 100 mesh sieve and step（1）Appropriate bio-fermentation agent is added after gains are well mixed to stir and evenly mix, composting
Fermentation 20-25 days, it is stand-by；
（3）Micro- charing process
By step（2）In gains feeding high temperature furnace, heating heating is then carried out, high temperature in-furnace temperature is quickly risen to 70-
After 90 DEG C, stable 15-30 minutes, then gradually equitemperature is raised to 100-130 DEG C to temperature, and keeps stablizing 5-15 minutes, during which
Stir for several times, take out after cooling, it is stand-by；
（4）The preparation of anti-biotic material
By step（3）Gains are placed on high mixer, and 5-10 parts by weight clay is added at room temperature and is stirred with 5-10 parts by weight bamboo charcoal grain
Reaction 40-50 minutes is mixed, 5-10 parts by weight of ethanol is added, added in ultrasonic cleaner after scattered, shaping, then filtered,
Washing, after drying both micro- compound kaolin fleshiness anti-biotic material of charing marine alga
Described step（1）High-speed stirred in high mixer 800-1000r/min rotating speeds be stirred or in magnetic stirrer
Upper 800-1000r/min rotating speeds are stirred.
Described starch is one or more of mixing of cornstarch, tapioca or farina.
Step（3）Described compost fermentation fermented using taper, bank up and be shaped as taper, time interval is enters for 2-3 days
Row is stirred once.
Described anti-biotic material is laid on the bottom, fleshiness compost laying upper strata when planting succulent.
It is an advantage of the invention that：
The present invention after sodium hydroxide regulation pH first with after marine alga crushing/dewatering and then with hydrogenperoxide steam generator, being reacted
Afterwards, stirring is aged to being formed after slurries while kaolin and starch are added into plant ash solution immersion after hydrochloric acid is neutralized, from
Bio-fermentation agent fermentation is added after heart drying and grinding and gained marine alga slurries are well mixed, is then placed in high temperature furnace and utilizes temperature
Change is carried out by the drying after the rear heating for dissolving such as urea after micro- charing, and granulation is mixed by the material of micro- charing and clay, bamboo charcoal grain
Conjunction is prepared, and has good film forming and biofermentation in marine alga, and the work of enzyme in increase plant can be induced after fermentation
Property, via plant immunity is improved, to promoting root system development effect significantly, after being mixed with starch, starch is also by the ion in kaolin
Influence produces a certain degree of complexing, can delay fertilizer dissolution velocity during applied to crop, extends fertilizer acquisition time, micro- charing
Plant absorption is more conducive to afterwards, and absorption organic substance produces antibiotic property, the effect with anti-corrosion and anti-biological invasion and attack simultaneously can be in soil
Slowly decomposed under earth microbial action.Anti-biotic material prepared by the present invention, the colleague for possessing antibiotic property can be the life of succulent
It is long that sufficient nutriment is provided, the survival rate of succulent is improved, and material source is wide, cost is low.
Embodiment
A kind of micro- charing marine alga is combined the preparation method of kaolin fleshiness anti-biotic material, it is characterised in that including following step
Suddenly：
（1）The preparation of marine alga homogenate
Exposure under sunlight is placed in after 35 parts by weight marine algas are crushed, progress extrusion dehydration is standby, then adds 70 parts by weight peroxides
Change in hydrogen solution, pH is adjusted to 9-9.5 with 30% sodium hydroxide, stirred 1.5 hours in 70 DEG C, to after room temperature after cooling, Ran Houjia
The hydrochloric acid for entering appropriate 30% be neutralized to after neutrality, and high-speed stirred is stand-by to being formed after slurries；
（2）Fermentation reactor system
The kaolin of 10 parts by weight and 10 weight starch are added after being well mixed in 70 parts by weight plant ash solutions, soaked old
Change 36 hours, the hydrochloric acid for then adding appropriate 20% be neutralized to after neutrality, is dried after being centrifuged, then ground 100 mesh
After sieve and step（1）Appropriate bio-fermentation agent is added after gains are well mixed to stir and evenly mix, fermentation reactor system 22 days is stand-by；
（3）Micro- charing process
By step（2）In gains feeding high temperature furnace, heating heating is then carried out, high temperature in-furnace temperature is quickly risen to 80
DEG C, stablize after 20 minutes, then gradually equitemperature is raised to 110 DEG C to temperature, and keeps stablizing 10 minutes, during which stirs for several times, takes
Go out after cooling, it is stand-by；
（4）The preparation of anti-biotic material
By step（3）Gains are placed on high mixer, and 8 parts by weight clay and 8 parts by weight bamboo charcoal grain stirring reactions are added at room temperature
45 minutes, 8 parts by weight of ethanol are added, are added in ultrasonic cleaner after scattered, shaping, then is filtered, washed, after drying both
Obtain micro- charing marine alga and be combined kaolin fleshiness anti-biotic material
Described step（1）High-speed stirred in high mixer 900r/min rotating speeds be stirred or on magnetic stirrer
900r/min rotating speeds are stirred.
Described starch is one or more of mixing of cornstarch, tapioca or farina.
Step（3）Described compost fermentation fermented using taper, bank up and be shaped as taper, time interval is enters for 2-3 days
Row is stirred once.
Described anti-biotic material is laid on the bottom, fleshiness compost laying upper strata when planting succulent.
Claims (5)
1. a kind of micro- charing marine alga is combined the preparation method of kaolin fleshiness anti-biotic material, it is characterised in that comprise the following steps：
（1）The preparation of marine alga homogenate
Exposure under sunlight is placed in after 30-40 parts by weight marine alga is crushed, progress extrusion dehydration is standby, then adds 60-80 weight
In part hydrogenperoxide steam generator, pH is adjusted to 9-9.5 with 20-40% sodium hydroxides, 1-2 hours are stirred in 60-80 DEG C, after cooling extremely
After room temperature, the hydrochloric acid for then adding appropriate 10-40% be neutralized to after neutrality, and high-speed stirred is stand-by to being formed after slurries；
（2）Fermentation reactor system
The kaolin of 5-15 parts by weight is added with 5-15 weight starch and is well mixed in 50-80 parts by weight plant ash solutions
Afterwards, immersion ageing 24-48 hours, the hydrochloric acid for then adding appropriate 10-40% be neutralized to after neutrality, is dried after being centrifuged,
Then after ground 100 mesh sieve and step（1）Appropriate bio-fermentation agent is added after gains are well mixed to stir and evenly mix, composting
Fermentation 20-25 days, it is stand-by；
（3）Micro- charing process
By step（2）In gains feeding high temperature furnace, heating heating is then carried out, high temperature in-furnace temperature is quickly risen to 70-
After 90 DEG C, stable 15-30 minutes, then gradually equitemperature is raised to 100-130 DEG C to temperature, and keeps stablizing 5-15 minutes, during which
Stir for several times, take out after cooling, it is stand-by；
（4）The preparation of anti-biotic material
By step（3）Gains are placed on high mixer, and 5-10 parts by weight clay is added at room temperature and is stirred with 5-10 parts by weight bamboo charcoal grain
Reaction 40-50 minutes is mixed, 5-10 parts by weight of ethanol is added, added in ultrasonic cleaner after scattered, shaping, then filtered,
Washing, after drying both micro- compound kaolin fleshiness anti-biotic material of charing marine alga.
2. the preparation method of kaolin fleshiness anti-biotic material is combined according to a kind of micro- charing marine alga of claim 1, it is characterised in that
Described step（1）High-speed stirred in high mixer 800-1000r/min rotating speeds be stirred or on magnetic stirrer
800-1000r/min rotating speeds are stirred.
3. the preparation method of kaolin fleshiness anti-biotic material is combined according to a kind of micro- charing marine alga of claim 1, it is characterised in that
Described starch is one or more of mixing of cornstarch, tapioca or farina.
4. the preparation method of kaolin fleshiness anti-biotic material is combined according to a kind of micro- charing marine alga of claim 1, it is characterised in that
Step（3）Described compost fermentation using taper ferment, bank up and be shaped as taper, time interval be 2-3 days progress stir one
It is secondary.
5. the preparation method of kaolin fleshiness anti-biotic material is combined according to a kind of micro- charing marine alga of claim 1, it is characterised in that
Described anti-biotic material is laid on the bottom, fleshiness compost laying upper strata when planting succulent.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710497667.0A CN107200638A (en) | 2017-06-27 | 2017-06-27 | A kind of micro- charing marine alga is combined the preparation method of kaolin fleshiness anti-biotic material |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710497667.0A CN107200638A (en) | 2017-06-27 | 2017-06-27 | A kind of micro- charing marine alga is combined the preparation method of kaolin fleshiness anti-biotic material |
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| CN201710497667.0A Pending CN107200638A (en) | 2017-06-27 | 2017-06-27 | A kind of micro- charing marine alga is combined the preparation method of kaolin fleshiness anti-biotic material |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108642712A (en) * | 2018-06-22 | 2018-10-12 | 合肥洁诺医疗用品有限公司 | A kind of non-woven fabrics for medical mask |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102229515A (en) * | 2011-04-27 | 2011-11-02 | 北京雷力农用化学有限公司 | Organic granular fertilizer and preparation method thereof |
| CN105819985A (en) * | 2016-05-27 | 2016-08-03 | 安徽云锦农业科技发展有限公司 | Rooting-promoting flower coated fertilizer |
-
2017
- 2017-06-27 CN CN201710497667.0A patent/CN107200638A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102229515A (en) * | 2011-04-27 | 2011-11-02 | 北京雷力农用化学有限公司 | Organic granular fertilizer and preparation method thereof |
| CN105819985A (en) * | 2016-05-27 | 2016-08-03 | 安徽云锦农业科技发展有限公司 | Rooting-promoting flower coated fertilizer |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108642712A (en) * | 2018-06-22 | 2018-10-12 | 合肥洁诺医疗用品有限公司 | A kind of non-woven fabrics for medical mask |
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Application publication date: 20170926 |