CN107177234A - A kind of ink and its production technology - Google Patents
A kind of ink and its production technology Download PDFInfo
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- CN107177234A CN107177234A CN201710486689.7A CN201710486689A CN107177234A CN 107177234 A CN107177234 A CN 107177234A CN 201710486689 A CN201710486689 A CN 201710486689A CN 107177234 A CN107177234 A CN 107177234A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
- C09D11/104—Polyesters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
A kind of ink and its production technology, are related to technical field of ink, are prepared from by the component of following parts by weight meter：30~35 parts of filming emulsions, 1~2 part of ammonia nertralizer, the fast dry emulsion of 25~30 parts low smell, 5~10 parts low smell slow curing emulsion, 0.2~0.4 part of beeswax, 0.5~1.5 part of defoamer, 4~6 parts of varnish, 30~35 parts of mill bases.Comprise the following steps, 1) filming emulsion is added into container, then it is stirred with high speed dispersor, ammonia nertralizer is progressively added dropwise while stirring, test mixing liquid pH value stops stirring between 7.5~8.5, carries out next step operation；2) low smell slow curing emulsion, beeswax, defoamer are added in container and is sufficiently mixed carry out emulsification treatment；3) mill base, the fast dry emulsion of low smell and varnish are added into container again, continues scattered 8~10 minutes, test pH value is made ink between 7~8.Environmental Safety of the present invention, pollution-free, hardness is high, be not easy to scratch, and is easy to production, and service life is long.
Description
Technical field：
The present invention relates to technical field of ink, and in particular to a kind of ink and preparation method thereof.
Background technology：
Ink is the important materials for printing, and it is shown pattern, word on stock by printing or air brushing.Oil
Ink includes main component and auxiliary element, and they equably mix and form a kind of stickiness colloidal fluid through repeat-rolling.By
Link stuff (resin), pigment, filler, auxiliary agent and solvent etc. are constituted.For books and periodicals, packing and decorating, building decoration and electronic circuit
The various printings such as sheet material.As social demand increases, ink kind and yield also respective extension and growth.Presently commercially available ink
Volatility is stronger, and taste is larger, low intensity after printing, is easily come off after scraping, indices are unsatisfactory for relevant laws and regulations,
The current development prospect of China is not met.
The content of the invention：
The technical problems to be solved by the invention are to overcome existing technological deficiency that there is provided a kind of Environmental Safety, no dirt
Dye, intensity is high, do not allow caducous ink and preparation method thereof.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of ink, it is characterised in that：It is prepared from by the component of following parts by weight meter：30~35 parts of filming emulsions, 1~
2 parts of ammonia nertralizers, the fast dry emulsion of 25~30 parts low smell, 5~10 parts low smell slow curing emulsion, 0.2~0.4 part of beeswax, 0.5~
1.5 parts of defoamers, 4~6 parts of varnish, 30~35 parts of mill bases.
A kind of production technology of ink, it is characterised in that：Comprise the following steps,
1) filming emulsion is added into container, be then stirred with high speed dispersor, ammonia is progressively added dropwise while stirring and neutralizes
Agent, is sufficiently stirred for after 6~8min, and test mixing liquid pH value stops stirring between 7.5~8.5, carries out next step operation；
2) low smell slow curing emulsion, beeswax, defoamer are added in container and is sufficiently mixed carry out emulsification treatment, during emulsification
60 DEG C of emulsifying temperature, 1500~1800r/min of emulsification stirring speed, 10~16min of emulsification times；
3) mill base, the fast dry emulsion of low smell and varnish are added into container again, continues scattered 8~10 minutes, tests pH
Value is made ink between 7~8.
Also include 4~6 parts of thickener, described thickener include by weight 5~8 parts of hydroxylmethyl cellulose, bentonite 2~
3~4 parts of 4 parts, 2~4 parts of apatite and sepiolite powder.
Described filming emulsion is aqueous saturated polyester resin liquid.
The mill base is to be prepared from according to the following steps：
1) by weight by 1~3 part of titanium dioxide, 8~10 parts of monoethanolamine, aqueous cured slurry 0.4~0.6 part, pigment powder
20~25 parts, 18~20 parts of deionized water, 0.2~0.4 part of dispersant, 0.3~0.5 part of defoamer, 0.2~0.4 part of cosolvent
Mixing, obtains mixed liquor；
2) mixed liquor is stirred into mixing under high speed dispersion agent, mixing speed is 1000r/min~1500r/min, stirring
0.4~0.6h of time, obtains stirring liquid；
3) stirring liquid is inserted in horizontal sand mill, bead mill is handled 3~5 times, mill base is made.
2. a kind of ink according to claim 1, it is characterised in that：Described defoamer includes wood three by weight
3~7 parts of 2~4 parts of monoethanolamine, 2~4 parts of triisopropanolamine and ethylene glycol.
The ammonia nertralizer is formic acid or acetic acid.
Described defoamer by weight include 2~3 parts of polyoxyethylene polyoxy propyl alcohol amidogen ether, have 1~3 part of silicone emulsion and
2~4 parts of high-carbon polyol fatty acid.
The described fast dry emulsion of low smell includes following components, 20~30 parts of dimethylethanolamine, dipropyl two by weight
1~2 part of 5~9 parts of alcohol methyl ether, 1~3 part of dispersant and surfactant.
Described low smell slow curing emulsion includes following components, 20~30 parts of acrylic resin soln, hydrotropy by weight
1~2 part of 0.5~0.7 part of agent, 1~3 part of zinc stearate and surfactant.
The varnish of the present invention is aqueous varnish, colourless, tasteless, nontoxic, transparent, liquid.Aqueous varnish is used for
Modulate ink.
Viscosity foot of the invention, intensity is high, and rate of drying is fast, it is not easy to drop.The defoamer of the present invention not only has efficient
Froth breaking effect, improve the uniformity, and play rapid ink drying and meanwhile strengthen ink setting after intensity and hardness purpose,
Thickener in the present invention can also strengthen ink bond and the intensity of itself, be encounter hard object also will not be broken
It is rotten.The preparation method of the present invention makes by emulsification and under specific temperature, time, and ink fineness, the uniformity are high, are conducive to
Improve the performance of product.
1st, water-based ink economy of the invention, durable, especially this water-based ink uses water as solvent and decentralized medium,
It is diluted with water and can be used, almost pollution-free to air, it is to avoid the poisonous and harmful property of organic solvent, environmental protection, energy-conservation is strong
Health；
2nd, water-based ink of the invention is by the use of aqueous saturated polyester resin as matrix resin, the ink have hardness height,
The advantages of flexible, impact resistance, UV resistant；Mill base in water-based ink can be used for the ink for preparing different colours, prepare
The ink gone out is bright-coloured, and service life is long；
3rd, the preparation method step of ink of the invention is simple, short the time required to preparation process, is given birth to beneficial to large-scale industry
Production, application, and the water-based ink environmental protection that the preparation method is prepared.
The beneficial effects of the invention are as follows：Environmental Safety of the present invention, pollution-free, hardness is high, be not easy to scratch, and is easy to life
Production, service life is long.
Embodiment：
With reference to instantiation, the present invention is expanded on further.
Embodiment 1
A kind of ink, is prepared from by the component of following parts by weight meter：30 parts of filming emulsions, 1 part of ammonia nertralizer is 25 parts low
The fast dry emulsion of smell, 5 parts low smell slow curing emulsion, 0.2 part of beeswax, 0.5 part of defoamer, 4 parts of varnish, 30 parts of mill bases.
A kind of production technology of ink, comprises the following steps,
1) filming emulsion is added into container, be then stirred with high speed dispersor, ammonia is progressively added dropwise while stirring and neutralizes
Agent, is sufficiently stirred for after 6min, and test mixing liquid pH value stops stirring between 7.5, carries out next step operation；
2) low smell slow curing emulsion, beeswax, defoamer are added in container and is sufficiently mixed carry out emulsification treatment, during emulsification
60 DEG C of emulsifying temperature, emulsification stirring speed 1500r/min, emulsification times 10min；
3) mill base, the fast dry emulsion of low smell and varnish are added into container again, continues scattered 8 minutes, test pH value is 7
Between, that is, ink is made.
Filming emulsion is aqueous saturated polyester resin liquid.
Mill base is to be prepared from according to the following steps：
1) by weight by 1 part of titanium dioxide, 8 parts of monoethanolamine, aqueous cured 0.4 part of slurry, 20 parts of pigment powder, deionized water
18 parts, 0.2 part of dispersant, 0.3 part of defoamer, the mixing of 0.2 part of cosolvent, obtain mixed liquor；
2) mixed liquor is stirred into mixing under high speed dispersion agent, mixing speed is 1000r/min, mixing time 0.4h, is obtained
To stirring liquid；
3) stirring liquid is inserted in horizontal sand mill, bead mill is handled 3 times, mill base is made.
Defoamer includes 3 parts of wooden 2 parts of triethanolamine, 2 parts of triisopropanolamine and ethylene glycol by weight.
Ammonia nertralizer is acetic acid.
Defoamer includes 2 parts of polyoxyethylene polyoxy propyl alcohol amidogen ether, has 1 part of silicone emulsion and high-carbon polyol fatty acid by weight
2 parts.
The low fast dry emulsion of smell by weight include following components, 20 parts of dimethylethanolamine, 5 parts of dipropylene glycol methyl ether,
1 part of 1 part of dispersant and surfactant.
Low smell slow curing emulsion includes following components by weight, 20 parts of acrylic resin soln, 0.5 part of cosolvent, hard
1 part of 1 part of ester acid zinc and surfactant.
The viscosity of the ink of the present embodiment is smaller, and viscosity is low, and Solid content amount is low, it is adaptable to have spongy object table
The product such as face, such as cloth, paper.
Embodiment two
A kind of ink, is prepared from by the component of following parts by weight meter：33 parts of filming emulsions, 1.5 parts of ammonia nertralizers, 28 parts
The low fast dry emulsion of smell, 8 parts low smell slow curing emulsion, 0.3 part of beeswax, 1 part of defoamer, 5 parts of varnish, 33 parts of mill bases.
A kind of production technology of ink, comprises the following steps,
1) filming emulsion is added into container, be then stirred with high speed dispersor, ammonia is progressively added dropwise while stirring and neutralizes
Agent, is sufficiently stirred for after 7min, and test mixing liquid pH value stops stirring between 8, carries out next step operation；
2) low smell slow curing emulsion, beeswax, defoamer are added in container and is sufficiently mixed carry out emulsification treatment, during emulsification
60 DEG C of emulsifying temperature, emulsification stirring speed 1650r/min, emulsification times 13min；
3) mill base, the fast dry emulsion of low smell and varnish are added into container again, continues scattered 9 minutes, test pH value exists
Between 7.5, that is, ink is made.
Also include 5 parts of thickener, described thickener includes 6 parts of hydroxylmethyl cellulose, 3 parts of bentonite, phosphorus ash by weight
3.5 parts of 3 parts of stone and sepiolite powder.
Filming emulsion is aqueous saturated polyester resin liquid.
Mill base is to be prepared from according to the following steps：
1) by weight by 2 parts of titanium dioxide, 9 parts of monoethanolamine, aqueous cured 0.5 part of slurry, 23 parts of pigment powder, deionized water
19 parts, 0.3 part of dispersant, 0.4 part of defoamer, the mixing of 0.3 part of cosolvent, obtain mixed liquor；
2) mixed liquor is stirred into mixing under high speed dispersion agent, mixing speed is 1350r/min, mixing time 0.5h, is obtained
To stirring liquid；
3) stirring liquid is inserted in horizontal sand mill, bead mill is handled 4 times, mill base is made.
Defoamer includes 5 parts of wooden 3 parts of triethanolamine, 3 parts of triisopropanolamine and ethylene glycol by weight.
Ammonia nertralizer is formic acid.
Defoamer includes 2.5 parts of polyoxyethylene polyoxy propyl alcohol amidogen ether, has 2 parts of silicone emulsion and higher alcohols fat by weight
3 parts of acid.
The low fast dry emulsion of smell by weight include following components, 25 parts of dimethylethanolamine, 7 parts of dipropylene glycol methyl ether,
1.5 parts of 2 parts of dispersant and surfactant.
Low smell slow curing emulsion includes following components by weight, 25 parts of acrylic resin soln, 0.6 part of cosolvent, hard
1.5 parts of 2 parts of ester acid zinc and surfactant.
The viscosity of the ink of the present embodiment is higher, and viscosity is compared with Solid content amount is relatively low, it is adaptable to metal product surface
Inkjet process.
Embodiment three
A kind of ink, is prepared from by the component of following parts by weight meter：35 parts of filming emulsions, 2 parts of ammonia nertralizers are 30 parts low
The 10 parts low smell slow curing emulsion of the fast dry emulsion of smell, 0.4 part of beeswax, 1.5 parts of defoamers, 6 parts of varnish, 35 parts of mill bases.
A kind of production technology of ink, comprises the following steps,
1) filming emulsion is added into container, be then stirred with high speed dispersor, ammonia is progressively added dropwise while stirring and neutralizes
Agent, is sufficiently stirred for after 8min, and test mixing liquid pH value stops stirring between 8.5, carries out next step operation；
2) low smell slow curing emulsion, beeswax, defoamer are added in container and is sufficiently mixed carry out emulsification treatment, during emulsification
60 DEG C of emulsifying temperature, emulsification stirring speed 1800r/min, emulsification times 16min；
3) mill base, the fast dry emulsion of low smell and varnish are added into container again, continues scattered 10 minutes, test pH value exists
Between 8, that is, ink is made.
Also include 6 parts of thickener, described thickener includes 8 parts of hydroxylmethyl cellulose, 4 parts of bentonite, phosphorus ash by weight
4 parts of 4 parts of stone and sepiolite powder.
Filming emulsion is aqueous saturated polyester resin liquid.
Mill base is to be prepared from according to the following steps：
1) by weight by 3 parts of titanium dioxide, 10 parts of monoethanolamine, aqueous cured 0.6 part of slurry, 25 parts of pigment powder, deionization
20 parts of water, 0.4 part of dispersant, 0.5 part of defoamer, 0.4 part of mixing of cosolvent, obtain mixed liquor；
2) mixed liquor is stirred into mixing under high speed dispersion agent, mixing speed is 1500r/min, mixing time 0.6h, is obtained
To stirring liquid；
3) stirring liquid is inserted in horizontal sand mill, bead mill is handled 5 times, mill base is made.
Defoamer includes 7 parts of wooden 4 parts of triethanolamine, 4 parts of triisopropanolamine and ethylene glycol by weight.
Ammonia nertralizer is formic acid.
Defoamer includes 3 parts of polyoxyethylene polyoxy propyl alcohol amidogen ether, has 3 parts of silicone emulsion and high-carbon polyol fatty acid by weight
4 parts.
The low fast dry emulsion of smell includes following components, 20~30 parts of dimethylethanolamine, dipropylene glycol methyl ether 5 by weight
2 parts of~9 parts, 3 parts of dispersant and surfactant.
Low smell slow curing emulsion by weight include following components, 20~30 parts of acrylic resin soln, cosolvent 0.5~
1~2 part of 0.7 part, 1~3 part of zinc stearate and surfactant.
The viscosity of the ink of the present embodiment is higher, and viscosity is high, and Solid content amount is high, it is adaptable to the spray of plastic product surface
Ink processing.
Experimental data is obtained to embodiments of the invention progress experiment detection as shown in the table：
| Inspection content | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Amount of solid content (%) | 68 | 72 | 80 |
| Ink viscosity (s) | 130 | 153 | 156 |
| PH value | 7.5 | 8 | 8.5 |
| Coating dry film thickness (μm) | 18 | 16 | 15 |
| Fineness (μm) | 19 | 21 | 17 |
| Surface gloss | 93 | 92 | 89 |
| Aberration | 0.3 | 0.2 | 0.3 |
Laboratory test results show that viscosity of the invention is more than 149, with very high viscosity, and intensity is high, and dries
Speed is fast, and in the case where coating layer thickness is relatively low, surface gloss is high, aberration very little, therefore suitable for various products
Ink-jet.
The embodiment of the present invention is above are only, but the design concept of the present invention is not limited thereto, it is all to utilize this
Conceive the change that unsubstantiality is carried out to the present invention, the behavior for invading the scope of the present invention all should be belonged to.
Claims (10)
1. a kind of ink, it is characterised in that：It is prepared from by the component of following parts by weight meter：30~35 parts of filming emulsions, 1~2
Part ammonia nertralizer, the fast dry emulsion of 25~30 parts low smell, 5~10 parts low smell slow curing emulsion, 0.2~0.4 part of beeswax, 0.5~
1.5 parts of defoamers, 4~6 parts of varnish, 30~35 parts of mill bases.
2. a kind of production technology of ink according to claim 1, it is characterised in that：Comprise the following steps,
1) filming emulsion is added into container, be then stirred with high speed dispersor, ammonia nertralizer is progressively added dropwise while stirring, fills
Divide after 6~8min of stirring, test mixing liquid pH value stops stirring between 7.5~8.5, carries out next step operation；
2) low smell slow curing emulsion, beeswax, defoamer are added in container and is sufficiently mixed carry out emulsification treatment, emulsification during emulsification
Temperature 60 C, 1500~1800r/min of emulsification stirring speed, 10~16min of emulsification times；
3) mill base, the fast dry emulsion of low smell and varnish are added into container again, continues scattered 8~10 minutes, test pH value is 7
Between~8, that is, ink is made.
3. a kind of ink according to claim 1, it is characterised in that also including 4~6 parts of thickener, described thickener
Include 3~4 parts of 5~8 parts of hydroxylmethyl cellulose, 2~4 parts of bentonite, 2~4 parts of apatite and sepiolite powder by weight.
4. a kind of ink according to claim 1, it is characterised in that described filming emulsion is aqueous saturated polyester resin
Liquid.
5. a kind of ink according to claim 1, it is characterised in that the mill base is to be prepared from according to the following steps：
1) by weight by 1~3 part of titanium dioxide, 8~10 parts of monoethanolamine, it is aqueous it is cured slurry 0.4~0.6 part, pigment powder 20~
25 parts, 18~20 parts of deionized water, 0.2~0.4 part of dispersant, 0.3~0.5 part of defoamer, the mixing of 0.2~0.4 part of cosolvent,
Obtain mixed liquor；
2) mixed liquor is stirred into mixing under high speed dispersion agent, mixing speed is 1000r/min~1500r/min, mixing time
0.4~0.6h, obtains stirring liquid；
3) stirring liquid is inserted in horizontal sand mill, bead mill is handled 3~5 times, mill base is made.
6. a kind of ink according to claim 1, it is characterised in that：Described defoamer includes wooden three ethanol by weight
3~7 parts of 2~4 parts of amine, 2~4 parts of triisopropanolamine and ethylene glycol.
7. a kind of ink according to claim 1, it is characterised in that：The ammonia nertralizer is formic acid or acetic acid.
8. a kind of ink according to claim 1, it is characterised in that：Described defoamer includes polyoxyethylene by weight
2~3 parts of polyoxy propyl alcohol amidogen ether, there are 2~4 parts of 1~3 part of silicone emulsion and high-carbon polyol fatty acid.
9. a kind of ink according to claim 1, it is characterised in that：The described fast dry emulsion of low smell includes by weight
Following components, 20~30 parts of dimethylethanolamine, 5~9 parts of dipropylene glycol methyl ether, 1~3 part of dispersant and surfactant 1~2
Part.
10. a kind of ink according to claim 1, it is characterised in that：Described low smell slow curing emulsion is wrapped by weight
Include following components, 20~30 parts of acrylic resin soln, 0.5~0.7 part of cosolvent, 1~3 part of zinc stearate and surfactant
1~2 part.
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| CN107936692A (en) * | 2017-12-28 | 2018-04-20 | 夏冬 | A kind of ink and preparation method thereof |
| CN108219579A (en) * | 2017-12-28 | 2018-06-29 | 夏冬 | A kind of ink and the method for being used to prepare the ink |
| CN107955455A (en) * | 2018-01-08 | 2018-04-24 | 林光波 | A kind of preparation method of ink and ink |
| CN108373650A (en) * | 2018-03-28 | 2018-08-07 | 深圳市美丽华科技股份有限公司 | A kind of aqueous PET ink for screen printing and preparation method thereof |
| CN111369269A (en) * | 2020-03-29 | 2020-07-03 | 武汉积墨包装印刷有限公司 | Printing ink tracing production process method based on block chain |
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Application publication date: 20170919 |