CN107156599A - Environment-friendly preservative for food and preservation method - Google Patents
Environment-friendly preservative for food and preservation method Download PDFInfo
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- CN107156599A CN107156599A CN201710425250.3A CN201710425250A CN107156599A CN 107156599 A CN107156599 A CN 107156599A CN 201710425250 A CN201710425250 A CN 201710425250A CN 107156599 A CN107156599 A CN 107156599A
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- antistaling agent
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- 235000013305 food Nutrition 0.000 title claims abstract description 58
- 238000000034 method Methods 0.000 title claims abstract description 41
- 238000004321 preservation Methods 0.000 title claims abstract description 23
- 239000003755 preservative agent Substances 0.000 title abstract description 8
- 230000002335 preservative effect Effects 0.000 title abstract description 8
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 57
- 235000013824 polyphenols Nutrition 0.000 claims abstract description 57
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 43
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 43
- 239000011734 sodium Substances 0.000 claims abstract description 43
- DBTMGCOVALSLOR-DEVYUCJPSA-N (2s,3r,4s,5r,6r)-4-[(2s,3r,4s,5r,6r)-3,5-dihydroxy-6-(hydroxymethyl)-4-[(2s,3r,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-2-yl]oxy-6-(hydroxymethyl)oxane-2,3,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](CO)O[C@H](O)[C@@H]2O)O)O[C@H](CO)[C@H]1O DBTMGCOVALSLOR-DEVYUCJPSA-N 0.000 claims abstract description 31
- 229920002101 Chitin Polymers 0.000 claims abstract description 31
- 229920001543 Laminarin Polymers 0.000 claims abstract description 31
- 239000005717 Laminarin Substances 0.000 claims abstract description 31
- 229920005610 lignin Polymers 0.000 claims abstract description 31
- 239000000203 mixture Substances 0.000 claims abstract description 26
- 241000305549 Platycarya strobilacea Species 0.000 claims description 65
- 239000003795 chemical substances by application Substances 0.000 claims description 55
- 238000000605 extraction Methods 0.000 claims description 31
- 239000003245 coal Substances 0.000 claims description 24
- 239000011347 resin Substances 0.000 claims description 23
- 229920005989 resin Polymers 0.000 claims description 23
- 239000006228 supernatant Substances 0.000 claims description 21
- 239000000463 material Substances 0.000 claims description 20
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 14
- 239000007864 aqueous solution Substances 0.000 claims description 14
- 238000006243 chemical reaction Methods 0.000 claims description 14
- 239000003456 ion exchange resin Substances 0.000 claims description 14
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 14
- 239000002245 particle Substances 0.000 claims description 14
- 239000002904 solvent Substances 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 9
- 230000002745 absorbent Effects 0.000 claims description 7
- 239000002250 absorbent Substances 0.000 claims description 7
- 239000007795 chemical reaction product Substances 0.000 claims description 7
- 238000004140 cleaning Methods 0.000 claims description 7
- 239000002817 coal dust Substances 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 7
- 238000000265 homogenisation Methods 0.000 claims description 7
- 239000012535 impurity Substances 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 7
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 7
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 7
- 238000009777 vacuum freeze-drying Methods 0.000 claims description 7
- 230000007613 environmental effect Effects 0.000 claims description 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 2
- 150000001768 cations Chemical class 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 3
- 239000005452 food preservative Substances 0.000 abstract description 3
- 235000019249 food preservative Nutrition 0.000 abstract description 3
- 230000001954 sterilising effect Effects 0.000 abstract description 3
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 3
- 230000003064 anti-oxidating effect Effects 0.000 abstract 1
- 238000009920 food preservation Methods 0.000 abstract 1
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 description 5
- 239000002253 acid Substances 0.000 description 5
- 239000004021 humic acid Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000000126 substance Substances 0.000 description 3
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 230000000215 hyperchromic effect Effects 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000000523 sample Substances 0.000 description 2
- IOVCWXUNBOPUCH-UHFFFAOYSA-N Nitrous acid Chemical compound ON=O IOVCWXUNBOPUCH-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000021393 food security Nutrition 0.000 description 1
- 235000012055 fruits and vegetables Nutrition 0.000 description 1
- 239000003630 growth substance Substances 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 239000003077 lignite Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 description 1
- 235000013923 monosodium glutamate Nutrition 0.000 description 1
- 239000004223 monosodium glutamate Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000003415 peat Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
- 235000010234 sodium benzoate Nutrition 0.000 description 1
- 239000004299 sodium benzoate Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3562—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3481—Organic compounds containing oxygen
- A23L3/349—Organic compounds containing oxygen with singly-bound oxygen
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3481—Organic compounds containing oxygen
- A23L3/3508—Organic compounds containing oxygen containing carboxyl groups
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
Abstract
The invention belongs to the technical field of food preservation, and provides an environment-friendly preservative for food and a preservation method, wherein the environment-friendly preservative for food comprises the following components: the composition of the first component is sodium humate; the second component comprises laminarin, cortex cinnamomi polyphenol extract, chitin and lignin. The preservative is an edible food preservative, and the effective and safe dose of the sodium humate used as the preservative is explored; meanwhile, the preservative has good water retention, bacteriostasis, sterilization and antioxidation effects, and can improve the edible and commodity values of food.
Description
Technical field
The invention belongs to food preservative technology field, in particular it relates to a kind of environmentally friendly antistaling agent for food and fresh-keeping
Method.
Background technology
On food fresh keeping, there are single performance, tin foil without nutrient, preservative film, freshness protection package and fresh-keeping electuary at present,
There are various chemical addition agents for food processing industry.It is hyperchromic to help fresh class to have chemical toner and common monosodium glutamate.It is tin foil, fresh-keeping
The fresh-keeping effect of film and freshness protection package is not good enough；It is inconvenient and cause remaining waste when electuary is used；Chemistry is hyperchromic to damage object battalion
Element is supported, helps fresh also undesirable；Food processing industry Food Chemistry preservative such as sodium benzoate, nitrous acid etc., not only without any battalion
Support value and belong to harmful material, its consumption is limited food additives harmful substance by national strict limitation, and country
Amount standard is with the fresh-keeping contradiction of the exceeded consumption of manufacturer.
At present for food processing, brewing industry and family, fresh-keeping is urgent problem to be solved.
Humic acid is the unbodied macromolecule organic of a class, is to be produced by dead organisms material through microbial degradation, extensively
It is general to be present in the low-order coals such as the lignite of nature, weathered coal, peat and soil.Humic acid it is widely used, may be used as
Water treatment agent, coal water mixture stabilizing agent, petroleum assistant etc., it is even more obtain extensive that humic acid, which is used as plant growth substance, in recent years
Research and application.Although humic acid has the function of antistaling agent, the present invention uses it for the antistaling agent of food.
The content of the invention
For defect of the prior art, it is an object of the invention to provide a kind of environmentally friendly antistaling agent for food and fresh-keeping
Method, the antistaling agent is edible food antistaling agent, probes into out the dose of virtual safe of sodium humate during as antistaling agent；Together
When, the antistaling agent has preferable water conservation, antibacterial, sterilization, antioxidant effect, can improve the edible and commodity value of food.
A kind of environmentally friendly antistaling agent for food, the environmental protection guarantor for food are provided according to an aspect of the present invention
Fresh dose includes component one and component two, and the composition of the component one is sodium humate；The composition of the component two be laminarin,
Platycarya strobilacea skin polyphenol extract, chitin and lignin,
The parts by weight of above-mentioned each material are specific as follows,
20-55 parts of sodium humate,
15-23 parts of laminarin,
1-3 parts of Platycarya strobilacea skin polyphenol extract,
4-6 parts of chitin,
5-9 parts of lignin.
Preferably, the environmentally friendly antistaling agent for food includes component one and component two, and the composition of the component one is
Sodium humate；The composition of the component two be laminarin, Platycarya strobilacea skin polyphenol extract, chitin and lignin,
The parts by weight of above-mentioned each material are specific as follows,
20-35 parts of sodium humate,
19-23 parts of laminarin,
1-2 parts of Platycarya strobilacea skin polyphenol extract,
4-5 parts of chitin,
5-7 parts of lignin.
Preferably, the environmentally friendly antistaling agent for food includes component one and component two, and the composition of the component one is
Sodium humate；The composition of the component two be laminarin, Platycarya strobilacea skin polyphenol extract, chitin and lignin,
The parts by weight of above-mentioned each material are specific as follows,
23 parts of sodium humate,
21 parts of laminarin,
1 part of Platycarya strobilacea skin polyphenol extract,
4 parts of chitin,
6 parts of lignin.
Preferably, the extracting method of the sodium humate is：
（1）Low-order coal is crushed to 150-400 mesh, the 5% sodium bicarbonate aqueous solution reaction 6-8h of 3-8 times of coal dust weight is added；
（2）After the completion of reaction, reaction product is purified and removed a huge sum of money alternately through macroreticular resin and strong ion exchange resin
Belong to element.
Preferably, the low-order coal is weathered coal.
Preferably, the macroreticular resin is middle polarity macroporous absorbent resin, and the strong ion exchange resin is weak to fold
Acidic cationic resin.
Preferably, the extracting method of the Platycarya strobilacea skin polyphenol extract comprises the following steps：
（1）Platycarya strobilacea skin through over cleaning removal of impurities is crushed, Platycarya strobilacea skin particle to be extracted is obtained；
（2）By step（1）Obtained Platycarya strobilacea skin particle to be extracted is with 1:9-1:21g/mL solid-liquid ratio is added to Extraction solvent
In, homogenization 7-10min, is separated by filtration supernatant liquor under 7000-11000r/min rotating speed, obtains polyphenol extraction supernatant
Liquid, wherein, the Extraction solvent is the aqueous solution for the ethanol that volume by volume concentration is 40-50%；
（3）By step（2）Obtained polyphenol extraction supernatant is concentrated in vacuo to sticky shape under conditions of 55-65 DEG C, goes forward side by side one
Vacuum freeze drying is walked into powdered, Platycarya strobilacea skin polyphenol is produced.
Another aspect of the present invention provides a kind of preservation method of environmentally friendly antistaling agent for food, the preservation method
Comprise the following steps：
The preservation method is specific as follows：
（1）Parts by weight according to each material weigh sodium humate, laminarin, Platycarya strobilacea skin polyphenol extract, chitin and
Lignin, is divided into component one and component two, and component one and component two press 4:Carried out after 1 mass ratio mixing packed；
（2）Packed antistaling agent is placed in the environment for placing food.
Compared with prior art, the present invention has following beneficial effect：
（1）The environmentally friendly antistaling agent that the present invention provides described in a kind of environmentally friendly antistaling agent for food for food includes the He of component one
Component two, the composition of the component one is sodium humate；The composition of the component two is laminarin, many phenol extractions of Platycarya strobilacea skin
Thing, chitin and lignin, antistaling agent of the present invention are edible food antistaling agent, probe into out sodium humate during as antistaling agent
Dose of virtual safe；Meanwhile, the antistaling agent has preferable water conservation, antibacterial, sterilization, antioxidant effect, can improve food
Edible and commodity value；
（2）The food that the present invention is provided environmentally friendly antistaling agent access humic acid, using sodium humate as food preservative purposes,
Accomplish food security rank, and fresh-keeping effect is good.Provide simultaneously and sodium humate fruits and vegetables guarantor is directly prepared by low-order coal
Fresh dose of method, the preparation method is simple to operate, easily realizes, and can effectively remove the member of the harmful heavy metal in antistaling agent
Element；
（3）Antistaling agent preparation method of the present invention is simple, and process is few, easy to use.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.It should be understood that these embodiments are merely to illustrate the present invention
Rather than limitation the scope of the present invention.
Embodiment 1
A kind of environmentally friendly antistaling agent for food that the present embodiment is provided, the environmentally friendly antistaling agent for food includes component one
With component two, the composition of the component one is sodium humate；The composition of the component two is laminarin, Platycarya strobilacea skin polyphenol is carried
Thing, chitin and lignin are taken,
The parts by weight of above-mentioned each material are specific as follows,
55 parts of sodium humate,
15 parts of laminarin,
3 parts of Platycarya strobilacea skin polyphenol extract,
4 parts of chitin,
9 parts of lignin.
The extracting method of the sodium humate is：
（1）Low-order coal is crushed to 150-400 mesh, the 5% sodium bicarbonate aqueous solution reaction 6h of 8 times of coal dust weight is added；
（2）After the completion of reaction, reaction product is purified and removed a huge sum of money alternately through macroreticular resin and strong ion exchange resin
Belong to element.
The low-order coal is weathered coal.
The macroreticular resin be middle polarity macroporous absorbent resin, the strong ion exchange resin for fold faintly acid sun from
Subtree fat.
The extracting method of the Platycarya strobilacea skin polyphenol extract comprises the following steps：
（1）Platycarya strobilacea skin through over cleaning removal of impurities is crushed, Platycarya strobilacea skin particle to be extracted is obtained；
（2）By step（1）Obtained Platycarya strobilacea skin particle to be extracted is with 1:21g/mL solid-liquid ratio is added in Extraction solvent,
Homogenization 7-10min, is separated by filtration supernatant liquor under 7000r/min rotating speed, obtains polyphenol extraction supernatant, wherein,
The Extraction solvent is the aqueous solution for the ethanol that volume by volume concentration is 40-50%；
（3）By step（2）Obtained polyphenol extraction supernatant is concentrated in vacuo to sticky shape under conditions of 55-65 DEG C, goes forward side by side one
Vacuum freeze drying is walked into powdered, Platycarya strobilacea skin polyphenol is produced.
Another aspect of the present invention provides a kind of preservation method of environmentally friendly antistaling agent for food, the preservation method
Comprise the following steps：
The preservation method is specific as follows：
（1）Parts by weight according to each material weigh sodium humate, laminarin, Platycarya strobilacea skin polyphenol extract, chitin and
Lignin, is divided into component one and component two, and component one and component two press 4:Carried out after 1 mass ratio mixing packed；
（2）Packed antistaling agent is placed in the environment for placing food.
Embodiment 2
A kind of environmentally friendly antistaling agent for food that the present embodiment is provided, the environmentally friendly antistaling agent for food includes component one
With component two, the composition of the component one is sodium humate；The composition of the component two is laminarin, Platycarya strobilacea skin polyphenol is carried
Thing, chitin and lignin are taken,
The parts by weight of above-mentioned each material are specific as follows,
20 parts of sodium humate,
23 parts of laminarin,
1 part of Platycarya strobilacea skin polyphenol extract,
6 parts of chitin,
5 parts of lignin.
The extracting method of the sodium humate is：
（1）Low-order coal is crushed to 150-400 mesh, the 5% sodium bicarbonate aqueous solution reaction 8h of 3 times of coal dust weight is added；
（2）After the completion of reaction, reaction product is purified and removed a huge sum of money alternately through macroreticular resin and strong ion exchange resin
Belong to element.
The low-order coal is weathered coal.
The macroreticular resin be middle polarity macroporous absorbent resin, the strong ion exchange resin for fold faintly acid sun from
Subtree fat.
The extracting method of the Platycarya strobilacea skin polyphenol extract comprises the following steps：
（1）Platycarya strobilacea skin through over cleaning removal of impurities is crushed, Platycarya strobilacea skin particle to be extracted is obtained；
（2）By step（1）Obtained Platycarya strobilacea skin particle to be extracted is with 1:9g/mL solid-liquid ratio is added in Extraction solvent,
Homogenization 7-10min, is separated by filtration supernatant liquor under 11000r/min rotating speed, obtains polyphenol extraction supernatant, wherein, institute
State the aqueous solution that Extraction solvent is the ethanol that volume by volume concentration is 40-50%；
（3）By step（2）Obtained polyphenol extraction supernatant is concentrated in vacuo to sticky shape under conditions of 55-65 DEG C, goes forward side by side one
Vacuum freeze drying is walked into powdered, Platycarya strobilacea skin polyphenol is produced.
Another aspect of the present invention provides a kind of preservation method of environmentally friendly antistaling agent for food, the preservation method
Comprise the following steps：
The preservation method is specific as follows：
（1）Parts by weight according to each material weigh sodium humate, laminarin, Platycarya strobilacea skin polyphenol extract, chitin and
Lignin, is divided into component one and component two, and component one and component two press 4:Carried out after 1 mass ratio mixing packed；
（2）Packed antistaling agent is placed in the environment for placing food.
Embodiment 3
A kind of environmentally friendly antistaling agent for food that the present embodiment is provided, the environmentally friendly antistaling agent for food includes component one
With component two, the composition of the component one is sodium humate；The composition of the component two is laminarin, Platycarya strobilacea skin polyphenol is carried
Thing, chitin and lignin are taken,
The parts by weight of above-mentioned each material are specific as follows,
35 parts of sodium humate,
19 parts of laminarin,
2 parts of Platycarya strobilacea skin polyphenol extract,
4 parts of chitin,
7 parts of lignin.
The extracting method of the sodium humate is：
（1）Low-order coal is crushed to 150-400 mesh, the 5% sodium bicarbonate aqueous solution reaction 6-8h of 5 times of coal dust weight is added；
（2）After the completion of reaction, reaction product is purified and removed a huge sum of money alternately through macroreticular resin and strong ion exchange resin
Belong to element.
The low-order coal is weathered coal.
The macroreticular resin be middle polarity macroporous absorbent resin, the strong ion exchange resin for fold faintly acid sun from
Subtree fat.
The extracting method of the Platycarya strobilacea skin polyphenol extract comprises the following steps：
（1）Platycarya strobilacea skin through over cleaning removal of impurities is crushed, Platycarya strobilacea skin particle to be extracted is obtained；
（2）By step（1）Obtained Platycarya strobilacea skin particle to be extracted is with 1:15g/mL solid-liquid ratio is added in Extraction solvent,
Homogenization 7-10min, is separated by filtration supernatant liquor under 8000r/min rotating speed, obtains polyphenol extraction supernatant, wherein, institute
State the aqueous solution that Extraction solvent is the ethanol that volume by volume concentration is 40-50%；
（3）By step（2）Obtained polyphenol extraction supernatant is concentrated in vacuo to sticky shape under conditions of 55-65 DEG C, goes forward side by side one
Vacuum freeze drying is walked into powdered, Platycarya strobilacea skin polyphenol is produced.
Another aspect of the present invention provides a kind of preservation method of environmentally friendly antistaling agent for food, the preservation method
Comprise the following steps：
The preservation method is specific as follows：
（1）Parts by weight according to each material weigh sodium humate, laminarin, Platycarya strobilacea skin polyphenol extract, chitin and
Lignin, is divided into component one and component two, and component one and component two press 4:Carried out after 1 mass ratio mixing packed；
（2）Packed antistaling agent is placed in the environment for placing food.
Embodiment 4
A kind of environmentally friendly antistaling agent for food that the present embodiment is provided, the environmentally friendly antistaling agent for food includes component one
With component two, the composition of the component one is sodium humate；The composition of the component two is laminarin, Platycarya strobilacea skin polyphenol is carried
Thing, chitin and lignin are taken,
The parts by weight of above-mentioned each material are specific as follows,
20 parts of sodium humate,
23 parts of laminarin,
1 part of Platycarya strobilacea skin polyphenol extract,
5 parts of chitin,
5 parts of lignin.
The extracting method of the sodium humate is：
（1）Low-order coal is crushed to 150-400 mesh, the 5% sodium bicarbonate aqueous solution reaction 6-8h of 7 times of coal dust weight is added；
（2）After the completion of reaction, reaction product is purified and removed a huge sum of money alternately through macroreticular resin and strong ion exchange resin
Belong to element.
The low-order coal is weathered coal.
The macroreticular resin be middle polarity macroporous absorbent resin, the strong ion exchange resin for fold faintly acid sun from
Subtree fat.
The extracting method of the Platycarya strobilacea skin polyphenol extract comprises the following steps：
（1）Platycarya strobilacea skin through over cleaning removal of impurities is crushed, Platycarya strobilacea skin particle to be extracted is obtained；
（2）By step（1）Obtained Platycarya strobilacea skin particle to be extracted is with 1:12g/mL solid-liquid ratio is added in Extraction solvent,
Homogenization 7-10min, is separated by filtration supernatant liquor under 7500r/min rotating speed, obtains polyphenol extraction supernatant, wherein,
The Extraction solvent is the aqueous solution for the ethanol that volume by volume concentration is 40-50%；
（3）By step（2）Obtained polyphenol extraction supernatant is concentrated in vacuo to sticky shape under conditions of 55-65 DEG C, goes forward side by side one
Vacuum freeze drying is walked into powdered, Platycarya strobilacea skin polyphenol is produced.
Another aspect of the present invention provides a kind of preservation method of environmentally friendly antistaling agent for food, the preservation method
Comprise the following steps：
The preservation method is specific as follows：
（1）Parts by weight according to each material weigh sodium humate, laminarin, Platycarya strobilacea skin polyphenol extract, chitin and
Lignin, is divided into component one and component two, and component one and component two press 4:Carried out after 1 mass ratio mixing packed；
（2）Packed antistaling agent is placed in the environment for placing food.
Embodiment 5
A kind of environmentally friendly antistaling agent for food that the present embodiment is provided, the environmentally friendly antistaling agent for food includes component one
With component two, the composition of the component one is sodium humate；The composition of the component two is laminarin, Platycarya strobilacea skin polyphenol is carried
Thing, chitin and lignin are taken,
The parts by weight of above-mentioned each material are specific as follows,
23 parts of sodium humate,
21 parts of laminarin,
1 part of Platycarya strobilacea skin polyphenol extract,
4 parts of chitin,
6 parts of lignin.
The extracting method of the sodium humate is：
（1）Low-order coal is crushed to 150-400 mesh, the 5% sodium bicarbonate aqueous solution reaction 6-8h of 4 times of coal dust weight is added；
（2）After the completion of reaction, reaction product is purified and removed a huge sum of money alternately through macroreticular resin and strong ion exchange resin
Belong to element.
The low-order coal is weathered coal.
The macroreticular resin be middle polarity macroporous absorbent resin, the strong ion exchange resin for fold faintly acid sun from
Subtree fat.
The extracting method of the Platycarya strobilacea skin polyphenol extract comprises the following steps：
（1）Platycarya strobilacea skin through over cleaning removal of impurities is crushed, Platycarya strobilacea skin particle to be extracted is obtained；
（2）By step（1）Obtained Platycarya strobilacea skin particle to be extracted is with 1:11g/mL solid-liquid ratio is added in Extraction solvent,
Homogenization 7-10min, is separated by filtration supernatant liquor under 9000r/min rotating speed, obtains polyphenol extraction supernatant, wherein,
The Extraction solvent is the aqueous solution for the ethanol that volume by volume concentration is 40-50%；
（3）By step（2）Obtained polyphenol extraction supernatant is concentrated in vacuo to sticky shape under conditions of 55-65 DEG C, goes forward side by side one
Vacuum freeze drying is walked into powdered, Platycarya strobilacea skin polyphenol is produced.
Another aspect of the present invention provides a kind of preservation method of environmentally friendly antistaling agent for food, the preservation method
Comprise the following steps：
The preservation method is specific as follows：
（1）Parts by weight according to each material weigh sodium humate, laminarin, Platycarya strobilacea skin polyphenol extract, chitin and
Lignin, is divided into component one and component two, and component one and component two press 4:Carried out after 1 mass ratio mixing packed；
（2）Packed antistaling agent is placed in the environment for placing food.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (8)
1. a kind of environmentally friendly antistaling agent for food, it is characterised in that：The environmentally friendly antistaling agent for food includes component one
With component two, the composition of the component one is sodium humate；The composition of the component two is laminarin, Platycarya strobilacea skin polyphenol is carried
Thing, chitin and lignin are taken,
The parts by weight of above-mentioned each material are specific as follows,
20-55 parts of sodium humate,
15-23 parts of laminarin,
1-3 parts of Platycarya strobilacea skin polyphenol extract,
4-6 parts of chitin,
5-9 parts of lignin.
2. the environmentally friendly antistaling agent according to claim 1 for food, it is characterised in that：The environmental protection guarantor for food
Fresh dose includes component one and component two, and the composition of the component one is sodium humate；The composition of the component two be laminarin,
Platycarya strobilacea skin polyphenol extract, chitin and lignin,
The parts by weight of above-mentioned each material are specific as follows,
20-35 parts of sodium humate,
19-23 parts of laminarin,
1-2 parts of Platycarya strobilacea skin polyphenol extract,
4-5 parts of chitin,
5-7 parts of lignin.
3. the environmentally friendly antistaling agent according to claim 2 for food, it is characterised in that：The environmental protection guarantor for food
Fresh dose includes component one and component two, and the composition of the component one is sodium humate；The composition of the component two be laminarin,
Platycarya strobilacea skin polyphenol extract, chitin and lignin,
The parts by weight of above-mentioned each material are specific as follows,
23 parts of sodium humate,
21 parts of laminarin,
1 part of Platycarya strobilacea skin polyphenol extract,
4 parts of chitin,
6 parts of lignin.
4. the environmentally friendly antistaling agent according to claim 1 for food, it is characterised in that：The extraction side of the sodium humate
Method is：
（1）Low-order coal is crushed to 150-400 mesh, the 5% sodium bicarbonate aqueous solution reaction 6-8h of 3-8 times of coal dust weight is added；
（2）After the completion of reaction, reaction product is purified and removed a huge sum of money alternately through macroreticular resin and strong ion exchange resin
Belong to element.
5. the environmentally friendly antistaling agent according to claim 4 for food, it is characterised in that：The low-order coal is weathered coal.
6. the environmentally friendly antistaling agent according to claim 1 for food, it is characterised in that：The macroreticular resin is medium pole
Property macroporous absorbent resin, the strong ion exchange resin for fold acidulous cation resin.
7. the environmentally friendly antistaling agent according to claim 1 for food, it is characterised in that：The many phenol extractions of Platycarya strobilacea skin
The extracting method of thing comprises the following steps：
（1）Platycarya strobilacea skin through over cleaning removal of impurities is crushed, Platycarya strobilacea skin particle to be extracted is obtained；
（2）By step（1）Obtained Platycarya strobilacea skin particle to be extracted is with 1:9-1:21g/mL solid-liquid ratio is added to Extraction solvent
In, homogenization 7-10min, is separated by filtration supernatant liquor under 7000-11000r/min rotating speed, obtains polyphenol extraction supernatant
Liquid, wherein, the Extraction solvent is the aqueous solution for the ethanol that volume by volume concentration is 40-50%；
（3）By step（2）Obtained polyphenol extraction supernatant is concentrated in vacuo to sticky shape under conditions of 55-65 DEG C, goes forward side by side one
Vacuum freeze drying is walked into powdered, Platycarya strobilacea skin polyphenol is produced.
8. the preservation method of the environmentally friendly antistaling agent for food as described in claim any one of 1-7, it is characterised in that：It is described
Preservation method is specific as follows：
（1）Parts by weight according to each material weigh sodium humate, laminarin, Platycarya strobilacea skin polyphenol extract, chitin and
Lignin, is divided into component one and component two, and component one and component two press 4:Carried out after 1 mass ratio mixing packed；
（2）Packed antistaling agent is placed in the environment for placing food.
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH1146731A (en) * | 1997-08-07 | 1999-02-23 | Daiichi Seimo Kk | Refrigeration preservative for raw laver |
| CN102550657A (en) * | 2010-12-15 | 2012-07-11 | 戚冬梅 | Slow-release preservative for grape |
| CN202574850U (en) * | 2011-11-14 | 2012-12-05 | 大理学院 | Fresh-keeping anti-bacteria anti-oxidation packaging envelope made of active carbon and plant polyphenol |
| CN103719255A (en) * | 2013-12-27 | 2014-04-16 | 太原师范学院 | Preparation method of natural and edible fruit and vegetable fresh-keeping agent and prepared fruit and vegetable fresh-keeping agent |
| CN104304424A (en) * | 2014-10-24 | 2015-01-28 | 烟台朗博商贸有限公司 | Litchi and longan preservative taking nano chitosan as main component |
| CN104938646A (en) * | 2015-05-29 | 2015-09-30 | 武汉轻工大学 | Lotus root polyphenol extraction method, lotus root polyphenol oil-resistant oxidant preparation method, lotus root polyphenols, lotus root polyphenol oil-resistant oxidant, application of lotus root polyphenols, and application of lotus root polyphenol oil-resistant oxidant |
| CN106615074A (en) * | 2016-12-27 | 2017-05-10 | 渤海大学 | Composite biological fresh-keeping agent used for squid, and fresh-keeping method thereof |
-
2017
- 2017-06-08 CN CN201710425250.3A patent/CN107156599A/en not_active Withdrawn
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH1146731A (en) * | 1997-08-07 | 1999-02-23 | Daiichi Seimo Kk | Refrigeration preservative for raw laver |
| CN102550657A (en) * | 2010-12-15 | 2012-07-11 | 戚冬梅 | Slow-release preservative for grape |
| CN202574850U (en) * | 2011-11-14 | 2012-12-05 | 大理学院 | Fresh-keeping anti-bacteria anti-oxidation packaging envelope made of active carbon and plant polyphenol |
| CN103719255A (en) * | 2013-12-27 | 2014-04-16 | 太原师范学院 | Preparation method of natural and edible fruit and vegetable fresh-keeping agent and prepared fruit and vegetable fresh-keeping agent |
| CN104304424A (en) * | 2014-10-24 | 2015-01-28 | 烟台朗博商贸有限公司 | Litchi and longan preservative taking nano chitosan as main component |
| CN104938646A (en) * | 2015-05-29 | 2015-09-30 | 武汉轻工大学 | Lotus root polyphenol extraction method, lotus root polyphenol oil-resistant oxidant preparation method, lotus root polyphenols, lotus root polyphenol oil-resistant oxidant, application of lotus root polyphenols, and application of lotus root polyphenol oil-resistant oxidant |
| CN106615074A (en) * | 2016-12-27 | 2017-05-10 | 渤海大学 | Composite biological fresh-keeping agent used for squid, and fresh-keeping method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 候萍等: "海藻多糖用于食品涂膜保鲜的研究现状", 《热带农业科学》 * |
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Application publication date: 20170915 |