CN107156565A - A kind of production method of dendrobium candidum hawthorn beverage - Google Patents
A kind of production method of dendrobium candidum hawthorn beverage Download PDFInfo
- Publication number
- CN107156565A CN107156565A CN201710375516.8A CN201710375516A CN107156565A CN 107156565 A CN107156565 A CN 107156565A CN 201710375516 A CN201710375516 A CN 201710375516A CN 107156565 A CN107156565 A CN 107156565A
- Authority
- CN
- China
- Prior art keywords
- hawthorn
- juice
- dendrobium candidum
- bottle
- technology
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000009917 Crataegus X brevipes Nutrition 0.000 title claims abstract description 73
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 title claims abstract description 73
- 235000009685 Crataegus X maligna Nutrition 0.000 title claims abstract description 73
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 title claims abstract description 73
- 235000009486 Crataegus bullatus Nutrition 0.000 title claims abstract description 73
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 title claims abstract description 73
- 235000009682 Crataegus limnophila Nutrition 0.000 title claims abstract description 73
- 235000004423 Crataegus monogyna Nutrition 0.000 title claims abstract description 73
- 235000002313 Crataegus paludosa Nutrition 0.000 title claims abstract description 73
- 235000009840 Crataegus x incaedua Nutrition 0.000 title claims abstract description 73
- 241000026010 Dendrobium candidum Species 0.000 title claims abstract description 61
- 235000013361 beverage Nutrition 0.000 title claims abstract description 12
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 9
- 240000000171 Crataegus monogyna Species 0.000 title 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 81
- 241001092040 Crataegus Species 0.000 claims abstract description 72
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 50
- 238000002386 leaching Methods 0.000 claims abstract description 27
- 238000009835 boiling Methods 0.000 claims abstract description 19
- 238000000034 method Methods 0.000 claims abstract description 10
- 230000001954 sterilising effect Effects 0.000 claims abstract description 10
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 10
- 229920001277 pectin Polymers 0.000 claims abstract description 6
- 235000010987 pectin Nutrition 0.000 claims abstract description 6
- 239000001814 pectin Substances 0.000 claims abstract description 6
- 239000002932 luster Substances 0.000 claims abstract description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 24
- 238000007689 inspection Methods 0.000 claims description 16
- 239000007788 liquid Substances 0.000 claims description 16
- 238000001914 filtration Methods 0.000 claims description 15
- 239000012153 distilled water Substances 0.000 claims description 14
- 238000000605 extraction Methods 0.000 claims description 14
- 238000010008 shearing Methods 0.000 claims description 13
- 238000001816 cooling Methods 0.000 claims description 9
- 230000001186 cumulative effect Effects 0.000 claims description 9
- 235000012907 honey Nutrition 0.000 claims description 9
- 238000007789 sealing Methods 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 9
- 241000206575 Chondrus crispus Species 0.000 claims description 8
- 239000011521 glass Substances 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- 238000012545 processing Methods 0.000 claims description 8
- 239000006185 dispersion Substances 0.000 claims description 7
- 230000001804 emulsifying effect Effects 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 3
- 238000002137 ultrasound extraction Methods 0.000 claims description 3
- 238000011049 filling Methods 0.000 claims description 2
- 238000000265 homogenisation Methods 0.000 claims description 2
- 238000007654 immersion Methods 0.000 claims description 2
- 230000014759 maintenance of location Effects 0.000 claims description 2
- 239000002893 slag Substances 0.000 claims description 2
- 241000256844 Apis mellifera Species 0.000 claims 1
- 240000008866 Ziziphus nummularia Species 0.000 claims 1
- 230000005611 electricity Effects 0.000 claims 1
- 238000005516 engineering process Methods 0.000 abstract description 16
- 150000004676 glycans Chemical class 0.000 abstract description 7
- 235000016709 nutrition Nutrition 0.000 abstract description 7
- 229920001282 polysaccharide Polymers 0.000 abstract description 7
- 239000005017 polysaccharide Substances 0.000 abstract description 7
- 239000002994 raw material Substances 0.000 abstract description 7
- 239000004615 ingredient Substances 0.000 abstract description 5
- 230000000050 nutritive effect Effects 0.000 abstract description 5
- 241001523681 Dendrobium Species 0.000 abstract description 4
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 2
- 239000000047 product Substances 0.000 description 24
- 241000238631 Hexapoda Species 0.000 description 10
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 10
- 241000607479 Yersinia pestis Species 0.000 description 10
- 239000002270 dispersing agent Substances 0.000 description 10
- 239000000706 filtrate Substances 0.000 description 10
- 239000002245 particle Substances 0.000 description 10
- 239000000463 material Substances 0.000 description 7
- 241001247821 Ziziphus Species 0.000 description 6
- 238000012935 Averaging Methods 0.000 description 5
- 240000004638 Dendrobium nobile Species 0.000 description 5
- 238000004458 analytical method Methods 0.000 description 5
- 239000008367 deionised water Substances 0.000 description 5
- 229910021641 deionized water Inorganic materials 0.000 description 5
- 229910052738 indium Inorganic materials 0.000 description 5
- 229910052742 iron Inorganic materials 0.000 description 5
- 238000005259 measurement Methods 0.000 description 5
- 238000003921 particle size analysis Methods 0.000 description 5
- 229920000642 polymer Polymers 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- 235000001014 amino acid Nutrition 0.000 description 4
- 150000001413 amino acids Chemical class 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- IAJILQKETJEXLJ-UHFFFAOYSA-N Galacturonsaeure Natural products O=CC(O)C(O)C(O)C(O)C(O)=O IAJILQKETJEXLJ-UHFFFAOYSA-N 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 229930003935 flavonoid Natural products 0.000 description 2
- 150000002215 flavonoids Chemical class 0.000 description 2
- 235000017173 flavonoids Nutrition 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 210000002784 stomach Anatomy 0.000 description 2
- 235000018553 tannin Nutrition 0.000 description 2
- 229920001864 tannin Polymers 0.000 description 2
- 239000001648 tannin Substances 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- AEMOLEFTQBMNLQ-YMDCURPLSA-N D-galactopyranuronic acid Chemical compound OC1O[C@H](C(O)=O)[C@H](O)[C@H](O)[C@H]1O AEMOLEFTQBMNLQ-YMDCURPLSA-N 0.000 description 1
- AEMOLEFTQBMNLQ-AQKNRBDQSA-N D-glucopyranuronic acid Chemical compound OC1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O AEMOLEFTQBMNLQ-AQKNRBDQSA-N 0.000 description 1
- RYAHJFGVOCZDEI-UFFNCVEVSA-N Dendrobine Chemical compound C([C@H]1CC[C@@H]2[C@@]31C)N(C)[C@@H]3[C@H]1[C@@H](C(C)C)[C@@H]2C(=O)O1 RYAHJFGVOCZDEI-UFFNCVEVSA-N 0.000 description 1
- 241001076416 Dendrobium tosaense Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 description 1
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 description 1
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 1
- PVNIIMVLHYAWGP-UHFFFAOYSA-N Niacin Chemical compound OC(=O)C1=CC=CN=C1 PVNIIMVLHYAWGP-UHFFFAOYSA-N 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 235000003704 aspartic acid Nutrition 0.000 description 1
- OQFSQFPPLPISGP-UHFFFAOYSA-N beta-carboxyaspartic acid Natural products OC(=O)C(N)C(C(O)=O)C(O)=O OQFSQFPPLPISGP-UHFFFAOYSA-N 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- RYAHJFGVOCZDEI-CZKZLRAZSA-N dendrobine Natural products O=C1O[C@@H]2[C@H](C(C)C)[C@H]1[C@H]1[C@@]3(C)[C@@H]2N(C)C[C@H]3CC1 RYAHJFGVOCZDEI-CZKZLRAZSA-N 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- XHCADAYNFIFUHF-TVKJYDDYSA-N esculin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC(C(=C1)O)=CC2=C1OC(=O)C=C2 XHCADAYNFIFUHF-TVKJYDDYSA-N 0.000 description 1
- QOLIPNRNLBQTAU-UHFFFAOYSA-N flavan Chemical compound C1CC2=CC=CC=C2OC1C1=CC=CC=C1 QOLIPNRNLBQTAU-UHFFFAOYSA-N 0.000 description 1
- 210000004051 gastric juice Anatomy 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 229940097043 glucuronic acid Drugs 0.000 description 1
- 235000013922 glutamic acid Nutrition 0.000 description 1
- 239000004220 glutamic acid Substances 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 229960003512 nicotinic acid Drugs 0.000 description 1
- 235000001968 nicotinic acid Nutrition 0.000 description 1
- 239000011664 nicotinic acid Substances 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- PJANXHGTPQOBST-UHFFFAOYSA-N stilbene Chemical class C=1C=CC=CC=1C=CC1=CC=CC=C1 PJANXHGTPQOBST-UHFFFAOYSA-N 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 150000003648 triterpenes Chemical class 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/04—Extraction of juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/42—Preservation of non-alcoholic beverages
- A23L2/46—Preservation of non-alcoholic beverages by heating
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a kind of production method of dendrobium candidum hawthorn beverage, using color protection technology of precooking, hawthorn is placed in boiling water the 10~15min that precooks, so that the pectin in hawthorn is sufficiently damaged, in addition to keeping the scarlet color and luster of hawthorn, the nutritional ingredient of hawthorn is also maintained to a certain extent, improves product nutritive value.Dendrobium candidum juice is prepared using crushing technology and ultrasonic microwave leaching technology, by increasing contact area and changing microwave leaching technology, the leaching rate of dendrobium polysaccharide is farthest improved, makes full use of raw material, enhance the medical value of dendrobium candidum, lift product nutritive value.Dendrobium candidum hawthorn beverage is handled using boiling water sterilization technology, while bactericidal effect is reached, maintains the nutritional ingredient of product stable, maintains the quality of product.The technology greatlys save production cost, shortens process time, improves raw material availability, lifts product quality.
Description
Technical field
The invention belongs to food-processing method technical field, and in particular to a kind of producer of dendrobium candidum hawthorn beverage
Method.
Background technology
Hawthorn nutritive value very abundant, wherein, the nutrition such as carbohydrate, dietary fiber, lipid, vitamin, inorganic salts, pectin
The rich content of material, also containing a small amount of niacin tannin etc..Containing 6.4% pectin in hawthorn, its content is in fruit
It is highest.Containing abundant amino acid in Fructus Crataegi, 1.57% one the 2.90% of hawthorn total amount are accounted for.
Dendrobium polysaccharide, dendrobine and total amino acid etc. are the most important effect compositions of dendrobium candidum.In addition, dendrobium candidum is also
Constituted containing stilbene class, volatility.Research finds that dendrobium candidum contains 17 kinds of amino acid such as glutamic acid, aspartic acid and Cu, Mn
Etc. a large amount of needed by human body metallic elements.Wherein dendrobium polysaccharide content number be identify dendrobium candidum quality important indicator.Stone
Dry measure used in former times polysaccharide is mainly made up of glucose, galactolipin, glucuronic acid, galacturonic acid etc., and specific composition is abundant in polysaccharide.
Dendrobium candidum contains the nutritional ingredients such as carbohydrate, amino acid, trace element, with very high nutritive value.And hawthorn
On the one hand be richly stored with organic acid, in addition to vitamin C can be protected not to be destroyed at high temperature, moreover it is possible to improve stomach enzyme activity
Property, stimulate gastric juice to produce, strengthen stomach regular movements, promote food to decompose to absorb；Crataegin, Hu Luo are also rich in another aspect hawthorn
The Flavonoid substances such as the triterpenes such as Bu Su olefin(e) acid and tannin, flavonoids poly flavane, can strengthen blood flow, reduce blood fat and blood pressure.
The material of dendrobium candidum, hawthorn, honey these three integration of drinking and medicinal herbs is combined, people can be met to a certain extent because of life
The raising of level and be particular about nutrition, focus on the requirement of health care, and greatly played effect of dendrobium candidum, hawthorn, honey.
The content of the invention
The problem of existing for prior art, it is an object of the invention to design to provide a kind of dendrobium candidum hawthorn beverage
The technical scheme of production method.
A kind of production method of described dendrobium candidum hawthorn beverage, is comprised the following steps that：
1) hawthorn is precooked color retention：5.0000g hawthorn are weighed with electronic balance, hawthorn is placed in boiling water and precooks 10~
15min so that the pectin in hawthorn is sufficiently damaged, keeps the scarlet color and luster of hawthorn；
2) hawthorn immersion treatment：By step 1) obtained hawthorn and distilled water by solid-liquid ratio is 1:40 (v/v) load glass
In bottle, bottle is placed in 70 DEG C of water-bath and soaks 50min；
3) hawthorn is squeezed the juice processing：By step 2) obtained hawthorn all poured into juice extractor, by the extraction of the 50mL in bottle
Liquid is poured into juice extractor, and first squeeze the juice 1min, then the leaching liquor of the 50mL in bottle is poured into juice extractor, then the 1min that squeezes the juice, finally
Remaining 100mL leaching liquors are poured into juice extractor, squeeze the juice 2min, after the completion of stand 1min；
4) haw juice filtration treatment：By step 3) obtained haw juice carries out filter cleaners by three layers of gauze；
5) dendrobium candidum break process；
6) dendrobium candidum extraction is handled：By step 5) obtained dendrobium candidum powder filters by 40 mesh standard inspection sieves,
With electronic balance weighing 5.0000g dendrobium candidum powder, load weighted powder is placed in ultrasound extraction in ultrasonic environment, extraction
Liquid is distilled water, and setting ultrasonic power is 105~135W, and ultrasonic time is 3~5h, and solid-liquid ratio is 1:40~1:45v/v, ultrasound
Temperature is 60 DEG C；
7) dendrobium candidum juice filtration treatment：By step 6) dendrobium candidum juice carried out by 80 mesh standard inspection sieves
Filter out slag；
8) hydromel preparation is handled：Jujube flower honey 100g is weighed with electronic analytical balance to be placed in beaker, in mass ratio for
1:8 amount adds 40 DEG C of warm water stirring and dissolving；
9) allocation processing：By step 4) filtering after haw juice, step 7) filtering after dendrobium candidum juice, step 8) obtain
Hydromel according to 2:1:12 volume ratio ratio mixing, addition 0.04% (by the calculating of mixed liquor cumulative volume) citric acid,
0.05% (being calculated by mixed liquor cumulative volume) carragheen stirs；
10) homogenization is sheared：Deployed mixed liquor is sheared into 2min with FA25 types high-shearing dispersion emulsifying machine, will be cut
Solution after cutting is preheated to 50 DEG C, homogeneous 2 times under 25MPa pressure, then with the filtering of 80 mesh standard inspection sieves once；
11) bottling is handled：By step 10) obtained mixed liquor is fitted into vial, per bottled 150mL, covers tightly bottle cap, make
Obtain vial sealing；
12) cooling treatment is sterilized, dendrobium candidum hawthorn beverage is obtained：By step 11) the good mixed liquor of filling and sealing is put into
Sterilization 20min is boiled in water-bath in 100 DEG C of boiling water, is placed on and is stored at room temperature cooling 15min.
The present invention is using dendrobium candidum, hawthorn as raw material, using anti-oxidation tech, cell breaking technology, ultrasound extraction skill
The food processing new technologies such as art, boiling water sterilization technology, are made dendrobium candidum hawthorn mixed juice, and in this, as dendrobium candidum hawthorn
The raw material of beverage processing；With the dispensing mixing preparation such as hydromel, carragheen and citric acid.In product processing, it is to avoid
Destruction of the hot-working to nutriments such as hawthorn vitamins, improves the leaching rate of Dendrobium officinale polysaccharide, improves raw material utilization
Rate, strengthens the medicinal efficacy of dendrobium candidum, greatlys save production cost, improves product quality.This is for the comprehensive of dendrobium candidum
Running the research and development of hair and higher value application and similar-type products jointly has practical significance.
Compared with prior art, the invention has the advantages that：
1. using color protection technology of precooking, hawthorn is placed in boiling water the 10~15min that precooks so that the pectin in hawthorn is filled
Divide destruction, in addition to keeping the scarlet color and luster of hawthorn, the nutritional ingredient of hawthorn is also maintained to a certain extent, improve product battalion
Support value.
2. preparing dendrobium candidum juice using crushing technology and ultrasonic microwave leaching technology, extracted by increasing contact area and changing
Technology, farthest improves the leaching rate of dendrobium polysaccharide, makes full use of raw material, enhances the medical value of dendrobium candidum,
Lift product nutritive value.
3. using boiling water sterilization technology processing dendrobium candidum hawthorn beverage, while bactericidal effect is reached, maintain product
Nutritional ingredient it is stable, maintain the quality of product.
4. the technology greatlys save production cost, process time is shortened, raw material availability is improved, product product are lifted
Matter.
Embodiment
Further illustrate the present invention with reference to embodiments.
Embodiment 1
From it is fresh, without rot, the dry hawthorn without insect pest, weigh 5.000g with electronic balance, hawthorn be placed in boiling water
Precook 10min, by solid-liquid ratio is 1 by the hawthorn after precooking and distilled water:40 (v/v) are fitted into vial, and bottle is placed on
50min is soaked in 70 DEG C of water-bath, all pours into hawthorn in juice extractor after the completion of extraction, by the leaching liquor of the 50mL in bottle
Pour into juice extractor, first squeeze the juice 1min, then the leaching liquor of the 50mL in bottle is poured into juice extractor, then the 1min that squeezes the juice, finally handle
Remaining 100mL leaching liquors pour into juice extractor, and squeeze the juice 2min.1min is stood after completing juice-extracting process, then by the mountain after squeezing the juice
Short, bristly hair or beard juice carries out filter cleaner by three layers of gauze.
Jujube flower honey 100g is weighed with electronic analytical balance to be placed in beaker, is in mass ratio 1:8 amount adds 40 DEG C
Warm water stirring and dissolving.
From it is fresh, without rot, the dry dendrobium candidum without insect pest, is carried out with disintegrating machine fully crush, with electronic analysis day
Flat to weigh the dendrobium candidum 5.000g crushed, it is 1 that dendrobium candidum and distilled water are pressed into solid-liquid ratio:40 (v/v) load vial
In, in the water that bottle is immersed in 60 DEG C, under the conditions of ultrasonic power is 105W, extract 5h.By the iron in bottle after the completion of extraction
Skin stem of noble dendrobium juice carries out filter cleaner by 80 mesh standard inspection sieves.By dendrobium candidum filtrate 10mL, hawthorn filtrate 20mL, hydromel
120mL, 0.04% citric acid (being calculated according to mixed liquor cumulative volume) and 0.05% carragheen are (according to mixed liquor total volume meter
Calculate) mixing, after being stirred with glass bar, 2min is sheared with FA25 types high-shearing dispersion emulsifying machine, the solution after shearing is pre-
Heat is to 50 DEG C, homogeneous 2 times under 25MPa pressure, then with the filtering of 80 mesh standard inspection sieves once, solution then is loaded into clean
And in dried vial, per bottled 150mL, canned rear sealing boiling water sterilization 20min is being stored at room temperature cooling
15min。
The product of gained measures product using hand-held saccharometer, and gained solid content 9.2% uses laser particle size analysis
Instrument measures product, and averaging of income particle diameter is 1039.0d.nm.Grain diameter measurement institute setting parameter：Measured material is high polymer, dispersant
For deionized water, the refraction index of sample particle is that 1.590, absorbancy index is 0.010, and dispersant refraction index is 1.330, glued
Degree be 0.8872cP, temperature be 25 DEG C.
Embodiment 2
From it is fresh, without rot, the dry hawthorn without insect pest, weigh 5.000g with electronic balance, hawthorn be placed in boiling water
Precook 12min, by solid-liquid ratio is 1 by the hawthorn after precooking and distilled water:40 (v/v) are fitted into vial, and bottle is placed on
50min is soaked in 70 DEG C of water-bath, all pours into hawthorn in juice extractor after the completion of extraction, by the leaching liquor of the 50mL in bottle
Pour into juice extractor, first squeeze the juice 1min, then the leaching liquor of the 50mL in bottle is poured into juice extractor, then the 1min that squeezes the juice, finally handle
Remaining 100mL leaching liquors pour into juice extractor, and squeeze the juice 2min.1min is stood after completing juice-extracting process, then by the mountain after squeezing the juice
Short, bristly hair or beard juice carries out filter cleaner by three layers of gauze.
Jujube flower honey 100g is weighed with electronic analytical balance to be placed in beaker, is in mass ratio 1:8 amount adds 40 DEG C
Warm water stirring and dissolving.
From it is fresh, without rot, the dry dendrobium candidum without insect pest, is carried out with disintegrating machine fully crush, with electronic analysis day
Flat to weigh the dendrobium candidum 5.000g crushed, it is 1 that dendrobium candidum and distilled water are pressed into solid-liquid ratio:40 (v/v) load vial
In, in the water that bottle is immersed in 60 DEG C, under the conditions of ultrasonic power is 110W, extract 5h.By the iron in bottle after the completion of extraction
Skin stem of noble dendrobium juice carries out filter cleaner by 80 mesh standard inspection sieves.By dendrobium candidum filtrate 10mL, hawthorn filtrate 20mL, hydromel
120mL, 0.04% citric acid (being calculated according to mixed liquor cumulative volume) and 0.05% carragheen are (according to mixed liquor total volume meter
Calculate) mixing, after being stirred with glass bar, 2min is sheared with FA25 types high-shearing dispersion emulsifying machine, the solution after shearing is pre-
Heat is to 50 DEG C, homogeneous 2 times under 25MPa pressure, then with the filtering of 80 mesh standard inspection sieves once, solution then is loaded into clean
And in dried vial, per bottled 150mL, canned rear sealing boiling water sterilization 20min is being stored at room temperature cooling
15min。
The product of gained measures product using hand-held saccharometer, and gained solid content 9.0% uses laser particle size analysis
Instrument measures product, and averaging of income particle diameter is 1048.1d.nm.Grain diameter measurement institute setting parameter：Measured material is high polymer, dispersant
For deionized water, the refraction index of sample particle is that 1.590, absorbancy index is 0.010, and dispersant refraction index is 1.330, glued
Degree be 0.8872cP, temperature be 25 DEG C.
Embodiment 3
From it is fresh, without rot, the dry hawthorn without insect pest, weigh 5.000g with electronic balance, hawthorn be placed in boiling water
Precook 12min, by solid-liquid ratio is 1 by the hawthorn after precooking and distilled water:40 (v/v) are fitted into vial, and bottle is placed on
50min is soaked in 70 DEG C of water-bath, all pours into hawthorn in juice extractor after the completion of extraction, by the leaching liquor of the 50mL in bottle
Pour into juice extractor, first squeeze the juice 1min, then the leaching liquor of the 50mL in bottle is poured into juice extractor, then the 1min that squeezes the juice, finally handle
Remaining 100mL leaching liquors pour into juice extractor, and squeeze the juice 2min.1min is stood after completing juice-extracting process, then by the mountain after squeezing the juice
Short, bristly hair or beard juice carries out filter cleaner by three layers of gauze.
Jujube flower honey 100g is weighed with electronic analytical balance to be placed in beaker, is in mass ratio 1:8 amount adds 40 DEG C
Warm water stirring and dissolving.
From it is fresh, without rot, the dry dendrobium candidum without insect pest, is carried out with disintegrating machine fully crush, with electronic analysis day
Flat to weigh the dendrobium candidum 5.000g crushed, it is 1 that dendrobium candidum and distilled water are pressed into solid-liquid ratio:40 (v/v) load vial
In, in the water that bottle is immersed in 60 DEG C, under the conditions of ultrasonic power is 115W, extract 4h.By the iron in bottle after the completion of extraction
Skin stem of noble dendrobium juice carries out filter cleaner by 80 mesh standard inspection sieves.By dendrobium candidum filtrate 10mL, hawthorn filtrate 20mL, hydromel
120mL, 0.04% citric acid (being calculated according to mixed liquor cumulative volume) and 0.05% carragheen are (according to mixed liquor total volume meter
Calculate) mixing, after being stirred with glass bar, 2min is sheared with FA25 types high-shearing dispersion emulsifying machine, the solution after shearing is pre-
Heat is to 50 DEG C, homogeneous 2 times under 25MPa pressure, then with the filtering of 80 mesh standard inspection sieves once, solution then is loaded into clean
And in dried vial, per bottled 150mL, canned rear sealing boiling water sterilization 20min is being stored at room temperature cooling
15min。
The product of gained measures product using hand-held saccharometer, and gained solid content 9.2% uses laser particle size analysis
Instrument measures product, and averaging of income particle diameter is 1031.0d.nm.Grain diameter measurement institute setting parameter：Measured material is high polymer, dispersant
For deionized water, the refraction index of sample particle is that 1.590, absorbancy index is 0.010, and dispersant refraction index is 1.330, glued
Degree be 0.8872cP, temperature be 25 DEG C.
Embodiment 4
From it is fresh, without rot, the dry hawthorn without insect pest, weigh 5.000g with electronic balance, hawthorn be placed in boiling water
Precook 12min, by solid-liquid ratio is 1 by the hawthorn after precooking and distilled water:40 (v/v) are fitted into vial, and bottle is placed on
50min is soaked in 70 DEG C of water-bath, all pours into hawthorn in juice extractor after the completion of extraction, by the leaching liquor of the 50mL in bottle
Pour into juice extractor, first squeeze the juice 1min, then the leaching liquor of the 50mL in bottle is poured into juice extractor, then the 1min that squeezes the juice, finally handle
Remaining 100mL leaching liquors pour into juice extractor, and squeeze the juice 2min.1min is stood after completing juice-extracting process, then by the mountain after squeezing the juice
Short, bristly hair or beard juice carries out filter cleaner by three layers of gauze.
Jujube flower honey 100g is weighed with electronic analytical balance to be placed in beaker, is in mass ratio 1:8 amount adds 40 DEG C
Warm water stirring and dissolving.
From it is fresh, without rot, the dry dendrobium candidum without insect pest, is carried out with disintegrating machine fully crush, with electronic analysis day
Flat to weigh the dendrobium candidum 5.000g crushed, it is 1 that dendrobium candidum and distilled water are pressed into solid-liquid ratio:40 (v/v) load vial
In, in the water that bottle is immersed in 60 DEG C, under the conditions of ultrasonic power is 120W, extract 4h.By the iron in bottle after the completion of extraction
Skin stem of noble dendrobium juice carries out filter cleaner by 80 mesh standard inspection sieves.By dendrobium candidum filtrate 10mL, hawthorn filtrate 20mL, hydromel
120mL, 0.04% citric acid (being calculated according to mixed liquor cumulative volume) and 0.05% carragheen are (according to mixed liquor total volume meter
Calculate) mixing, after being stirred with glass bar, 2min is sheared with FA25 types high-shearing dispersion emulsifying machine, the solution after shearing is pre-
Heat is to 50 DEG C, homogeneous 2 times under 25MPa pressure, then with the filtering of 80 mesh standard inspection sieves once, solution then is loaded into clean
And in dried vial, per bottled 150mL, canned rear sealing boiling water sterilization 20min is being stored at room temperature cooling
15min。
The product of gained measures product using hand-held saccharometer, and gained solid content 9.1% uses laser particle size analysis
Instrument measures product, and averaging of income particle diameter is 1033.6d.nm.Grain diameter measurement institute setting parameter：Measured material is high polymer, dispersant
For deionized water, the refraction index of sample particle is that 1.590, absorbancy index is 0.010, and dispersant refraction index is 1.330, glued
Degree be 0.8872cP, temperature be 25 DEG C.
Embodiment 5
From it is fresh, without rot, the dry hawthorn without insect pest, weigh 5.000g with electronic balance, hawthorn be placed in boiling water
Precook 12min, by solid-liquid ratio is 1 by the hawthorn after precooking and distilled water:40 (v/v) are fitted into vial, and bottle is placed on
50min is soaked in 70 DEG C of water-bath, all pours into hawthorn in juice extractor after the completion of extraction, by the leaching liquor of the 50mL in bottle
Pour into juice extractor, first squeeze the juice 1min, then the leaching liquor of the 50mL in bottle is poured into juice extractor, then the 1min that squeezes the juice, finally handle
Remaining 100mL leaching liquors pour into juice extractor, and squeeze the juice 2min.1min is stood after completing juice-extracting process, then by the mountain after squeezing the juice
Short, bristly hair or beard juice carries out filter cleaner by three layers of gauze.
Jujube flower honey 100g is weighed with electronic analytical balance to be placed in beaker, is in mass ratio 1:8 amount adds 40 DEG C
Warm water stirring and dissolving.
From it is fresh, without rot, the dry dendrobium candidum without insect pest, is carried out with disintegrating machine fully crush, with electronic analysis day
Flat to weigh the dendrobium candidum 5.000g crushed, it is 1 that dendrobium candidum and distilled water are pressed into solid-liquid ratio:40 (v/v) load vial
In, in the water that bottle is immersed in 60 DEG C, under the conditions of ultrasonic power is 130W, extract 3h.By the iron in bottle after the completion of extraction
Skin stem of noble dendrobium juice carries out filter cleaner by 80 mesh standard inspection sieves.By dendrobium candidum filtrate 10mL, hawthorn filtrate 20mL, hydromel
120mL, 0.04% citric acid (being calculated according to mixed liquor cumulative volume) and 0.05% carragheen are (according to mixed liquor total volume meter
Calculate) mixing, after being stirred with glass bar, 2min is sheared with FA25 types high-shearing dispersion emulsifying machine, the solution after shearing is pre-
Heat is to 50 DEG C, homogeneous 2 times under 25MPa pressure, then with the filtering of 80 mesh standard inspection sieves once, solution then is loaded into clean
And in dried vial, per bottled 150mL, canned rear sealing boiling water sterilization 20min is being stored at room temperature cooling
15min。
The product of gained measures product using hand-held saccharometer, and gained solid content 9.3% uses laser particle size analysis
Instrument measures product, and averaging of income particle diameter is 1040.5d.nm.Grain diameter measurement institute setting parameter：Measured material is high polymer, dispersant
For deionized water, the refraction index of sample particle is that 1.590, absorbancy index is 0.010, and dispersant refraction index is 1.330, glued
Degree be 0.8872cP, temperature be 25 DEG C.
Claims (1)
1. a kind of production method of dendrobium candidum hawthorn beverage, it is characterised in that comprise the following steps that：
1) hawthorn is precooked color retention：5.0000g hawthorn are weighed with electronic balance, hawthorn is placed in boiling water and precooks 10~
15min so that the pectin in hawthorn is sufficiently damaged, keeps the scarlet color and luster of hawthorn；
2) hawthorn immersion treatment：By step 1) obtained hawthorn and distilled water by solid-liquid ratio is 1:40 (v/v) are fitted into vial,
Bottle is placed in 70 DEG C of water-bath and soaks 50min；
3) hawthorn is squeezed the juice processing：By step 2) obtained hawthorn all pours into juice extractor, the leaching liquor of the 50mL in bottle fallen
Enter in juice extractor, first squeeze the juice 1min, then the leaching liquor of the 50mL in bottle is poured into juice extractor, then the 1min that squeezes the juice, finally surplus
Remaining 100mL leaching liquors pour into juice extractor, and squeeze the juice 2min, after the completion of stand 1min；
4) haw juice filtration treatment：By step 3) obtained haw juice carries out filter cleaners by three layers of gauze；
5) dendrobium candidum break process；
6) dendrobium candidum extraction is handled：By step 5) obtained dendrobium candidum powder filters by 40 mesh standard inspection sieves, electricity consumption
Sub- balance weighs 5.0000g dendrobium candidum powder, and load weighted powder is placed in into ultrasound extraction in ultrasonic environment, and leaching liquor is
Distilled water, setting ultrasonic power is 105~135W, and ultrasonic time is 3~5h, and solid-liquid ratio is 1:40~1:45v/v, ultrasonic temperature
For 60 DEG C；
7) dendrobium candidum juice filtration treatment：By step 6) dendrobium candidum juice filtered out by 80 mesh standard inspection sieves
Slag；
8) hydromel preparation is handled：Jujube flower honey 100g is weighed with electronic analytical balance to be placed in beaker, is in mass ratio 1:8
Amount adds 40 DEG C of warm water stirring and dissolving；
9) allocation processing：By step 4) haw juice after filtering, step 7) dendrobium candidum juice after filtering, step 8) obtained honeybee
Mulse is according to 2:1:12 volume ratio ratio mixing, addition 0.04% (by the calculating of mixed liquor cumulative volume) citric acid, 0.05% (are pressed
Mixed liquor cumulative volume is calculated) carragheen stirs；
10) homogenization is sheared：Deployed mixed liquor is sheared into 2min with FA25 types high-shearing dispersion emulsifying machine, after shearing
Solution be preheated to 50 DEG C, homogeneous 2 times under 25MPa pressure, then with 80 mesh standard inspection sieves filtering once；
11) bottling is handled：By step 10) obtained mixed liquor is fitted into vial, per bottled 150mL, covers tightly bottle cap so that glass
Glass bottle sealing；
12) cooling treatment is sterilized, dendrobium candidum hawthorn beverage is obtained：By step 11) the good mixed liquor of filling and sealing is put into 100 DEG C
Boiling water in water-bath boil sterilization 20min, be placed on be stored at room temperature cooling 15min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710375516.8A CN107156565A (en) | 2017-05-24 | 2017-05-24 | A kind of production method of dendrobium candidum hawthorn beverage |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710375516.8A CN107156565A (en) | 2017-05-24 | 2017-05-24 | A kind of production method of dendrobium candidum hawthorn beverage |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107156565A true CN107156565A (en) | 2017-09-15 |
Family
ID=59822335
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710375516.8A Pending CN107156565A (en) | 2017-05-24 | 2017-05-24 | A kind of production method of dendrobium candidum hawthorn beverage |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107156565A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107788310A (en) * | 2017-09-27 | 2018-03-13 | 霍山宝信园石斛开发有限公司 | A kind of dendrobium stem beverage formula |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1943450A (en) * | 2005-10-09 | 2007-04-11 | 葛松松 | Method for making dendrobe compound tea (beverage) |
| CN101744334A (en) * | 2008-12-09 | 2010-06-23 | 杨军 | Health-care drink containing dendrobium |
| CN103564587A (en) * | 2013-11-05 | 2014-02-12 | 云南韵雅生物科技有限公司 | Natural fulvic acid compound health-care beverage as well as preparation method thereof |
| CN104041874A (en) * | 2013-03-14 | 2014-09-17 | 沭阳县苏合农产品销售专业合作联社 | Processing method for hawthorn drink |
| CN104491478A (en) * | 2015-01-15 | 2015-04-08 | 福建农林大学 | Sedum aizoon buccal tablet and preparation method thereof |
| CN104643078A (en) * | 2015-02-15 | 2015-05-27 | 福建卫生职业技术学院 | Compound dendrobium officinale health oral liquid and preparation method thereof |
| CN106509523A (en) * | 2016-09-30 | 2017-03-22 | 林伟欣 | Deer skin glue beverage |
-
2017
- 2017-05-24 CN CN201710375516.8A patent/CN107156565A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1943450A (en) * | 2005-10-09 | 2007-04-11 | 葛松松 | Method for making dendrobe compound tea (beverage) |
| CN101744334A (en) * | 2008-12-09 | 2010-06-23 | 杨军 | Health-care drink containing dendrobium |
| CN104041874A (en) * | 2013-03-14 | 2014-09-17 | 沭阳县苏合农产品销售专业合作联社 | Processing method for hawthorn drink |
| CN103564587A (en) * | 2013-11-05 | 2014-02-12 | 云南韵雅生物科技有限公司 | Natural fulvic acid compound health-care beverage as well as preparation method thereof |
| CN104491478A (en) * | 2015-01-15 | 2015-04-08 | 福建农林大学 | Sedum aizoon buccal tablet and preparation method thereof |
| CN104643078A (en) * | 2015-02-15 | 2015-05-27 | 福建卫生职业技术学院 | Compound dendrobium officinale health oral liquid and preparation method thereof |
| CN106509523A (en) * | 2016-09-30 | 2017-03-22 | 林伟欣 | Deer skin glue beverage |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107788310A (en) * | 2017-09-27 | 2018-03-13 | 霍山宝信园石斛开发有限公司 | A kind of dendrobium stem beverage formula |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102919417A (en) | Honey tea and preparation method thereof | |
| CN102578648A (en) | Fruit juice beverage | |
| CN102138604A (en) | Blood activating and menstruation normalizing tea | |
| CN103719677A (en) | Lotus root glutinous rice cake | |
| CN106666007A (en) | Preparation method of camellia ampiexicaulis tea beverage and camellia ampiexicaulis tea prepared by preparation method | |
| CN102228468A (en) | Preparation method for granular Chinese herbal pieces | |
| CN107156565A (en) | A kind of production method of dendrobium candidum hawthorn beverage | |
| CN106889386A (en) | A kind of ginger juice and black tea health-care composite beverage and preparation method thereof | |
| CN106135571A (en) | A kind of Lycium ruthenicum Murr. Flos Rosae Rugosae alternative tea formula and production technology thereof | |
| CN105851390A (en) | Rhizoma gastrodiae, Flos chrysanthemi and Momordica grosvenori tea and making method thereof | |
| CN106962908A (en) | A kind of preparation method of antidepression rose enzyme | |
| CN103654044B (en) | Production process for camptotheca acuminata fruit Chinese yew health pillow | |
| CN108541852A (en) | A kind of Hawthorn Juice Beverages and its processing technology | |
| CN106174281B (en) | A kind of grape wine jelly and preparation method thereof | |
| CN101427768A (en) | Health tea with beauty treatment and anti-aging function | |
| CN102919825B (en) | Donkey-hide gelatin paste for heart fire clearing, and its preparation method | |
| CN102696803A (en) | Jujube tea and method for preparing beverage of same | |
| CN103125625A (en) | Intestine-lubricating Chinese medicine tea drink | |
| CN102319286B (en) | Hair blackening liquid and preparation method thereof | |
| CN109315638A (en) | A kind of sea-buckthorn honey semisolid beverage and preparation method thereof | |
| CN105420023B (en) | A kind of health care wine of Chinese magnoliaving and its production method | |
| CN103844301A (en) | Lemon and mint compound beverage and preparation method thereof | |
| CN107201291A (en) | A kind of preparation method of high protein alcohol based composition | |
| CN202151434U (en) | Preparation system of granular type traditional Chinese medicine decoction piece | |
| CN108354095A (en) | It is a kind of to have effects that alleviate the dendrobium nobile healthcare beverage of abdomen distending pain |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170915 |