CN107156195A - A kind of botanical pesticide for preventing and treating plant insect and its application - Google Patents

A kind of botanical pesticide for preventing and treating plant insect and its application Download PDF

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Publication number
CN107156195A
CN107156195A CN201710568252.8A CN201710568252A CN107156195A CN 107156195 A CN107156195 A CN 107156195A CN 201710568252 A CN201710568252 A CN 201710568252A CN 107156195 A CN107156195 A CN 107156195A
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Prior art keywords
extract
composition
botanical pesticide
jervine
gynura bicolor
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CN201710568252.8A
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Chinese (zh)
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CN107156195B (en
Inventor
冷鹏
周绪元
穆清泉
杨加鑫
崔爱华
宿刚爱
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Linyi Academy of Agricultural Sciences
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Linyi Academy of Agricultural Sciences
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A01N25/04Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16Heavy metals; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/36Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Plant Pathology (AREA)
  • Environmental Sciences (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Pest Control & Pesticides (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Botany (AREA)
  • Dispersion Chemistry (AREA)
  • Toxicology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of botanical pesticide for preventing and treating plant insect, the composition being made up of jervine, common smoketree extract and Gynura bicolor extract, microemulsion or aqueous emulsion that supplying auxiliary agent is made;The mass percentage content of each component is in the composition:Jervine 30 40%, common smoketree extract 20 40%, Gynura bicolor extract 20 50%.Jervine, common smoketree extract and the Gynura bicolor extract of the present invention compounds obtained composition according to a certain percentage has obvious synergistic effect, has good preventive and therapeutic effect to fleahopper silk worm or Bemisia tabaci or small heart-eating peach worm.Composition supplying the auxiliary agent microemulsion or aqueous emulsion that are made of the present invention, it is steady quality, shelf-stable, environmentally safe.

Description

A kind of botanical pesticide for preventing and treating plant insect and its application
Technical field
The invention belongs to technical field of pesticide, and in particular to a kind of botanical pesticide of preventing and treating plant insect and its application.
Background technology
For a long time, cause due in production in order to ensure that agricultural output and quality largely use chemical insecticide Immense pressure is produced to ecological environment, and causes some insects to develop immunity to drugs rapidly, if further increasing insecticide consumption, So as to cause Practice for Pesticide Residue in Agricultural Products amount severe overweight, significant damage is caused to people and animals, environment.Therefore, development and utilization has Environmental compatibility and the agricultural chemicals resource harmless to the mankind are increasingly subject to the favor of various countries.
Botanical pesticide is the insecticides for being processed into the extract solution of plant or plant, with microbial insecticide one Sample belongs to biological pesticide, what its active ingredient was naturally occurring, general nontoxic, it is easy to degrade, accumulation toxicity can in ecological environment Energy property is small, with Environmental compatibility.To the ever-increasing organic food of demand, pollution-free food there is guarantee effect, it is to avoid should The negative effect caused with chemical pesticide, and with making insect be difficult to develop immunity to drugs, the advantages of not killing pest natural enemy is reason The agricultural chemicals type thought.
With the development of the society, food-safety problem is just being increasingly subject to the concern of people, and as during planting Pesticide Residue is the most concerned problem of people, is constantly studied by people, has developed various plants insecticide, its By the effective component extracting from the plant for possessing desinsection special efficacy, the medicament being made after auxiliary agent dissolving is added, it is generally acknowledged wide Spectrum, efficient, low toxicity, degradable, noresidue insecticide are smaller to people and animals and ambient contamination.But the plant of each manufacturer production Thing insecticide has in the selection of component, the determination of consumption can not meet in the consideration of oneself, but the effect of actual use The need for growing agriculture deinsectization.
The content of the invention
In view of the deficiencies of the prior art, the present invention provides it is a kind of prevent and treat plant insect botanical pesticide, the agricultural chemicals by Natural plants are synthesized, environmentally friendly, efficient, nontoxic without any toxic chemicals.
The invention also discloses the application of the botanical pesticide of the preventing and treating plant insect.
The purpose of the present invention is achieved by the following technical solution:
A kind of botanical pesticide for preventing and treating plant insect, is by jervine, common smoketree extract and Gynura bicolor extract group Into composition, supplying the auxiliary agent microemulsion or aqueous emulsion that are made;
The mass percentage content of each component is in the composition:Jervine 30-40%, common smoketree extract 20-40%, Gynura bicolor extract 20-50%;
The microemulsion is as made from the component of following mass percent:Composition 20-40%, organic solvent 10- 20%th, surfactant 10-20%, synergist 5-15%, surplus is deionized water;
The aqueous emulsion is as made from the component of following mass percent:Composition 30-50%, organic solvent 5- 15%th, surfactant 5-15%, thickener 1-2%, surplus is deionized water.
The microemulsion of the present invention is as made from following methods:After composition organic solvent is dissolved, add surface and live Property agent, be well mixed;Synergist and deionized water are slowly added under 800-1000 revs/min of mixing speed, and stirs straight To transparent, produce.
The aqueous emulsion of the present invention is as made from following methods:After composition organic solvent is dissolved, add surface and live Property agent, be well mixed;Thickener and deionized water are added, in high-speed shearing emulsion machine with 9000-10000 revs/min of turn The lower stirring and emulsifying of speed is disperseed, and is produced.
Described, common smoketree extract acetone is extracted from smoke tree by extraction and obtained.
The common smoketree extract of the present invention is as made from following methods:The woody part of smoke tree is cut, cool place is lower to dry 1 Individual month, 40 mesh sieves are crossed after crushing, smoke tree powder is obtained;Appropriate smoke tree powder is taken, according to solid-liquid ratio 1:20 add acetone, in 50 DEG C of leachings 5h is carried, leaching liquor the medicinal extract that water content is 3-5% is concentrated in vacuo to, you can common smoketree extract is made.
Described, Gynura bicolor extract ethanol is extracted from the leaf of new light violet back of the body India by extraction and obtained.
The extraction of the Gynura bicolor extract of the present invention is as made from following methods:Fresh Gynura bicolor leaf is taken to wash Only, drain, in 60 DEG C of drying and processing 24h, crushed after cooling, cross 50 mesh sieves, obtain Gynura bicolor powder;Take appropriate Gynura bicolor powder End, by solid-liquid ratio 1:25 add 70% ethanol, and 3h is extracted in 60 DEG C, and extract is concentrated in vacuo into the leaching that water content is 2-5% Cream, you can Gynura bicolor extract is made.
Described, organic solvent is one kind in ethanol, methanol and acetone.
Described, surfactant is alkyl benzene sulfonate, APES class and aliphatic alcohol polyethenoxy One kind in ethers.
Described, synergist is that mass concentration is 5.6% orange oil aqua or nano titanium oxide.
The particle diameter of nano titanium oxide used of the invention is 5-10nm.
Described, thickener is guar gum or Arabic gum.
A kind of application for the botanical pesticide for preventing and treating plant insect, is extracted by jervine, common smoketree extract and Gynura bicolor The microemulsion or aqueous emulsion that the composition supplying auxiliary agent of thing composition is made are applied to preventing and treating fleahopper silk worm or Bemisia tabaci or the small food heart of peach Worm.
The application method of botanical pesticide of present invention preventing and treating plant insect is:The water that 1000 times are added in finished product is dilute Release, be sprayed on plant.
Beneficial effects of the present invention:Jervine, common smoketree extract and the Gynura bicolor extract of the present invention is according to certain ratio The composition that example compounding is obtained has obvious synergistic effect, has to fleahopper silk worm or Bemisia tabaci or small heart-eating peach worm anti-well Control effect.Composition supplying the auxiliary agent microemulsion or aqueous emulsion that are made of the present invention, it is steady quality, shelf-stable, environmentally safe.
Embodiment
The present invention is described further for following examples, rather than limits the scope of the invention.
Embodiment 1
A kind of botanical pesticide for preventing and treating plant insect, is by jervine, common smoketree extract and Gynura bicolor extract group Into composition, supplying the auxiliary agent microemulsion or aqueous emulsion that are made;
The mass percentage content of each component is in the composition:Jervine 30%, common smoketree extract 20%, purple back of the body day Certain herbaceous plants with big flowers extract 50%;
The microemulsion is as made from the component of following mass percent:Composition 20%, organic solvent 20%, surface Activating agent 20%, synergist 5%, surplus is deionized water;
The aqueous emulsion is as made from the component of following mass percent:Composition 50%, organic solvent 5%, surface Activating agent 5%, thickener 2%, surplus is deionized water.
The microemulsion of the present invention is as made from following methods:After composition organic solvent is dissolved, add surface and live Property agent, be well mixed;Synergist and deionized water are slowly added under 800-1000 revs/min of mixing speed, and stirs straight To transparent, produce.
The aqueous emulsion of the present invention is as made from following methods:After composition organic solvent is dissolved, add surface and live Property agent, be well mixed;Thickener and deionized water are added, in high-speed shearing emulsion machine with 9000-10000 revs/min of turn The lower stirring and emulsifying of speed is disperseed, and is produced.
Described, common smoketree extract acetone is extracted from smoke tree by extraction and obtained.
The common smoketree extract of the present invention is as made from following methods:The woody part of smoke tree is cut, cool place is lower to dry 1 Individual month, 40 mesh sieves are crossed after crushing, smoke tree powder is obtained;Appropriate smoke tree powder is taken, according to solid-liquid ratio 1:20 add acetone, in 50 DEG C of leachings 5h is carried, leaching liquor the medicinal extract that water content is 3-5% is concentrated in vacuo to, you can common smoketree extract is made.
Described, Gynura bicolor extract ethanol is extracted from the leaf of new light violet back of the body India by extraction and obtained.
The extraction of the Gynura bicolor extract of the present invention is as made from following methods:Fresh Gynura bicolor leaf is taken to wash Only, drain, in 60 DEG C of drying and processing 24h, crushed after cooling, cross 50 mesh sieves, obtain Gynura bicolor powder;Take appropriate Gynura bicolor powder End, by solid-liquid ratio 1:25 add 70% ethanol, and 3h is extracted in 60 DEG C, and extract is concentrated in vacuo into the leaching that water content is 2-5% Cream, you can Gynura bicolor extract is made.
Described, organic solvent is ethanol.
Described, surfactant is fatty alcohol polyethenoxy ether class.
Described, synergist is that mass concentration is 5.6% orange oil aqua.
Described, thickener is guar gum.
A kind of application for the botanical pesticide for preventing and treating plant insect, is extracted by jervine, common smoketree extract and Gynura bicolor The microemulsion or aqueous emulsion that the composition supplying auxiliary agent of thing composition is made are applied to preventing and treating fleahopper silk worm or Bemisia tabaci or the small food heart of peach Worm.
The application method of botanical pesticide of present invention preventing and treating plant insect is:The water that 1000 times are added in finished product is dilute Release, be sprayed on plant.
Embodiment 2
A kind of botanical pesticide for preventing and treating plant insect, is by jervine, common smoketree extract and Gynura bicolor extract group Into composition, supplying the auxiliary agent microemulsion or aqueous emulsion that are made;
The mass percentage content of each component is in the composition:Jervine 35%, common smoketree extract 30%, purple back of the body day Certain herbaceous plants with big flowers extract 35%;
The microemulsion is as made from the component of following mass percent:Composition 30%, organic solvent 15%, surface Activating agent 15%, synergist 10%, surplus is deionized water;
The aqueous emulsion is as made from the component of following mass percent:Composition 40%, organic solvent 10%, surface Activating agent 10%, thickener 1%, surplus is deionized water.
Described, common smoketree extract acetone is extracted from smoke tree by extraction and obtained.
Described, Gynura bicolor extract ethanol is extracted from the leaf of new light violet back of the body India by extraction and obtained.
Described, organic solvent is methanol.
Described, surfactant is APES class.
Described, synergist is that mass concentration is 5.6% orange oil aqua.
Described, thickener is Arabic gum.
A kind of application for the botanical pesticide for preventing and treating plant insect, is extracted by jervine, common smoketree extract and Gynura bicolor The microemulsion or aqueous emulsion that the composition supplying auxiliary agent of thing composition is made are applied to preventing and treating fleahopper silk worm or Bemisia tabaci or the small food heart of peach Worm.
Remaining be the same as Example 1.
Embodiment 3
A kind of botanical pesticide for preventing and treating plant insect, is by jervine, common smoketree extract and Gynura bicolor extract group Into composition, supplying the auxiliary agent microemulsion or aqueous emulsion that are made;
The mass percentage content of each component is in the composition:Jervine 40%, common smoketree extract 40%, purple back of the body day Certain herbaceous plants with big flowers extract 20%;
The microemulsion is as made from the component of following mass percent:Composition 40%, organic solvent 10%, surface Activating agent 10%, synergist 15%, surplus is deionized water;
The aqueous emulsion is as made from the component of following mass percent:Composition 30%, organic solvent 15%, surface Activating agent 15%, thickener 2%, surplus is deionized water.
Described, common smoketree extract acetone is extracted from smoke tree by extraction and obtained.
Described, Gynura bicolor extract ethanol is extracted from the leaf of new light violet back of the body India by extraction and obtained.
Described, organic solvent is acetone.
Described, surfactant is alkyl benzene sulfonate.
Described, synergist is nano titanium oxide.
The particle diameter of nano titanium oxide used of the invention is 5-10nm.
Described, thickener is guar gum.
A kind of application for the botanical pesticide for preventing and treating plant insect, is extracted by jervine, common smoketree extract and Gynura bicolor The microemulsion or aqueous emulsion that the composition supplying auxiliary agent of thing composition is made are applied to preventing and treating fleahopper silk worm or Bemisia tabaci or the small food heart of peach Worm.
Remaining be the same as Example 1.
Insecticidal test
Botanical pesticide prepared by embodiment 1-3 is used as experimental group 1-3 with 1000 times of water dilution respectively;Set pair simultaneously According to a group 1-3, respectively with 1000 times of water-reducible jervine, common smoketree extract (preparation of the method for embodiment 1) and Gynura bicolor Extract (preparation of the method for embodiment 1), insecticidal test is carried out to fleahopper silk worm, Bemisia tabaci and small heart-eating peach worm.As a result such as the institute of table 1 Show.
The insecticidal test of table 1
In addition to the implementation, the present invention can also have other embodiment.All use equivalent substitution or equivalent transformation shape Into technical scheme, all fall within the protection domain of application claims.

Claims (8)

1. a kind of botanical pesticide for preventing and treating plant insect, it is characterised in that be by jervine, common smoketree extract and Gynura bicolor The composition of extract composition, microemulsion or aqueous emulsion that supplying auxiliary agent is made;
The mass percentage content of each component is in the composition:Jervine 30-40%, common smoketree extract 20-40%, the purple back of the body Semiaquilegia root extract 20-50%;
The microemulsion is as made from the component of following mass percent:Composition 20-40%, organic solvent 10-20%, table Face activating agent 10-20%, synergist 5-15%, surplus is deionized water;
The aqueous emulsion is as made from the component of following mass percent:Composition 30-50%, organic solvent 5-15%, table Face activating agent 5-15%, thickener 1-2%, surplus is deionized water.
2. botanical pesticide according to claim 1, it is characterised in that the common smoketree extract is to pass through extraction with acetone Method extracts what is obtained from smoke tree.
3. botanical pesticide according to claim 1, it is characterised in that the Gynura bicolor extract is passed through with ethanol Extraction extracts what is obtained from the leaf of new light violet back of the body India.
4. botanical pesticide according to claim 1, it is characterised in that the organic solvent is ethanol, methanol and acetone In one kind.
5. botanical pesticide according to claim 1, it is characterised in that the surfactant is alkylbenzenesulfonate One kind in class, APES class and fatty alcohol polyethenoxy ether class.
6. botanical pesticide according to claim 1, it is characterised in that the synergist is that mass concentration is 5.6% orange Profit agent or nano titanium oxide.
7. botanical pesticide according to claim 1, it is characterised in that the thickener is guar gum or Arabic gum.
8. the application of the botanical pesticide of plant insect is prevented and treated any one of a kind of claim 1-7, it is characterised in that by Microemulsion or aqueous emulsion application that the composition supplying auxiliary agent of jervine, common smoketree extract and Gynura bicolor extract composition is made In preventing and treating fleahopper silk worm or Bemisia tabaci or small heart-eating peach worm.
CN201710568252.8A 2017-07-13 2017-07-13 Botanical pesticide for preventing and treating plant pests and application thereof Active CN107156195B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109793009A (en) * 2019-03-25 2019-05-24 陕西省生物农业研究所 It is a kind of to walk quickly and keep away pharmaceutical preparation for prevent and treat TYLCV infection insect

Citations (2)

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CN106135323A (en) * 2016-06-29 2016-11-23 固镇县华丰蔬菜专业合作社 A kind of insecticide preventing and treating Fructus Benincasae liriomyza bryoniae insect pest
CN106490022A (en) * 2016-10-31 2017-03-15 郑州思辩科技有限公司 A kind of plant compound pesticide containing jervine and preparation method thereof

Patent Citations (2)

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Publication number Priority date Publication date Assignee Title
CN106135323A (en) * 2016-06-29 2016-11-23 固镇县华丰蔬菜专业合作社 A kind of insecticide preventing and treating Fructus Benincasae liriomyza bryoniae insect pest
CN106490022A (en) * 2016-10-31 2017-03-15 郑州思辩科技有限公司 A kind of plant compound pesticide containing jervine and preparation method thereof

Non-Patent Citations (2)

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杨艳等: "0.5%藜芦碱可溶液剂防治蔬菜烟粉虱田间药效试验", 《上海农业科技》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109793009A (en) * 2019-03-25 2019-05-24 陕西省生物农业研究所 It is a kind of to walk quickly and keep away pharmaceutical preparation for prevent and treat TYLCV infection insect

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