CN107130768A - A kind of double layer fibre felt enhancing plastic floor and preparation method thereof - Google Patents
A kind of double layer fibre felt enhancing plastic floor and preparation method thereof Download PDFInfo
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- CN107130768A CN107130768A CN201710284476.6A CN201710284476A CN107130768A CN 107130768 A CN107130768 A CN 107130768A CN 201710284476 A CN201710284476 A CN 201710284476A CN 107130768 A CN107130768 A CN 107130768A
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- egative film
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- fibre felt
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- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04F—FINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
- E04F15/00—Flooring
- E04F15/02—Flooring or floor layers composed of a number of similar elements
- E04F15/10—Flooring or floor layers composed of a number of similar elements of other materials, e.g. fibrous or chipped materials, organic plastics, magnesite tiles, hardboard, or with a top layer of other materials
- E04F15/107—Flooring or floor layers composed of a number of similar elements of other materials, e.g. fibrous or chipped materials, organic plastics, magnesite tiles, hardboard, or with a top layer of other materials composed of several layers, e.g. sandwich panels
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29D—PRODUCING PARTICULAR ARTICLES FROM PLASTICS OR FROM SUBSTANCES IN A PLASTIC STATE
- B29D99/00—Subject matter not provided for in other groups of this subclass
- B29D99/0057—Producing floor coverings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B9/00—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B9/00—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00
- B32B9/04—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00 comprising such particular substance as the main or only constituent of a layer, which is next to another layer of the same or of a different material
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/02—Organic and inorganic ingredients
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/04—Carbon
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
- C08K5/098—Metal salts of carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/10—Esters; Ether-esters
- C08K5/12—Esters; Ether-esters of cyclic polycarboxylic acids
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04F—FINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
- E04F15/00—Flooring
- E04F15/02—Flooring or floor layers composed of a number of similar elements
- E04F15/10—Flooring or floor layers composed of a number of similar elements of other materials, e.g. fibrous or chipped materials, organic plastics, magnesite tiles, hardboard, or with a top layer of other materials
- E04F15/105—Flooring or floor layers composed of a number of similar elements of other materials, e.g. fibrous or chipped materials, organic plastics, magnesite tiles, hardboard, or with a top layer of other materials of organic plastics with or without reinforcements or filling materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2260/00—Layered product comprising an impregnated, embedded, or bonded layer wherein the layer comprises an impregnation, embedding, or binder material
- B32B2260/04—Impregnation, embedding, or binder material
- B32B2260/046—Synthetic resin
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/30—Properties of the layers or laminate having particular thermal properties
- B32B2307/308—Heat stability
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/50—Properties of the layers or laminate having particular mechanical properties
- B32B2307/554—Wear resistance
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/70—Other properties
- B32B2307/732—Dimensional properties
- B32B2307/734—Dimensional stability
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2471/00—Floor coverings
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Architecture (AREA)
- Polymers & Plastics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Mechanical Engineering (AREA)
- Ceramic Engineering (AREA)
- Floor Finish (AREA)
Abstract
The invention discloses a kind of double layer fibre felt enhancing plastic floor and preparation method thereof, the defect existed for existing plastic floor, propose one kind and be followed successively by slide from top to bottom, color film, fibrofelt, middle level egative film, Chopped Strand Mat, the double layer fibre felt enhancing plastic floor that the stepped construction of bottom egative film is composited, and to optimization that middle level egative film and bottom egative film are formulated, prepare a kind of good texture, effectively improve the dimensional stability on floor, reduce its thermal coefficient of expansion, also ensure double layer fibre felt enhancing plastic floor of the warpage on finished product floor within critical field simultaneously, and preparation method simple possible, commercial Application generalization is strong.
Description
Technical field
The present invention relates to a kind of preparation field on floor, more particularly, to a kind of double layer fibre felt strengthen plastic floor and its
Preparation method.
Background technology
Plastic cement (PVC) floor is a kind of high-grade and environmental protection ornament materials, with the excellent properties such as light weight, sound insulation, wear-resisting,
There are very good market prospects in developed country in overseas.
Although PVC floor has above-mentioned advantage, there is also certain limitation performance.Simple modeling such as without fibrofelt
It is poor to there is dimensional stability in adhesive floor, the problem of thermal coefficient of expansion is larger, in order to which the dimensional stability and heat that improve product are swollen
Swollen coefficient (CTE), has research to be prepared into individual layer or double layer fibre felt floor, but the single layer fibre felt prepared in the prior art
Still there is dimensions above stability and the defect of thermal coefficient of expansion in plate, and double layer fibre felt floor has warpage or distortion
Defect.
If double-deck or multi-layer fiber felt can be added, in common PVC plastic adhesive floor effectively to reduce the expansion on floor
Coefficient, improve its dimensional stability, and seek rational formula and structure, with ensure the warpage on floor critical field it
Interior, it will effectively to solve the above problems, the development to plastic floor brings very big innovation.
The content of the invention
Goal of the invention:In order to solve the problems of in the prior art, the present invention proposes a kind of compatible with PVC floor
Property it is good, effectively improve floor dimensional stability, reduce floor thermal coefficient of expansion, ensure floor warpage in critical field
Within double layer fibre felt enhancing plastic floor and preparation method thereof.
Technical scheme:To achieve these objectives, the present invention takes following technical scheme:A kind of double layer fibre felt enhancing plastic cement
Plate, be followed successively by from top to bottom slide, color film, Chopped Strand Mat, middle level egative film, Chopped Strand Mat, bottom egative film stepped construction it is compound and
Into.
It is more highly preferred to, the formula of the middle level egative film is calculated by mass as follows:PVC15%-20%, plasticizer 5%-
7.5%th, stone flour 70%-78%, stabilizer 0.5%-0.8%, carbon black 0.09%-1.3%.
Further, the formula of the middle level egative film is calculated by mass as follows:PVC 18%, plasticizer 5%, stone flour
76%, stabilizer 0.6%, carbon black 0.4%.
It is more highly preferred to, the formula of the bottom egative film is calculated by mass as follows:PVC 20%-25%, plasticizer
8.5%-10%, stone flour 63%-71%, stabilizer 0.5%-0.8%, carbon black 0.09%-1.3%.
Further, the formula of the bottom egative film is calculated by mass as follows:PVC 24%, plasticizer 9%, stone flour
66%, stabilizer 0.7%, small powder 0.3%.
It is more highly preferred to, the plasticizer is specially DOTP.
It is more highly preferred to, the stabilizer is specially calcium stearate.
Strengthen the preparation method of plastic floor the invention also discloses a kind of above-mentioned double layer fibre felt, comprise the following steps:
(1) egative film is produced:Raw material are tested first it is qualified after, according to middle level egative film and bottom egative film formula lead to
The cold mixed heat of crossing mixing material is mixed, banburying, four-roll calendaring, cooling, the process of winding draw out it is various needed for specification requirement thickness
Corresponding egative film;
(2) press:Folded successively by the stepped construction of slide, color film, Chopped Strand Mat, middle level egative film, Chopped Strand Mat, bottom egative film
Material, hot pressing, temperature control is at 140-160 DEG C, and time control is in 26-34min;
(3) UV is heat-treated:Hydrothermal area's temperature is 80-90 DEG C, and speed is 14-15.5m/min;Cold water area temperature is 20-45
DEG C, speed is 15-18m/min, and rewinding temperature is 20-33 DEG C;
(4) stand:Ensure that time of repose is not less than 72h;
(5) it is punched:Floor is fitly deposited on pallet, is punched out according to specification requirement, and punching temperature control exists
25—28℃;
(6) slot:The floor of punching is slotted, upper compression plate pressure is in 0.05~0.1MPa;
(7) pack:By every box quantity of customer requirement, every layer of box number, the specification of pallet, the floor for stacking number of plies cross-notching
Packed;
(8) properties of product are detected:Dimensional stability and thermal coefficient of expansion CTE to finished product carry out qualification detection.
Beneficial effect:A kind of double layer fibre felt enhancing plastic floor that the present invention is provided and preparation method thereof, for existing
The defect that plastic floor is present, it is proposed that one kind is followed successively by slide, color film, fibrofelt, middle level egative film, glass from top to bottom
The double layer fibre felt enhancing plastic floor that felt, the stepped construction of bottom egative film are composited, and to middle level egative film and bottom egative film
The optimization being formulated, prepares a kind of good texture, effectively improves the dimensional stability on floor, reduce its thermal coefficient of expansion,
Also ensure double layer fibre felt enhancing plastic floor of the warpage on finished product floor within critical field, and preparation method letter simultaneously
Single feasible, commercial Application generalization is strong.
Embodiment
Embodiment 1:
A kind of double layer fibre felt strengthens plastic floor, be followed successively by from top to bottom slide, color film, fibrofelt, middle level egative film,
Chopped Strand Mat, the stepped construction of bottom egative film are composited;The formula of wherein middle level egative film is calculated by mass as follows:PVC15%, increasing
Mould agent 6%, stone flour 78%, stabilizer 0.5%, small powder 0.5%;The formula of bottom egative film is calculated by mass as follows:PVC20%,
Plasticizer 9%, stone flour 70%, stabilizer 0.6%, small powder 0.4%.The plasticizer is specially DOTP;The stabilizer is specific
For calcium stearate.
Embodiment 2:
A kind of double layer fibre felt strengthens plastic floor, be followed successively by from top to bottom slide, color film, fibrofelt, middle level egative film,
Chopped Strand Mat, the stepped construction of bottom egative film are composited;The formula of wherein middle level egative film is calculated by mass as follows:PVC 20%,
Plasticizer 6%, stone flour 73%, stabilizer 0.5%, carbon black 0.5%. bottom egative films formula it is calculated by mass as follows:PVC
25%th, plasticizer 9%, stone flour 65%, stabilizer 0.6%, small powder 0.4%.The plasticizer is specially DOTP;The stabilizer
Specially calcium stearate.
Embodiment 3:
A kind of double layer fibre felt strengthens plastic floor, be followed successively by from top to bottom slide, color film, fibrofelt, middle level egative film,
Chopped Strand Mat, the stepped construction of bottom egative film are composited;The formula of wherein middle level egative film is calculated by mass as follows:PVC18%, increasing
Mould agent 5%, stone flour 76%, stabilizer 0.6%, carbon black 0.4%. bottom egative films formula it is calculated by mass as follows:PVC24%,
Plasticizer 9%, stone flour 66%, stabilizer 0.7%, small powder 0.3%.The plasticizer is specially DOTP;The stabilizer is specific
For calcium stearate.
Embodiment 4:
Double layer fibre felt enhancing plastic floor is carried out using the formula of above-described embodiment 3 using following methods to be prepared:
(1) egative film is produced:Raw material are tested first it is qualified after, according to middle level egative film and bottom egative film formula lead to
The cold mixed heat of crossing mixing material is mixed, banburying, four-roll calendaring, cooling, the process of winding draw out it is various needed for specification requirement thickness
Corresponding egative film;
(2) press:Folded successively by the stepped construction of slide, color film, Chopped Strand Mat, middle level egative film, Chopped Strand Mat, bottom egative film
Material, hot pressing, temperature control is at 140-160 DEG C, and time control is in 26-34min;
(3) UV is heat-treated:Hydrothermal area's temperature is 80-90 DEG C, and speed is 14-15.5m/min;Cold water area temperature is 20-45
DEG C, speed is 15-18m/min, and rewinding temperature is 20-33 DEG C;
(4) stand:Ensure that time of repose is not less than 72h;
(5) it is punched:Floor is fitly deposited on pallet, is punched out according to specification requirement, and punching temperature control exists
25—28℃;
(6) slot:The floor of punching is slotted, upper compression plate pressure is in 0.05~0.1MPa;
(7) pack:By every box quantity of customer requirement, every layer of box number, the specification of pallet, the floor for stacking number of plies cross-notching
Packed;
(8) properties of product are detected:Dimensional stability and thermal coefficient of expansion CTE to finished product carry out qualification detection.
With separately setting the commercially available double layer fibre felt plastic cement prepared without fibrofelt floor and single layer fibre felt floor with embodiment 4
The finished product of plate carries out performance test comparison, and specific performance index is:
Dimensional stability, thermal coefficient of expansion, warpage, are measured with clearance gauge etc..
Test result is as shown in table 1:
The embodiment 4 of table 1 and comparative example floor all-round property testing result
Wherein:MD refers to refer to perpendicular to the direction of color film along the direction of color film, CD
From the data in table 1 can be seen that the double layer fibre felt plastic floor embodiment 4 for preparing of the present invention and comparative example without
Fibrofelt floor and single layer fibre felt floor are compared, and effectively increase the dimensional stability of ground board finished product and to reduce ground
The thermal coefficient of expansion of plate, and warpage (≤1.0mm) within critical field.
It should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention,
Some improvement can also be made, these improvement also should be regarded as protection scope of the present invention.
Claims (8)
1. a kind of double layer fibre felt strengthens plastic floor, it is characterised in that be followed successively by from top to bottom slide, color film, Chopped Strand Mat,
Middle level egative film, Chopped Strand Mat, the stepped construction of bottom egative film are composited.
2. double layer fibre felt according to claim 1 strengthens plastic floor, it is characterised in that:The formula of the middle level egative film
It is calculated by mass as follows:PVC15%-20%, plasticizer 5%-7.5%, stone flour 70%-78%, stabilizer 0.5%-0.8%,
Carbon black 0.09%-1.3%.
3. double layer fibre felt according to claim 2 strengthens plastic floor, it is characterised in that:The formula of the middle level egative film
It is calculated by mass as follows:PVC 18%, plasticizer 5%, stone flour 76%, stabilizer 0.6%, carbon black 0.4%.
4. double layer fibre felt according to claim 1 strengthens plastic floor, it is characterised in that:The formula of the bottom egative film
It is calculated by mass as follows:PVC20%-25%, plasticizer 8.5%-10%, stone flour 63%-71%, stabilizer 0.5%-0.8%,
Carbon black 0.09%-1.3%.
5. double layer fibre felt according to claim 4 strengthens plastic floor, it is characterised in that:The formula of the bottom egative film
It is calculated by mass as follows:PVC 24%, plasticizer 9%, stone flour 66%, stabilizer 0.7%, small powder 0.3%.
6. double layer fibre felt according to claim 1 strengthens plastic floor, it is characterised in that:The plasticizer is specially
DOTP。
7. double layer fibre felt according to claim 1 strengthens plastic floor, it is characterised in that:The stabilizer is specially hard
Resin acid calcium.
8. a kind of double layer fibre felt as claimed in claim 1 strengthens the preparation method of plastic floor, it is characterised in that including such as
Lower step:
(1) egative film is produced:Raw material are tested first it is qualified after, according to the formula of middle level egative film and bottom egative film by matching somebody with somebody
The cold mixed hot mixed, banburying of batch mixing, four-roll calendaring, cooling, the process of winding draw out the corresponding of various required specification requirement thickness
Egative film;
(2) press:By slide, color film, Chopped Strand Mat, middle level egative film, Chopped Strand Mat, bottom egative film stepped construction stack successively,
Hot pressing, temperature control is at 140-160 DEG C, and time control is in 26-34min;
(3) UV is heat-treated:Hydrothermal area's temperature is 80-90 DEG C, and speed is 14-15.5m/min;Cold water area temperature is 20-45 DEG C, speed
Spend for 15-18m/min, rewinding temperature is 20-33 DEG C;
(4) stand:Ensure that time of repose is not less than 72h;
(5) it is punched:Floor is fitly deposited on pallet, is punched out according to specification requirement, and punching temperature control is 25-28
℃;
(6) slot:The floor of punching is slotted, upper compression plate pressure is in 0.05~0.1MPa;
(7) pack:By every box quantity of customer requirement, every layer of box number, the specification of pallet, the floor of stacking number of plies cross-notching are carried out
Packaging;
(8) properties of product are detected:Dimensional stability and thermal coefficient of expansion CTE to finished product carry out qualification detection.
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CN201710284476.6A CN107130768A (en) | 2017-04-25 | 2017-04-25 | A kind of double layer fibre felt enhancing plastic floor and preparation method thereof |
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CN201710284476.6A CN107130768A (en) | 2017-04-25 | 2017-04-25 | A kind of double layer fibre felt enhancing plastic floor and preparation method thereof |
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108104414A (en) * | 2017-12-25 | 2018-06-01 | 帝高力装饰材料(江苏)有限公司 | A kind of suspension floor and preparation method and application |
CN108116019A (en) * | 2017-12-25 | 2018-06-05 | 帝高力装饰材料(江苏)有限公司 | A kind of energy conservation and environmental protection EVA floors and preparation method thereof |
CN108189509A (en) * | 2017-12-25 | 2018-06-22 | 帝高力装饰材料(江苏)有限公司 | A kind of TPU floors and preparation method thereof |
CN110157115A (en) * | 2019-05-23 | 2019-08-23 | 福建思嘉环保材料科技有限公司 | A kind of antistatic PVC floor and preparation method thereof |
CN112519363A (en) * | 2020-10-29 | 2021-03-19 | 帝高力装饰材料(江苏)有限公司 | Low-heat-sensitivity PVC (polyvinyl chloride) floor and preparation method thereof |
CN115139616A (en) * | 2021-08-30 | 2022-10-04 | 浙江海象新材料股份有限公司 | Low-cost soft non-halogen floor and preparation method thereof |
CN117341299A (en) * | 2023-10-12 | 2024-01-05 | 明和科技(唐山)股份有限公司 | High-stability mute glass fiber felt floor and preparation method thereof |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108104414A (en) * | 2017-12-25 | 2018-06-01 | 帝高力装饰材料(江苏)有限公司 | A kind of suspension floor and preparation method and application |
CN108116019A (en) * | 2017-12-25 | 2018-06-05 | 帝高力装饰材料(江苏)有限公司 | A kind of energy conservation and environmental protection EVA floors and preparation method thereof |
CN108189509A (en) * | 2017-12-25 | 2018-06-22 | 帝高力装饰材料(江苏)有限公司 | A kind of TPU floors and preparation method thereof |
CN110157115A (en) * | 2019-05-23 | 2019-08-23 | 福建思嘉环保材料科技有限公司 | A kind of antistatic PVC floor and preparation method thereof |
CN112519363A (en) * | 2020-10-29 | 2021-03-19 | 帝高力装饰材料(江苏)有限公司 | Low-heat-sensitivity PVC (polyvinyl chloride) floor and preparation method thereof |
CN115139616A (en) * | 2021-08-30 | 2022-10-04 | 浙江海象新材料股份有限公司 | Low-cost soft non-halogen floor and preparation method thereof |
CN115139616B (en) * | 2021-08-30 | 2023-10-17 | 浙江海象新材料股份有限公司 | Low-cost soft non-halogen floor and preparation method thereof |
CN117341299A (en) * | 2023-10-12 | 2024-01-05 | 明和科技(唐山)股份有限公司 | High-stability mute glass fiber felt floor and preparation method thereof |
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