CN107080699A - A kind of attapulgite modified high-comfort shaving cream and preparation method thereof - Google Patents
A kind of attapulgite modified high-comfort shaving cream and preparation method thereof Download PDFInfo
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- CN107080699A CN107080699A CN201710305219.6A CN201710305219A CN107080699A CN 107080699 A CN107080699 A CN 107080699A CN 201710305219 A CN201710305219 A CN 201710305219A CN 107080699 A CN107080699 A CN 107080699A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/0279—Porous; Hollow
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q9/00—Preparations for removing hair or for aiding hair removal
- A61Q9/02—Shaving preparations
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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- A61K2800/524—Preservatives
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses the attapulgite modified high-comfort shaving cream of one kind, include the raw material of following parts by weight：10 20 parts of attapulgite modified 25 35 parts, 10 20 parts of stearic acid, 5 15 parts of triethanolamine, 15 25 parts of emulsifying agent, 48 parts of glycerine, 13 parts of sodium carboxymethylcellulose, 0.5 0.9 parts of sodium tripolyphosphate, 0.3 0.7 parts of menthol, 0.3 0.7 parts of sterilization and anticorrosion additive and deionized water.The skin feel of the attapulgite modified high-comfort shaving cream of the present invention preferably, moderate performance, excitant it is less, the friction and skin injury in shaving session can effectively be reduced, in addition with the function of sterilizing, the preparation method material cost of the invention provided is relatively low simultaneously, raw material is easy to get, technique concise, with higher use value and good application prospect.
Description
Technical field
The present invention relates to shaving cream preparing technical field, and in particular to a kind of attapulgite modified high-comfort shaving cream and
Its preparation method.
Background technology
In general, postpubertal healthy male can all grow a beard, initially soft rare, gradually become later thick and stiff thick
It is close.Modern medicine finds that at this time secreting out of more male sex hormone in man's body makes hair not only black but also thick, and the generation of beard is just
It is a kind of typical performance.Because bearded skin oil and fat secretes more, dust stratification dirt is easily glued, it is difficult to clean, so shaving
Beard is very important for health.
Shaving cream can soften beard, relatively good when scraping to scrape, and without shaving cream, be scraped because beard is very firmly bad,
If overexerted, it is easy to skin is injured, shaving cream can reduce the friction of blade and skin in shaving session, so as to protect
Sheath skin.
The shaving cream supplied on existing market is directly to be synthesized to obtain by industrial chemicals mostly, is applied to the attachment on beard
Power is bad, and shaving cream is easily dried, larger to skin irritation, can also cause allergic anti-for sensitive skin user
Should, and general rarer sterilizing effect.
Therefore formula and preparation technology how are improved, there is higher practical value with the properties for improving shaving cream.
The content of the invention
For the defect of prior art, it is an object of the invention to provide the attapulgite modified high-comfort shaving cream of one kind,
The skin feel of the shaving cream preferably, moderate performance, excitant it is less, can effectively reduce the friction in shaving session and skin is damaged
Wound, in addition with the function of sterilizing, while the preparation method material cost that the present invention is provided is relatively low, raw material is easy to get, technique
It is concise, with higher use value and good application prospect.
The present invention solves technical problem and adopted the following technical scheme that：
The invention provides the attapulgite modified high-comfort shaving cream of one kind, include the raw material of following parts by weight：
Attapulgite modified 25-35 parts, 10-20 parts of stearic acid, 5-15 parts of triethanolamine, 15-25 parts of emulsifying agent, 4-8 parts of glycerine,
1-3 parts of sodium carboxymethylcellulose, 0.5-0.9 parts of sodium tripolyphosphate, 0.3-0.7 parts of menthol, sterilization and anticorrosion additive 0.3-
0.7 part and 10-20 parts of deionized water.
Preferably, the attapulgite modified high-comfort shaving cream includes the raw material of following parts by weight：
Attapulgite modified 30 parts, 15 parts of stearic acid, 10 parts of triethanolamine, 20 parts of emulsifying agent, 6 parts of glycerine, carboxymethyl cellulose
15 parts of 2 parts of sodium, 0.7 part of sodium tripolyphosphate, 0.5 part of menthol, 0.5 part of sterilization and anticorrosion additive and deionized water.
Preferably, the emulsifying agent is lanolin and polysorbate fat according to weight ratio 1:The mixture of 1.5 compositions.
Preferably, the sterilization and anticorrosion additive is that ethylparaben, propylben, sorbic acid compare 1 according to weight:1:
The mixture of 5 compositions.
Present invention also offers a kind of preparation method of attapulgite modified high-comfort shaving cream, comprise the following steps：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 200 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, sodium tripolyphosphate, menthol, stir 15-25 minutes, speed of agitator is 850-950r/min, is obtained
Mixture A；
Step 3, by mixture A made from step 2, stearic acid, triethanolamine, emulsifying agent, glycerine, sterilization and anticorrosion additive,
Deionized water is added in Multifunction colloid grinder, and grinding rotating speed is in 3000-4000r/min, and milling time is 40-70 points
Clock, obtains paste mixture, and paste mixture grain fineness is less than 0.01 millimeter, and paste mixture is added in vacuum degassing machine
Vacuum degassing process processing is carried out, vacuum packaging obtains attapulgite modified high-comfort shaving cream.
Preferably, the preparation process of the attapulgite modified high-comfort shaving cream is：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 200 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, sodium tripolyphosphate, menthol, stir 20 minutes, speed of agitator is 900r/min, obtains mixture
A；
Step 3, by mixture A made from step 2, stearic acid, triethanolamine, emulsifying agent, glycerine, sterilization and anticorrosion additive,
Deionized water is added in Multifunction colloid grinder, and grinding rotating speed is 55 minutes in 3500r/min, milling time, obtains cream
Shape mixture, paste mixture grain fineness is less than 0.01 millimeter, and paste mixture is added in vacuum degassing machine and carries out vacuum
Degasification technique processing, vacuum packaging obtains attapulgite modified high-comfort shaving cream.
Preferably, the attapulgite modified preparation method is as follows：A, following component raw material is weighed by weight：It is concavo-convex
100 parts of rod soil, 2 parts of calgon, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, dodecyl sulphate
2 parts of sodium；B, attapulgite is put into the hydrochloric acid solution that concentration is 1mol/L, heating water bath is to 65-75 DEG C, with 500-
1000r/min speed of agitator stirring 1-2h, filtering, filter residue is washed with deionized to neutrality, drying；C, by gains in b
Matter is mixed with calgon, Sodium Polyacrylate, polyvinyl alcohol, silane coupler, lauryl sodium sulfate, and heating water bath is extremely
85-95 DEG C, with 500-1000r/min speed of agitator, stir 40-70 minutes, centrifuge, sediment is washed with deionized
To neutral, drying, it is subsequently placed in Muffle furnace at 420-480 DEG C and calcines 1-2h, cooling produces attapulgite modified.
Preferably, the attapulgite modified preparation method is as follows：A, following component raw material is weighed by weight：It is concavo-convex
100 parts of rod soil, 2 parts of calgon, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, dodecyl sulphate
2 parts of sodium；B, attapulgite is put into the hydrochloric acid solution that concentration is 1mol/L, heating water bath is to 70 DEG C, with stirring for 700r/min
Mix rotating speed stirs 1.5h, filtering, and filter residue is washed with deionized to neutrality, drying；C, by gained material and hexa metaphosphoric acid in b
Sodium, Sodium Polyacrylate, polyvinyl alcohol, silane coupler, lauryl sodium sulfate mixing, and heating water bath is to 90 DEG C, with 750r/
Min speed of agitator, is stirred 55 minutes, is centrifuged, and sediment is washed with deionized to neutrality, drying, is subsequently placed in horse
1.5h is not calcined in stove at 450 DEG C, cooling produces attapulgite modified.
Compared with prior art, the present invention has following beneficial effect：
（1）A kind of attapulgite modified high-comfort shaving cream of the present invention employs attapulgite as major ingredient carrier, due to
Attapulgite has higher specific surface area, it is possible to increase the adsorption capacity of shaving cream, the attapulgite that the present invention is used in addition
The needle bar shape group accumulated in a jumble can be caused to become loose porous after acid modification, its thixotropy and gumminess is all carried significantly
Height, makes the shaving cream of preparation can be good at being attached to the surface of skin, adds the contact area with beard, improves and shave
The service efficiency of cream.
（2）A kind of sterilization and anticorrosion additive of attapulgite modified high-comfort shaving cream addition of the present invention includes Ni Bo
Golden ethyl ester, propylben and sorbic acid have preferable disinfection effect, and the bacteriostatic activity of nipagin esters is mainly molecule
State works, and sorbic acid is acid preservative, best disinfection effect can be reached by proportioning, while to the thorn of skin
Sharp property is preferably minimized.
（3）A kind of stearic acid of attapulgite modified high-comfort shaving cream addition of the present invention is a kind of preferably emulsification
Agent, glycerine, lanolin, stearic acid and triethanolamine are used in combination with, and can allow shaving cream surfactant emulsion, and in fine and close bubble
Foam shape, greatly enhances its adhesive capacity.
（4）It is refrigerant that a kind of menthol of attapulgite modified high-comfort shaving cream addition of the present invention has skin
Sense, plays a part of anesthesia and sterilization and anticorrosion.
（5）The offer of the present invention the attapulgite modified high-comfort ointment preparation material cost that shaves is relatively low, raw material
Be easy to get, technique it is concise, with higher use value and good application prospect.
Embodiment
With reference to specific embodiment, the technical scheme in the embodiment of the present invention is clearly and completely described, shown
So, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based on the reality in the present invention
Example is applied, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made all belongs to
In the scope of protection of the invention.
Embodiment 1.
A kind of attapulgite modified high-comfort shaving cream of the present embodiment, includes the raw material of following parts by weight：
Attapulgite modified 25 parts, 10 parts of stearic acid, 5 parts of triethanolamine, 15 parts of emulsifying agent, 4 parts of glycerine, sodium carboxymethylcellulose
10 parts of 1 part, 0.5 part of sodium tripolyphosphate, 0.3 part of menthol, 0.3 part of sterilization and anticorrosion additive and deionized water.
Emulsifying agent is lanolin and polysorbate fat according to weight ratio 1 in the present embodiment:The mixture of 1.5 compositions.
Sterilization and anticorrosion additive is that ethylparaben, propylben, sorbic acid compare 1 according to weight in the present embodiment:1:5
The mixture of composition.
A kind of preparation method of attapulgite modified high-comfort shaving cream of the present embodiment, comprises the following steps：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 200 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, sodium tripolyphosphate, menthol, stir 25 minutes, speed of agitator is 850r/min, obtains mixture
A；
Step 3, by mixture A made from step 2, stearic acid, triethanolamine, emulsifying agent, glycerine, sterilization and anticorrosion additive,
Deionized water is added in Multifunction colloid grinder, and grinding rotating speed is 70 minutes in 3000r/min, milling time, obtains cream
Shape mixture, paste mixture grain fineness is less than 0.01 millimeter, and paste mixture is added in vacuum degassing machine and carries out vacuum
Degasification technique processing, vacuum packaging obtains attapulgite modified high-comfort shaving cream.
Attapulgite modified preparation method is as follows in the present embodiment：A, following component raw material is weighed by weight：It is concavo-convex
100 parts of rod soil, 2 parts of calgon, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, dodecyl sulphate
2 parts of sodium；B, attapulgite is put into the hydrochloric acid solution that concentration is 1mol/L, heating water bath is to 65 DEG C, with stirring for 500r/min
Mix rotating speed stirs 2h, filtering, and filter residue is washed with deionized to neutrality, drying；C, by b gained material and calgon,
Sodium Polyacrylate, polyvinyl alcohol, silane coupler, lauryl sodium sulfate mixing, and heating water bath is to 85 DEG C, with 500r/min
Speed of agitator, stir 70 minutes, centrifuge, sediment is washed with deionized to neutrality, drying is subsequently placed in Muffle furnace
In calcine 2h at 420 DEG C, cooling produces attapulgite modified.
Embodiment 2.
A kind of attapulgite modified high-comfort shaving cream of the present embodiment, includes the raw material of following parts by weight：
Attapulgite modified 35 parts, 20 parts of stearic acid, 15 parts of triethanolamine, 25 parts of emulsifying agent, 8 parts of glycerine, carboxymethyl cellulose
20 parts of 3 parts of sodium, 0.9 part of sodium tripolyphosphate, 0.7 part of menthol, 0.7 part of sterilization and anticorrosion additive and deionized water.
Emulsifying agent is lanolin and polysorbate fat according to weight ratio 1 in the present embodiment:The mixture of 1.5 compositions.
Sterilization and anticorrosion additive is that ethylparaben, propylben, sorbic acid compare 1 according to weight in the present embodiment:1:5
The mixture of composition.
A kind of preparation method of attapulgite modified high-comfort shaving cream of the present embodiment, comprises the following steps：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 200 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, sodium tripolyphosphate, menthol, stir 15 minutes, speed of agitator is 950r/min, obtains mixture
A；
Step 3, by mixture A made from step 2, stearic acid, triethanolamine, emulsifying agent, glycerine, sterilization and anticorrosion additive,
Deionized water is added in Multifunction colloid grinder, and grinding rotating speed is 40 minutes in 4000r/min, milling time, obtains cream
Shape mixture, paste mixture grain fineness is less than 0.01 millimeter, and paste mixture is added in vacuum degassing machine and carries out vacuum
Degasification technique processing, vacuum packaging obtains attapulgite modified high-comfort shaving cream.
Attapulgite modified preparation method is as follows in the present embodiment：A, following component raw material is weighed by weight：It is concavo-convex
100 parts of rod soil, 2 parts of calgon, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, dodecyl sulphate
2 parts of sodium；B, attapulgite is put into the hydrochloric acid solution that concentration is 1mol/L, heating water bath is to 75 DEG C, with 1000r/min's
Speed of agitator stirs 1h, filtering, and filter residue is washed with deionized to neutrality, drying；C, by gained material and hexa metaphosphoric acid in b
Sodium, Sodium Polyacrylate, polyvinyl alcohol, silane coupler, lauryl sodium sulfate mixing, and heating water bath is to 95 DEG C, with
1000r/min speed of agitator, is stirred 40 minutes, is centrifuged, and sediment is washed with deionized to neutrality, is dried, then
It is placed in Muffle furnace at 480 DEG C and calcines 1h, cooling produces attapulgite modified.
Embodiment 3.
A kind of attapulgite modified high-comfort shaving cream of the present embodiment, includes the raw material of following parts by weight：
Attapulgite modified 30 parts, 15 parts of stearic acid, 10 parts of triethanolamine, 20 parts of emulsifying agent, 6 parts of glycerine, carboxymethyl cellulose
15 parts of 2 parts of sodium, 0.7 part of sodium tripolyphosphate, 0.5 part of menthol, 0.5 part of sterilization and anticorrosion additive and deionized water.
Emulsifying agent is lanolin and polysorbate fat according to weight ratio 1 in the present embodiment:The mixture of 1.5 compositions.
Sterilization and anticorrosion additive is that ethylparaben, propylben, sorbic acid compare 1 according to weight in the present embodiment:1:5
The mixture of composition.
A kind of preparation method of attapulgite modified high-comfort shaving cream of the present embodiment, comprises the following steps：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 200 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, sodium tripolyphosphate, menthol, stir 20 minutes, speed of agitator is 900r/min, obtains mixture
A；
Step 3, by mixture A made from step 2, stearic acid, triethanolamine, emulsifying agent, glycerine, sterilization and anticorrosion additive,
Deionized water is added in Multifunction colloid grinder, and grinding rotating speed is 55 minutes in 3500r/min, milling time, obtains cream
Shape mixture, paste mixture grain fineness is less than 0.01 millimeter, and paste mixture is added in vacuum degassing machine and carries out vacuum
Degasification technique processing, vacuum packaging obtains attapulgite modified high-comfort shaving cream.
Attapulgite modified preparation method is as follows in the present embodiment：A, following component raw material is weighed by weight：It is concavo-convex
100 parts of rod soil, 2 parts of calgon, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, dodecyl sulphate
2 parts of sodium；B, attapulgite is put into the hydrochloric acid solution that concentration is 1mol/L, heating water bath is to 70 DEG C, with stirring for 700r/min
Mix rotating speed stirs 1.5h, filtering, and filter residue is washed with deionized to neutrality, drying；C, by gained material and hexa metaphosphoric acid in b
Sodium, Sodium Polyacrylate, polyvinyl alcohol, silane coupler, lauryl sodium sulfate mixing, and heating water bath is to 90 DEG C, with 750r/
Min speed of agitator, is stirred 55 minutes, is centrifuged, and sediment is washed with deionized to neutrality, drying, is subsequently placed in horse
1.5h is not calcined in stove at 450 DEG C, cooling produces attapulgite modified.
A kind of skin feel of attapulgite modified high-comfort shaving cream of the present invention is preferable, moderate performance, excitant
It is less, the friction and skin injury in shaving session can be effectively reduced, in addition with the function of sterilizing, while the present invention is carried
The preparation method material cost of confession is relatively low, raw material is easy to get, technique is concise, before higher use value and good application
Scape.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit is required rather than described above is limited, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that for clarity, those skilled in the art should
Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
It may be appreciated other embodiment.
Claims (8)
1. a kind of attapulgite modified high-comfort shaving cream, it is characterised in that include the raw material of following parts by weight：
Attapulgite modified 25-35 parts, 10-20 parts of stearic acid, 5-15 parts of triethanolamine, 15-25 parts of emulsifying agent, 4-8 parts of glycerine,
1-3 parts of sodium carboxymethylcellulose, 0.5-0.9 parts of sodium tripolyphosphate, 0.3-0.7 parts of menthol, sterilization and anticorrosion additive 0.3-
0.7 part and 10-20 parts of deionized water.
2. the attapulgite modified high-comfort shaving cream of one kind according to claim 1, it is characterised in that the modification is recessed
The high-comfort shaving cream of convex rod soil includes the raw material of following parts by weight：
Attapulgite modified 30 parts, 15 parts of stearic acid, 10 parts of triethanolamine, 20 parts of emulsifying agent, 6 parts of glycerine, carboxymethyl cellulose
15 parts of 2 parts of sodium, 0.7 part of sodium tripolyphosphate, 0.5 part of menthol, 0.5 part of sterilization and anticorrosion additive and deionized water.
3. the attapulgite modified high-comfort shaving cream of one kind according to claim 1 or 2, it is characterised in that the breast
Agent is lanolin and polysorbate fat according to weight ratio 1:The mixture of 1.5 compositions.
4. the attapulgite modified high-comfort shaving cream of one kind according to claim 1 or 2, it is characterised in that described to kill
Bacterium anticorrosive additive is ethylparaben, propylben, sorbic acid compare 1 according to weight:1:The mixture of 5 compositions.
5. a kind of method for preparing attapulgite modified high-comfort shaving cream as claimed in claim 1 or 2, its feature exists
In comprising the following steps：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 200 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, sodium tripolyphosphate, menthol, stir 15-25 minutes, speed of agitator is 850-950r/min, is obtained
Mixture A；
Step 3, by mixture A made from step 2, stearic acid, triethanolamine, emulsifying agent, glycerine, sterilization and anticorrosion additive,
Deionized water is added in Multifunction colloid grinder, and grinding rotating speed is in 3000-4000r/min, and milling time is 40-70 points
Clock, obtains paste mixture, and paste mixture grain fineness is less than 0.01 millimeter, and paste mixture is added in vacuum degassing machine
Vacuum degassing process processing is carried out, vacuum packaging obtains attapulgite modified high-comfort shaving cream.
6. a kind of preparation method of attapulgite modified high-comfort shaving cream according to claim 5, it is characterised in that
The preparation process is：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 200 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, sodium tripolyphosphate, menthol, stir 20 minutes, speed of agitator is 900r/min, obtains mixture
A；
Step 3, by mixture A made from step 2, stearic acid, triethanolamine, emulsifying agent, glycerine, sterilization and anticorrosion additive,
Deionized water is added in Multifunction colloid grinder, and grinding rotating speed is 55 minutes in 3500r/min, milling time, obtains cream
Shape mixture, paste mixture grain fineness is less than 0.01 millimeter, and paste mixture is added in vacuum degassing machine and carries out vacuum
Degasification technique processing, vacuum packaging obtains attapulgite modified high-comfort shaving cream.
7. a kind of preparation method of attapulgite modified high-comfort shaving cream according to claim 5 or 6, its feature exists
In the attapulgite modified preparation method is as follows：A, following component raw material is weighed by weight：100 parts of attapulgite, six
2 parts of sodium metaphosphate, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, 2 parts of lauryl sodium sulfate；B, will be recessed
Convex rod soil is put into the hydrochloric acid solution that concentration is 1mol/L, and heating water bath is turned to 65-75 DEG C with 500-1000r/min stirring
Speed stirring 1-2h, filtering, filter residue is washed with deionized to neutrality, drying；C, by gained material and calgon in b, gather
PAA, polyvinyl alcohol, silane coupler, lauryl sodium sulfate mixing, and heating water bath is to 85-95 DEG C, with 500-
1000r/min speed of agitator, is stirred 40-70 minutes, is centrifuged, and sediment is washed with deionized to neutrality, is dried, so
After be placed in Muffle furnace at 420-480 DEG C and calcine 1-2h, cooling produces attapulgite modified.
8. a kind of preparation method of attapulgite modified high-comfort shaving cream according to claim 5 or 6, its feature exists
In the attapulgite modified preparation method is as follows：A, following component raw material is weighed by weight：100 parts of attapulgite, six
2 parts of sodium metaphosphate, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, 2 parts of lauryl sodium sulfate；B, will be recessed
Convex rod soil is put into the hydrochloric acid solution that concentration is 1mol/L, and heating water bath is stirred to 70 DEG C with 700r/min speed of agitator
1.5h, filtering, filter residue is washed with deionized to neutrality, drying；C, by gained material and calgon, polyacrylic acid in b
Sodium, polyvinyl alcohol, silane coupler, lauryl sodium sulfate mixing, and heating water bath is to 90 DEG C, is turned with 750r/min stirring
Speed, is stirred 55 minutes, is centrifuged, and sediment is washed with deionized to neutrality, drying, is subsequently placed in Muffle furnace 450
1.5h is calcined at DEG C, cooling produces attapulgite modified.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108852906A (en) * | 2018-07-09 | 2018-11-23 | 安徽衣露士生物科技有限公司 | A kind of hand cleanser that dirt-removing power is strong |
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| CN101401772A (en) * | 2008-10-28 | 2009-04-08 | 郁承耀 | Attapulgite shaving cream |
| CN103694769A (en) * | 2013-12-23 | 2014-04-02 | 明光市天骄科技发展有限公司 | Preparation method of activated organic attapulgite for coating |
| CN103724569A (en) * | 2013-12-23 | 2014-04-16 | 杨立新 | Polymer attapulgite plural gel and preparation method thereof |
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| CN101401778A (en) * | 2008-10-28 | 2009-04-08 | 郁承耀 | Shaving cream without foam of attapulgite |
| CN101401776A (en) * | 2008-10-28 | 2009-04-08 | 郁承耀 | Attapulgite gas-dissoluble shaving foam |
| CN101401772A (en) * | 2008-10-28 | 2009-04-08 | 郁承耀 | Attapulgite shaving cream |
| CN103694769A (en) * | 2013-12-23 | 2014-04-02 | 明光市天骄科技发展有限公司 | Preparation method of activated organic attapulgite for coating |
| CN103724569A (en) * | 2013-12-23 | 2014-04-16 | 杨立新 | Polymer attapulgite plural gel and preparation method thereof |
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