CN1070659A - From cottonseed, bran chaff, the dregs of fat, extract the method for humic acids - Google Patents
From cottonseed, bran chaff, the dregs of fat, extract the method for humic acids Download PDFInfo
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- CN1070659A CN1070659A CN 92110708 CN92110708A CN1070659A CN 1070659 A CN1070659 A CN 1070659A CN 92110708 CN92110708 CN 92110708 CN 92110708 A CN92110708 A CN 92110708A CN 1070659 A CN1070659 A CN 1070659A
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Abstract
The present invention relates to a kind of method of from cottonseed, bran chaff, the dregs of fat, extracting humic acids, with cottonseed, the dregs of fat (soya-bean cake, sesame oil, peanut cake), bark, leaf mix and add 10～15% water through feed grinder separated pulverizing, screening and bran chaff (corn, millet, wheat), the woven bag of packing into is deposited in fermentation in the semi-underground glasshouse, naturally cooling is put into and is stirred altar then, with Hot water immersion 10～14 hours, carry out liquid-solid separation, filtrate is carried out concentration and evaporation, it is thick that solution to be concentrated presents Vandyke brown, stop evaporation, carry out drying and separate out the Vandyke brown crystal.
The product that the present invention produces contains total humic acid 61.0% (butt), and wherein xanthohumic acid is 50.5% (butt), field, obvious economic such as can be widely used in worker, farming, herd.
Description
The present invention relates to from cottonseed, bran chaff, the dregs of fat, extract the method for humic acids.
Humic acids is a kind of worker of being widely used in, farming, the organic substance in field such as cure, herd, seed amino acid surplus it contains ten, the L-glutamic acid that wherein internationally recognized physiologically active is stronger, glycine, lysine content are all very abundant, also have VITMAIN B1, B2, B6, B12 and Yeast Nucleic Acid in addition, its economical effectiveness is noticeable.Be subjected to domestic and international expert's attention in recent years, extract humic acids at present, be from mineral substance such as peat, brown coal, weathered coal, to extract with strong acid, highly basic, complex manufacturing, the cost height, and contain certain hazardous and noxious substances in the humic acids that extracts, at nature, humic acids is richly stored with in the organic substance waste material, make organic fertilizer in China's general using straw, green grass, dregs of fat fermentation, can partly form corruption in the decomposition and inversion process of microorganism and plant matter, but therefrom not extract useful humic acids as organic fertilizer.
The objective of the invention is to fill up the blank of prior art, a kind of method of extracting humic acids from cottonseed, bran chaff, the dregs of fat is provided, another object of the present invention is to seek one to extract humic acids with biochemical process from organic substance.
Adopt the inventive method, from cottonseed, bran chaff, the dregs of fat, extract humic acids, measure through unit analysises such as chemistry institute of the Chinese Academy of Sciences, Chinese forestry institute analytic centre and Beijing Agricultural University, wherein organic composition reaches (butt) more than 50%, contain 15 kinds in the organic composition with upper amino acid, total amino acid content reaches 1060mg/100ml, and the base of giving money as a gift calculates total amino acid content and reaches 25%, surpasses the dark county of like product 10%().The L-glutamic acid that wherein internationally recognized physiologically active is stronger, glycine, Methionin equal size are 418mg/ml.In addition, also contain a large amount of humic acidss, total humic acid content reaches the 61%(butt).Wherein brown Ulmic acids 10.5%, and active stronger xanthohumic acid accounts for the 50.5%(butt, sees chemistry institute of Chinese Academy of Sciences analysis report), there is important exploitation to be worth.Also have VITAMIN such as B1, B2, B6, B12 and solubility low-carbon (LC) sugar (content is 1.49%) and Yeast Nucleic Acid, nucite (inositol) etc. in the biochemical fermentation liquid.
Realize that concrete technical scheme of the present invention is:
1, raw material is formed (weight %)
Cottonseed 50～70 bran chaffs 15～25 dregs of fat 5～15 barks, leaf 5～15
Vegetables oil means phosphide materials such as soya-bean cake, sesame oil cake, peanut cake, cottonseed cake in the above-mentioned composition.The bran chaff means the wheat bran powder that corn, millet, wheat flour milling process produce.
2, extraction process
Leaf, bark, cottonseed, a vegetables oil blob of slag are pulverized through feed grinder respectively, divide and bran chaff powder (corn, millet, wheat) is mixed in proportion and adds 10～15% water by 50 mesh sieves, the woven bag of packing into is deposited in fermentation in the semi-underground glasshouse, temperature is controlled at 65～80 ℃, less than 80 ℃, kept 13～16 days, and then lowered the temperature 5～8 days naturally.Material after fermentation is put into steel basin and was flooded 10～14 hours with 30～40 ℃ of warm water (solid-to-liquid ratio 1: 5～10), carries out liquid-solid separation then, and filter cake is as fertilizer, its filtrate is the liquid humic acids, and this humic acids carries out evaporation concentration, and vaporization temperature is 50～80 ℃, must not be above 80 ℃, it is thick to treat that liquid presents Vandyke brown, stops evaporation, and material is moved into the kiln inner drying, keep 50～80 ℃ of temperature, be lower than 80 ℃, form the chocolate crystal, be treated as finished product through packaging sterilizing.
The product that uses the inventive method to produce has extensive use, and being applied in has multiple effect on the crop, mainly be:
(1) improve rate of emergence, emerge ahead of time, seedling is neat, and seedling is complete, and seedling is strong.
(2) to promoting root system development early stage, it is favourable that the later stage is recovered the root system vigor.
(3) increase chlorophyll content, strengthen intensity of photosynthesis.
(4) activity of plurality of enzymes enhances metabolism in the enhancing body.
(5) increase the receptivity of crop, and make and plant that nutrient shifts to the fruit seed in the pearl body soil nutrient.
(6) strengthen the crop anti-adversity ability, comprise low temperature, arid, the natural disaster abilities such as disease of resisting.
(7) comprehensive action result causes acting on the improvement of output increase and quality of agricultural product.
Main using method is soaked seed, is soaked root, soaks cutting, foliage-spray.
In industrial aspect:
(1) concrete additive, have the effect of improving execution conditions, helping mechanized, reduce curing time and save cement.
(2) drilling fluid additive has effects such as viscosity reduction, dilution, anti-well slough.
(3) ceramic additive can improve pottery moulded pottery not yet put in a kiln to bake intensity 90%, and has effects such as plasticising, dilution, absorption.
(4) boiler water tank scale remover can be removed rust deposite and incrustation scale, and can slow down incrustation scale formation speed, can reduce by 5～10 ℃ of water temperatures.
Aspect animal husbandry, be used for fodder additives, it can promote promote growth of farm animal, saves feed and shortens the nursing time.
Aspect medical, it has anti-inflammatory, pain relieving, stops blooding, prevents and treats hypertension, heart trouble, anticancer, go multiple functions such as saprophytic machine.
The present invention compares with other humic acids has following characteristics:
(1) of light color, transparency is high, and is soluble in water, nontoxic, nuisanceless.
(2) characteristics of anti-hard water are arranged.
(3) molecular weight is little, and is active high.
(4) be easy to promote vegeto-animal absorption and utilization.
(5) as medicine can external application, inject and take.
Product of the present invention through the chemistry analytical test result of institute of the Chinese Academy of Sciences is:
Sample is a brown aqueous solution, and recording solids content through 70 ℃ of following infrared dryings is 4.0%.The easy moisture absorption of solids becomes the thickness body.Conform to conventional humic acids according to its infrared spectrum of this institute Infrared spectroscopy, illustrate that the main body thing is a humic acids.Through quantitative analysis, detecting total humic acid is the 61%(butt), brown Ulmic acids is 10.5%, xanthohumic acid is that 50.5%(is butt).Infrared spectra is seen accompanying drawing 2.
Description of drawings:
Fig. 1 extracts the humic acids process flow diagram from cottonseed, bran chaff, the dregs of fat
Fig. 2 infrared spectrogram
Claims (6)
1, a kind of method of from cottonseed, bran chaff, the dregs of fat, extracting humic acids, it is characterized in that cottonseed, the dregs of fat, bark, leaf mix and add 10～15% water through feed grinder separated pulverizing, screening and bran chaff, the woven bag of packing into is deposited in fermentation in the semi-underground glasshouse, naturally cooling then, put into and stir altar, with Hot water immersion 10～14 hours, carry out liquid-solid separation, filtrate is carried out concentration and evaporation, it is thick that solution to be concentrated presents Vandyke brown, stop evaporation, carry out drying and separate out the Vandyke brown crystal, be finished product through packaging sterilizing.
2, method according to claim 1 is characterized in that raw material composition (weight %) is:
Cottonseed 50～70 bran chaffs 15～25 dregs of fat 5～15 barks, leaf 5～15
3, method according to claim 1 is characterized in that the described dregs of fat are that soya-bean cake, sesame oil cake, rapeseed cake, peanut cake, described bran chaff are the wheat bran that corn, millet, wheat grind flour.
4, method according to claim 1 is characterized in that leavening temperature is 65～80 ℃, must not be greater than 80 ℃, and fermentation time is 13～16 days, lowers the temperature 5～8 days naturally then.
5, method according to claim 1, the hot water temperature is 30～40 ℃ when it is characterized in that flooding, and solid-to-liquid ratio is 1: 5～10, and evaporation remains on 50～80 ℃ with drying temperature, is not higher than 80 ℃.
6, method according to claim 1 is characterized in that humic acids is divided into liquid and solid, is the liquid humic acids through the filtrate after dipping, the liquid-solid separation, proceeds evaporation drying and handles, and separating out the Vandyke brown crystal becomes the solid humic acids.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92110708 CN1070659A (en) | 1992-09-22 | 1992-09-22 | From cottonseed, bran chaff, the dregs of fat, extract the method for humic acids |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92110708 CN1070659A (en) | 1992-09-22 | 1992-09-22 | From cottonseed, bran chaff, the dregs of fat, extract the method for humic acids |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1070659A true CN1070659A (en) | 1993-04-07 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 92110708 Pending CN1070659A (en) | 1992-09-22 | 1992-09-22 | From cottonseed, bran chaff, the dregs of fat, extract the method for humic acids |
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| CN (1) | CN1070659A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1081651C (en) * | 1999-09-23 | 2002-03-27 | 中国科学院化工冶金研究所 | Process for preparing humic acid by aerating stalks |
| CN103820500A (en) * | 2014-02-17 | 2014-05-28 | 塔里木大学 | Technology method utilizing waste cotton seeds to produce humic acid |
| CN105838376A (en) * | 2016-03-15 | 2016-08-10 | 石河子大学 | Humic acid soil conditioner, and composition, preparation method and application method thereof |
| CN107828505A (en) * | 2017-11-11 | 2018-03-23 | 蒋世芬 | A kind of extraction extracts peanut oil from the peanut dregs of fat |
| CN108424304A (en) * | 2018-06-11 | 2018-08-21 | 深圳市环资源科创投资有限公司 | The method for producing humic acid fertilizer |
| CN110833115A (en) * | 2019-11-21 | 2020-02-25 | 南京胜昔实业有限公司 | Comprehensive utilization method of cotton production by-products by using biochemical fulvic acid as main product |
-
1992
- 1992-09-22 CN CN 92110708 patent/CN1070659A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1081651C (en) * | 1999-09-23 | 2002-03-27 | 中国科学院化工冶金研究所 | Process for preparing humic acid by aerating stalks |
| CN103820500A (en) * | 2014-02-17 | 2014-05-28 | 塔里木大学 | Technology method utilizing waste cotton seeds to produce humic acid |
| CN103820500B (en) * | 2014-02-17 | 2015-12-02 | 塔里木大学 | Waste cotton seed is utilized to produce the processing method of humic acid |
| CN105838376A (en) * | 2016-03-15 | 2016-08-10 | 石河子大学 | Humic acid soil conditioner, and composition, preparation method and application method thereof |
| CN105838376B (en) * | 2016-03-15 | 2020-03-27 | 石河子大学 | Humic acid soil conditioner and composition, preparation method and use method thereof |
| CN107828505A (en) * | 2017-11-11 | 2018-03-23 | 蒋世芬 | A kind of extraction extracts peanut oil from the peanut dregs of fat |
| CN108424304A (en) * | 2018-06-11 | 2018-08-21 | 深圳市环资源科创投资有限公司 | The method for producing humic acid fertilizer |
| CN110833115A (en) * | 2019-11-21 | 2020-02-25 | 南京胜昔实业有限公司 | Comprehensive utilization method of cotton production by-products by using biochemical fulvic acid as main product |
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| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |