CN107050092A - It is a kind of to reduce the processing method of content of beary metal in honeysuckle medicine materical crude slice - Google Patents
It is a kind of to reduce the processing method of content of beary metal in honeysuckle medicine materical crude slice Download PDFInfo
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- CN107050092A CN107050092A CN201710336306.8A CN201710336306A CN107050092A CN 107050092 A CN107050092 A CN 107050092A CN 201710336306 A CN201710336306 A CN 201710336306A CN 107050092 A CN107050092 A CN 107050092A
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- honeysuckle
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- crude slice
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/37—Extraction at elevated pressure or temperature, e.g. pressurized solvent extraction [PSE], supercritical carbon dioxide extraction or subcritical water extraction
Abstract
The present invention relates to prepared slices of Chinese crude drugs processing technique field, a kind of processing method of content of beary metal in reduction honeysuckle medicine materical crude slice is disclosed, is comprised the following steps：（1）The honeysuckle newly won is put in soak and soaked, the Adsorption of Heavy Metals and chemical residue on surface can be removed, is cleaned up after immersion and is put in the activity that inhibitory enzyme is capable of in refrigerating chamber refrigeration, prevent the decomposition of chlorogenic acid and galuteolin；（2）It ensure that after refrigeration after honeysuckle quality of colour, using the heavy metal inside supercritical carbon dioxide extraction method removing, the use of compounding and process condition and additive, with very strong penetrability, removal rate reaches 70 80%；（3）Color protection is further carried out after extraction, while using the moisture removed compared with low temperature process in honeysuckle medicine materical crude slice, its drug effect can be kept again；（4）Honeysuckle drink after air-drying is preserved using natural Vermins-proof mildew-proof method, it is therefore prevented that the element that chemical agent is brought is climbed to a higher point, and improves the security of honeysuckle medicine materical crude slice.
Description
Technical field
The invention belongs to prepared slices of Chinese crude drugs processing technique field, and in particular to content of beary metal in one kind reduction honeysuckle medicine materical crude slice
Processing method.
Background technology
Honeysuckle, also known as honeysuckle, " honeysuckle " one is come from《Compendium of Materia Medica》, due to being opened at the beginning of honeysuckle flowers as white, rear turn
For yellow, hence obtain one's name honeysuckle.Honeysuckle, March blooms, and five go out, micro-perfume, and redly, then color is white by Hua Chukai, through one, two for the base of a fruit
Day, then color was yellow, therefore named honeysuckle.Again because a base of a fruit two is spent, two pistils are visited outside, in pairs, are never left each other, and shape is such as male female
Together, and like mandarin duck to dance, therefore there is the title of mandarin duck rattan.This kind be most significantly characterized by big shape lobate bract.It
In person somewhat like Lonicera confusa, but that bract planted is narrow thin rather than lobate, the close raw pubescence of calyx tube, the close raw curling of sprig
Pubescence, it is significantly different with this kind.The morphological variation of this kind is very big, no matter branch, the fleece of leaf, leaf shapes and sizes
And in terms of length, fleece and the lip of corolla and the length ratio in cylinder portion, all vary widely.But all these changes
Apparently more it is associated with ecological environment, not display and the correlation between geographical distribution.
Honeysuckle is described as clearing heat and detoxicating good medicine from ancient times, the sweet cold air fragrance of its property, and clear heat with drugs of sweet flavour and cold nature is without injuring one's stomach, and fragrance is thoroughly
Up to again can eliminating evil.Honeysuckle can dispelling wind-heat, also kind removing summer-heat blood poison, for various febrile diseases, such as body heat, dermexanthesis, hair spot, heat
The diseases such as carbuncle carbuncle, abscess of throat, equal effect is notable.
In order to meet the market requirement, the honeysuckle often processing sell in the form of medicine materical crude slice, because the medicinal part of honeysuckle is
Bud, the flower and leaf of plant adsorb the heavy metal in soil and air in growth, and enriching quantity will be high than other positions, gold and silver
It is covered with fine hair on colored bud, easily Adsorption of Heavy Metals, causes heavy metal deposition, honeysuckle medicine materical crude slice can not be kept away through artificial processing
The meeting exempted from is polluted by heavy metal and harmful element, and common heavy metal and harmful element pollution have lead (Pb), cadmium (Cd), arsenic
(As), mercury (Hg), copper (Cu) etc. pollute.Heavy metal and harmful element enter the not only possible acute poisoning for causing body of human body,
It can also be accumulated in human body, cause slow poisoning, endangered extremely serious.
The content of the invention
The purpose of the present invention be for it is existing the problem of there is provided it is a kind of reduction honeysuckle medicine materical crude slice in content of beary metal plus
Work preparation method, being reduced to content of beary metal in honeysuckle medicine materical crude slice during raw material selection, processing will not be to human body
The safe range caused harm.
The present invention is achieved by the following technical solutions：
It is a kind of to reduce the processing method of content of beary metal in honeysuckle medicine materical crude slice, comprise the following steps：
（1）The honeysuckle that is produced from selection air quality high-quality area is harvested as processing raw material at the 7-9 o'clock in the morning,
Obtained honeysuckle, which is put into soak, to be soaked 30-40 minutes, and the soak contains following component：Pure water, activated carbon, acid iodide
Honeysuckle is pulled out after potassium, vitamin C, tannic acid, immersion, is rinsed 3-5 times using the clear water of flowing, drying naturally after surface moisture makes
It is fresh-keeping with freshness protection package, it is put into 0-5 DEG C of refrigerating chamber and refrigerates 2-3 days；
（2）Honeysuckle after refrigeration is extracted using supercritical carbon dioxide extraction method, mass fraction is added in extraction process is
0.5-0.7% methanol adds mass fraction and is used as cooperation for 5.5-6.5% diethyl-dithio sodium formate as modifying agent
Agent, extraction time is 15-20 minutes, and extracting pressure is 18-20MPa, and extraction temperature is 60-70 DEG C；
（3）By after extraction honeysuckle take out, be put into 80-90 DEG C of hot water and scald 15-20 seconds, pull out immediately be put into it is cold in cold water
But, excessive moisture then is removed using microwave drying, drying temperature is 30-35 DEG C, and it is 10-15% to dry to water content, in drying
Honeysuckle surface afterwards uniformly sprinkles a thin layer of starch, and the starch usage amount of every 1 kilogram of honeysuckle is 20-30 grams, then is made
Hung with rope, it is 5-8% to continue to dry in the shade at gravity-flow ventilation to water content；
（4）Honeysuckle after air-drying is fitted into ventilative gauze, is placed in dry while being put into the champignon bag of preparation, every 10 kilograms
Honeysuckle is using 8-10 champignon bag, each 10-15 grams of bag weight, and the champignon bag contains following component in parts by weight：Chrysanthemum
12-14 parts, 9-11 parts of Momordica grosvenori, 7-9 parts of radix glycyrrhizae, 4-6 parts of lavender, 3-5 parts of camphortree bark, 2-4 parts of lemon tablet, soapberry 1-3
Part.
It is used as further improvement of these options, step（1）Described soak is according to mass percent meter by following
Composition is made：Particle size for 1-2 centimetres of activated carbon account for 3-5%, Potassiumiodate account for 0.2-0.5%, vitamin account for 0.05-0.07%,
Tannic acid accounts for 0.03-0.05%, remaining as pure water.
It is used as further improvement of these options, step（2）Titanium dioxide in the described carbon dioxide extraction method of boundary over zero
Carbon flow speed is 50-60kg/h.
The present invention has advantages below compared with prior art：Exist to solve existing honeysuckle medicine materical crude slice in processing method
The problem of content of beary metal is higher, the processing and fabricating side of content of beary metal in honeysuckle medicine materical crude slice is reduced the invention provides a kind of
Method, comprises the following steps：（1）The honeysuckle newly won is put in soak and soaked, the Adsorption of Heavy Metals on surface can be removed
And chemical residue, cleaned up after immersion and be put in the activity that inhibitory enzyme is capable of in refrigerating chamber refrigeration, prevent chlorogenic acid and sweet-scented osmanthus
The decomposition of careless glycosides；（2）It ensure that after honeysuckle quality of colour, removed using supercritical carbon dioxide extraction method internal after refrigeration
Heavy metal, the use of compounding and process condition and additive, with very strong penetrability, removal rate reaches 70-80%；（3）Extraction
Color protection is further carried out afterwards, while using the moisture removed compared with low temperature process in honeysuckle medicine materical crude slice, its drug effect can be kept again；（4）Wind
Honeysuckle drink after dry is preserved using natural Vermins-proof mildew-proof method, it is therefore prevented that the element that chemical agent is brought is climbed to a higher point, and is improved
The security of honeysuckle medicine materical crude slice.
Embodiment
With reference to specific embodiment, the present invention will be further described.
Embodiment 1
It is a kind of to reduce the processing method of content of beary metal in honeysuckle medicine materical crude slice, comprise the following steps：
（1）The honeysuckle that is produced from selection air quality high-quality area is harvested as processing raw material at the 7-9 o'clock in the morning,
Obtained honeysuckle, which is put into soak, to be soaked 30 minutes, and the soak contains following component：Pure water, activated carbon, Potassiumiodate,
Honeysuckle is pulled out after vitamin C, tannic acid, immersion, is rinsed 3 times using the clear water of flowing, is dried naturally after surface moisture using guarantor
Fresh bag is fresh-keeping, is put into 0 DEG C of refrigerating chamber and refrigerates 2 days；
（2）Honeysuckle after refrigeration is extracted using supercritical carbon dioxide extraction method, mass fraction is added in extraction process is
0.5% methanol is as modifying agent, and the diethyl-dithio sodium formate that addition mass fraction is 5.5% is as compounding ingredient, during extraction
Between be 15 minutes, extracting pressure is 18MPa, and extraction temperature is 60 DEG C；
（3）Honeysuckle after extraction is taken out, is put into 80 DEG C of hot water and scalds 15 seconds, pulls out be put into cooling in cold water immediately, then
Excessive moisture is removed using microwave drying, drying temperature is 30 DEG C, it is 10%, honeysuckle table after the drying to dry to water content
Face uniformly sprinkles a thin layer of starch, and the starch usage amount of every 1 kilogram of honeysuckle is 20 grams, rope suspension is reused, certainly
It is 5% that right ventilation, which continues to dry in the shade to water content,；
（4）Honeysuckle after air-drying is fitted into ventilative gauze, is placed in dry while being put into the champignon bag of preparation, every 10 kilograms
Honeysuckle weighs 10 grams using 8 champignon bags, each bag, and the champignon bag contains following component in parts by weight：12 parts of chrysanthemum, sieve
9 parts of Chinese fruit, 7 parts of radix glycyrrhizae, 4 parts of lavender, 3 parts of camphortree bark, 2 parts of lemon tablet, 1 part of soapberry.
It is used as further improvement of these options, step（1）Described soak is according to mass percent meter by following
Composition is made：Particle size, which accounts for 3%, Potassiumiodate for 1-2 centimetres of activated carbon and accounts for 0.2%, vitamin and account for 0.05%, tannic acid, to be accounted for
0.03%, remaining as pure water.
It is used as further improvement of these options, step（2）Titanium dioxide in the described carbon dioxide extraction method of boundary over zero
Carbon flow speed is 50kg/h.
Embodiment 2
It is a kind of to reduce the processing method of content of beary metal in honeysuckle medicine materical crude slice, comprise the following steps：
（1）The honeysuckle that is produced from selection air quality high-quality area is harvested as processing raw material at the 7-9 o'clock in the morning,
Obtained honeysuckle, which is put into soak, to be soaked 35 minutes, and the soak contains following component：Pure water, activated carbon, Potassiumiodate,
Honeysuckle is pulled out after vitamin C, tannic acid, immersion, is rinsed 4 times using the clear water of flowing, is dried naturally after surface moisture using guarantor
Fresh bag is fresh-keeping, is put into 2 DEG C of refrigerating chambers and refrigerates 2 days；
（2）Honeysuckle after refrigeration is extracted using supercritical carbon dioxide extraction method, mass fraction is added in extraction process is
0.6% methanol is as modifying agent, and the diethyl-dithio sodium formate that addition mass fraction is 6.0% is as compounding ingredient, during extraction
Between be 17 minutes, extracting pressure is 19MPa, and extraction temperature is 65 DEG C；
（3）Honeysuckle after extraction is taken out, is put into 85 DEG C of hot water and scalds 17 seconds, pulls out be put into cooling in cold water immediately, then
Excessive moisture is removed using microwave drying, drying temperature is 32 DEG C, it is 12%, honeysuckle table after the drying to dry to water content
Face uniformly sprinkles a thin layer of starch, and the starch usage amount of every 1 kilogram of honeysuckle is 25 grams, rope suspension is reused, certainly
It is 6% that right ventilation, which continues to dry in the shade to water content,；
（4）Honeysuckle after air-drying is fitted into ventilative gauze, is placed in dry while being put into the champignon bag of preparation, every 10 kilograms
Honeysuckle weighs 12 grams using 9 champignon bags, each bag, and the champignon bag contains following component in parts by weight：13 parts of chrysanthemum, sieve
10 parts of Chinese fruit, 8 parts of radix glycyrrhizae, 5 parts of lavender, 4 parts of camphortree bark, 3 parts of lemon tablet, 2 parts of soapberry.
It is used as further improvement of these options, step（1）Described soak is according to mass percent meter by following
Composition is made：Particle size, which accounts for 4%, Potassiumiodate for 1-2 centimetres of activated carbon and accounts for 0.3%, vitamin and account for 0.06%, tannic acid, to be accounted for
0.04%, remaining as pure water.
It is used as further improvement of these options, step（2）Titanium dioxide in the described carbon dioxide extraction method of boundary over zero
Carbon flow speed is 55kg/h.
Embodiment 3
It is a kind of to reduce the processing method of content of beary metal in honeysuckle medicine materical crude slice, comprise the following steps：
（1）The honeysuckle that is produced from selection air quality high-quality area is harvested as processing raw material at the 7-9 o'clock in the morning,
Obtained honeysuckle, which is put into soak, to be soaked 40 minutes, and the soak contains following component：Pure water, activated carbon, Potassiumiodate,
Honeysuckle is pulled out after vitamin C, tannic acid, immersion, is rinsed 5 times using the clear water of flowing, is dried naturally after surface moisture using guarantor
Fresh bag is fresh-keeping, is put into 5 DEG C of refrigerating chambers and refrigerates 3 days；
（2）Honeysuckle after refrigeration is extracted using supercritical carbon dioxide extraction method, mass fraction is added in extraction process is
0.7% methanol is as modifying agent, and the diethyl-dithio sodium formate that addition mass fraction is 6.5% is as compounding ingredient, during extraction
Between be 20 minutes, extracting pressure is 20MPa, and extraction temperature is 70 DEG C；
（3）Honeysuckle after extraction is taken out, is put into 90 DEG C of hot water and scalds 20 seconds, pulls out be put into cooling in cold water immediately, then
Excessive moisture is removed using microwave drying, drying temperature is 35 DEG C, it is 15%, honeysuckle table after the drying to dry to water content
Face uniformly sprinkles a thin layer of starch, and the starch usage amount of every 1 kilogram of honeysuckle is 30 grams, rope suspension is reused, certainly
It is 8% that right ventilation, which continues to dry in the shade to water content,；
（4）Honeysuckle after air-drying is fitted into ventilative gauze, is placed in dry while being put into the champignon bag of preparation, every 10 kilograms
Honeysuckle weighs 15 grams using 10 champignon bags, each bag, and the champignon bag contains following component in parts by weight：14 parts of chrysanthemum,
11 parts of Momordica grosvenori, 9 parts of radix glycyrrhizae, 6 parts of lavender, 5 parts of camphortree bark, 4 parts of lemon tablet, 3 parts of soapberry.
It is used as further improvement of these options, step（1）Described soak is according to mass percent meter by following
Composition is made：Particle size, which accounts for 5%, Potassiumiodate for 1-2 centimetres of activated carbon and accounts for 0.5%, vitamin and account for 0.07%, tannic acid, to be accounted for
0.05%, remaining as pure water.
It is used as further improvement of these options, step（2）Titanium dioxide in the described carbon dioxide extraction method of boundary over zero
Carbon flow speed is 60kg/h.
Comparative example 1
With differing only in for embodiment 1, step（1）In be consistent without using soak immersion treatment, remaining step.
Comparative example 2
With differing only in for embodiment 2, step（2）It is middle to be extracted using conventional supercritical carbon dioxide extraction method, its
Remaining step is consistent.
Comparative example 3
With differing only in for embodiment 3, step（3）Middle use high temperature fumigation method removes moisture, and remaining step is consistent.
Contrast test
Embodiment 1-3 and comparative example 1-3 method processing and fabricating honeysuckle medicine materical crude slice is used respectively, while the gold sold with the market
Honeysuckle flower medicine materical crude slice as a control group, is randomly selected 5 products for every group and detected as sample, determines wherein content of beary metal, takes
Average value, records as shown in the table by result：
| Project | Copper（mg/kg） | Lead（mg/kg） | Mercury（mg/kg） | Chromium（mg/kg） |
| Embodiment 1 | 0.13 | 0.06 | 0.05 | 0.09 |
| Embodiment 2 | 0.11 | 0.05 | 0.04 | 0.08 |
| Embodiment 3 | 0.12 | 0.07 | 0.05 | 0.07 |
| Comparative example 1 | 0.39 | 0.33 | 0.27 | 0.41 |
| Comparative example 2 | 0.42 | 0.38 | 0.29 | 0.43 |
| Comparative example 3 | 0.35 | 0.31 | 0.24 | 0.37 |
| Control group | 0.56 | 0.47 | 0.45 | 0.52 |
The method of present invention preparation honeysuckle medicine materical crude slice is can be seen that by comparing can effectively reduce the content of heavy metal, improve it
Security and quality.
Claims (3)
1. a kind of reduce the processing method of content of beary metal in honeysuckle medicine materical crude slice, it is characterised in that comprises the following steps：
（1）The honeysuckle that is produced from selection air quality high-quality area is harvested as processing raw material at the 7-9 o'clock in the morning,
Obtained honeysuckle, which is put into soak, to be soaked 30-40 minutes, and the soak contains following component：Pure water, activated carbon, acid iodide
Honeysuckle is pulled out after potassium, vitamin C, tannic acid, immersion, is rinsed 3-5 times using the clear water of flowing, drying naturally after surface moisture makes
It is fresh-keeping with freshness protection package, it is put into 0-5 DEG C of refrigerating chamber and refrigerates 2-3 days；
（2）Honeysuckle after refrigeration is extracted using supercritical carbon dioxide extraction method, mass fraction is added in extraction process is
0.5-0.7% methanol adds mass fraction and is used as cooperation for 5.5-6.5% diethyl-dithio sodium formate as modifying agent
Agent, extraction time is 15-20 minutes, and extracting pressure is 18-20MPa, and extraction temperature is 60-70 DEG C；
（3）By after extraction honeysuckle take out, be put into 80-90 DEG C of hot water and scald 15-20 seconds, pull out immediately be put into it is cold in cold water
But, excessive moisture then is removed using microwave drying, drying temperature is 30-35 DEG C, and it is 10-15% to dry to water content, in drying
Honeysuckle surface afterwards uniformly sprinkles a thin layer of starch, and the starch usage amount of every 1 kilogram of honeysuckle is 20-30 grams, then is made
Hung with rope, it is 5-8% to continue to dry in the shade at gravity-flow ventilation to water content；
（4）Honeysuckle after air-drying is fitted into ventilative gauze, is placed in dry while being put into the champignon bag of preparation, every 10 kilograms
Honeysuckle is using 8-10 champignon bag, each 10-15 grams of bag weight, and the champignon bag contains following component in parts by weight：Chrysanthemum
12-14 parts, 9-11 parts of Momordica grosvenori, 7-9 parts of radix glycyrrhizae, 4-6 parts of lavender, 3-5 parts of camphortree bark, 2-4 parts of lemon tablet, soapberry 1-3
Part.
2. a kind of as claimed in claim 1 reduce the processing method of content of beary metal in honeysuckle medicine materical crude slice, it is characterised in that
Step（1）Described soak is made up according to mass percent meter of following component：Particle size accounts for for 1-2 centimetres of activated carbon
3-5%, Potassiumiodate, which account for 0.2-0.5%, vitamin and account for 0.05-0.07%, tannic acid, accounts for 0.03-0.05%, remaining as pure water.
3. a kind of as claimed in claim 1 reduce the processing method of content of beary metal in honeysuckle medicine materical crude slice, it is characterised in that
Step（2）Carbon dioxide flow rate is 50-60kg/h in the described carbon dioxide extraction method of boundary over zero.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112007376A (en) * | 2020-08-10 | 2020-12-01 | 安徽鑫泰药业有限公司 | Process for reducing heavy metal content of honeysuckle |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104352544A (en) * | 2014-10-08 | 2015-02-18 | 南江县百草中药材有限公司 | Processing method of honeysuckle decoction pieces |
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2017
- 2017-05-13 CN CN201710336306.8A patent/CN107050092A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104352544A (en) * | 2014-10-08 | 2015-02-18 | 南江县百草中药材有限公司 | Processing method of honeysuckle decoction pieces |
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| 化学工业部天津化工研究院等编: "《化工产品手册 无机化工产品》", 31 August 1983, 化学工业出版社 * |
| 张楠楠等: "超临界CO2配合萃取技术去除中药中重金属研究进展", 《亚太传统医药》 * |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112007376A (en) * | 2020-08-10 | 2020-12-01 | 安徽鑫泰药业有限公司 | Process for reducing heavy metal content of honeysuckle |
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Application publication date: 20170818 |