CN107043891B - 一种谐振杆用冷镦丝的生产方法 - Google Patents
一种谐振杆用冷镦丝的生产方法 Download PDFInfo
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- CN107043891B CN107043891B CN201710308109.5A CN201710308109A CN107043891B CN 107043891 B CN107043891 B CN 107043891B CN 201710308109 A CN201710308109 A CN 201710308109A CN 107043891 B CN107043891 B CN 107043891B
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 22
- 239000000463 material Substances 0.000 claims abstract description 35
- 238000000137 annealing Methods 0.000 claims abstract description 34
- 238000005554 pickling Methods 0.000 claims abstract description 27
- 238000000034 method Methods 0.000 claims abstract description 20
- 238000012545 processing Methods 0.000 claims abstract description 20
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000002844 melting Methods 0.000 claims abstract description 17
- 230000008018 melting Effects 0.000 claims abstract description 17
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000010438 heat treatment Methods 0.000 claims abstract description 13
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 10
- 239000011572 manganese Substances 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 239000010703 silicon Substances 0.000 claims abstract description 10
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 10
- 239000000126 substance Substances 0.000 claims abstract description 8
- 229910052742 iron Inorganic materials 0.000 claims abstract description 7
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims abstract description 6
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims abstract description 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000005864 Sulphur Substances 0.000 claims abstract description 6
- 229910052748 manganese Inorganic materials 0.000 claims abstract description 6
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 6
- 229910052698 phosphorus Inorganic materials 0.000 claims abstract description 6
- 239000011574 phosphorus Substances 0.000 claims abstract description 6
- 238000005498 polishing Methods 0.000 claims abstract description 5
- 229910000831 Steel Inorganic materials 0.000 claims description 26
- 239000010959 steel Substances 0.000 claims description 26
- 238000005242 forging Methods 0.000 claims description 19
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 15
- 238000007670 refining Methods 0.000 claims description 13
- 239000002893 slag Substances 0.000 claims description 12
- 239000002253 acid Substances 0.000 claims description 9
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 230000007547 defect Effects 0.000 claims description 8
- 238000012360 testing method Methods 0.000 claims description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 6
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 claims description 6
- 239000007789 gas Substances 0.000 claims description 6
- 230000006698 induction Effects 0.000 claims description 6
- 150000003839 salts Chemical class 0.000 claims description 6
- 238000003723 Smelting Methods 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 238000004321 preservation Methods 0.000 claims description 5
- 238000002791 soaking Methods 0.000 claims description 5
- 229910052786 argon Inorganic materials 0.000 claims description 4
- 238000010622 cold drawing Methods 0.000 claims description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 3
- 229910001634 calcium fluoride Inorganic materials 0.000 claims description 3
- 229910052593 corundum Inorganic materials 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 239000010436 fluorite Substances 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 239000004408 titanium dioxide Substances 0.000 claims description 3
- 229910001845 yogo sapphire Inorganic materials 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 2
- 238000007689 inspection Methods 0.000 claims 1
- 235000021110 pickles Nutrition 0.000 description 8
- 229910000851 Alloy steel Inorganic materials 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 6
- 208000037656 Respiratory Sounds Diseases 0.000 description 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 6
- 229910017604 nitric acid Inorganic materials 0.000 description 6
- 238000005096 rolling process Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 239000000956 alloy Substances 0.000 description 4
- 238000005336 cracking Methods 0.000 description 4
- 229910045601 alloy Inorganic materials 0.000 description 3
- 238000010273 cold forging Methods 0.000 description 3
- 238000004891 communication Methods 0.000 description 3
- 230000008602 contraction Effects 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 239000000314 lubricant Substances 0.000 description 3
- 238000005461 lubrication Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000011780 sodium chloride Substances 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 210000003953 foreskin Anatomy 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000013138 pruning Methods 0.000 description 2
- 239000004576 sand Substances 0.000 description 2
- 239000011265 semifinished product Substances 0.000 description 2
- 238000005491 wire drawing Methods 0.000 description 2
- 229910000975 Carbon steel Inorganic materials 0.000 description 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical group [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910001374 Invar Inorganic materials 0.000 description 1
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 1
- 241001062472 Stokellia anisodon Species 0.000 description 1
- 229910001069 Ti alloy Inorganic materials 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000010962 carbon steel Substances 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000008358 core component Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000010721 machine oil Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 238000010295 mobile communication Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001256 stainless steel alloy Inorganic materials 0.000 description 1
- 238000007514 turning Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/08—Ferrous alloys, e.g. steel alloys containing nickel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21C—MANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
- B21C37/00—Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape
- B21C37/04—Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of bars or wire
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21C—MANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
- B21C37/00—Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape
- B21C37/04—Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of bars or wire
- B21C37/047—Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of bars or wire of fine wires
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/26—Methods of annealing
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
- C21D8/06—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires
- C21D8/065—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires of ferrous alloys
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/16—Remelting metals
- C22B9/18—Electroslag remelting
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C33/00—Making ferrous alloys
- C22C33/04—Making ferrous alloys by melting
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/02—Ferrous alloys, e.g. steel alloys containing silicon
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/04—Ferrous alloys, e.g. steel alloys containing manganese
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/25—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Heat Treatment Of Articles (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Heat Treatment Of Steel (AREA)
Abstract
Description
类别 | 状态 | 规格mm | 加热温度℃ | 保温时间 | 冷却方式 |
镍基合金 | 半成品 | ≥¢8 | 800-850 | ≥40分钟 | 空冷 |
酸洗液配比 | 浓度% | 温度℃ | 时间 |
HCL:HNO3:H2O=1:1:余量 | 15 | 30-50 | 10-20 |
酸洗液配比 | 浓度% | 温度℃ | 时间 |
H2SO4:HNO3:NaCl:H2O=4:1:1:余量 | 30 | 50-70 | 10-15 |
原材料名称 | 技术要求 | 数量(kg) |
石墨粉 | 200-300# | 50 |
机油 | 20# | 50 |
肥皂 | 5 | |
石灰 | 10 | |
水 | 500 |
类别 | 状态 | 规格mm | 加热温度℃ | 保温时间 | 冷却方式 |
镍基合金 | 半成品 | ≥¢8 | 800-850 | ≥40分钟 | 空冷 |
酸洗液配比 | 浓度% | 温度℃ | 时间 |
HCL:HNO3:H2O=1:1:余量 | 15 | 30-50 | 10-20 |
酸洗液配比 | 浓度% | 温度℃ | 时间 |
H2SO4:HNO3:NaCl:H2O=4:1:1:余量 | 30 | 50-70 | 10-15 |
酸洗液配比 | 浓度% | 温度℃ | 时间 |
HCL:HNO3:H2O=1:1:余量 | 15 | 30-50 | 3-15 |
酸洗液配比 | 浓度% | 温度℃ | 时间 |
H2SO4:HNO3:NaCl:H2O=4:1:1:余量 | 30 | 50-70 | 5-10 |
Claims (1)
Priority Applications (1)
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CN201710308109.5A CN107043891B (zh) | 2014-06-11 | 2014-06-11 | 一种谐振杆用冷镦丝的生产方法 |
Applications Claiming Priority (2)
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CN201410255425.7A CN105316575B (zh) | 2014-06-11 | 2014-06-11 | 谐振杆用冷镦丝及其生产方法 |
CN201710308109.5A CN107043891B (zh) | 2014-06-11 | 2014-06-11 | 一种谐振杆用冷镦丝的生产方法 |
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CN201410255425.7A Division CN105316575B (zh) | 2014-06-11 | 2014-06-11 | 谐振杆用冷镦丝及其生产方法 |
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Publication Number | Publication Date |
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CN107043891A CN107043891A (zh) | 2017-08-15 |
CN107043891B true CN107043891B (zh) | 2018-09-21 |
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CN201410255425.7A Active CN105316575B (zh) | 2014-06-11 | 2014-06-11 | 谐振杆用冷镦丝及其生产方法 |
CN201710307825.1A Pending CN107022720A (zh) | 2014-06-11 | 2014-06-11 | 材料利用率较高的谐振杆用冷镦丝的生产方法 |
CN201710308109.5A Active CN107043891B (zh) | 2014-06-11 | 2014-06-11 | 一种谐振杆用冷镦丝的生产方法 |
CN201710308108.0A Pending CN107130182A (zh) | 2014-06-11 | 2014-06-11 | 一种材料利用率较高的谐振杆用冷镦丝 |
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CN201410255425.7A Active CN105316575B (zh) | 2014-06-11 | 2014-06-11 | 谐振杆用冷镦丝及其生产方法 |
CN201710307825.1A Pending CN107022720A (zh) | 2014-06-11 | 2014-06-11 | 材料利用率较高的谐振杆用冷镦丝的生产方法 |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN109023142A (zh) * | 2018-08-21 | 2018-12-18 | 丹阳市凯鑫合金材料有限公司 | 一种真空集热管用玻封合金及其生产方法 |
CN111383861B (zh) * | 2018-12-28 | 2022-06-17 | 东莞科力线材技术有限公司 | 一种电磁继电器用的导磁材料及其制备方法 |
CN112458374A (zh) * | 2020-10-26 | 2021-03-09 | 江苏新核合金科技有限公司 | 一种杜镁丝材料及其制备方法 |
CN113102671A (zh) * | 2021-04-06 | 2021-07-13 | 无锡透平叶片有限公司 | 一种锥桶形回转体超硬铝合金锻件的模锻方法 |
CN115652182B (zh) * | 2022-11-04 | 2024-02-02 | 江苏隆达超合金航材有限公司 | 一种控制Invar36合金中气体及夹杂物的方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS55152153A (en) * | 1979-05-15 | 1980-11-27 | Nisshin Steel Co Ltd | Invar alloy having good welding property |
CN101310917A (zh) * | 2007-05-24 | 2008-11-26 | 宝山钢铁股份有限公司 | 一种Fe-Ni低膨胀合金线材的生产方法 |
CN102230120A (zh) * | 2011-06-20 | 2011-11-02 | 丹阳市龙鑫合金有限公司 | 航空高压舱用高性能弹性合金材料及其生产方法 |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN100447275C (zh) * | 2005-09-23 | 2008-12-31 | 宝山钢铁股份有限公司 | 一种高强度因瓦合金及其合金线材的生产方法 |
CN101741333A (zh) * | 2008-11-04 | 2010-06-16 | 日照旭日电子有限公司 | 一种谐振器基座的生产工艺 |
CN102978361B (zh) * | 2012-11-29 | 2014-01-29 | 深圳市欣天科技有限公司 | 一种Invar合金的热处理工艺 |
-
2014
- 2014-06-11 CN CN201410255425.7A patent/CN105316575B/zh active Active
- 2014-06-11 CN CN201710307825.1A patent/CN107022720A/zh active Pending
- 2014-06-11 CN CN201710308109.5A patent/CN107043891B/zh active Active
- 2014-06-11 CN CN201710308108.0A patent/CN107130182A/zh active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS55152153A (en) * | 1979-05-15 | 1980-11-27 | Nisshin Steel Co Ltd | Invar alloy having good welding property |
CN101310917A (zh) * | 2007-05-24 | 2008-11-26 | 宝山钢铁股份有限公司 | 一种Fe-Ni低膨胀合金线材的生产方法 |
CN102230120A (zh) * | 2011-06-20 | 2011-11-02 | 丹阳市龙鑫合金有限公司 | 航空高压舱用高性能弹性合金材料及其生产方法 |
Non-Patent Citations (1)
Title |
---|
4J36低膨胀合金及其工艺性;佟晓静;《机械》;20021231;第205-207页 * |
Also Published As
Publication number | Publication date |
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CN107043891A (zh) | 2017-08-15 |
CN105316575A (zh) | 2016-02-10 |
CN107130182A (zh) | 2017-09-05 |
CN105316575B (zh) | 2017-05-10 |
CN107022720A (zh) | 2017-08-08 |
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