CN106983680A - A kind of frosted mildy wash - Google Patents
A kind of frosted mildy wash Download PDFInfo
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- CN106983680A CN106983680A CN201710026487.4A CN201710026487A CN106983680A CN 106983680 A CN106983680 A CN 106983680A CN 201710026487 A CN201710026487 A CN 201710026487A CN 106983680 A CN106983680 A CN 106983680A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/232—Angelica
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/483—Gleditsia (locust)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
- A61K36/704—Polygonum, e.g. knotweed
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/756—Phellodendron, e.g. corktree
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8962—Allium, e.g. garden onion, leek, garlic or chives
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/906—Zingiberaceae (Ginger family)
- A61K36/9066—Curcuma, e.g. common turmeric, East Indian arrowroot or mango ginger
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
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- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses a kind of frosted mildy wash, the frosted mildy wash includes the Traditional Chinese medicine collagen protein particle as abrasive material, also comprising fruit ferment concentrate, surfactant, thickener, mint juice, tea tree ethereal oil, deionized water.Frosted mildy wash prepared by the present invention is using Traditional Chinese medicine collagen protein particle as abrasive material, serve the cuticula for effectively removing dirt and skin aging, with the slow release of Chinese medicine, the control to disease of skin such as acnes and therapeutic action are also achieved, its discharge is also pollution-free to environment.In addition, with the addition of fruit ferment in frosted mildy wash, the free radical and oxide eliminated in facial skin is realized, vigor is brought to Skin Cell, accelerated its metabolism, decompose dirt and dead cell.
Description
Technical field
The invention belongs to daily necessities field, more particularly, to a kind of frosted mildy wash.
Background technology
Frosted mildy wash is a kind of facial skin cleaning products extensively used.Ground by adding little particle in mildy wash
Material effectively removes the cuticula of dirt and skin aging to increase the rubbing action of skin surface.The mill of common mildy wash
Material has two kinds, and one kind is natural abrasive, such as levigate fruit stone, natural mineral matter；Another is compound abrasive, such as polyethylene,
The fine-powder such as polystyrene or polyester.Natural abrasive lacks elasticity, harder, and the scuffing of skin is easily caused during use.Close
Though being made moderate progress into abrasive material in hardness, certain geometry can also be moulded into, due to meeting in the manufacturing process of the abrasive material
Using to plasticizer or additive, the risk with the allergy for causing skin more causes environment after being finished because it is difficult to degraded
Pollution.In addition, for the user that face there are the disease of skin such as acne, suffer from that area skin is more fragile, the effect of abrasive material
Bacterium infection is easily caused, even if not breaking, the stimulation of friction can also excite the aggravation of inflammation.
The content of the invention
Use for traditional frosted mildy wash easily causes the allergy of skin, bacterium infection and aggravates asking for scytitis
Topic, the invention provides a kind of frosted mildy wash.The frosted mildy wash has used the mill compared with soft, Bc well
Material, more has functions that to alleviate or even treats without anaphylaxis to facial skin to facial skin disease.
The present invention is realized by following technology：
A kind of frosted mildy wash, comprising the Traditional Chinese medicine collagen protein particle as abrasive material, also lives comprising fruit ferment concentrate, surface
Property agent, thickener, mint juice, tea tree ethereal oil, deionized water；The Traditional Chinese medicine collagen protein particle is prepared by the following procedure step and obtained
Arrive：
1) by weight 1：1~2 mixing collagen and chitosan and using the mixture as solute, mass concentration is 0.1~
0.4% glacial acetic acid aqueous solution is solvent, with the collagen solution that obtained mass concentration is 6~10%；
2) by weight 1：30~50 add Chinese medical extract in collagen solution, and it is 65~75 to stir after temperature
DEG C, vacuum obtains the Traditional Chinese medicine collagen protein that water content is 40~50% and concentrated to be concentrated in vacuo under the conditions of 5~20KPa
Liquid；
3) in wet spinning equipment, by step 2) obtained by Traditional Chinese medicine collagen protein concentrate by aperture be 0.5~2 millimeter of spray
Silk mouth is extruded and enters solidified forming in the metabisulfite solution of mass concentration 0.5~2%, collects and through mass concentration 30~60%
Ethanol water cleaning after, obtain Traditional Chinese medicine collagen protein fiber；
4) the Traditional Chinese medicine collagen protein fiber after drying is crushed to 10~30 mesh, produces Traditional Chinese medicine collagen protein particle.
It has been recognised by the inventors that the use of mildy wash will not only play a part of face cleaning, skin is more carried out during face cleaning
The nursing of skin.The cleaning that traditional abrasive material is mainly to skin dirt provides help, and for skin-nourishing supplement, skin symptom
Disappearance have no substantial help.In the present invention, inventor improves that traditional natural abrasive hardness is higher, easily cause first
The shortcoming of skin tears, has been used using the Traditional Chinese medicine collagen protein particle prepared by collagen and chitosan as abrasive material, the Chinese medicine
Collagen pellet hardness is much lower with respect to natural abrasive.In addition, collagen there is good biocompatibility, can be biological
Degradability and bioactivity.Chinese medical extract is mixed into Traditional Chinese medicine collagen protein particle, Chinese medical extract used has antibacterial, disappeared
Inflammation etc. is acted on, and has good the alleviation even effect for the treatment of to disease of skin.Traditional Chinese medicine collagen protein obtained by the present invention
The characteristics of grain has sustained release, during being cleaned to facial skin, realizes the slow release of Chinese medicine, is absorbed by skin,
Realize the treatment to disease of skin such as acnes.
Therefore, the present invention serves using Traditional Chinese medicine collagen protein particle as abrasive material and effectively removes dirt and skin aging
Cuticula, with the slow release of Chinese medicine, also achieves the control to disease of skin such as acnes and therapeutic action, and it is discharged to ring
Border is also pollution-free.
Preferably, the frosted mildy wash includes the raw material of following weight proportion：3~5 parts of Traditional Chinese medicine collagen protein particle, water
5~8 parts of fruit ferment concentrate, 5~8 parts of surfactant, 3~5 parts of thickener, 1~3 part of mint juice, 1~2 part of tea tree ethereal oil,
20~30 parts of deionized water.
Preferably, the fruit ferment concentrate includes the raw material of following weight proportion：35~45 parts of green plum, apple 5~
10 parts, 6~10 parts of pears, 6~15 parts of shaddock, 3~15 parts of mulberry fruit, 5~15 parts of Kiwi berry, 3~5 parts of strawberry, 3~10 parts of pawpaw,
3~6 parts of carambola, 5~10 parts of grape, 5~15 parts of brown sugar.
In the raw material selection of fruit ferment, inventor, which uses, is rich in amino acid, vitamin, mineral matter, other flavonoids
Apple, pears, shaddock, mulberry fruit, Kiwi berry, strawberry, pawpaw, carambola, the grape of compound, the ferment obtained by these fruit raw materials
With stronger oxidation resistance, increase elasticity of skin, moisten moisturizing and realize the quick skin whitening effect of skin.In fruit raw material
In, inventor is special, it is more must use green plum, green plum is in alkalescent, with sterilization, regulation pH value of body, improves stomach and intestine
Road function, dispelling fatigue, release stress, improve calcareous absorption, regulation blood pressure, antiallergy, reinforcing liver detoxification function,
16 health-nutritions values such as beauty, improvement blood circulation, immune raising, pre- anti-cancer, prevention calculus, analgesia, anti-oxidant.
Green plum is used for the preparation of fruit ferment, regulation ferment acid-base property can be played, during the use of mildy wash, can also be risen
To the effect of regulation acid-base scale of skin, the cleaning and nursing good to skin is realized.
In the present invention, prepared fruit ferment realizes the free radical and oxide eliminated in facial skin, is ferment
Element realizes that Skin Cell brings vigor, accelerates its metabolism, decomposes dirt and dead cell offer precondition.Inventor passes through
Detection finds that addition of the fruit ferment in frosted mildy wash of the present invention plays vital work for mildy wash using effect
With.
Preferably, the preparation process of the fruit ferment concentrate is as follows：By green plum, apple, pears, shaddock, mulberry fruit, macaque
Peach, strawberry, pawpaw, carambola, grape are cleaned, chopping, be put into sterile fermentation tank after ozone sterilization, are added brown sugar, are stirred,
Seal and in being fermented 8~10 months under room temperature condition, fermentation is finished, and 200~300 filter now, and gained filtrate is carried out into vacuum
Freeze concentration, is concentrated into water content for 65~75wt%, as fruit ferment concentrate.
Preferably, ozone sterilization condition is as follows：Ozone concentration is 30~60mg/m3, temperature is 30~50 DEG C, and the time is 60
~120 minutes；The temperature of vacuum refrigeration concentration is -65~-45 DEG C, and vacuum is 5~20KPa.
Preferably, the Chinese medical extract includes the raw material of following weight proportion：5~15 parts of gleditsia sinensis, 5~15 parts of Radix Angelicae Sinensis,
3~6 parts of turmeric, 1~3 part of garlic, 5~10 parts of giant knotweed, 3~6 parts of golden cypress, 2~5 parts of radix scutellariae.
In the present invention, inventor's multiselect, which is used, has good antibacterial, the Chinese medicine material of anti-inflammatory.
Gleditsia sinensis have detumescence eliminating toxic, apocenosis, desinsection the effects such as, it is adaptable to ulcer from the beginning of or purulenceization not burst etc. disease of skin；
Radix Angelicae Sinensis have the effect of promoting circulation of blood, enrich blood, relieve pain, moisturizing, also have expansion skin capillary, stimulate circulation, antivitamin E
Lack effect；Turmeric have anti-oxidant, antitumor, reducing blood lipid, hypoglycemic, antiulcer, protection liver, resist myocardial ischemia, anti-suppression
Strongly fragrant, antibacterial, anti-inflammatory, antiviral and antimycotic etc. effect；Garlic has removing toxic substances desinsection, swelling and pain relieving effect；Giant knotweed has anti-inflammation,
It is anti-oxidant, it is antiviral, it is antitumor, improve microcirculation, antalgic and sedative, the effect such as Hemorrhagic shock and treatment malignant sore tinea；Golden cypress contains
The main components such as berberine, obakunone, there is antibacterial, convergence, anti-inflammatory, to symptoms, effect such as various skin wet poisons, sores
Well；The clinical antibiotic property of radix scutellariae is better than the coptis, and does not develop immunity to drugs, and has the effects such as heat-clearing and damp-drying drug, purging intense heat and detonicating.
Preferably, the preparation process of the Chinese medical extract is as follows：
A) weigh and mix gleditsia sinensis, Radix Angelicae Sinensis, turmeric, garlic, giant knotweed, golden cypress, radix scutellariae, be crushed to 200 after cleaned, drying~
300 mesh, are made Chinese medicine mixed-powder；
B) gained Chinese medicine mixed-powder is compared 1 by solid-liquid weight：20~30 are immersed in the water, after soaking 2~3 hours, carry out boiling and boil 2
~4 hours, boiling, which is boiled, to be finished, and 200~300 filter now, and Chinese medicine liquid is made；
C) obtained Chinese medicine liquid is concentrated in vacuo, is concentrated into water content for 55~65wt%, as the concentrated liquid of tradition Chinese medicine, will
The concentrated liquid of tradition Chinese medicine of gained carries out vacuum freeze drying, produces Chinese medical extract.
Preferably, the temperature that step c) is concentrated in vacuo is 65~75 DEG C, and vacuum is 5~20KPa；Vacuum freeze drying
Temperature is -65~-45 DEG C, and vacuum is 5~20KPa, and the time is 120~144 hours.
Preferably, the surfactant is dodecyl sulphate triethanol ammonium, cocoyl ethylene hydroxy sulfuric acid sodium or the moon
Osmanthus acylsarcosine sodium；The thickener is sodium carboxymethylcellulose, carragheen or xanthans.
Preferably, the frosted mildy wash preparation process is as follows：Mixed surfactant, thickener, mint juice, tea tree essence
After oil, deionized water, fruit ferment concentrate, Traditional Chinese medicine collagen protein particle are added, stirs, produces frosted mildy wash.
A kind of frosted mildy wash disclosed by the invention, its advantage is：
1) using Traditional Chinese medicine collagen protein particle as abrasive material, the cuticula for effectively removing dirt and skin aging is served, in
The slow release of medicine, also achieves the control to disease of skin such as acnes and therapeutic action, and its discharge is also pollution-free to environment；
2) fruit ferment is with the addition of in frosted mildy wash, the free radical and oxide eliminated in facial skin is realized, to skin
Skin cell brings vigor, accelerates its metabolism, decomposes dirt and dead cell；
3) scientific formulation, rationally, while being cleaned to face, is realized to effective nursing of skin with treating, with good
Good using effect.
Embodiment
Embodiment 1
Gleditsia sinensis 5Kg, Radix Angelicae Sinensis 5Kg, turmeric 3Kg, garlic 1Kg, giant knotweed 5Kg, golden cypress 3Kg, radix scutellariae 2Kg are weighed, cleaned, baking is mixed
200 mesh are crushed to after dry, Chinese medicine mixed-powder is made；Gained Chinese medicine mixed-powder is compared 1 by solid-liquid weight：20 are immersed in the water,
After immersion 2 hours, carry out boiling and boil 2 hours, boiling, which is boiled, to be finished, and 200 filter now, and Chinese medicine liquid is made；Obtained Chinese medicine liquid is entered
Row is concentrated in vacuo, and the temperature of vacuum concentration is 65 DEG C, and vacuum is 5KPa, is concentrated into water content for 55wt%, as Chinese medicine is dense
Contracting liquid, carries out vacuum freeze drying, the temperature of vacuum freeze drying is -65 DEG C, and vacuum is by the concentrated liquid of tradition Chinese medicine of gained
5KPa, the time is 120 hours, and vacuum freeze drying is finished, and produces Chinese medical extract.
Collagen 1Kg, chitosan 1Kg are weighed, is well mixed and using the mixture as solute, mass concentration is 0.1%
Glacial acetic acid aqueous solution is solvent, with the collagen solution that obtained mass concentration is 6%；By weight 1：30 by Chinese medical extract
Add in collagen solution, be concentrated in vacuo after stirring, the temperature of vacuum concentration is 65 DEG C, and vacuum is 5KPa,
Obtain the Traditional Chinese medicine collagen protein concentrate that water content is 40%；It is in wet spinning equipment, the Traditional Chinese medicine collagen protein of gained is dense
Contracting liquid is extruded for 0.5 millimeter of spinning nozzle by aperture and enters solidified forming in the metabisulfite solution of mass concentration 0.5%, collects
And after the ethanol water cleaning through mass concentration 30%, obtain Traditional Chinese medicine collagen protein fiber；Chinese medicine collagen egg after drying
White fiber is crushed to 10 mesh, produces Traditional Chinese medicine collagen protein particle.
By green plum 35Kg, apple 5Kg, pears 6Kg, shaddock 6Kg, mulberry fruit 3Kg, Kiwi berry 5Kg, strawberry 3Kg, pawpaw 3Kg, poplar
Peach 3Kg, grape 5Kg are cleaned, shredded, (ozone concentration is 30mg/m to ozone sterilization3, temperature is 30 DEG C, and the time is 120 minutes) after
It is put into sterile fermentation tank, adds brown sugar 5Kg, stir, seals and in being fermented 8 months under room temperature condition, fermentation is finished,
200 filter now, gained filtrate are carried out into vacuum refrigeration concentration, the temperature of vacuum refrigeration concentration is -65 DEG C, and vacuum is
5KPa, is concentrated into water content for 65wt%, as fruit ferment concentrate.
Weigh dodecyl sulphate triethanol ammonium 5Kg, sodium carboxymethylcellulose 3Kg, mint juice 1Kg, tea tree ethereal oil 1Kg,
Deionized water 20Kg, after mixing, adds fruit ferment concentrate 5Kg, Traditional Chinese medicine collagen protein particle 3Kg, stirs, produce mill
Sand mildy wash.
Embodiment 2
Gleditsia sinensis 15Kg, Radix Angelicae Sinensis 15Kg, turmeric 6Kg, garlic 3Kg, giant knotweed 10Kg, golden cypress 6Kg, radix scutellariae 5Kg are weighed, mixing is through clear
Wash, dry after be crushed to 300 mesh, Chinese medicine mixed-powder is made；Gained Chinese medicine mixed-powder is compared 1 by solid-liquid weight：30 immersions
In water, after soaking 3 hours, carry out boiling and boil 4 hours, boiling, which is boiled, to be finished, and 300 filter now, and Chinese medicine liquid is made；By obtained Chinese medicine
Liquid is concentrated in vacuo, and the temperature of vacuum concentration is 75 DEG C, and vacuum is 20KPa, water content is concentrated into for 65wt%, in being
Medicine concentrate, carries out vacuum freeze drying, the temperature of vacuum freeze drying is -45 DEG C, vacuum by the concentrated liquid of tradition Chinese medicine of gained
For 20KPa, the time is 144 hours, and vacuum freeze drying is finished, and produces Chinese medical extract.
Collagen 1Kg, chitosan 2Kg are weighed, is well mixed and using the mixture as solute, mass concentration is 0.4%
Glacial acetic acid aqueous solution is solvent, with the collagen solution that obtained mass concentration is 10%；By weight 1：50 by traditional Chinese medicine extraction
Thing is added in collagen solution, is concentrated in vacuo after stirring, and the temperature of vacuum concentration is 75 DEG C, and vacuum is
20KPa, obtains the Traditional Chinese medicine collagen protein concentrate that water content is 50%；In wet spinning equipment, by the Chinese medicine collagen of gained
Protein concentrated solution is extruded for 2 millimeters of spinning nozzle by aperture and enters solidified forming in the metabisulfite solution of mass concentration 2%, receives
Collect and after the ethanol water cleaning through mass concentration 60%, obtain Traditional Chinese medicine collagen protein fiber；Chinese medicine collagen after drying
Azelon is crushed to 30 mesh, produces Traditional Chinese medicine collagen protein particle.
By green plum 45Kg, apple 10Kg, pears 10Kg, shaddock 15Kg, mulberry fruit 15Kg, Kiwi berry 15Kg, strawberry 5Kg, pawpaw
10Kg, carambola 6Kg, grape 10Kg are cleaned, shredded, (ozone concentration is 60mg/m to ozone sterilization3, temperature is 50 DEG C, and the time is 60
Minute) after be put into sterile fermentation tank, add brown sugar 15Kg, stir, seal and under room temperature condition ferment 10 months, hair
Ferment is finished, and 300 filter now, gained filtrate is carried out into vacuum refrigeration concentration, the temperature of vacuum refrigeration concentration is -45 DEG C, vacuum
Spend for 20KPa, be concentrated into water content for 75wt%, as fruit ferment concentrate.
Weigh cocoyl ethylene hydroxy sulfuric acid sodium 8Kg, carragheen 5Kg, mint juice 3Kg, tea tree ethereal oil 2Kg, deionized water
30Kg, after mixing, adds fruit ferment concentrate 8Kg, Traditional Chinese medicine collagen protein particle 5Kg, stirs, produce frosted face cleaning
Breast.
Embodiment 3
Gleditsia sinensis 8Kg, Radix Angelicae Sinensis 7Kg, turmeric 4Kg, garlic 2Kg, giant knotweed 8Kg, golden cypress 4Kg, radix scutellariae 4Kg are weighed, cleaned, baking is mixed
250 mesh are crushed to after dry, Chinese medicine mixed-powder is made；Gained Chinese medicine mixed-powder is compared 1 by solid-liquid weight：25 are immersed in the water,
After immersion 2.5 hours, carry out boiling and boil 3 hours, boiling, which is boiled, to be finished, and 250 filter now, and Chinese medicine liquid is made；By obtained Chinese medicine liquid
It is concentrated in vacuo, the temperature of vacuum concentration is 70 DEG C, and vacuum is 10KPa, is concentrated into water content for 60wt%, as Chinese medicine
Concentrate, carries out vacuum freeze drying, the temperature of vacuum freeze drying is -50 DEG C, and vacuum is by the concentrated liquid of tradition Chinese medicine of gained
10KPa, the time is 132 hours, and vacuum freeze drying is finished, and produces Chinese medical extract.
Collagen 1Kg, chitosan 1.5Kg are weighed, is well mixed and using the mixture as solute, mass concentration is
0.2% glacial acetic acid aqueous solution is solvent, with the collagen solution that obtained mass concentration is 8%；By weight 1：40 by Chinese medicine
Extract is added in collagen solution, is concentrated in vacuo after stirring, and the temperature of vacuum concentration is 70 DEG C, and vacuum is
10KPa, obtains the Traditional Chinese medicine collagen protein concentrate that water content is 45%；In wet spinning equipment, by the Chinese medicine collagen of gained
Protein concentrated solution is extruded for 1 millimeter of spinning nozzle by aperture and enters solidified forming in the metabisulfite solution of mass concentration 1%, receives
Collect and after the ethanol water cleaning through mass concentration 50%, obtain Traditional Chinese medicine collagen protein fiber；Chinese medicine collagen after drying
Azelon is crushed to 20 mesh, produces Traditional Chinese medicine collagen protein particle.
By green plum 40Kg, apple 8Kg, pears 8Kg, shaddock 10Kg, mulberry fruit 6Kg, Kiwi berry 10Kg, strawberry 4Kg, pawpaw 6Kg,
Carambola 4Kg, grape 7Kg are cleaned, shredded, (ozone concentration is 50mg/m to ozone sterilization3, temperature is 40 DEG C, and the time is 90 minutes)
After be put into sterile fermentation tank, add brown sugar 10Kg, stir, seal and under room temperature condition ferment 9 months, fermented
Finish, 250 filter now, gained filtrate is subjected to vacuum refrigeration concentration, the temperature of vacuum refrigeration concentration is -55 DEG C, and vacuum is
10KPa, is concentrated into water content for 70wt%, as fruit ferment concentrate.
Sodium lauroyl sarcosine 6Kg, xanthans 4Kg, mint juice 2Kg, tea tree ethereal oil 1.5Kg, deionized water 25Kg are weighed,
After mixing, fruit ferment concentrate 6Kg, Traditional Chinese medicine collagen protein particle 4Kg are added, stirs, produces frosted mildy wash.
Claims (10)
1. a kind of frosted mildy wash, it is characterized in that, it is also dense comprising fruit ferment comprising the Traditional Chinese medicine collagen protein particle as abrasive material
Contracting liquid, surfactant, thickener, mint juice, tea tree ethereal oil, deionized water；The Traditional Chinese medicine collagen protein particle passes through as follows
Preparation process is obtained：
1) by weight 1：1~2 mixing collagen and chitosan and using the mixture as solute, mass concentration is 0.1~
0.4% glacial acetic acid aqueous solution is solvent, with the collagen solution that obtained mass concentration is 6~10%；
2) by weight 1：30~50 add Chinese medical extract in collagen solution, and it is 65~75 to stir after temperature
DEG C, vacuum obtains the Traditional Chinese medicine collagen protein that water content is 40~50% and concentrated to be concentrated in vacuo under the conditions of 5~20KPa
Liquid；
3) in wet spinning equipment, by step 2) obtained by Traditional Chinese medicine collagen protein concentrate by aperture be 0.5~2 millimeter of spray
Silk mouth is extruded and enters solidified forming in the metabisulfite solution of mass concentration 0.5~2%, collects and through mass concentration 30~60%
Ethanol water cleaning after, obtain Traditional Chinese medicine collagen protein fiber；
4) the Traditional Chinese medicine collagen protein fiber after drying is crushed to 10~30 mesh, produces Traditional Chinese medicine collagen protein particle.
2. a kind of frosted mildy wash according to claim 1, it is characterized in that, the frosted mildy wash is matched somebody with somebody comprising following weight
The raw material of ratio：3~5 parts of Traditional Chinese medicine collagen protein particle, 5~8 parts of fruit ferment concentrate, 5~8 parts of surfactant, thickener 3
~5 parts, 1~3 part of mint juice, 1~2 part of tea tree ethereal oil, 20~30 parts of deionized water.
3. a kind of frosted mildy wash according to claim 1 or 2, it is characterized in that, the fruit ferment concentrate is comprising such as
The raw material of lower weight proportion：35~45 parts of green plum, 5~10 parts of apple, 6~10 parts of pears, 6~15 parts of shaddock, 3~15 parts of mulberry fruit,
5~15 parts of Kiwi berry, 3~5 parts of strawberry, 3~10 parts of pawpaw, 3~6 parts of carambola, 5~10 parts of grape, 5~15 parts of brown sugar.
4. a kind of frosted mildy wash according to claim 3, it is characterized in that, the preparation process of the fruit ferment concentrate
It is as follows：After green plum, apple, pears, shaddock, mulberry fruit, Kiwi berry, strawberry, pawpaw, carambola, clean grape, chopping, ozone sterilization
It is put into sterile fermentation tank, adds brown sugar, stir, seals and in being fermented 8~10 months under room temperature condition, fermentation is finished,
200~300 are filtered now, and gained filtrate is carried out into vacuum refrigeration concentration, are concentrated into water content for 65~75wt%, as fruit
Ferment concentrate.
5. a kind of frosted mildy wash according to claim 4, it is characterized in that, ozone sterilization condition is as follows：Ozone concentration is
30~60mg/m3, temperature is 30~50 DEG C, and the time is 60~120 minutes；The temperature of vacuum refrigeration concentration is -65~-45 DEG C,
Vacuum is 5~20KPa.
6. a kind of frosted mildy wash according to claim 1, it is characterized in that, the Chinese medical extract is matched somebody with somebody comprising following weight
The raw material of ratio：5~15 parts of gleditsia sinensis, 5~15 parts of Radix Angelicae Sinensis, 3~6 parts of turmeric, 1~3 part of garlic, 5~10 parts of giant knotweed, golden cypress 3~6
Part, 2~5 parts of radix scutellariae.
7. a kind of frosted mildy wash according to claim 6, it is characterized in that, the preparation process of the Chinese medical extract is such as
Under：
A) weigh and mix gleditsia sinensis, Radix Angelicae Sinensis, turmeric, garlic, giant knotweed, golden cypress, radix scutellariae, be crushed to 200 after cleaned, drying~
300 mesh, are made Chinese medicine mixed-powder；
B) gained Chinese medicine mixed-powder is compared 1 by solid-liquid weight：20~30 are immersed in the water, after soaking 2~3 hours, carry out boiling and boil 2
~4 hours, boiling, which is boiled, to be finished, and 200~300 filter now, and Chinese medicine liquid is made；
C) obtained Chinese medicine liquid is concentrated in vacuo, is concentrated into water content for 55~65wt%, as the concentrated liquid of tradition Chinese medicine, will
The concentrated liquid of tradition Chinese medicine of gained carries out vacuum freeze drying, produces Chinese medical extract.
8. a kind of frosted mildy wash according to claim 7, it is characterized in that, the temperature that step c) is concentrated in vacuo is 65~75
DEG C, vacuum is 5~20KPa；The temperature of vacuum freeze drying is -65~-45 DEG C, and vacuum is 5~20KPa, and the time is 120
~144 hours.
9. a kind of frosted mildy wash according to claim 1, it is characterized in that, the surfactant is dodecyl sulphate
Triethanol ammonium, cocoyl ethylene hydroxy sulfuric acid sodium or sodium lauroyl sarcosine；The thickener is sodium carboxymethylcellulose, OK a karaoke club
Glue or xanthans.
10. a kind of frosted mildy wash according to claim 1, it is characterized in that, the frosted mildy wash preparation process is as follows：
After mixed surfactant, thickener, mint juice, tea tree ethereal oil, deionized water, fruit ferment concentrate, Chinese medicine collagen are added
Protein body, stirs, and produces frosted mildy wash.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109432376A (en) * | 2018-12-24 | 2019-03-08 | 东莞御叶香媛生物科技有限公司 | A kind of tabernaemontanus bulrush perfume fruit environmental protection ferment, preparation method and applications |
| CN111494279A (en) * | 2020-05-07 | 2020-08-07 | 广东柏俐臣生物科技有限公司 | Cleaning cosmetic and preparation method thereof |
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| KR0163834B1 (en) * | 1995-12-01 | 1998-12-01 | 이능희 | Cosmetic compositions of scrub agents containing spheric collagen particle |
| CN1584150A (en) * | 2004-05-28 | 2005-02-23 | 四川大学 | Preparing method for collagen stroma composite medical fibre spinning stoste |
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| CN109432376A (en) * | 2018-12-24 | 2019-03-08 | 东莞御叶香媛生物科技有限公司 | A kind of tabernaemontanus bulrush perfume fruit environmental protection ferment, preparation method and applications |
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