CN106958043A - Fresh cocoon reeling method - Google Patents

Fresh cocoon reeling method Download PDF

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Publication number
CN106958043A
CN106958043A CN201710294282.4A CN201710294282A CN106958043A CN 106958043 A CN106958043 A CN 106958043A CN 201710294282 A CN201710294282 A CN 201710294282A CN 106958043 A CN106958043 A CN 106958043A
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CN
China
Prior art keywords
cocoon
silk
filature
fresh
fresh cocoon
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Pending
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CN201710294282.4A
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Chinese (zh)
Inventor
蒋芳
李利军
林海涛
岳新霞
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Guangxi University of Science and Technology
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Guangxi University of Science and Technology
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Application filed by Guangxi University of Science and Technology filed Critical Guangxi University of Science and Technology
Priority to CN201710294282.4A priority Critical patent/CN106958043A/en
Publication of CN106958043A publication Critical patent/CN106958043A/en
Pending legal-status Critical Current

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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01BMECHANICAL TREATMENT OF NATURAL FIBROUS OR FILAMENTARY MATERIAL TO OBTAIN FIBRES OF FILAMENTS, e.g. FOR SPINNING
    • D01B7/00Obtaining silk fibres or filaments
    • D01B7/04Reeling silk

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Textile Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)

Abstract

The invention discloses a kind of fresh cocoon reeling method, comprise the following steps:(1) Microwave Pretreatment is carried out to fresh cocoon;(2) cocoon after processing is subjected to vacuum infiltration water suction, chemical assistant is added in infiltration water, the chemical assistant is the one or two in sodium carbonate or sodium metasilicate, then carries out filature.The silk reeling method of the present invention, microwave treatment is carried out to fresh cocoon, and microwave treatment can be moderately denatured with fresh silk glue, make silk gum " not loose not tight ", swelling capacity is moderate, is conducive to filature.Fresh cocoon microwave treatment silk reeling technology, it is possible to achieve low energy consumption, efficient filature, and raw silk quality is improved, and avoid the high energy consumption of traditional cocoon drying.Chemical assistant is added in vacuum infiltration water, further to improve the swelling capacity of silk gum, is easy to filature.Silk reeling method of the present invention compared with the fresh cocoon reeling without Microwave Pretreatment, filature reelability percentage improve the folding reduction of more than 3%, reel silk from cocoons 48 kilogram/quintal silks, myriametre hang it is rough reduce 13 times, it is clean improve 0.3 1 points, grade improve 0.5 1.0.

Description

Fresh cocoon reeling method
Technical field
The present invention relates to silk cocoon manufacture field, more particularly to a kind of fresh cocoon reeling method.
Background technology
The technique for extracting silk cocoon out silk generally claims filature.Original silk reeling method, is that silk cocoon is immersed in hot bathtub cubicle, uses hand Reel off raw silk from cocoons, be wound on silk basket.
At present, the problem of fresh cocoon reeling and dried cocoon filature have many:(1) because the silk gum swelling capacity of fresh cocoon is excessive, lead Sericin degumming loss percentage height, silk during fresh cocoon reeling is caused easily to cut off, fall the increase of thread number of times, reelability percentage reduction, reel silk from cocoons folding increase.(2) do Cocoon filature is related to cocoon drying, technical requirements height, and cocoon drying causes silk gum to be denatured completely;Before filature, but must cocoon cooking make silk gum swollen Profit, the energy consumption of whole process is big, and cocoon drying, the quality of cocoon cooking and degree can all influence filature quality.
The information for being disclosed in the background section is merely intended to understanding of the increase to the general background of the present invention, without answering When the prior art for being considered as recognizing or implying the information structure in any form well known to persons skilled in the art.
The content of the invention
It is an object of the invention to provide a kind of fresh cocoon reeling method, so as to overcome, existing silk reeling method reelability percentage is low, reel silk from cocoons Folding is big, energy consumption is big and the shortcoming of the numerous and diverse bad control filature quality of process.
To achieve the above object, the invention provides a kind of fresh cocoon reeling method, comprise the following steps:
(1) Microwave Pretreatment is carried out to fresh cocoon;
(2) cocoon after the step (1) processing is subjected to vacuum infiltration water suction, adds chemical assistant in infiltration water, institute It is the one or two in sodium carbonate or sodium metasilicate to state chemical assistant, then carries out filature.
Preferably, in above-mentioned technical proposal, in the step (1) during Microwave Pretreatment, the power of microwave treatment is 125- 500w;The time of microwave treatment is 1-6min.
Preferably, in above-mentioned technical proposal, in the step (1) during Microwave Pretreatment, the power of microwave treatment is 200w; The time of microwave treatment is 1.5min.
Preferably, in above-mentioned technical proposal, the water temperature of vacuum infiltration is 20-50 DEG C in the step (2).
Preferably, in above-mentioned technical proposal, the water temperature of vacuum infiltration is 35 DEG C in the step (2).
Preferably, in above-mentioned technical proposal, the concentration of addition chemical assistant is 1-6g/L in step (2) the infiltration water.
Preferably, in above-mentioned technical proposal, the concentration of addition chemical assistant is 2g/L in step (2) the infiltration water.
Preferably, in above-mentioned technical proposal, addition chemical assistant is that two kinds of sodium carbonate and sodium metasilicate are mixed in the step (2) Close, mixed proportion is 1:1.
Preferably, in above-mentioned technical proposal, beating, beating water temperature is carried out for 85-90 before filature in the step (2) ℃。
Compared with prior art, the present invention has the advantages that:
(1) silk reeling method of the invention, microwave treatment is carried out to fresh cocoon, and microwave treatment can be moderately denatured with fresh silk glue, Make silk gum " not loose not tight ", swelling capacity is moderate, is conducive to filature.It is fresh with dried cocoon after traditional cocoon cooking process compared with filature Cocoon microwave treatment silk reeling technology, it is possible to achieve low energy consumption, efficient filature, and raw silk quality is improved, and avoid tradition The high energy consumption of cocoon drying.Chemical assistant is added in vacuum infiltration water, further to improve the swelling capacity of silk gum, is easy to filature.This Invention silk reeling method is compared with the fresh cocoon reeling without Microwave Pretreatment, and filature reelability percentage improves more than 3%, reel silk from cocoons folding reduction 4- 8 kilogram/quintal silks, myriametre, which are hung, rough to be reduced 1-3 time, clean improves 0.3-1 points, grade raising 0.5-1.0.
(2) silkworm chrysalis in fresh cocoon can be quickly killed using the stronger penetration power of microwave, the problem of solving pupal cell moth.Microwave Fresh cocoon can also be sterilized and be removed the part moisture of fresh cocoon while pupa killing, can so realize the long period at room temperature Storage, solve the freezer investment of fresh cocoon storage and huge energy consumption problem.
(3) after the processing for carrying out the short time to fresh cocoon using microwave, 10 days can be stored at normal temperatures or even the longer time, Silkworm chrysalis will not degenerate.After the fresh cocoon of microwave reasonable sanding is stored 10 days, absorb water, without cocoon cooking, directly use through vacuum infiltration In filature, its filature performance is substantially better than the direct filature of fresh cocoon.
Embodiment
With reference to specific embodiment, the embodiment to the present invention is described in detail, it is to be understood that this hair Bright protection domain is not limited by embodiment.
Embodiment 1
A kind of fresh cocoon reeling method, comprises the following steps:
(1) fresh cocoon is subjected to microwave treatment;Fresh cocoon 100 is taken, fresh cocoon is carried out microwave by weight in 148.78 ± 0.02g Processing, the processing power of microwave is 200W, and treatment time is 120s.
(2) cocoon after step (1) processing is subjected to vacuum infiltration water suction, infiltration water temperature is 35 DEG C, is carried out after vacuum infiltration Beating, beating water temperature is 90 DEG C, obtains raw silk after then carrying out filature, filature, raw silk is dried, weigh, and records number According to.
Embodiment 2
A kind of fresh cocoon reeling method, comprises the following steps:
(1) fresh cocoon is subjected to microwave treatment;Fresh cocoon 100 is taken, fresh cocoon is carried out microwave by weight in 148.78 ± 0.02g Processing, the processing power of microwave is 200W, and treatment time is 30s.
(2) cocoon after step (1) processing is subjected to vacuum infiltration water suction, infiltration water temperature is 35 DEG C, is carried out after vacuum infiltration Beating, beating water temperature is 90 DEG C, obtains raw silk after then carrying out filature, filature, raw silk is dried, weigh, and records number According to.
Embodiment 3
A kind of fresh cocoon reeling method, comprises the following steps:
(1) fresh cocoon is subjected to microwave treatment;Fresh cocoon 100 is taken, fresh cocoon is carried out microwave by weight in 148.78 ± 0.02g Processing, the processing power of microwave is 300W, and treatment time is 120s.
(2) cocoon after step (1) processing is subjected to vacuum infiltration water suction, infiltration water temperature is 35 DEG C, is carried out after vacuum infiltration Beating, beating water temperature is 90 DEG C, obtains raw silk after then directly carrying out filature, filature, raw silk is dried, weighed, and is remembered Record data.
Embodiment 4
A kind of fresh cocoon reeling method, comprises the following steps:
(1) fresh cocoon is subjected to microwave treatment;Fresh cocoon 100 is taken, fresh cocoon is carried out microwave by weight in 148.78 ± 0.02g Processing, the processing power of microwave is 200W, and treatment time is 90s.
(2) cocoon after step (1) processing is subjected to vacuum infiltration water suction, infiltration water temperature is 35 DEG C, it is past during vacuum infiltration to ooze Permeable middle sodium carbonate, permeates the content of sodium carbonate in water for 2g/L, and beating, beating water temperature is carried out after vacuum infiltration for 90 DEG C, Then raw silk is obtained after directly carrying out filature, filature, raw silk is dried, weighed, record data.
Embodiment 5
A kind of fresh cocoon reeling method, comprises the following steps:
(1) fresh cocoon is subjected to microwave treatment;Fresh cocoon 100 is taken, fresh cocoon is carried out microwave by weight in 148.78 ± 0.02g Processing, the processing power of microwave is 200W, and treatment time is 120s.
(2) cocoon after step (1) processing is subjected to vacuum infiltration water suction, infiltration water temperature is 35 DEG C, it is past during vacuum infiltration to ooze Permeable middle sodium carbonate, permeates the content of sodium carbonate in water for 2g/L, and beating, beating water temperature is carried out after vacuum infiltration for 90 DEG C, Then raw silk is obtained after directly carrying out filature, filature, raw silk is dried, weighed, record data.
Embodiment 6
A kind of fresh cocoon reeling method, comprises the following steps:
(1) fresh cocoon is subjected to microwave treatment;Fresh cocoon 100 is taken, fresh cocoon is carried out microwave by weight in 148.78 ± 0.02g Processing, the processing power of microwave is 500W, and treatment time is 60s.
(2) cocoon after step (1) processing is subjected to vacuum infiltration water suction, infiltration water temperature is 35 DEG C, it is past during vacuum infiltration to ooze Permeable middle sodium carbonate, permeates the content of sodium metasilicate in water for 6g/L, and beating, beating water temperature is carried out after vacuum infiltration for 90 DEG C, Then raw silk is obtained after directly carrying out filature, filature, raw silk is dried, weighed, record data.
Embodiment 7
A kind of fresh cocoon reeling method, comprises the following steps:
(1) fresh cocoon is subjected to microwave treatment;Fresh cocoon 100 is taken, fresh cocoon is carried out microwave by weight in 148.78 ± 0.02g Processing, the processing power of microwave is 125W, and treatment time is 360s.
(2) cocoon after step (1) processing is subjected to vacuum infiltration water suction, infiltration water temperature is 35 DEG C, it is past during vacuum infiltration to ooze Permeable middle sodium carbonate, permeates the content of sodium carbonate in water for 1g/L, and beating, beating water temperature is carried out after vacuum infiltration for 90 DEG C, Then raw silk is obtained after directly carrying out filature, filature, raw silk is dried, weighed, record data.
Comparative example 1
A kind of fresh cocoon reeling method, comprises the following steps:
(1) prepare fresh cocoon, take fresh cocoon 100, weight is in 148.78 ± 0.02g.
(2) the fresh cocoon that step (1) prepares is subjected to vacuum infiltration water suction, infiltration water temperature is 35 DEG C, is carried out after vacuum infiltration Beating, beating water temperature is 90 DEG C, obtains raw silk after then directly carrying out filature, filature, raw silk is dried, weighed, and is remembered Record data.
Embodiment and comparative example silk reeling method are contrasted, conciliate with the average silk length of silk, average length of non broken filament The rate of relaxing is contrasted.As shown in table 1.
Average length of non broken filament=average silk length/(1+ averagely falls thread number of times);
Reelability percentage=altogether tries cocoon number/(cocoon number is tried altogether+fall thread number of times).
The silk parameter comparison of table 1
As shown in table 1, fresh cocoon is carried out after microwave treatment, silk cocoon and the fresh cocoon reeling without Microwave Pretreatment after filature Compare, average length of non broken filament is longer, filature reelability percentage also increases, reduce reel silk from cocoons folding, reduce myriametre hangs rough, and raw silk cleaning is carried It is high.
Silk cocoon is added after chemical assistant, filature in vacuum infiltration and passes through Microwave Pretreatment, during vacuum infiltration without The silk cocoon filature of chemical assistant is compared, and the length of non broken filament that is averaged after silk cocoon filature is longer, filature reelability percentage also increases.
It is foregoing to the present invention specific illustrative embodiment description be in order to illustrate and illustration purpose.These descriptions It is not wishing to limit the invention to disclosed precise forms, and it will be apparent that according to above-mentioned teaching, can be much changed And change.The purpose of selecting and describing the exemplary embodiment is that explaining that the certain principles and its reality of the present invention should With so that those skilled in the art can realize and using the present invention a variety of exemplaries and A variety of selections and change.The scope of the present invention is intended to be limited by claims and its equivalents.

Claims (9)

1. a kind of fresh cocoon reeling method, it is characterised in that comprise the following steps:
(1) Microwave Pretreatment is carried out to fresh cocoon;
(2) cocoon after the step (1) processing is subjected to vacuum infiltration water suction, chemical assistant, describedization is added in infiltration water It is the one or two in sodium carbonate or sodium metasilicate to learn auxiliary agent, then carries out filature.
2. fresh cocoon reeling method according to claim 1, it is characterised in that micro- in the step (1) during Microwave Pretreatment The power of ripple processing is 125-500w;The time of microwave treatment is 1-6min.
3. fresh cocoon reeling method according to claim 2, it is characterised in that micro- in the step (1) during Microwave Pretreatment The power of ripple processing is 200w;The time of microwave treatment is 1.5min.
4. fresh cocoon reeling method according to claim 1, it is characterised in that the water temperature of vacuum infiltration in the step (2) For 20-50 DEG C.
5. fresh cocoon reeling method according to claim 4, it is characterised in that the water temperature of vacuum infiltration in the step (2) For 35 DEG C.
6. fresh cocoon reeling method according to claim 1, it is characterised in that add chemistry in step (2) the infiltration water The concentration of auxiliary agent is 1-6g/L.
7. fresh cocoon reeling method according to claim 1, it is characterised in that add chemistry in step (2) the infiltration water The concentration of auxiliary agent is 2g/L.
8. fresh cocoon reeling method according to claim 1, it is characterised in that addition chemical assistant is in the step (2) The two kinds of mixing of sodium carbonate and sodium metasilicate, mixed proportion is 1:1.
9. fresh cocoon reeling method according to claim 1, it is characterised in that carried out in the step (2) before filature it is beating, Beating water temperature is 85-90 DEG C.
CN201710294282.4A 2017-04-28 2017-04-28 Fresh cocoon reeling method Pending CN106958043A (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108265336A (en) * 2018-01-23 2018-07-10 广西立盛茧丝绸有限公司 A kind of cocoon cooking process of fresh cocoon infiltration

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102251290A (en) * 2011-07-13 2011-11-23 广西工学院 Method for processing silkworm cocoon before silk reeling
CN103938278A (en) * 2014-04-23 2014-07-23 辽宁柞蚕丝绸科学研究院有限责任公司 Silk-reeling technology by utilization of tussah fresh cocoon live pupae
CN105887210A (en) * 2016-06-03 2016-08-24 浙江理工大学 Silk reeling production technology for improving fresh cocoon raw silk reelability and cohesion stability
CN106119979A (en) * 2016-08-31 2016-11-16 广西融安县金鼎制丝有限责任公司 Fresh cocoon reeling cryogenic vacuum osmosis process
CN106480511A (en) * 2016-12-08 2017-03-08 广西凯喜雅丝绸有限公司 The preparation method of silkworm silk

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102251290A (en) * 2011-07-13 2011-11-23 广西工学院 Method for processing silkworm cocoon before silk reeling
CN103938278A (en) * 2014-04-23 2014-07-23 辽宁柞蚕丝绸科学研究院有限责任公司 Silk-reeling technology by utilization of tussah fresh cocoon live pupae
CN105887210A (en) * 2016-06-03 2016-08-24 浙江理工大学 Silk reeling production technology for improving fresh cocoon raw silk reelability and cohesion stability
CN106119979A (en) * 2016-08-31 2016-11-16 广西融安县金鼎制丝有限责任公司 Fresh cocoon reeling cryogenic vacuum osmosis process
CN106480511A (en) * 2016-12-08 2017-03-08 广西凯喜雅丝绸有限公司 The preparation method of silkworm silk

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108265336A (en) * 2018-01-23 2018-07-10 广西立盛茧丝绸有限公司 A kind of cocoon cooking process of fresh cocoon infiltration

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Application publication date: 20170718