CN106957626B - Peelable blue glue of a kind of volatile-type and preparation method thereof - Google Patents

Peelable blue glue of a kind of volatile-type and preparation method thereof Download PDF

Info

Publication number
CN106957626B
CN106957626B CN201710294555.5A CN201710294555A CN106957626B CN 106957626 B CN106957626 B CN 106957626B CN 201710294555 A CN201710294555 A CN 201710294555A CN 106957626 B CN106957626 B CN 106957626B
Authority
CN
China
Prior art keywords
parts
volatile
type
blue glue
peelable blue
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201710294555.5A
Other languages
Chinese (zh)
Other versions
CN106957626A (en
Inventor
叶耀辉
孙毅
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
R & D Welding Technology (huizhou) Co Ltd
Original Assignee
R & D Welding Technology (huizhou) Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by R & D Welding Technology (huizhou) Co Ltd filed Critical R & D Welding Technology (huizhou) Co Ltd
Priority to CN201710294555.5A priority Critical patent/CN106957626B/en
Publication of CN106957626A publication Critical patent/CN106957626A/en
Application granted granted Critical
Publication of CN106957626B publication Critical patent/CN106957626B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J153/00Adhesives based on block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Adhesives based on derivatives of such polymers
    • C09J153/02Vinyl aromatic monomers and conjugated dienes
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/08Macromolecular additives
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J153/00Adhesives based on block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Adhesives based on derivatives of such polymers
    • C09J153/02Vinyl aromatic monomers and conjugated dienes
    • C09J153/025Vinyl aromatic monomers and conjugated dienes modified
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2207/00Properties characterising the ingredient of the composition
    • C08L2207/04Thermoplastic elastomer

Abstract

Peelable blue glue of a kind of volatile-type and preparation method thereof, the wherein peelable blue glue of volatile-type, in parts by weight, raw material composition and content are as follows:10-20 parts of thermoplastic elastomer resin, 1-10 parts of hydrocarbon resin, 1-10 parts of Petropols, 0.1-1 parts of silane coupling agent, 20-50 parts of Porous deproteinized bone white spirit, 1-10 parts of esters solvent, 10-30 parts of alkanes solvent, 0.1-1 parts of antifoaming agent, 0.1-1 parts of levelling agent, 0.1-1 parts of wetting dispersing agent, 0.1-1 parts of blue or green blue pigment, peelable blue glue of volatile-type provided by the invention and preparation method thereof have high insulation resistance to provide excellent insulation effect;With up to 400% or more elongation percentage, toughness by force to provide peeling effect;And have the function of very strong adhesive force and adherence to provide effectively anti-moisture, salt fog, mould; in addition; the peelable blue glue of volatile-type is not only effectively protected the cleaning of product surface, moreover it is possible to play proofing dust and protecting, salt spray proof protection and moisture-proof gas shielded to product.

Description

Peelable blue glue of a kind of volatile-type and preparation method thereof
Technical field
The present invention relates to technical field of polymer materials, and in particular to one kind having three proofings (salt spray proof, moisture-proof, mould proof) Function and the peelable blue glue of the volatile-type of resistance insulation defencive function and preparation method thereof.
Background technology
In recent years, with technologically fast development, domestic industry industry development is swift and violent, and in the development of industrial trade Cheng Zhong, many production technologies can encounter bottleneck, to solve the technique bottleneck problem, and some new and high technologies also begin to meet the tendency of and It is raw, such as more demanding to surface smooth pieces degree at some and surface is not allowed to occur in any technique for scratching trace, need Surface protection film or Protection glue are used, however these are needed in technique to be protected after using Protection glue, Protection glue can not shell From reprocessed or sur-face peeling after there is residue glue to be retained in protection substrate surface.
Such as in terms of PCB golden finger three proofings protections, currently, PCB golden fingers protection mainly use common adhesive tape into Row protection, which pastes after mainly manually cutting through manual, but has been easy to residue glue in stripping process and has left, at this moment Have to be cleaned using organic solvent, therefore add additional the technique of one of removal residue glue, to increase technique Fussy degree, it is therefore, this that working efficiency is leveraged using the method manually taped.
In addition, for example in terms of the protection of mobile phone ITO electrode glass surface, the guarantor of mobile phone ITO electrode glass surface at present Shield is mainly protected using organic silica gel, and organic silica gel is mainly moisture solidification, and needs the time since speed is fully cured The problems such as growing, and be unable to full wafer stripping after organic silica gel solidification, therefore can not reprocessing.
Invention content
The present invention provides one kind and being effectively protected clean surface to solve the above problem of the existing technology, and Can reach proofing dust and protecting, salt spray proof protection, moisture-proof gas shielded the peelable blue glue of volatile-type and preparation method thereof.
Realize above-mentioned purpose, the present invention provides a kind of peelable blue glue of volatile-type, in parts by weight, raw material group At and content it is as follows:10-20 parts of thermoplastic elastomer resin, 1-10 parts of hydrocarbon resin, 1-10 parts of Petropols, silane coupling agent 0.1-1 parts, 20-50 parts of Porous deproteinized bone white spirit, 1-10 parts of esters solvent, 10-30 parts of alkanes solvent, 0.1-1 parts of antifoaming agent, 0.1-1 parts of levelling agent, 0.1-1 parts of wetting dispersing agent, 0.1-1 parts of blue or green blue pigment.
As the preferred technical solution of the present invention, the thermoplastic elastomer (TPE) is styrene resin, styrene resin Model SBS, SIS, SEBS or SEPS.
As the preferred technical solution of the present invention, the hydrocarbon resin is arene, aliphatic class, ring grease dienes, pure One or more of monomer class.
As the preferred technical solution of the present invention, the pure monomer class is poly SM or alpha methyl styrene, Model TN 150, the TN 160T or TN 170 of the Petropols.
As the preferred technical solution of the present invention, model KBM-403, KBM-503, KBM- of the silane coupling agent 5103, KBM-603 or KBP-43.
As the preferred technical solution of the present invention, model D20, D30 of the Porous deproteinized bone white spirit, D40, D60, D70 or D80.
As the preferred technical solution of the present invention, the esters solvent oil is ethyl acetate, butyl acetate, isobutyl acetate One or more of.
As the preferred technical solution of the present invention, the alkanes solvent is ethyl cyclohexane or hexahydrotoluene.
The present invention also provides a kind of preparation methods of the peelable blue glue of volatile-type, include the following steps:
Esters solvent and alkanes solvent are added in closed A containers, after mixing and mixing time 10-15min, then exists A containers are added Petropols and fully dissolve, to obtain mixed solution one;
Porous deproteinized bone white spirit and alkanes solvent are added in closed B containers, the temperature that B containers are controlled after mixing exists Within the scope of 25 ± 2 DEG C, and mixing time 10-15min, thermoplastic elastomer resin and hydrocarbon resin are then added in B containers, And carry out high speed dispersion, stirring fully to dissolve thermoplastic elastomer resin and hydrocarbon resin, mixing time be 60min ± 10%, to obtain mixed solution two;
Mixed solution one in A containers is added in the mixed solution two in B containers, high speed dispersion, stirring is carried out, stirs It is 45min ± 5% to mix the time, to obtain mixed solution three;
Antifoaming agent, levelling agent, wetting dispersing agent, silane coupling agent, phthalocyanine blue pigment and esters deodorant are added to B to hold In mixed solution three in device, high speed dispersion, stirring are carried out, mixing time is 45min ± 10%, obtains the peelable indigo plant of volatile-type Glue.
As the preferred technical solution of the present invention, when carrying out high speed dispersion, stirring, rate of dispersion is 20000 ± 10% Rpm, mixing speed are 2000 ± 10%rpm.
Peelable blue glue of volatile-type of the present invention and preparation method thereof can reach following advantageous effect:
The peelable blue glue of volatile-type of the present invention, by including 10-20 parts of thermoplastic elastomer resin, hydrocarbon resin 1-10 Part, 1-10 parts of Petropols, 0.1-1 parts of silane coupling agent, 20-50 parts of Porous deproteinized bone white spirit, 1-10 parts of esters solvent, alkane 10-30 parts of class solvent, 0.1-1 parts of antifoaming agent, 0.1-1 parts of levelling agent, 0.1-1 parts of wetting dispersing agent, blue or green blue pigment 0.1-1 Part so that the peelable blue glue of volatile-type of the invention has high insulation resistance to provide excellent insulation effect, has up to 400% or more elongation percentage, toughness by force to provide peeling effect there is very strong adhesive force and adherence effectively to prevent to provide Moisture, salt fog, mould function, in addition, will not be produced by protection material surface after the peelable blue glue stripping of the volatile-type of the present invention Raw residual, can be applied to interim in the production processes such as PCB surface, golden finger, metal surface and glass surface or Person permanently protects, and production method is simple, and raw material is easy to get.
The preparation method of the peelable blue glue of volatile-type of the present invention, by including step:Ester is added in closed A containers Class solvent and alkanes solvent after mixing and mixing time 10-15min, are then added Petropols in A containers and fully dissolve, To obtain mixed solution one;Porous deproteinized bone white spirit and alkanes solvent are added in closed B containers, B containers are controlled after mixing Temperature within the scope of 25 ± 2 DEG C, and mixing time 10-15min, be then added in B containers thermoplastic elastomer resin and Hydrocarbon resin, and high speed dispersion, stirring are carried out fully to dissolve thermoplastic elastomer resin and hydrocarbon resin, mixing time is 60min ± 10%, to obtain mixed solution two;The mixed solution two mixed solution one in A containers being added in B containers In, high speed dispersion, stirring are carried out, mixing time is 45min ± 5%, to obtain mixed solution three;By antifoaming agent, levelling agent, profit Hygroscopic water powder, silane coupling agent, phthalocyanine blue pigment and esters deodorant are added in the mixed solution three in B containers, are carried out high Speed dispersion, stirring, mixing time are 45min ± 10%, obtain the peelable blue glue of volatile-type so that waved made from the method for the present invention The peelable blue glue of hair style has high insulation resistance to provide excellent insulation effect, with up to 400% or more elongation percentage, tough Property has the function of very strong adhesive force and adherence to provide effectively anti-moisture, salt fog, mould by force to provide peeling effect, In addition, being protected material surface not will produce residual after the peelable blue glue stripping of the volatile-type of the present invention, PCB can be applied to Interim or permanent protection in the production processes such as surface, golden finger, metal surface and glass surface, and the side of making Method is simple, and raw material is easy to get.
Description of the drawings
The present invention will be further described in detail below with reference to the accompanying drawings and specific embodiments.
Fig. 1 is the flow chart that the preparation method of the peelable blue glue of volatile-type of the present invention provides.
The object of the invention is realized, the embodiments will be further described with reference to the accompanying drawings for functional characteristics and advantage.
Specific implementation mode
Below in conjunction with attached drawing and specific implementation mode, the present invention is described further.Drawn in preferred embodiment Such as "upper", "lower", "left", "right", " centre " and " one " term, only being illustrated for ease of narration, rather than to limit The enforceable range of the present invention, relativeness are altered or modified, in the case where changing technology contents without essence, when being also considered as this hair Bright enforceable scope.
The present invention provides a kind of peelable blue glue of volatile-type, and in parts by weight, raw material composition and content are as follows: 10-20 parts of thermoplastic elastomer resin, 1-10 parts of hydrocarbon resin, 1-10 parts of Petropols, 0.1-1 parts of silane coupling agent, de- virtue 20-50 parts of hydrocarbon white spirit, 1-10 parts of esters solvent, 10-30 parts of alkanes solvent, 0.1-1 parts of antifoaming agent, levelling agent 0.1-1 Part, 0.1-1 parts of wetting dispersing agent, 0.1-1 parts of blue or green blue pigment.
In specific implementation, the thermoplastic elastomer (TPE) be styrene resin, the model SBS of styrene resin, SIS, SEBS or SEPS.
In specific implementation, the hydrocarbon resin is one kind in arene, aliphatic class, ring grease dienes, pure monomer class Or it is several, the pure monomer class is poly SM or alpha methyl styrene.
In specific implementation, model TN 150, the TN 160T or TN 170 of the Petropols.
In specific implementation, model KBM-403, KBM-503, KBM-5103, KBM-603 of the silane coupling agent or KBP-43。
In specific implementation, model D20, D30, D40, D60, D70 or D80 of the Porous deproteinized bone white spirit.
In specific implementation, the esters solvent oil is ethyl acetate, butyl acetate, one kind in isobutyl acetate or several Kind.
In specific implementation, the alkanes solvent is ethyl cyclohexane or hexahydrotoluene.
The peelable blue glue of volatile-type of the embodiment has high insulation resistance to provide excellent insulation effect, has up to 400% or more elongation percentage, toughness by force to provide peeling effect there is very strong adhesive force and adherence effectively to prevent to provide Moisture, salt fog, mould function, in addition, will not be produced by protection material surface after the peelable blue glue stripping of the volatile-type of the present invention Raw residual, can be applied to interim in the production processes such as PCB surface, golden finger, metal surface and glass surface or Person permanently protects, and production method is simple, and raw material is easy to get.
As shown in Figure 1, the present invention also provides a kind of preparation method of the peelable blue glue of volatile-type, include the following steps:
Esters solvent and alkanes solvent is added in step 11 in closed A containers, after mixing and mixing time 10- Then 15min is added Petropols in A containers and fully dissolves, to obtain mixed solution one;
Porous deproteinized bone white spirit and alkanes solvent is added in step 12 in closed B containers, and B containers are controlled after mixing Temperature within the scope of 25 ± 2 DEG C, and mixing time 10-15min, be then added in B containers thermoplastic elastomer resin and Hydrocarbon resin, and high speed dispersion, stirring are carried out fully to dissolve thermoplastic elastomer resin and hydrocarbon resin, mixing time is 60min ± 10%, to obtain mixed solution two;
Mixed solution one in A containers is added in the mixed solution two in B containers by step 13, progress high speed dispersion, Stirring, mixing time is 45min ± 5%, to obtain mixed solution three;
Step 14 adds antifoaming agent, levelling agent, wetting dispersing agent, silane coupling agent, phthalocyanine blue pigment and esters deodorant Enter into the mixed solution three in B containers, carry out high speed dispersion, stirring, mixing time is 45min ± 10%, obtains volatile-type Peelable indigo plant glue.
Preferably, the carry out high speed dispersion in above-mentioned steps 12, step 13 and step 14, in stirring, rate of dispersion is 20000 ± 10%rpm, mixing speed be 2000 ± 10%rpm, certainly its can also be other concrete numerical values, the present invention not Do any restrictions.
In order to allow those skilled in the art to more fully understand and realize technical scheme of the present invention, below by embodiment The mode effect that is specifically described technical scheme of the present invention and brings.
Embodiment 1
The peelable blue glue of volatile-type, in parts by weight, raw material composition and content are as follows:Thermoplastic elastomer resin 13 parts, 4 parts of hydrocarbon resin, 3 parts of Petropols, 0.5 part of silane coupling agent, 50 parts of Porous deproteinized bone white spirit, esters solvent 6 Part, 22 parts of alkanes solvent, 0.5 part of antifoaming agent, 0.3 part of levelling agent, 0.5 part of wetting dispersing agent, 0.2 part of phthalocyanine blue pigment.It will be upper State preparation method of the raw material according to the peelable blue glue of volatile-type, by high speed dispersion, stir to get it is (salt spray proof, anti-with three proofings It is damp, mould proof) the peelable blue glue of volatile-type of function and resistance insulation defencive function.
Embodiment 2
The peelable blue glue of volatile-type, in parts by weight, raw material composition and content are as follows:Thermoplastic elastomer resin 14.5 parts, 6 parts of hydrocarbon resin, 5 parts of Petropols, 0.5 part of silane coupling agent, 43 parts of Porous deproteinized bone white spirit, esters solvent 6 Part, 22 parts of alkanes solvent, 0.7 part of antifoaming agent, 0.5 part of levelling agent, 0.5 part of wetting dispersing agent, 0.3 part of phthalocyanine blue pigment.It will be upper State preparation method of the raw material according to the peelable blue glue of volatile-type, by high speed dispersion, stir to get it is (salt spray proof, anti-with three proofings It is damp, mould proof) the peelable blue glue of volatile-type of function and resistance insulation defencive function.
Embodiment 3
The peelable blue glue of volatile-type, in parts by weight, raw material composition and content are as follows:Thermoplastic elastomer resin 17 parts, 8 parts of hydrocarbon resin, 5 parts of Petropols, 0.5 part of silane coupling agent, 40 parts of Porous deproteinized bone white spirit, esters solvent 6 Part, 22 parts of alkanes solvent, 0.7 part of antifoaming agent, 0.5 part of levelling agent, 0.5 part of wetting dispersing agent, 0.5 part of phthalocyanine blue pigment.It will be upper State preparation method of the raw material according to the peelable blue glue of volatile-type, by high speed dispersion, stir to get it is (salt spray proof, anti-with three proofings It is damp, mould proof) the peelable blue glue of volatile-type of function and resistance insulation defencive function.
Indigo plant glue peelable to the volatile-type made in embodiment 1-3 is tested for the property, and it is peelable in addition to choose commercially available volatile-type From blue glue, group, testing result are as shown in table 1 below as a comparison:
Detect example 1
Varnish and coating-rotational viscometer recorded with reference to international standard (ISO 2884-2-2003) measure viscosity methods The viscosity of indigo plant glue peelable to above-mentioned volatile-type is detected.
Detect example 2
The paint film recorded with reference to national standard (GB/T1728-1979), putty membrane drying time measuring method is to above-mentioned volatilization The surface drying of the peelable blue glue of type is detected.
Detect example 3
With reference to the measuring method pair for the paint resistance to neutral salt spray performance of paint and varnish that national standard (GB/T1771-1991) is recorded The salt spray proof of the peelable blue glue of above-mentioned volatile-type is detected.
Detect example 4
With reference to International Electro industry connection association criterion (IPC-TM-650 2.5.17.1:94) dielectric material recorded Volume and the surface impedance of non-essential resistance rate method blue glue peelable to above-mentioned volatile-type are detected.
Table 1
It is provided by the invention by the contrast test to above three embodiments it is found that wherein embodiment 2 is preferred embodiment The peelable blue glue of volatile-type has quite excellent physical and mechanical properties, and excellent insulation can be provided with high insulation resistance Effect;There is up to 400% or more elongation percentage, toughness can provide peeling effect by force for it;And with very strong adhesive force and close The property can provide effectively anti-moisture, salt fog, mould.
The construction technology of the peelable blue glue of volatile-type provided by the invention has diversification, can carry out dip-coating, spot printing, spraying Mode batch is overlying on to the more demanding product surface of surface smooth pieces degree, to improve the working efficiency of production technology, is being criticized During covering, it is not only effectively protected the cleaning of product surface, moreover it is possible to proofing dust and protecting, salt spray proof protection be accomplished to product and prevented Moisture is protected.
Although specific embodiments of the present invention have been described above, those skilled in the art should be appreciated that this It is merely illustrative of, various changes or modifications can be made to present embodiment, without departing from the principle and substance of the present invention, Protection scope of the present invention is only limited by the claims that follow.

Claims (9)

1. a kind of peelable blue glue of volatile-type, which is characterized in that in parts by weight, raw material composition and content are as follows:Heat 10-20 parts of thermoplastic elastic resin, 1-10 parts of hydrocarbon resin, 1-10 parts of Petropols, 0.1-1 parts of silane coupling agent, Porous deproteinized bone 20-50 parts of white spirit, 1-10 parts of esters solvent, 10-30 parts of alkanes solvent, 0.1-1 parts of antifoaming agent, 0.1-1 parts of levelling agent, 0.1-1 parts of wetting dispersing agent, 0.1-1 parts of phthalocyanine blue pigment;
The thermoplastic elastomer (TPE) is styrene resin, model SBS, SIS, SEBS or SEPS of styrene resin.
2. the peelable blue glue of volatile-type described in accordance with the claim 1, which is characterized in that the hydrocarbon resin be arene, One or more of aliphatic class, ring grease dienes, pure monomer class, the pure monomer class are poly SM or poly alpha methyl styrene。
3. the peelable blue glue of volatile-type described in accordance with the claim 1, which is characterized in that the model of the Petropols TN150, TN 160T or TN 170.
4. the peelable blue glue of volatile-type described in accordance with the claim 1, which is characterized in that the model of the silane coupling agent KBM-403, KBM-503, KBM-5103, KBM-603 or KBP-43.
5. the peelable blue glue of volatile-type described in accordance with the claim 1, which is characterized in that the type of the Porous deproteinized bone white spirit Number be D20, D30, D40, D60, D70 or D80.
6. the peelable blue glue of volatile-type described in accordance with the claim 1, which is characterized in that the esters solvent be ethyl acetate, One or more of butyl acetate, isobutyl acetate.
7. according to the peelable blue glue of claim 1 to 6 any one of them volatile-type, which is characterized in that the alkanes solvent is Ethyl cyclohexane or hexahydrotoluene.
8. a kind of preparation method of the peelable blue glue of volatile-type, which is characterized in that include the following steps:
Esters solvent and alkanes solvent are added in closed A containers, after mixing and mixing time 10-15min, then holds in A Device is added Petropols and fully dissolves, to obtain mixed solution one;
Porous deproteinized bone white spirit and alkanes solvent are added in closed B containers, controlled after mixing the temperature of B containers 25 ± Within the scope of 2 DEG C, and mixing time 10-15min, thermoplastic elastomer resin and hydrocarbon resin are then added in B containers, goes forward side by side Fully to dissolve thermoplastic elastomer resin and hydrocarbon resin, mixing time is 60min ± 10% for row high speed dispersion, stirring, with Obtain mixed solution two;
Mixed solution one in A containers is added in the mixed solution two in B containers, high speed dispersion, stirring are carried out, when stirring Between be 45min ± 5%, to obtain mixed solution three;
Antifoaming agent, levelling agent, wetting dispersing agent, silane coupling agent, phthalocyanine blue pigment and esters deodorant are added in B containers Mixed solution three in, carry out high speed dispersion, stirring, mixing time is 45min ± 10%, obtains the peelable blue glue of volatile-type.
9. the preparation method of the peelable blue glue of volatile-type according to claim 8, which is characterized in that progress high speed dispersion, When stirring, rate of dispersion is 20000 ± 10%rpm, and mixing speed is 2000 ± 10%rpm.
CN201710294555.5A 2017-04-28 2017-04-28 Peelable blue glue of a kind of volatile-type and preparation method thereof Expired - Fee Related CN106957626B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710294555.5A CN106957626B (en) 2017-04-28 2017-04-28 Peelable blue glue of a kind of volatile-type and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710294555.5A CN106957626B (en) 2017-04-28 2017-04-28 Peelable blue glue of a kind of volatile-type and preparation method thereof

Publications (2)

Publication Number Publication Date
CN106957626A CN106957626A (en) 2017-07-18
CN106957626B true CN106957626B (en) 2018-11-06

Family

ID=59484037

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710294555.5A Expired - Fee Related CN106957626B (en) 2017-04-28 2017-04-28 Peelable blue glue of a kind of volatile-type and preparation method thereof

Country Status (1)

Country Link
CN (1) CN106957626B (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108107619B (en) * 2017-12-26 2021-06-08 上海展扬通信技术有限公司 Display module structure and terminal equipment
JP6506461B1 (en) * 2018-02-01 2019-04-24 積水化学工業株式会社 Conductive adhesive tape
CN110484172A (en) * 2019-08-06 2019-11-22 广州慧谷化学有限公司 Quick detachable glue and preparation method thereof, adhesive tape, electronic product
CN111500230B (en) * 2020-05-23 2021-07-23 深圳宝利树脂有限公司 All-purpose adhesive with good bonding effect and preparation method thereof

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3005361B2 (en) * 1992-04-28 2000-01-31 日石三菱株式会社 Binder composition
CN105176448A (en) * 2015-07-24 2015-12-23 中山市伯伦克专用化学产品有限公司 Protective elastic peelable blue glue and preparation method therefor
CN105733393B (en) * 2016-04-14 2018-05-11 顺德职业技术学院 The preparation method of the peelable blue glue of environment-friendly type room temperature fast-curing

Also Published As

Publication number Publication date
CN106957626A (en) 2017-07-18

Similar Documents

Publication Publication Date Title
CN106957626B (en) Peelable blue glue of a kind of volatile-type and preparation method thereof
CN102504733B (en) Water-blush-resistant fluoride and siloxane modified waterborne pressure-sensitive adhesive and polyethylene protective film
CN102936469B (en) Heat drying type transference resistant stripping blue gel and preparation method thereof
CN101942153B (en) Single-component chlorosulfonated polyethylene anticorrosive paint and preparation method thereof
CN103666250A (en) Organic silicon coating rubber and preparation method thereof
CN107057481A (en) A kind of peelable blue glue of heat cure
CN102408808B (en) Aqueous fluorocarbon coating for painting metal base materials
CN103897586A (en) Coating composition, method for preparing the same, and film layer formed from the coating composition
CN107163761A (en) A kind of colorful base paint emulsion of excellent performance and preparation method thereof
CN104293062B (en) Soft raw matter antifouling paint of aqueous and preparation method thereof
CN106280820A (en) A kind of fluorine silicon acrylate paint
CN106349842B (en) A kind of terpene resin modification thermoplastic acrylic acid resin quick-drying paint and preparation method thereof
CN108841263A (en) The preparation method and applications of hydrophobic material for antenna house surface
CN103254715B (en) Transparent acrylic acid intermediate-coating paint base stock and preparation method thereof
JP5623094B2 (en) Moisture-proof insulating paint for mounting circuit boards and electronic components
CN104004458B (en) Applying method
CN103467890B (en) A kind of peelable protective film and composite formula thereof
CN108084828A (en) A kind of high durable for lamp stand plates spelter coating and preparation method thereof
CN108192356A (en) A kind of carrier model organosilicon adhesion promoter and preparation method thereof
CN109868095A (en) In-situ polymerization type has organic silicon-acrylate adhesive preparation method of light diffusion function and products thereof and application
CN104231810B (en) Protection glue and preparation method thereof for a kind of touch-screen
CN102382509A (en) Water-based ink, elastic emulsion used for water-based ink and preparation method of elastic emulsion
CN105131719B (en) A kind of alcohol radical nano silver wire conductive ink for protecting caking property strong
CN108034343A (en) A kind of anti-fouling type water paint
WO2007049488A1 (en) Composition for coating ceramics

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20181106

Termination date: 20200428

CF01 Termination of patent right due to non-payment of annual fee