CN106946424A - Dirty plant source deodorant of a kind of pig farm excrement and its preparation method and application - Google Patents

Dirty plant source deodorant of a kind of pig farm excrement and its preparation method and application Download PDF

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Publication number
CN106946424A
CN106946424A CN201710166215.4A CN201710166215A CN106946424A CN 106946424 A CN106946424 A CN 106946424A CN 201710166215 A CN201710166215 A CN 201710166215A CN 106946424 A CN106946424 A CN 106946424A
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weight
deodorant
plant source
powder
pig farm
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张昌爱
赵艳兰
辛淑荣
刘兆辉
杨正涛
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Shandong Jichang Agriculture Technology Co ltd
Institute of Agricultural Resources and Environment of Shandong Academy of Agricultural Sciences
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Shandong Jichang Agriculture Technology Co ltd
Institute of Agricultural Resources and Environment of Shandong Academy of Agricultural Sciences
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2303/00Specific treatment goals
    • C02F2303/02Odour removal or prevention of malodour

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  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Agronomy & Crop Science (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Plant Pathology (AREA)
  • Environmental Sciences (AREA)
  • Biotechnology (AREA)
  • Zoology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

The present invention relates to a kind of dirty plant source deodorant of pig farm excrement, a kind of preparation method of the dirty plant source deodorant of above-mentioned pig farm excrement, and application of the dirty plant source deodorant of above-mentioned pig farm excrement when producing crop organic fertilizer are further related to.The dirty plant source deodorant of pig farm excrement of the present invention is prepared from by following ingredients:Calamus, mulberry leaf, lotus leaf, enteromorpha powder, Shi Water-shield powder, pomelo peel, folium artemisiae argyi, green tea, zeolite powder.The dirty deodorant of pig farm excrement obtained by the present invention can quickly and efficiently remove pig manure stink, and deodorizing effect significantly, can effectively reduce influence of the pig manure stink to environment, suppress the generation of the pernicious gas such as hydrogen sulfide and ammonia, reduce pollution of the pig manure to environment.

Description

Dirty plant source deodorant of a kind of pig farm excrement and its preparation method and application
Technical field
The invention belongs to technical field of ecological agriculture, more particularly to a kind of dirty plant source deodorant of pig farm excrement, further relate to A kind of preparation method of the dirty plant source deodorant of above-mentioned pig farm excrement, and the dirty plant source deodorant of above-mentioned pig farm excrement is in production Application during crop organic fertilizer.
Background technology
At present, with the development of various regions pastoral industry, intensive culture is emerged in multitude, and the discharge capacity of excrement is more and more, The pollution problem of excrement becomes increasingly conspicuous.The quality of pig manure is thinner, and composition is more complicated, containing protein, fats, organic acid, fiber Element, hemicellulose and inorganic salts.As people gradually increase the demand of pollution-free food, the usage amount of chemicals by Increasingly stricter limitation, is becoming widely adopted with the organic fertilizer of excrement retting.Yet with piggery waste pathogen it is many, The features such as cause of disease harm is serious, while the foul smell produced as well as piggery waste directly affects human and livestock health, also deteriorates Recycling operating personnel are engaged in the working environment of Collection utilization, thus become recycling in livestock and poultry cultivation night soil The worst species of degree.
Foul smell complicated component produced by pig excrement, including indoles organic acid, scatol, fats amine mercaptan, vulcanization Hydrogen, ammonia etc., wherein maximum with the harm of hydrogen sulfide and ammonia.Pig manure foul smell available physical, chemistry and biological method are removed at present Handled.Physical deodorization method mainly has WATER-WASHING METHOD, absorption method, screening agent method and high-altitude diffusion method, and chemical deodorizing method mainly has Direct combustion method, chemical oxidization method, neutralisation and high-temperature oxidation, biological odor removal method be decomposed using microorganism, convert it is smelly Gas composition is also microbial deodorant method to reach deodorization purpose, and the microorganism worked in deodoring materials mainly has nitre Change bacterium, Nitrosomas, denitrifying bacteria, sulfur bacteria etc..Effect using the method deodorization of physics and chemistry is preferable, but exists The problems such as investment and operating cost are high, secondary pollution is serious.Effect using biological method deodorization in laboratory may be fine, but Because microbial activity is limited by environmental condition, it is difficult to ensure that the deodorizing effect of compost.
The content of the invention
An object of the present invention is to provide dirty plant source deodorant of a kind of pig farm excrement and preparation method thereof.
In order to solve the above-mentioned technical problem, the present invention uses following technical scheme:A kind of dirty plant source deodorization of pig farm excrement The preparation method of agent, comprises the following steps:
(1) Enteromorpha salvaged in seawater and stone Water-shield are cleaned up with clear water respectively, puts 60 DEG C of constant temperatures in an oven Lower drying to the percentage by weight of moisture is 15~20%, takes out and crushes respectively, obtains enteromorpha powder He Shi Water-shield powder;
(2) calamus, mulberry leaf, lotus leaf are cleaned respectively and dried, then press calamus, mulberry leaf, lotus leaf, enteromorpha powder, Shi Water-shield powder According to 1:2~3:3~5:8~10:6~8 weight is than mixing, and additions weight is that calamus, mulberry leaf, lotus leaf, enteromorpha powder, Shi Water-shield powder are total 0.5~0.6 times of vinegar of weight, is mixed, soak at room temperature 30 minutes, and supernatant is removed in centrifugation, stays sediment, 40 DEG C of drying Percentage by weight to moisture is 15~20%;
(3) the drying product obtained by step (2) is put into Muffle furnace, in 350 DEG C~400 DEG C 2~3h of calcination, be cooled to Room temperature, then at 500 DEG C~550 DEG C calcinations 2~3 hours;
(4) pomelo peel is chopped up and ground;
(5) by folium artemisiae argyi, green tea according to 5:1 weight is than mixing, and addition weight is 15 times of folium artemisiae argyi and green tea gross weight Boiling water, soaks 5~8 hours, takes soak;
(6) zeolite is crushed to 100 mesh and 200 mesh, by the zeolite powder of the zeolite powder of 100 mesh and 200 mesh according to 1:2 ratio Example mixing;
(7) by the calcination thing obtained by step (3), the pomelo peel obtained by step (4), the soak obtained by step (5), step (6) zeolite powder obtained by is according to 1:2~3:9~10:2~3 weight is than mixing, and ultrasonication 30 minutes is produced.
The invention also discloses a kind of dirty deodorant of the plant source pig farm excrement obtained by above-mentioned preparation method.
The application method of the dirty deodorant of plant source pig farm excrement is as follows:Pig manure is filtered, liquid is discarded, by excrement with Deodorant is according to 1:40~50 weight ratio is mixed and stirred for uniform;Or dilute the deodorant of the present invention with clear water, it is sprayed onto (spray form in pump type small plastic sprayer can be fitted into use) on pig manure.
The dirty deodorant of plant source pig farm excrement obtained by the present invention can quickly and efficiently remove pig manure stink, deodorization effect Fruit significantly, can effectively reduce influence of the pig manure stink to environment, suppress the generation of the pernicious gas such as hydrogen sulfide and ammonia, reduce pig manure Pollution to environment.Peculiar smell can not only be improved by adding calamus, mulberry leaf, pomelo peel, folium artemisiae argyi, green tea etc. in deodorant, also Certain bactericidal action can be played to the pathogen in pig manure, solves easily to bring disease to crops in the traditional application method of pig manure The harm of pathogen in the problem of insect pest, reduction pig manure, therefore be conducive to improving the rationalization of the utilization rate and resource of pig manure Utilize, twice laid and the material circulation of nature are promoted, with important economic worth and the value of environmental protection.At the same time, The dirty deodorant of plant source pig farm excrement of the present invention can effectively reduce ammonia and hydrogen sulfide content, reduce dirt of the pig manure to environment Dye, while also improving pig class living environment, is conducive to keeping with fresh air, improves the working environment of poultry feeders.In addition, Compared with existing chemically and physically deodorization process, the cost of raw material used in the dirty deodorant of plant source pig farm excrement of the invention Cheap, wide material sources, and be green natural material, it is degradable, secondary pollution will not be brought to environment;Compared to existing life Thing deodorization process, the dirty deodorant of plant source pig farm excrement of the invention is difficult to be limited by environmental condition, therefore is conducive to popularization to answer With.
Preferably, in step (2), calamus, mulberry leaf, lotus leaf, enteromorpha powder, Shi Water-shield powder are according to 1:2:4:8:8 weight is than mixed Close.
Preferably, in step (7), by the calcination thing obtained by step (3), the pomelo peel obtained by step (4), step (5) institute Soak, the zeolite powder obtained by step (6) is according to 1:3:10:2 weight is than mixing.
The invention also discloses a kind of dirty deodorant of above-mentioned plant source pig farm excrement answering when preparing crop organic fertilizer With.Specifically, the special odorless organic fertilizer of cotton is being prepared the invention discloses a kind of dirty deodorant of above-mentioned plant source pig farm excrement When application, comprise the following steps that:
(1) pig manure is filtered, discards liquid, by excrement with deodorant of the invention according to 1:40~50 weight is than mixing And stir, obtain swine manure treatment thing;
(2) each component of following parts by weight is weighed according to proportioning:80~100 parts of cotton stalk, swine manure treatment thing 60~ 70 parts, 10~15 parts of wheat straw, 10~15 parts of beanstalk, 8~10 parts of bone meal, 1~3 part of microbial fermentation inoculum;
(3) cotton stalk, swine manure treatment thing, wheat straw, beanstalk, bone meal, microbial fermentation inoculum are mixed, adds weight phase When in 0.6~0.8 times of clear water of total weight of the mixture, stir, Natural compost, at interval of turning in 5-7 days once, fermentation Complete compost fermentation within 15-20 days;
(4) tunning obtained by step (3) is put into 60 DEG C of drying in an oven to water content within 15%, with crushing Machine is ground into the powder of 100~200 mesh, granulates, granular material is dried, drier heat source maximum temperature is in comminutor 200~250 DEG C, 50~70 DEG C of outlet temperature, water content is less than 5% after dry materials, finally sieves, by grain diameter 1.00 ~3.00mm fertilizer weighs, packs and produces.
Further, the microbial fermentation inoculum can be dusty yeast, lactic acid bacteria or its mixture.
Preferably, in step (2), each component of following parts by weight is weighed according to proportioning:At 80 parts of cotton stalk, pig manure Manage 65 parts of thing, 15 parts of wheat straw, 10 parts of beanstalk, 8 parts of bone meal, 2 parts of microbial fermentation inoculum.
The invention also discloses a kind of special odorless organic fertilizer of cotton by obtained by the above method.Usage and dosage:Make Used for base fertilizer, every mu of 50~60kg of fertilising can consider increase and decrease according to soil regime.
Utilize the preparation side of the special odorless organic fertilizer of cotton obtained by the dirty deodorant of the plant source pig farm excrement of the present invention Method is simple, obtained organic fertilizer free from extraneous odour, prepares the equal environmental protection of all raw material components, with low cost of organic fertilizer, carries The high utilization rate of pig manure, takes full advantage of the active ingredient of cotton stalk, pig manure, wheat straw, beanstalk, bone meal, is the life of cotton Nutriment needed for long supplement, is conducive to the re-using of waste and the material circulation of nature, and also help improved soil, Culture fertility.
Compared with prior art, the beneficial effects of the present invention are:
(1) the dirty deodorant of plant source pig farm excrement obtained by the present invention can quickly and efficiently remove pig manure stink, deodorization Effect significantly, can effectively reduce influence of the pig manure stink to environment, suppress the generation of the pernicious gas such as hydrogen sulfide and ammonia, reduce pig Pollution of the excrement to environment.
(2) the dirty deodorant of plant source pig farm excrement of the invention can effectively reduce ammonia and hydrogen sulfide content, reduce pig manure Pollution to environment, while also improving pig class living environment, is conducive to keeping with fresh air, improves the work of poultry feeders Environment.
(3) compared with existing chemically and physically deodorization process, the dirty deodorant of plant source pig farm excrement of the invention is used The cost of raw material is cheap, wide material sources, and be green natural material, it is degradable, secondary pollution will not be brought to environment;Phase Than in existing biological odor removal method, the dirty deodorant of plant source pig farm excrement of the invention is difficult to be limited by environmental condition, therefore Be conducive to popularization and application.
(4) preparation of the special odorless organic fertilizer of cotton obtained by the dirty deodorant of plant source pig farm excrement of the present invention is utilized Method is simple, obtained organic fertilizer free from extraneous odour, prepares the equal environmental protection of all raw material components, with low cost of organic fertilizer, The utilization rate of pig manure is improved, the active ingredient of cotton stalk, pig manure, wheat straw, beanstalk, bone meal is taken full advantage of, is cotton The nutriment needed for supplement is grown, is conducive to the re-using of waste and the material circulation of nature, and also help conditioned soil Earth, culture fertility.
Embodiment
Following embodiment facilitates a better understanding of the present invention, but does not limit the present invention.Experiment in following embodiments Method, unless otherwise specified, is conventional method.
Embodiment 1
A kind of preparation method of the dirty deodorant of plant source pig farm excrement, comprises the following steps:
(1) Enteromorpha salvaged in seawater and stone Water-shield are cleaned up with clear water respectively, puts 60 DEG C of constant temperatures in an oven Lower drying to the percentage by weight of moisture is 15~20%, takes out and crushes respectively, obtains enteromorpha powder He Shi Water-shield powder;
(2) calamus, mulberry leaf, lotus leaf are cleaned respectively and dried, then press calamus, mulberry leaf, lotus leaf, enteromorpha powder, Shi Water-shield powder According to 1:2:4:8:8 weight than mixing, additions weight be calamus, mulberry leaf, lotus leaf, 0.5 times of enteromorpha powder, Shi Water-shield powder gross weights Vinegar, is mixed, and soak at room temperature 30 minutes is transferred in centrifuge tube, 3000r/min centrifugation 5min, is removed supernatant, is stayed precipitation Thing, is 15~20% by the percentage by weight that sediment is dried in 40 DEG C to moisture;
(3) the drying product obtained by step (2) is put into Muffle furnace, in 350 DEG C~400 DEG C 2~3h of calcination, be cooled to Room temperature, then at 500 DEG C~550 DEG C calcinations 2~3 hours;
(4) pomelo peel is chopped up and ground;
(5) by folium artemisiae argyi, green tea according to 5:1 weight is than mixing, and addition weight is 15 times of folium artemisiae argyi and green tea gross weight Boiling water, soaks 5~8 hours, takes soak;
(6) zeolite is crushed to 100 mesh and 200 mesh, by the zeolite powder of the zeolite powder of 100 mesh and 200 mesh according to 1:2 ratio Example mixing;
(7) by the calcination thing obtained by step (3), the pomelo peel obtained by step (4), the soak obtained by step (5), step (6) zeolite powder obtained by is according to 1:3:10:2 weight is than mixing, and ultrasonication 30 minutes is produced.
A kind of plant source pig farm excrement dirty deodorant obtained by above-mentioned preparation method.
Embodiment 2
A kind of preparation method of the dirty deodorant of plant source pig farm excrement, comprises the following steps:
(1) Enteromorpha salvaged in seawater and stone Water-shield are cleaned up with clear water respectively, puts 60 DEG C of constant temperatures in an oven Lower drying to the percentage by weight of moisture is 15~20%, takes out and crushes respectively, obtains enteromorpha powder He Shi Water-shield powder;
(2) calamus, mulberry leaf, lotus leaf are cleaned respectively and dried, then press calamus, mulberry leaf, lotus leaf, enteromorpha powder, Shi Water-shield powder According to 1:3:3:8:6 weight than mixing, additions weight be calamus, mulberry leaf, lotus leaf, 0.6 times of enteromorpha powder, Shi Water-shield powder gross weights Vinegar, is mixed, and soak at room temperature 30 minutes is transferred in centrifuge tube, 3000r/min centrifugation 5min, is removed supernatant, is stayed precipitation Thing, is 15~20% by the percentage by weight that sediment is dried in 40 DEG C to moisture;
(3) the drying product obtained by step (2) is put into Muffle furnace, in 350 DEG C~400 DEG C 2~3h of calcination, be cooled to Room temperature, then at 500 DEG C~550 DEG C calcinations 2~3 hours;
(4) pomelo peel is chopped up and ground;
(5) by folium artemisiae argyi, green tea according to 5:1 weight is than mixing, and addition weight is 15 times of folium artemisiae argyi and green tea gross weight Boiling water, soaks 5~8 hours, takes soak;
(6) zeolite is crushed to 100 mesh and 200 mesh, by the zeolite powder of the zeolite powder of 100 mesh and 200 mesh according to 1:2 ratio Example mixing;
(7) by the calcination thing obtained by step (3), the pomelo peel obtained by step (4), the soak obtained by step (5), step (6) zeolite powder obtained by is according to 1:2:10:3 weight is than mixing, and ultrasonication 30 minutes is produced.
A kind of plant source pig farm excrement dirty deodorant obtained by above-mentioned preparation method.
Embodiment 3
A kind of preparation method of the dirty deodorant of plant source pig farm excrement, comprises the following steps:
(1) Enteromorpha salvaged in seawater and stone Water-shield are cleaned up with clear water respectively, puts 60 DEG C of constant temperatures in an oven Lower drying to the percentage by weight of moisture is 15~20%, takes out and crushes respectively, obtains enteromorpha powder He Shi Water-shield powder;
(2) calamus, mulberry leaf, lotus leaf are cleaned respectively and dried, then press calamus, mulberry leaf, lotus leaf, enteromorpha powder, Shi Water-shield powder According to 1:2:5:10:7 weight than mixing, additions weight be calamus, mulberry leaf, lotus leaf, 0.5 times of enteromorpha powder, Shi Water-shield powder gross weights Vinegar, mix, soak at room temperature 30 minutes is transferred in centrifuge tube, 3000r/min centrifugation 5min remove supernatant, stay precipitation Thing, is 15~20% by the percentage by weight that sediment is dried in 40 DEG C to moisture;
(3) the drying product obtained by step (2) is put into Muffle furnace, in 350 DEG C~400 DEG C 2~3h of calcination, be cooled to Room temperature, then at 500 DEG C~550 DEG C calcinations 2~3 hours;
(4) pomelo peel is chopped up and ground;
(5) by folium artemisiae argyi, green tea according to 5:1 weight is than mixing, and addition weight is 15 times of folium artemisiae argyi and green tea gross weight Boiling water, soaks 5~8 hours, takes soak;
(6) zeolite is crushed to 100 mesh and 200 mesh, by the zeolite powder of the zeolite powder of 100 mesh and 200 mesh according to 1:2 ratio Example mixing;
(7) by the calcination thing obtained by step (3), the pomelo peel obtained by step (4), the soak obtained by step (5), step (6) zeolite powder obtained by is according to 1:3:9:3 weight is than mixing, and ultrasonication 30 minutes is produced.
A kind of plant source pig farm excrement dirty deodorant obtained by above-mentioned preparation method.
Embodiment 4
A kind of preparation method of the dirty deodorant of plant source pig farm excrement, comprises the following steps:
(1) Enteromorpha salvaged in seawater and stone Water-shield are cleaned up with clear water respectively, puts 60 DEG C of constant temperatures in an oven Lower drying to the percentage by weight of moisture is 15~20%, takes out and crushes respectively, obtains enteromorpha powder He Shi Water-shield powder;
(2) calamus, mulberry leaf, lotus leaf are cleaned respectively and dried, then press calamus, mulberry leaf, lotus leaf, enteromorpha powder, Shi Water-shield powder According to 1:3:4:9:6 weight than mixing, additions weight be calamus, mulberry leaf, lotus leaf, 0.6 times of enteromorpha powder, Shi Water-shield powder gross weights Vinegar, is mixed, and soak at room temperature 30 minutes is transferred in centrifuge tube, 3000r/min centrifugation 5min, is removed supernatant, is stayed precipitation Thing, is 15~20% by the percentage by weight that sediment is dried in 40 DEG C to moisture;
(3) the drying product obtained by step (2) is put into Muffle furnace, in 350 DEG C~400 DEG C 2~3h of calcination, be cooled to Room temperature, then at 500 DEG C~550 DEG C calcinations 2~3 hours;
(4) pomelo peel is chopped up and ground;
(5) by folium artemisiae argyi, green tea according to 5:1 weight is than mixing, and addition weight is 15 times of folium artemisiae argyi and green tea gross weight Boiling water, soaks 5~8 hours, takes soak;
(6) zeolite is crushed to 100 mesh and 200 mesh, by the zeolite powder of the zeolite powder of 100 mesh and 200 mesh according to 1:2 ratio Example mixing;
(7) by the calcination thing obtained by step (3), the pomelo peel obtained by step (4), the soak obtained by step (5), step (6) zeolite powder obtained by is according to 1:3:9:2 weight is than mixing, and ultrasonication 30 minutes is produced.
A kind of plant source pig farm excrement dirty deodorant obtained by above-mentioned preparation method.
Embodiment 5
A kind of preparation method of the dirty deodorant of plant source pig farm excrement, comprises the following steps:
(1) Enteromorpha salvaged in seawater and stone Water-shield are cleaned up with clear water respectively, puts 60 DEG C of constant temperatures in an oven Lower drying to the percentage by weight of moisture is 15~20%, takes out and crushes respectively, obtains enteromorpha powder He Shi Water-shield powder;
(2) calamus, mulberry leaf, lotus leaf are cleaned respectively and dried, then press calamus, mulberry leaf, lotus leaf, enteromorpha powder, Shi Water-shield powder According to 1:3:5:9:8 weight than mixing, additions weight be calamus, mulberry leaf, lotus leaf, 0.5 times of enteromorpha powder, Shi Water-shield powder gross weights Vinegar, is mixed, and soak at room temperature 30 minutes is transferred in centrifuge tube, 3000r/min centrifugation 5min, is removed supernatant, is stayed precipitation Thing, is 15~20% by the percentage by weight that sediment is dried in 40 DEG C to moisture;
(3) the drying product obtained by step (2) is put into Muffle furnace, in 350 DEG C~400 DEG C 2~3h of calcination, be cooled to Room temperature, then at 500 DEG C~550 DEG C calcinations 2~3 hours;
(4) pomelo peel is chopped up and ground;
(5) by folium artemisiae argyi, green tea according to 5:1 weight is than mixing, and addition weight is 15 times of folium artemisiae argyi and green tea gross weight Boiling water, soaks 5~8 hours, takes soak;
(6) zeolite is crushed to 100 mesh and 200 mesh, by the zeolite powder of the zeolite powder of 100 mesh and 200 mesh according to 1:2 ratio Example mixing;
(7) by the calcination thing obtained by step (3), the pomelo peel obtained by step (4), the soak obtained by step (5), step (6) zeolite powder obtained by is according to 1:2:10:2 weight is than mixing, and ultrasonication 30 minutes is produced.
A kind of plant source pig farm excrement dirty deodorant obtained by above-mentioned preparation method.
Embodiment 6
A kind of application of the dirty deodorant of plant source pig farm excrement obtained by embodiment 1:
The side of the special odorless organic fertilizer of cotton is prepared using the dirty deodorant of plant source pig farm excrement obtained by embodiment 1 Method, is comprised the following steps that:
(1) pig manure is filtered, discards liquid, by excrement with deodorant of the invention according to 1:40 weight is than mixing and stirring Mix uniform, obtain swine manure treatment thing;
(2) each component of following parts by weight is weighed according to proportioning:80 parts of cotton stalk, 65 parts of swine manure treatment thing, wheat straw 15 parts, 10 parts of beanstalk, 8 parts of bone meal, 2 parts of microbial fermentation inoculum;
(3) cotton stalk, swine manure treatment thing, wheat straw, beanstalk, bone meal, microbial fermentation inoculum are mixed, adds weight phase When in 0.6 times of clear water of total weight of the mixture, stir, Natural compost, at interval of turning in 5-7 days once, ferment 15-20 It completes compost fermentation;
(4) tunning obtained by step (3) is put into 60 DEG C of drying in an oven to water content within 15%, with crushing Machine is ground into the powder of 80~200 mesh, granulates, granular material is dried, drier heat source maximum temperature is in comminutor 200~250 DEG C, 50~70 DEG C of outlet temperature, water content is less than 5% after dry materials, finally sieves, grain diameter is existed 1.00-3.00mm fertilizer weighs, packs and produces.
Embodiment 7
A kind of application of the dirty deodorant of plant source pig farm excrement obtained by embodiment 1:
The side of the special odorless organic fertilizer of cotton is prepared using the dirty deodorant of plant source pig farm excrement obtained by embodiment 1 Method, is comprised the following steps that:
(1) pig manure is filtered, discards liquid, by excrement with deodorant of the invention according to 1:50 weight is than mixing and stirring Mix uniform, obtain swine manure treatment thing;
(2) each component of following parts by weight is weighed according to proportioning:90 parts of cotton stalk, 60 parts of swine manure treatment thing, wheat straw 10 parts, 10 parts of beanstalk, 10 parts of bone meal, 1 part of microbial fermentation inoculum;
(3) cotton stalk, swine manure treatment thing, wheat straw, beanstalk, bone meal, microbial fermentation inoculum are mixed, adds weight phase When in 0.8 times of clear water of total weight of the mixture, stir, Natural compost, at interval of turning in 5-7 days once, ferment 15-20 It completes compost fermentation;
(4) tunning obtained by step (3) is put into 60 DEG C of drying in an oven to water content within 15%, with crushing Machine is ground into the powder of 80~200 mesh, granulates, granular material is dried, drier heat source maximum temperature is in comminutor 200~250 DEG C, 50~70 DEG C of outlet temperature, water content is less than 5% after dry materials, finally sieves, grain diameter is existed 1.00-3.00mm fertilizer weighs, packs and produces.
Embodiment 8
A kind of application of the dirty deodorant of plant source pig farm excrement obtained by embodiment 1:
The side of the special odorless organic fertilizer of cotton is prepared using the dirty deodorant of plant source pig farm excrement obtained by embodiment 1 Method, is comprised the following steps that:
(1) pig manure is filtered, discards liquid, by excrement with deodorant of the invention according to 1:45 weight is than mixing and stirring Mix uniform, obtain swine manure treatment thing;
(2) each component of following parts by weight is weighed according to proportioning:100 parts of cotton stalk, 70 parts of swine manure treatment thing, wheat straw 15 parts, 15 parts of beanstalk, 8 parts of bone meal, 3 parts of microbial fermentation inoculum;
(3) cotton stalk, swine manure treatment thing, wheat straw, beanstalk, bone meal, microbial fermentation inoculum are mixed, adds weight phase When in 0.7 times of clear water of total weight of the mixture, stir, Natural compost, at interval of turning in 5-7 days once, ferment 15-20 It completes compost fermentation;
(4) tunning obtained by step (3) is put into 60 DEG C of drying in an oven to water content within 15%, with crushing Machine is ground into the powder of 80~200 mesh, granulates, granular material is dried, drier heat source maximum temperature is in comminutor 200~250 DEG C, 50~70 DEG C of outlet temperature, water content is less than 5% after dry materials, finally sieves, grain diameter is existed 1.00-3.00mm fertilizer weighs, packs and produces.
Experimental result
Stink is tested
Control group:Pig manure is filtered, liquid is discarded, by excrement and clear water according to 1:50 weight ratio is mixed and stirred for equal It is even.
Experimental group 1:Pig manure is filtered, liquid is discarded, by the plant source pig farm obtained by excrement and the embodiment of the present invention 1 Excrement dirt deodorant is according to 1:50 weight ratio is mixed and stirred for uniform, obtains swine manure treatment thing.
Experimental group 2:Pig manure is filtered, liquid is discarded, by the plant source pig farm obtained by excrement and the embodiment of the present invention 2 Excrement dirt deodorant is according to 1:50 weight ratio is mixed and stirred for uniform, obtains swine manure treatment thing.
Experimental group 3:Pig manure is filtered, liquid is discarded, by the plant source pig farm obtained by excrement and the embodiment of the present invention 3 Excrement dirt deodorant is according to 1:50 weight ratio is mixed and stirred for uniform, obtains swine manure treatment thing.
Experimental group 4:Pig manure is filtered, liquid is discarded, by the plant source pig farm obtained by excrement and the embodiment of the present invention 4 Excrement dirt deodorant is according to 1:50 weight ratio is mixed and stirred for uniform, obtains swine manure treatment thing.
Experimental group 5:Pig manure is filtered, liquid is discarded, by the plant source pig farm obtained by excrement and the embodiment of the present invention 5 Excrement dirt deodorant is according to 1:50 weight ratio is mixed and stirred for uniform, obtains swine manure treatment thing.
By stink index using six grades of classification:Ms0:Odorless, Ms1:Feel stink, Ms2 reluctantly:Faint is smelly Taste, Ms3:Obvious stink, Ms4:Very strong stink, Ms5:Insufferable stink.
The deodorizing effect of the control group of table 1 and the deodorant of embodiment of the present invention 1- embodiments 5
As a result show, after 4~6 hours, the swine manure treatment thing free from extraneous odour of gained.
Ammonia and hydrogen sulfide content situation of change in pig house
Test and carried out in Jinan City, Shandong Province pig farm.The processing of experimental group and control group is as follows respectively:
Experimental group 1:Deodorant clear water obtained by the embodiment of the present invention 1 is diluted into (10 times of dilution), pig house is sprayed at Rubbish transmission mouth at, sprinkling 2 times, once in the morning and once at night (morning 8 daily:00 and afternoon 5:00), spray the 30g present invention's every time Deodorant.Daily noon (12 during experiment:00 or so) sampling detection odor concentration (concentration of hydrogen sulfide and ammonia concentration), and remembering Record.
Experimental group 2:Deodorant clear water obtained by the embodiment of the present invention 2 is diluted into (10 times of dilution), pig house is sprayed at Rubbish transmission mouth at, sprinkling 2 times, once in the morning and once at night (morning 8 daily:00 and afternoon 5:00), spray the 30g present invention's every time Deodorant.Daily noon (12 during experiment:00 or so) sampling detection odor concentration (concentration of hydrogen sulfide and ammonia concentration), and remembering Record.
Experimental group 3:Deodorant clear water obtained by the embodiment of the present invention 3 is diluted into (10 times of dilution), pig house is sprayed at Rubbish transmission mouth at, sprinkling 2 times, once in the morning and once at night (morning 8 daily:00 and afternoon 5:00), spray the 30g present invention's every time Deodorant.Daily noon (12 during experiment:00 or so) sampling detection odor concentration (concentration of hydrogen sulfide and ammonia concentration), and remembering Record.
Experimental group 4:Deodorant clear water obtained by the embodiment of the present invention 4 is diluted into (10 times of dilution), pig house is sprayed at Rubbish transmission mouth at, sprinkling 2 times, once in the morning and once at night (morning 8 daily:00 and afternoon 5:00), spray the 30g present invention's every time Deodorant.Daily noon (12 during experiment:00 or so) sampling detection odor concentration (concentration of hydrogen sulfide and ammonia concentration), and remembering Record.
Experimental group 5:Deodorant clear water obtained by the embodiment of the present invention 5 is diluted into (10 times of dilution), pig house is sprayed at Rubbish transmission mouth at, sprinkling 2 times, once in the morning and once at night (morning 8 daily:00 and afternoon 5:00), spray the 30g present invention's every time Deodorant.Daily noon (12 during experiment:00 or so) sampling detection odor concentration (concentration of hydrogen sulfide and ammonia concentration), and remembering Record.
Control group:Transmitted in the rubbish of pig house and clear water is sprayed at mouth, daily sprinkling 2 times, once in the morning and once at night (morning 8:00 He Afternoon 5:00) 30g, is sprayed every time.Daily noon (12 during experiment:00 or so) sampling detection odor concentration (concentration of hydrogen sulfide And ammonia concentration), and record.
Ammonia assay method:The central point type air samplers of the GS- III collection air of mouth is transmitted in rubbish, using capacity Assay ammonia level.Hydrogen sulfide is determined using alarm analyzer.Wherein:Ammonia average content rate of descent (%)=(right According to a group ammonia average content-test group ammonia average content)/control group ammonia average content × 100%;Hydrogen sulfide averagely contains Amount rate of descent (%)=(control group hydrogen sulfide average content-test group hydrogen sulfide average content)/control group hydrogen sulfide averagely contains Amount × 100%
The content situation of ammonia and hydrogen sulfide is shown in Table 2.
The removal effect of the control group of table 2 and the deodorant of the embodiment of the present invention 1 to hydrogen sulfide and ammonia
As a result show, the dirty deodorant of plant source pig farm excrement of the invention can effectively reduce ammonia and hydrogen sulfide content, go Except the stink of pig manure, pollution of the pig manure to environment is reduced, while also improving pig class living environment, is conducive to keeping air clear Newly, the working environment of poultry feeders is improved.
Cotton planting is tested
Test site is Qingdao farmland, farmland cotton planting continuous cropping 5 years before experiment.Test process is as follows:
Control group:Before sowing, the change that 50kg and the identical N-P-K content of the embodiment of the present invention 6 are applied in field is tested in every mu Fertilizer;
Test group 1:Before sowing, field is tested in every mu using the organic fertilizer obtained by the 50kg embodiment of the present invention 6;
Experimental group 2:Before sowing, field is tested in every mu using the organic fertilizer obtained by the 50kg embodiment of the present invention 7;
Experimental group 3:Before sowing, field is tested in every mu using the organic fertilizer obtained by the 50kg embodiment of the present invention 8.
Control group sets 2 parallel, each one mu of parallel processing occupations of land respectively with each experimental group.Plant height 20cm or so When, every mu of control group and experimental group are topdressed urea 15kg, and the daily management of reason group is conventional daily management everywhere during experiment.
During experiment, observe and record the verticillium wilt incidence of disease of cotton, the droop incidence of disease, when autumn harvests, record skin Ginnings, the results are shown in Table 3:
The cotton growth situation of the control group of table 3 and experimental group compares
Test result indicate that, have using the special odorless of cotton obtained by the dirty deodorant of the plant source pig farm excrement of the present invention Machine fertilizer free from extraneous odour, prepares the equal environmental protection of all raw material components, with low cost of organic fertilizer, improves the utilization rate of pig manure, The active ingredient of cotton stalk, pig manure, wheat straw, beanstalk, bone meal is taken full advantage of, for the nutriment needed for the growth supplement of cotton, Be conducive to the re-using of waste and the material circulation of nature, and also help the growth of cotton, improve the production of cotton Amount.
The above is only the preferred embodiment of the present invention, it should be pointed out that:For the ordinary skill people of the art For member, under the premise without departing from the principles of the invention, some improvement can also be made, these improvement should be regarded as the guarantor of the present invention Protect scope.

Claims (9)

1. a kind of preparation method of the dirty plant source deodorant of pig farm excrement, it is characterised in that:Comprise the following steps:
(1) Enteromorpha salvaged in seawater and stone Water-shield are cleaned up with clear water respectively, puts and dried under 60 DEG C of constant temperatures in an oven It is 15~20% to do to the percentage by weight of moisture, takes out and crushes respectively, obtains enteromorpha powder He Shi Water-shield powder;
(2) calamus, mulberry leaf, lotus leaf are cleaned respectively and dried, then by calamus, mulberry leaf, lotus leaf, enteromorpha powder, Shi Water-shield powder according to 1:2 ~3:3~5:8~10:6~8 weight is than mixing, and addition weight is calamus, mulberry leaf, lotus leaf, enteromorpha powder, Shi Water-shield powder gross weights 0.5~0.6 times of vinegar, mix, soak at room temperature 30 minutes, centrifugation removes supernatant, stays sediment, 40 DEG C of drying to water The percentage by weight divided is 15~20%;
(3) the drying product obtained by step (2) is put into Muffle furnace, in 350 DEG C~400 DEG C 2~3h of calcination, is cooled to room Temperature, then at 500 DEG C~550 DEG C calcinations 2~3 hours;
(4) pomelo peel is chopped up and ground;
(5) by folium artemisiae argyi, green tea according to 5:1 weight adds 15 times of the boiling water that weight is folium artemisiae argyi and green tea gross weight than mixing, Immersion 5~8 hours, takes soak;
(6) zeolite is crushed to 100 mesh and 200 mesh, by the zeolite powder of the zeolite powder of 100 mesh and 200 mesh according to 1:2 ratio is mixed Close;
(7) by the calcination thing obtained by step (3), the pomelo peel obtained by step (4), the soak obtained by step (5), step (6) The zeolite powder of gained is according to 1:2~3:9~10:2~3 weight is than mixing, and ultrasonication 30 minutes is produced.
2. the preparation method of the dirty plant source deodorant of pig farm excrement according to claim 1, it is characterised in that:Step (2) In, calamus, mulberry leaf, lotus leaf, enteromorpha powder, Shi Water-shield powder are according to 1:2:4:8:8 weight is than mixing.
3. the preparation method of the dirty plant source deodorant of pig farm excrement according to claim 1, it is characterised in that:Step (7) In, by obtained by the calcination thing obtained by step (3), the pomelo peel obtained by step (4), the soak obtained by step (5), step (6) Zeolite powder according to 1:3:10:2 weight is than mixing.
4. supporting obtained by a kind of preparation method of the dirty plant source deodorant of pig farm excrement any one of claim 1-3 Piggery waste plant source deodorant.
5. application of the excrement dirty plant source deodorant in pig farm when preparing crop organic fertilizer described in a kind of claim 4.
6. the dirty plant source deodorant of pig farm excrement the answering in the special odorless organic fertilizer of preparation cotton described in a kind of claim 5 With, it is characterised in that:Its preparation method comprises the following steps:
(1) pig manure is filtered, discards liquid, by excrement with deodorant of the invention according to 1:40~50 weight is than mixing and stirring Mix uniform, obtain swine manure treatment thing;
(2) each component of following parts by weight is weighed according to proportioning:80~100 parts of cotton stalk, 60~70 parts of swine manure treatment thing, 10~15 parts of wheat straw, 10~15 parts of beanstalk, 8~10 parts of bone meal, 1~3 part of microbial fermentation inoculum;
(3) by cotton stalk, swine manure treatment thing, wheat straw, beanstalk, bone meal, microbial fermentation inoculum mix, add weight equivalent to 0.6~0.8 times of clear water of total weight of the mixture, stirs, Natural compost, at interval of turning in 5-7 days once, and ferment 15- Complete compost fermentation within 20 days;
(4) by the tunning obtained by step (3) put in an oven 60 DEG C drying to water content within 15%, use pulverizer powder The powder of 100~200 mesh is broken into, is granulated in comminutor, granular material is dried, drier heat source maximum temperature is 200 ~250 DEG C, 50~70 DEG C of outlet temperature, water content is less than 5% after dry materials, finally sieves, by grain diameter 1.00~ 3.00mm fertilizer weighs, packs and produces.
7. the dirty plant source deodorant of pig farm excrement according to claim 6 answering in the special odorless organic fertilizer of preparation cotton With, it is characterised in that:The microbial fermentation inoculum can be dusty yeast, lactic acid bacteria or its mixture.
8. the dirty plant source deodorant of pig farm excrement according to claim 6 answering in the special odorless organic fertilizer of preparation cotton With, it is characterised in that:In step (2), each component of following parts by weight is weighed according to proportioning:At 80 parts of cotton stalk, pig manure Manage 65 parts of thing, 15 parts of wheat straw, 10 parts of beanstalk, 8 parts of bone meal, 2 parts of microbial fermentation inoculum.
9. the dirty plant source deodorant of pig farm excrement any one of a kind of claim 6-8 has in the preparation special odorless of cotton The machine special odorless organic fertilizer of cotton obtained when fertile.
CN201710166215.4A 2017-03-20 2017-03-20 Dirty plant source deodorant of a kind of pig farm excrement and its preparation method and application Pending CN106946424A (en)

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