CN106912484B - Xinjunan acetate aqua, method and the application of anti-edible mushroom bacterial decay disease - Google Patents
Xinjunan acetate aqua, method and the application of anti-edible mushroom bacterial decay disease Download PDFInfo
- Publication number
- CN106912484B CN106912484B CN201710038963.4A CN201710038963A CN106912484B CN 106912484 B CN106912484 B CN 106912484B CN 201710038963 A CN201710038963 A CN 201710038963A CN 106912484 B CN106912484 B CN 106912484B
- Authority
- CN
- China
- Prior art keywords
- xinjunan acetate
- edible mushroom
- disease
- surfactant
- xinjunan
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/04—Nitrogen directly attached to aliphatic or cycloaliphatic carbon atoms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention provides Xinjunan acetate aqua, method and the applications of a kind of anti-edible mushroom bacterial decay disease, based on parts by weight, be made of following raw material: Xinjunan acetate is 2%~25%, surfactant is 5%~8%, antifreezing agent is 4%~8%, surplus is water, and the sum of parts by weight of component are 100%.After Xinjunan acetate mother medicine is made in octyl trichlamide mother medicine and acetic acidreaction first, Xinjunan acetate is pre-mixed with surfactant, antifreezing agent and water by formula, stirring is sufficiently mixed, filtered, be then packed and stored.The present invention is more thorough to target disease-controlling effect, and safer to user and environmental organism.The present invention ecological benefits more friendly to human body and environmental organism.Toxicity and field control effect experimental study show that Xinjunan acetate aqua shows excellent bacteriostatic activity to edible mushroom bacterial decay disease, and the effective agent that can be used as field control is promoted the use of.
Description
Technical field
The invention belongs to technical field of pesticide, are related to Xinjunan acetate, and in particular to a kind of anti-bacillary corruption of edible mushroom
Xinjunan acetate aqua, method and the application of rotten disease.
Background technique
The edible mushroom yield in China rises to 3169.68 in 2013 from 1978 60000 tons (5.7% of Zhan Quanqiu)
Ten thousand tons (edible fungi of china association statistical data), 170,700,000,000 yuan of the direct output value, 682,800,000,000 yuan of the indirect output value, working population exceed 2000
Ten thousand, yield has accounted for global 75% or more total output.Edible mushroom has become the fifth-largest farming after China's grain, dish, fruit, oil
Object accounts for the 5% of the planting industry gross output value, considerably beyond cotton, sugar material, silkworm and mulberry and tealeaves.Edible mushroom be also the U.S., Britain, France,
The special crop that the developed countries such as South Korea, Japan, Canada cultivate extensively worldwide has important market position.
In recent years, with the rapid development of mushroom industry, the continuous increase of edible fungus culturing scale, edible mushroom pest and disease damage is also increasingly
It is rampant.In the course of cultivation, mycelia, as good nutrient matrix, provides edible mushroom outside being exposed to for pest and disease damage
Convenient condition.According to ASSOCIATE STATISTICS, the edible mushroom that China enters commercialization cultivation shares a kind more than 50, is used for commerial growing
Kind have more than 30 kinds, wherein vulnerable to pest and disease damage harm kind have more than 20 kinds.Pest and disease damage can make the Edible Fungi underproduction 20%
~30%, it even has no harvest when serious.It can be seen that the research important prevention and control of plant diseases, pest control strategy of edible mushroom has important production practices
Directive significance.
The edible mushroom bacterial decay disease as caused by pseudomonad (Pseudomonas tolaasii) is Edible Fungi
On important disease, 30%~80% production loss can be caused.Pseudomonad is widely present in compost, earthing, in air
Dust in, the soil to carry disease germs is primary source of infection, and mushroom fly and watering can cause disease spread.It is real that germ infects edible mushroom
Body makes cap or stem faint yellow water stain shape scab occur, and under the condition of high temperature and high humidity, Spot expansion is rapid, cause cap or
Stem rots in faint yellow water stain shape, and gives out unpleasant foul odour, and sick mushroom loses economic value, cannot eat, cause
Serious financial consequences.
(Xinjunan acetate is a kind of existence form of octyl trichlamide, effectively for octyl trichlamide and its derivative Xinjunan acetate
Ingredient is octyl trichlamide) it is low toxicity, broad-spectrum germicide that China develops, belong to amino acids systemic fungicide, to various plants
Fungi, bacterium and virus disease show excellent control efficiency.The mycelia growth and spore germination that can inhibit germ, are destroyed
Cell membrane, inhibits respiratory system, and solidifying protein makes enzyme denaturation.It is reported that the substance is to pseudomonas, Xanthomonas campestris
The various plants pathogenetic bacterias such as category, Erwinia, clavibacter category have very excellent bacteriostatic activity, are that bacteriosis is anti-
Control an important species in limited pharmacy variety.
China's edible mushroom Pathogen identification and disease prevention techniques research are started late, and relevant registration medicament kind is also very
It is limited.Currently, the domestic effective agent kind that do not register specially still for preventing and treating edible mushroom bacterial decay disease.The country is edible
There is most of peasant household dispersion plantation type in planting in strain, degree of specialization is not high, and most of operation adds nothing by by hand
Bacteriumization condition is poor, easily bacterial infection rot disease.It is badly in need of exploitation effective agent in production to spread to control disease.
Some researches show that agricultural streptomycin, kasugarnycin show preferable inhibitory activity to edible mushroom bacterial decay germ.Due to
Agricultural streptomycin limits use, and the medicament that edible mushroom bacterial decay disease can be effectively prevented in production is extremely limited.It is badly in need of exploitation
The mechanism of action is unique, the fungicide of superior activity.Octyl trichlamide and a kind of exactly such medicament of Xinjunan acetate, the mechanism of action
Uniqueness, and conventional sterilization agent no interactions drug resistance, and higher bioactivity is shown to various plants pathogenetic bacteria.Therefore,
The effective agent that can be used as the prevention and treatment of edible mushroom bacterial decay disease is developed, great caused by disease great outburst to effectively prevent
Economic loss.
It is showed according to Xinjunan acetate physicochemical property and preventive effect, is suitable for that Xinjunan acetate is processed into aqua.Currently,
The Xinjunan acetate preparation of China's registration is largely also aqua.
Based on the above research background, it is necessary to Xinjunan acetate aqua is developed, it is anti-for edible mushroom bacterial decay disease
Control field.With important production practices meaning.
Summary of the invention
In view of the deficiencies of the prior art, the present invention intends to provide a kind of anti-edible mushroom bacterial decay disease
Xinjunan acetate aqua, method and application, for prevent and treat cultivated under the indoor conditions such as vinyl house, glasshouse it is edible
Bacterium bacterial decay disease.To reach more efficiently controlling disease, while the Ecological Effect more friendly to human body and environmental organism
Benefit.
In order to solve the above-mentioned technical problem, the present invention is realised by adopting the following technical scheme:
A kind of Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease, including following raw material: Xinjunan acetate,
Surfactant, antifreezing agent and water.
The present invention also has following distinguishing feature:
Specifically, based on parts by weight, being made of following raw material: based on parts by weight, composed of the following components: octyl trichlamide
Acetate is 1%~30%, and surfactant is 1%~15%, and antifreezing agent is 1%~10%, and surplus is water, the weight of component
The sum of number is 100%.
Preferably, based on parts by weight, be made of following raw material: Xinjunan acetate is 2%~25%, surfactant
It is 5%~8%, antifreezing agent is 4%~8%, and surplus is water, and the sum of parts by weight of component are 100%.
Specifically, the surfactant is alkyl phenol polyoxyethylene ether, polystyrylphenol polyoxyethylene ether, castor
Sesame oil polyoxyethylene ether, fatty alcohol polyoxyethylene ether, tallow amine polyoxyethylene ether, sorbitan fatty acid ester, Sorbitan
Polyol fatty acid ester APEO, oxireme propylene oxide block copolymer, aliphatic acid polyethenoxy ether ester, fatty amine polyoxy
The combination of one or more of vinethene, trisiloxanes polyethers and alkyl polyglycoside.
Specifically, the antifreezing agent is the combination of one or more of ethylene glycol, propylene glycol, glycerine and diethylene glycol.
The preparation method of the Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease as described above, first by pungent bacterium
After Xinjunan acetate mother medicine is made in amine mother medicine and acetic acidreaction, by Xinjunan acetate and surfactant, antifreezing agent and water
It is pre-mixed by formula, is sufficiently mixed stirring, filtered, be then packed and stored.
The Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease as described above is bacillary for preventing and treating edible mushroom
The application of rot disease.
Compared with prior art, the present invention having the following technical effect that
Xinjunan acetate aqua of the invention, it is more thorough to target disease-controlling effect relative to conventional medicament,
And it is safer to user and environmental organism.Xinjunan acetate aqua of the invention, which can reach, more efficiently to be prevented curing the disease
Evil, while the ecological benefits more friendly to human body and environmental organism.Toxicity and field control effect experimental study
Show that Xinjunan acetate aqua shows excellent bacteriostatic activity to edible mushroom bacterial decay disease, it is anti-to can be used as field
The effective agent controlled is promoted the use of.
Detailed description of the invention
Fig. 1 is the preparation technology figure of Xinjunan acetate aqua.
Auxiliary agent in figure refers to surfactant and antifreezing agent.Only octyl trichlamide mother medicine registration at present, does not have octyl trichlamide vinegar
The registration of hydrochlorate mother's medicine, registered Xinjunan acetate product are that octyl trichlamide acetic acid is made in octyl trichlamide mother medicine and acetic acidreaction
Salt.Therefore, the present invention is also to prepare Xinjunan acetate mother medicine by octyl trichlamide mother medicine and acetic acidreaction, is used for octyl trichlamide acetic acid
The processing of salt aqua and toxicity test measurement.
Explanation is further explained in detail to particular content of the invention with reference to embodiments.
Specific embodiment
In compliance with the above technical solution, it should be understood that
(1) publication No. is the Chinese patent of CN105724383A: what a kind of novel paint for preventing fruit tree putrefaction disease was mentioned
Fruit tree putrefaction disease pathogen is black skin shell Pseudomonas fungi (Valsa sp.), if canker of apple fruit cause of disease is (Valsa
Ceratosperma), Fungus of Pear Canker Disease cause of disease is black skin shell (Valsa ambiens), peach rotten pathogenic bacteria (Valsa
leucostoma)；Edible mushroom bacterial decay disease cause of disease of the present invention is pseudomonad (Pseudomonas tolaasii), is one
Kind bacterium.Although the two disease is nominally all rot disease, cause of disease is widely different on classification position, and (this is also plant disease
In common Different Kinds of Pathogens phenomenon of the same name, it should be noted that difference), there is very big difference on pesticide control, do not have comparativity.This
Invention belongs to new application invention, has creativeness.
(2) present invention with publication No. be CN105724383A Chinese patent in application method difference it is huge, by announcement
Number for CN105724383 Chinese patent smear use, do not meet disease pests occurrence rule, can not meet production actual requirement.Fruit
Tree rot disease generally uses smearing mode to carry out, and publication No. is that the Chinese patent of CN105724383A is also the smearing used.And
Edible mushroom bacterial decay germ (pseudomonad, Pseudomonas tolaasii) of the present invention is widely present in culture
Material, earthing, in the dust in air, the soil to carry disease germs is primary source of infection, and germ infects fruit body of edible fungi.It is real to earthing or son
Body disinfection treatment is key, if handled using smearing, operates very inconvenient, low efficiency, and application is very uneven, is unable to reach
Ideal control efficiency.Therefore, the present invention is based on productions actually to set out, and the method for use is spraying.It is with publication No.
The Chinese patent of CN105724383A has very big difference.
(3) present invention lacks a variety of key components, more passes through compared with publication No. is the Chinese patent of CN105724383A
Ji, effective and environmental protection, have creativeness.The present invention has lacked very compared with publication No. is the Chinese patent of CN105724383A
The key component of liniment is made, such as more；Acrylic resin soln, resin, heat stabilizer, plasticizing promotor etc..And this hair
Bright group is divided into the spraying conventional constituents using dosage form aqua.The two difference is huge, and there was only a small amount of surface in aqua component
The liniment of activating agent and antifreezing agent, a large amount of plasticisers of relative usage is also more environmentally friendly.The present invention uses a variety of auxiliary agent items few
Under part, it still can reach ideal control efficiency, it is more economical, effective and environmentally friendly, have creativeness.
(4) prior art can not prevent and treat edible mushroom bacterial decay disease well, and the disease occurs serious in production, anxious
Related product need to be badly in need of developing to meet production actual demand.
Specific embodiments of the present invention are given below, it should be noted that the invention is not limited to implement in detail below
Example, all equivalent transformations made on the basis of the technical solutions of the present application each fall within protection scope of the present invention.
In addition it is also necessary to explanation:
Octyl trichlamide and the reaction equation that acetic acidreaction generates Xinjunan acetate are as follows:
1 mole of octyl trichlamide is reacted with 3 mole of acetic acid generates 1 mole of Xinjunan acetate.Octyl trichlamide empirical formula C20H45N3, point
Son amount is 327.59, Xinjunan acetate empirical formula C26H57N3O6, molecular weight 507.75, acetic acid empirical formula is CH3COOH, point
Son amount is 60.05.
Specific embodiments of the present invention are given below, it should be noted that the invention is not limited to implement in detail below
Example, all equivalent transformations made on the basis of the technical solutions of the present application each fall within protection scope of the present invention.
Embodiment 1:
The present embodiment provides a kind of Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease, by following components group
At: Xinjunan acetate 2g, surfactant fatty alcohol polyoxyethylene ether are 5g, antifreeze glycol 5g, water 88g.
As shown in Figure 1, the preparation method of the Xinjunan acetate aqua of the anti-edible mushroom bacterial decay disease of the present embodiment,
After Xinjunan acetate mother medicine is made in octyl trichlamide mother medicine and acetic acidreaction first, by Xinjunan acetate and surfactant,
Antifreezing agent and water are pre-mixed by formula, are sufficiently mixed stirring, then filtering is packed and stored.
The Xinjunan acetate aqua of the anti-edible mushroom bacterial decay disease of the present embodiment is bacillary for preventing and treating edible mushroom
The application of rot disease.
Embodiment 2:
The present embodiment provides a kind of Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease, by following components group
At: Xinjunan acetate 5g, surfactant aliphatic amine polyoxyethylene ether are 6g, antifreeze glycol 4g, water 85g.
The preparation method of the present embodiment is substantially the same manner as Example 1.
The Xinjunan acetate aqua of the anti-edible mushroom bacterial decay disease of the present embodiment is bacillary for preventing and treating edible mushroom
The application of rot disease.
Embodiment 3:
The present embodiment provides a kind of Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease, by following components group
At: Xinjunan acetate 10g, surfactant alkyl polyglycoside are 5g, and antifreezing agent glycerine is 5g, water 80g.
The preparation method of the present embodiment is substantially the same manner as Example 1.
The Xinjunan acetate aqua of the anti-edible mushroom bacterial decay disease of the present embodiment is bacillary for preventing and treating edible mushroom
The application of rot disease.
Embodiment 4:
The present embodiment provides a kind of Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease, by following components group
At: Xinjunan acetate 15g, surfactant tallow amine polyoxyethylene ether are 7g, and antifreezing agent glycerine is 6g, water 72g.
The preparation method of the present embodiment is substantially the same manner as Example 1.
The Xinjunan acetate aqua of the anti-edible mushroom bacterial decay disease of the present embodiment is bacillary for preventing and treating edible mushroom
The application of rot disease.
Embodiment 5:
The present embodiment provides a kind of Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease, by following components group
At Xinjunan acetate 20g, surfactant polystyrylphenol polyoxyethylene ether is 6g, antifreeze glycol 7g,
Water is 67g.
The preparation method of the present embodiment is substantially the same manner as Example 1.
The Xinjunan acetate aqua of the anti-edible mushroom bacterial decay disease of the present embodiment is bacillary for preventing and treating edible mushroom
The application of rot disease.
Embodiment 6:
The present embodiment provides a kind of Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease, by following components group
At Xinjunan acetate 25g, surfactant fatty acid polyoxyethylene ether-ester is 8g, antifreeze glycol 8g, and water is
59g。
The preparation method of the present embodiment is substantially the same manner as Example 1.
The Xinjunan acetate aqua of the anti-edible mushroom bacterial decay disease of the present embodiment is bacillary for preventing and treating edible mushroom
The application of rot disease.
Embodiment 7:
The present embodiment provides a kind of Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease, other components and pungent bacterium
Amine acetic acid salt content is same as Example 1, and difference is only in that: by the 5g surfactant fatty alcohol polyoxy second in embodiment 1
Alkene ether replaces with 5g surfactant alkyl phenol polyoxyethylene ether or 5g surfactant polystyrylphenol polyoxy second
Alkene ether perhaps 5g surfactant castor oil polyoxyethylene ether perhaps 5g surfactant fatty alcohol polyoxyethylene ether or 5g
Surfactant tallow amine polyoxyethylene ether perhaps 5g surfactant sorbitan fatty acid ester or 5g surface-active
Agent sorbitan fatty acid ester polyoxyethylene ether or 5g surfactant oxireme propylene oxide block copolymer, or
Person's 5g surfactant fatty acid polyoxyethylene ether-ester perhaps 5g surfactant aliphatic amine polyoxyethylene ether or the surface 5g
Activating agent trisiloxanes polyethers or 5g surfactant alkyl polyglycoside.Surfactant is commercially available common surface-active
Agent.
The preparation method of the present embodiment is substantially the same manner as Example 1.
The Xinjunan acetate aqua of the anti-edible mushroom bacterial decay disease of the present embodiment is bacillary for preventing and treating edible mushroom
The application of rot disease.
Embodiment 8:
The present embodiment provides a kind of Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease, other components and pungent bacterium
Amine acetic acid salt content is same as Example 1, and difference is only in that: by the 5g antifreeze glycol in embodiment 1, it is anti-to replace with 5g
Freeze agent propylene glycol, perhaps replaces with 5g antifreezing agent glycerine or replace with 5g antifreezing agent diethylene glycol.Antifreezing agent is commercially available general
Logical antifreezing agent.
The preparation method of the present embodiment is substantially the same manner as Example 1.
The Xinjunan acetate aqua of the anti-edible mushroom bacterial decay disease of the present embodiment is bacillary for preventing and treating edible mushroom
The application of rot disease.
Application effect:
Toxicity measures effect:
Test medicine be mass fraction be 46% Xinjunan acetate mother medicine (by the processing method in such as embodiment 1,
It is prepared with octyl trichlamide mother medicine and acetic acidreaction)；Comparison medicament is that mass fraction is 91% sodium dichloro cyanurate raw medicine (state
Outer report sodium dichloro cyanurate has excellent activity to edible mushroom bacterial decay germ).Pathogen is that edible mushroom is bacillary
Rotten pathogenic bacteria (Pseudomonas tolaasii).
Appropriate Xinjunan acetate mother medicine and sodium dichloro cyanurate raw medicine are weighed with electronic balance, is spat respectively with 0.1%
Mother liquor is further diluted to 5 series of concentrations gradient medicines with 0.1% Tween-80 aqueous solution at mother liquor by warm -80 aqueous dissolutions
Liquid is spare.And the processing without medicament is set as blank control, it compares as 0.1% Tween-80 aqueous solution.
Test method reference " the 16th part of NYT 1156.16-2008 farm-chemical indoor determination test rule fungicide:
Bacterial growth amount is inhibited to test turbidity method ", concrete operations are as follows:
1, culture medium prepares:
NA (nutrient agar) culture medium (preparing bacteria suspension for actication of culture, routine culture): 1L NA culture medium
Peptone containing polyprotein 5g, yeast powder 1g, beef extract 3g, sucrose 15g, agar 17g, are adjusted to pH7.0 with the NaOH of 10mol/L.
NB (nutrient broth) fluid nutrient medium (measures) for toxicity: 1L NB culture medium peptone containing polyprotein
5g, yeast powder 1g, beef extract 3g, sucrose 15g are adjusted to pH7.0 with the NaOH of 10mol/L.
The above-mentioned culture medium of 50mL is sub-packed in the wide-mouth triangular flask of 100mL, sealing sterilizing is spare.
2, chemicals treatment:
It is quantitatively adding corresponding medical fluid in the NB culture medium cooled down after sterilization by experimental design concentration, production is cultivated in NA
Strain on base plate is diluted to 1 × 10 with aqua sterilisa7A spore/mL concentration bacteria suspension, respectively into each processing culture medium
It is inoculated with 100uL bacterium solution, shaken cultivation under the conditions of being placed in 28~30 DEG C, revolving speed 120r/min.
3, investigation and result calculate:
Start the preceding turbidity for measuring each processing respectively of culture to measure and remember when control treatment reaches logarithmic growth phase
Carry the turbidity of each processing.Compared with not dosing compares turbidity value added, bacterial growth inhibiting rate is calculated.
Bacterial growth inhibiting rate (%)=[(check plot turbidity value added-treatment region turbidity value added)/check plot
Turbidity value added] × 100
Drug concentration logarithm and corresponding bacterial growth inhibiting rate probability value are made into regression analysis, with DPS data processing
Software finds out virulence regression equation, calculates the EC of each medicament50、EC90And 95% confidence limit.
4, result:
Toxicity measurement result shows (see Table 1 for details and table 2), reagent agent Xinjunan acetate and comparison medicament dichloro
Sodium isocyanurate enhances the activity of edible mushroom bacterial decay germ with the raising of liquor strength.Reagent agent octyl trichlamide
EC of the acetate to edible mushroom bacterial decay germ50Value is 1.5126mg/L, and comparison medicament sodium dichloro cyanurate is to edible
The EC of bacterium bacterial decay germ50Value is 3.3354mg/L.As it can be seen that Xinjunan acetate is to edible mushroom bacterial decay germ
Toxicity is substantially better than comparison medicament sodium dichloro cyanurate.Therefore, Xinjunan acetate can be developed into prevention and treatment edible mushroom
The medicament of bacterial decay disease.
Toxicity measurement result of 1 Xinjunan acetate of table to edible mushroom bacterial decay germ
Toxicity measurement result summary table of 2 Xinjunan acetate of table to edible mushroom bacterial decay germ
Field information effect:
Test is located in the Yuncheng Yanhu District Dongguo town government circle simple mushroom house in village and carries out, and agaricus bisporus uses bed
Posture cultivation, 6 layers of layer frame, every 12 square metres of level product.
10% Xinjunan acetate aqua (formula i.e. in embodiment 3) setting effective component dosage is 0.6 gram/square
Rice, 0.8 gram/m, 1.0 grams/m, comparison medicament are chosen the solvable pulvis of 20% sodium dichloro cyanurate and (are purchased in the market
Buy Ministry of Agriculture's registration qualified products), effective component dosage is 0.8 gram/m, 1.2 grams/m, 1.6 grams/m.
5~9 days after earthing, even spraying earthing.Every square metre of medication water is 1 liter.4 repetitions are arranged in every processing, and every time repeatedly 3
Square metre (for 1 cell).And clear water processing is set as control.
The edible mushroom pesticide field efficacy medicine test criterion announced with reference to the Ministry of Agriculture provides investigation method, when the 1st damp mushroom harvests
Preventive effect, 2 square metres of every cell random searching are investigated, the sick mushroom number on investigation records compost adds up the sick mushroom number of each cell, counts
Calculate control efficiency.
Control efficiency (%)=[(check plot disease mushroom number-treatment region disease mushroom number)/check plot disease mushroom number] × 100
It is good that test result (see Table 3 for details) shows that 10% Xinjunan acetate aqua has edible mushroom bacterial decay disease
Good control efficiency, preventive effect requirement of the high dose up to the Ministry of Agriculture to 80% or more fungicide preventive effect.In the less condition of dosage
Under, preventive effect is substantially better than the solvable pulvis of 20% sodium dichloro cyanurate of comparison medicament.
Field control effect of 3 Xinjunan acetate of table to edible mushroom bacterial decay disease
Toxicity and field control effect experimental study show Xinjunan acetate aqua to edible mushroom bacterium
Property rot disease shows excellent bacteriostatic activity, and the effective agent that can be used as field control is promoted the use of.
Claims (3)
1. a kind of Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease, which is characterized in that based on parts by weight, by with
Lower raw material composition:
Xinjunan acetate is 2g, and surfactant fatty alcohol polyoxyethylene ether is 5g, antifreeze glycol 5g, water 88g；
Or Xinjunan acetate is 5g, surfactant aliphatic amine polyoxyethylene ether is 6g, antifreeze glycol 4g, and water is
85g；
Or Xinjunan acetate is 10g, surfactant alkyl polyglycoside is 5g, and antifreezing agent glycerine is 5g, water 80g；
Or Xinjunan acetate is 15g, surfactant tallow amine polyoxyethylene ether is 7g, and antifreezing agent glycerine is 6g, and water is
72g；
Or Xinjunan acetate is 20g, surfactant polystyrylphenol polyoxyethylene ether is 6g, and antifreeze glycol is
7g, water 67g；
Or Xinjunan acetate is 25g, surfactant fatty acid polyoxyethylene ether-ester is 8g, antifreeze glycol 8g, water
For 59g.
2. the preparation method of the Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease as described in claim 1, special
Sign is, after Xinjunan acetate mother medicine is made in octyl trichlamide mother medicine and acetic acidreaction first, by Xinjunan acetate and surface
Activating agent, antifreezing agent and water are pre-mixed by formula, are sufficiently mixed stirring, then filtering is packed and stored.
3. the Xinjunan acetate aqua of anti-edible mushroom bacterial decay disease as described in claim 1 is thin for preventing and treating edible mushroom
The application of bacterium property rot disease.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710038963.4A CN106912484B (en) | 2017-01-19 | 2017-01-19 | Xinjunan acetate aqua, method and the application of anti-edible mushroom bacterial decay disease |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710038963.4A CN106912484B (en) | 2017-01-19 | 2017-01-19 | Xinjunan acetate aqua, method and the application of anti-edible mushroom bacterial decay disease |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106912484A CN106912484A (en) | 2017-07-04 |
| CN106912484B true CN106912484B (en) | 2019-11-15 |
Family
ID=59454133
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710038963.4A Active CN106912484B (en) | 2017-01-19 | 2017-01-19 | Xinjunan acetate aqua, method and the application of anti-edible mushroom bacterial decay disease |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106912484B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107624784A (en) * | 2017-10-30 | 2018-01-26 | 陕西省石油化工研究设计院 | A kind of Edible Fungi mildewcide |
| CN109221131B (en) * | 2018-10-31 | 2021-02-19 | 安徽省锦江农化有限公司 | Aqueous solution containing amino-oligosaccharin and kasugamycin and application thereof |
| CN113545365A (en) * | 2021-08-31 | 2021-10-26 | 河北科技大学 | Composition for preventing and treating bacterial diseases of edible fungi, preparation and preparation method thereof |
| CN115152782A (en) * | 2022-06-23 | 2022-10-11 | 泰安市农业科学院(山东省农业科学院泰安市分院) | Bactericide composition for preventing and treating agaricus bisporus diseases and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102715158A (en) * | 2012-06-29 | 2012-10-10 | 青岛星牌作物科学有限公司 | Sterilization composition containing cyazofamid and kasugamycin and application thereof |
| CN103636624A (en) * | 2013-12-03 | 2014-03-19 | 海利尔药业集团股份有限公司 | Sterilizing composition containing tetramycin and symplectic bacteria amine acetate |
| CN104970021A (en) * | 2015-07-25 | 2015-10-14 | 海利尔药业集团股份有限公司 | Sterilization composition containing oxine-copper and xinjunan acetate |
| CN105340915A (en) * | 2015-10-31 | 2016-02-24 | 海利尔药业集团股份有限公司 | Sterilization composition containing benziothiazolinone and Xinjunan acetate |
-
2017
- 2017-01-19 CN CN201710038963.4A patent/CN106912484B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102715158A (en) * | 2012-06-29 | 2012-10-10 | 青岛星牌作物科学有限公司 | Sterilization composition containing cyazofamid and kasugamycin and application thereof |
| CN103636624A (en) * | 2013-12-03 | 2014-03-19 | 海利尔药业集团股份有限公司 | Sterilizing composition containing tetramycin and symplectic bacteria amine acetate |
| CN104970021A (en) * | 2015-07-25 | 2015-10-14 | 海利尔药业集团股份有限公司 | Sterilization composition containing oxine-copper and xinjunan acetate |
| CN105340915A (en) * | 2015-10-31 | 2016-02-24 | 海利尔药业集团股份有限公司 | Sterilization composition containing benziothiazolinone and Xinjunan acetate |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106912484A (en) | 2017-07-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102776130B (en) | Metarhizium anisopliae and application thereof | |
| CN106912484B (en) | Xinjunan acetate aqua, method and the application of anti-edible mushroom bacterial decay disease | |
| CN102461653B (en) | Application of polyhexamethylene guanidine in citrus sour rot prevention and treatment, and citrus antistaling agent containing polyhexamethylene guanidine | |
| CN105039167B (en) | A kind of beauveria bassiana DSXJ 07 and its application | |
| CN101502271B (en) | Method for producing fungal granular formulation for preventing and treating pest | |
| CN105875592B (en) | One kind killing Neurospora composite drug | |
| CN102021122B (en) | High-efficiency insecticidal fungus and applications thereof | |
| CN105316243A (en) | Preparing method and application of composite biological agent for agricultural root-knot nematodes | |
| CN104904761A (en) | Biopesticide and usage method thereof | |
| CN108559719B (en) | Liquid microbial fertilizer | |
| CN106259411A (en) | Suspension seed-coating agent containing CGA-173506, Difenoconazole and imidacloprid | |
| CN101536649A (en) | Organic culture method of edible wood-rotting fungi | |
| CN107258823A (en) | A kind of beauveria bassiana granular formulation preparation method and applications of control of grubs | |
| CN114668004A (en) | Application of perillaldehyde in preparation of bactericide for preventing and treating plant diseases | |
| KR20060015600A (en) | Antibacterial antiviral composition | |
| CN101658171A (en) | Pesticide composition and application thereof | |
| CN107372556A (en) | A kind of suspension seed-coating agent containing pyraclostrobin, amino-oligosaccharide and Diacloden | |
| CN101502275A (en) | Plant source pesticide | |
| US5194258A (en) | Production of enhanced biocontrol agents | |
| CN103988896A (en) | Prevention and treatment on postharvest diseases of fruits by using glycine betaine-induced culture of pichia caribbica | |
| CN106489997A (en) | A kind of process for preparing microbial insecticide | |
| CN113367160B (en) | Application of trichoderma viride preparation in preventing and treating tomato gray mold | |
| CN108812707A (en) | One kind killing thrips plant essential oil composition, preparation and its application | |
| CN107801727A (en) | One kind compounding seed coat agent | |
| EP0544039B1 (en) | Production of enhanced biocontrol agents |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |